EPA Method 8000 Series

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EPA Method 8000 Series Method 8270C/D (Continued) Auxiliary Standards Internal Standard Z-014J $ 80 / 1 x 1 mL Z-014J-PAK SAVE 37% $ 250 / 5 x 1 mL 4.0 mg/mL each in CH 2 Cl 2 6 comps. Naphthalene-d Acenaphthene-d 10 1,4-Dichlorobenzene-d 4 Phenanthrene-d 10 Chrysene-d 12 8 Perylene-d 12 Surrogate Standards M-8270-SS $ 80 / 1 x 1 mL M-8270-SS-PAK SAVE 20% $ 320 / 5 x 1 mL 4.0 mg/mL each in CH 2 Cl 2 6 comps. Phenol-d 2-Fluorobiphenyl Nitrobenzene-d 5 2,4,6-Tribromophenol 2-Fluorophenol 5 p-Terphenyl-d 14 M-8270-SS-R M-8270-SS-R-PAK At stated conc.each in CH 2 Cl 2 :MeOH (4:1) 2-Fluorobiphenyl (1.0 mg/mL) 2-Fluorophenol (2.0 mg/mL) Nitrobenzene-d 5 (1.0 mg/mL) Base/Neutrals & Acids - Matrix Standard Spiking Solutions CLP-007-SET CLP-007-SET-PAK Base/Neutrals $ 75 / 1 x 1 mL SAVE 20% $ 300 / 5 x 1 mL 6 comps. Phenol-d 5 (2.0 mg/mL) Terphenyl-d 14 (1.0 mg/mL) 2,4,6-Tribromophenol (2.0 mg/mL) $ 35 / 2 x 1 mL SAVE 20% $ 140 / 5 x (2 x 1 mL) (CLP-007A, CLP-007B) CLP-007A $ 20 / 1 x 1 mL 1.0 mg/mL each in MeOH 6 comps. GC/MSTuning Standard M-625-TS-20X $ 40 / 1 x 1 mL 1.0 mg/mL each in CH 2 Cl 2 4 comps. Benzidine p,p'-DDT Calibration Check Compounds (CCC) CLP-011-SET Base/Neutrals $ 35 / set of 2 x 1 mL (includes CLP-011A and CLP-011B) CLP-011A $ 20 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 7 comps. Acenaphthene Benzo[a]pyrene 1,4-Dichlorobenzene Di-n-octylphthalate Acids DFTPP Pentachlorophenol CLP-011B $ 20 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 6 comps. 4-Chloro-3-methylphenol 2,4-Dichlorophenol 2-Nitrophenol System Performance Check Compounds (SPCC) CLP-010 $ 25 / 1 x 1 mL 0.2 mg/mL each in CH 2 Cl 2 4 comps. CLP-010-10X $ 25 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 4 comps. 2,4-Dinitrophenol Hexachlorocyclopentadiene Hexachlorobutadiene Fluoranthene N-nitroso-diphenylamine Pentachlorophenol Phenol 2,4,6-Trichlorophenol 4-Nitrophenol N-nitroso-di-n-propylamine Method 8270 Acenaphthene 1,4-Dichlorobenzene 2,4-Dinitrotoluene Acids N-nitroso-di-n-propylamine Pyrene 1,2,4-Trichlorobenzene CLP-007B $ 20 / 1 x 1 mL 2.0 mg/mL each in MeOH 5 comps. 2-Chlorophenol 4-Chloro-3-methylphenol 4-Nitrophenol Pentachlorophenol Phenol Multi-Component Analytes Polychlorinated Biphenyls, Chlordane &Toxaphene Each at 1,000 µg/mL in Hexane AccuPAK (5 x 1 mL) SAVE 20% Aroclors# Cat. No. 1 mL Cat. No. PAK Aroclor 1016 C-216S-H-10X $ 20 C-216S-H-10X-PAK $ 80 Aroclor 1221 C-221S-H-10X 20 C-221S-H-10X-PAK 80 Aroclor 1232 C-232S-H-10X 20 C-232S-H-10X-PAK 80 Aroclor 1242 C-242S-H-10X 20 C-242S-H-10X-PAK 80 Aroclor 1248 C-248S-H-10X 20 C-248S-H-10X-PAK 80 Aroclor 1254 C-254S-H-10X 20 C-254S-H-10X-PAK 80 Aroclor 1260 C-260S-H-10X 20 C-260S-H-10X-PAK 80 Aroclor 1262 C-262S-H-10X 20 C-262S-H-10X-PAK 80 Aroclor 1268 C-268S-H-10X 20 C-268S-H-10X-PAK 80 Pesticides Chlordane P-017S-H-10X $ 15 P-017S-H-10X-PAK $ 80 Toxaphene P-093S-H-10X 15 P-093S-H-10X-PAK 80 Tel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • Web AccuStandard.com 243
EPA Method 8000 Series Method 8270C/D (Continued) Semi-Volatiles by Capillary Column GC/MS Method 8270 These Method 8270C/D formulations are designed based on the association of the analyte to a specific internal standard. These formulations allow for easy preparation of the typical analytes in the calibration curve. In addition, instrument/method problems can be rapidly diagnosed by examining those specific analytes and the associated internal standard in the affected part of the analysis. Save when ordering a complete set over individual solutions Complete 8270 Method Mixture Set M-8270-SET M-8270-R-SET M-8270-01 $ 80 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 17 comps. Aniline Benzyl alcohol bis(2-Chloroethyl)ether bis(2-Chloro-1-methylethyl)ether 2-Chlorophenol 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Ethylmethanesulfonate Hexachloroethane Methylmethanesulfonate 2-Methylphenol 4-Methylphenol N-Nitrosodimethylamine N-Nitrosodi-n-propylamine Phenol 2-Picoline M-8270-04A $ 45 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 9 comps. 