EPA Method 8000 Series

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EPA Method 8000 Series Ready-to-Inject Working Level Semi-Volatile Standards Method 8270C/D (Continued) Matrix Spike (SW 846) CLP-007-WL-50ML At stated conc.in MeOH 4-Chloro-3-methyl phenol (200 µg/mL) 2-Chlorophenol (200 µg/mL) 4-Nitrophenol (200 µg/mL) Pentachlorophenol (200 µg/mL) Phenol (200 µg/mL) Acenaphthene (100 µg/mL) Internal Standard Prep Note $ 115 / 1 x 50 mL 11 comps. 1,4-Dichlorobenzene (100 µg/mL) 2,4-Dinitrotoluene (100 µg/mL) N-Nitrosodi-n-propylamine (100 µg/mL) Pyrene (100 µg/mL) 1,2,4-Trichlorobenzene (100 µg/mL) To help maximize instrument performance, add 10 µL of internal standard to a 1 mL sample extract. Z-014J $ 80 / 1 x 1 mL Z-014J-PAK SAVE 37% $ 250 / 5 x 1 mL 4.0 mg/mL each in CH 2 Cl 2 6 comps. Method 8270 Surrogate Spiking Solution M-8270-SS-R-WL-PAK M-8270-SS-R-WL-VAP At stated conc.in CH 2 Cl 2 :MeOH (4:1) 2-Fluorobiphenyl (100 µg/mL) 2-Fluorophenol (200 µg/mL) Nitrobenzene-d 5 (100 µg/mL) M-8270-SS-R M-8270-SS-R-PAK At stated conc.in CH 2 Cl 2 :MeOH (4:1) 2-Fluorobiphenyl (1000 µg/mL) 2-Fluorophenol (2000 µg/mL) Nitrobenzene-d 5 (1000 µg/mL) Prep Note $ 190 / 5 x 10 mL $ 300 / 10 x 10 mL 6 comps. Phenol-d 5 (200 µg/mL) Terphenyl-d 14 (100 µg/mL) 2,4,6-Tribromophenol (200 µg/mL) $ 75 / 1 x 1 mL SAVE 20% $ 300 / 5 x 1 mL 6 comps. Phenol-d 5 (2000 µg/mL) Terphenyl-d 14 (1000 µg/mL) 2,4,6-Tribromophenol (2000 µg/mL) To ensure extraction efficiency add, 1 mL of Surrogate to the sample. Method 8270-8275 Naphthalene-d Acenaphthene-d 10 1,4-Dichlorobenzene-d 4 Phenanthrene-d 10 Chrysene-d 12 8 Perylene-d 12 Benzidine Solution M-625C-1-40X 2.0 mg/mL in CH 2 Cl 2 Benzidine $ 20 / 1 x 1 mL CLP Surrogate Spiking Solution CLP-031-R-WL-25ML $ 110 / 1 x 25 mL CLP-031-R-WL-50ML $ 190 / 1 x 50 mL At stated conc.in MeOH 8 comps. 2-Chlorophenol-d 4 (150 µg/mL) Nitrobenzene-d 5 (100 µg/mL) 1,2-Dichlorobenzene-d 4 (100 µg/mL) Phenol-d 6 (150 µg/mL) 2-Fluorobiphenyl (100 µg/mL) p-Terphenyl-d 14 (100 µg/mL) 2-Fluorophenol (150 µg/mL) 2,4,6-Tribromophenol (150 µg/mL) GC/MSTuning Solution M-625-TS $ 40 / 1 x 1 mL M-625-TS-PAK SAVE 20% $ 160 / 5 x 1 mL 50 µg/mL each in CH 2 Cl 2 4 comps. Benzidine p,p'-DDT DFTPP GC/MSTuning Solution M-625C-3 M-625C-3-PAK 25 µg/mL in CH 2 Cl 2 Decafluorotriphenylphosphine (DFTPP) Matrix Spike (3/90 SOW) CLP-007R-WL-50ML At stated conc.in MeOH 4-Chloro-3-methyl phenol (150 µg/mL) 2-Chlorophenol (150 µg/mL) 4-Nitrophenol (150 µg/mL) Pentachlorophenol (150 µg/mL) Phenol (150 µg/mL) Acenaphthene (100 µg/mL) Technical Note DFTPP Pentachlorophenol $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL $ 115 / 1 x 50 mL 11 comps. 1,4-Dichlorobenzene (100 µg/mL) 2,4-Dinitrotoluene