4-Aminobiphenyl Anthracene 4-Bromophenyl phenyl ether Di-n-butyl phthalate 4,6-Dinitro-2-methylphenol Fluoranthene Hexachlorobenzene Pentachlorophenol Phenanthrene Technical Note $ 505 / 7 x 1 mL (M-8270-01,M-8270-02,M-8270-03,M-8270-04A,M-8270-04B,M-8270-05,M-8270-06) $ 480 / 7 x 1 mL (M-8270-01,M-8270-02,M-8270-03,M-8270-04A,M-8270-04B-R1,M-8270-05,M-8270-06) M-8270-02 $ 80 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 18 comps. Acetophenone Benzoic acid bis(2-Chloroethoxy)methane 4-Chloroaniline 4-Chloro-3-methylphenol 2,4-Dichlorophenol 2,6-Dichlorophenol α,α-Dimethylphenethylamine 2,4-Dimethylphenol Hexachlorobutadiene Isophorone 2-Methylnaphthalene Naphthalene Nitrobenzene 2-Nitrophenol N-Nitroso-di-n-butylamine N-Nitrosopiperidine 1,2,4-Trichlorobenzene M-8270-04B $ 35 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 6 comps. Diphenylamine 1,2-Diphenylhydrazine N-Nitrosodiphenylamine Pentachloronitrobenzene Phenacetin Pronamide Under EPA recommended GC conditions (Method 8270) the analyte 1,2-Diphenylhydrazine is converted in varying degrees to Azobenzene and breakdown products. According to our study, the use of an injection port temperature range (240°C - 300°C) will cause the 1,2-Diphenylhydrazine to break down. Substituting Azobenzene for 1,2-Diphenylhydrazine will allow analysis yielding a single peak regardless of the EPA recommended injection port temperature range used. Alternate Formulation M-8270-04B-R1 $ 35 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 6 comps. Azobenzene Diphenylamine N-Nitrosodiphenylamine Pentachloronitrobenzene Phenacetin Pronamide M-8270-03 $ 120 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 24 comps. Acenaphthene Acenaphthylene 1-Chloronaphthalene 2-Chloronaphthalene 4-Chlorophenyl phenyl ether Dibenzofuran Diethyl phthalate Dimethyl phthalate 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluorene Hexachlorocyclopentadiene 1-Naphthylamine 2-Naphthylamine 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline 4-Nitrophenol Pentachlorobenzene 1,2,4,5-Tetrachlorobenzene 2,3,4,6-Tetrachlorophenol 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol M-8270-05 $ 80 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 8 comps. Benzidine Benzo[a]anthracene bis(2-Ethylhexyl)phthalate Butylbenzylphthalate Chrysene 3,3'-Dichlorobenzidine p-Dimethylaminoazobenzene Pyrene M-8270-06 $ 120 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 10 comps. Benzo[b]fluoranthene Benzo[k]fluoranthene Benzo[g,h,i]perylene Benzo[a]pyrene Dibenz[a,j]acridine Dibenz[a,h]anthracene 7,12-Dimethylbenz[a]anthracene Di-n-octylphthalate Indeno[1,2,3-cd]pyrene 3-Methylcholanthrene M-8270-07 $ 160 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 15 comps. Aramite Chlorobenzilate Diallate 2,4-D Dimethoate Dinoseb Disulfoton Famphur Kepone Methyl parathion Parathion Phorate Silvex (2,4,5-TP) Sulfotep Thionazin M-8270-08 $ 65 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 9 comps. 3,3'-Dimethyl benzidine 4-Nitroquinoline-1-oxide N-Nitrosodiethylamine N-Nitrosomethylethylamine N-Nitrosomorpholine N-Nitrosopyrrolidine 5-Nitro-o-toluidine p-Phenylenediamine o-Toluidine M-8270-09 $ 65 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 10 comps. 2-Acetyl aminofluorene 1,3-Dinitrobenzene Hexachlorophene Hexachloropropene Isodrin Isosafrole Methapyrilene 1,4-Naphthoquinone Safrole O,O,O-Triethylphosphorothioate 244 AccuStandard is accredited to ISO/IEC 17025 and certified to ISO 9001
Page 1: EPA Method 8000 Series Method 8270C
Page 5 and 6: Method 8270C/D 5 point Semi-Volatil
Page 7 and 8: EPA Method 8000 Series Method 8280-
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EPA Method 8000 Series

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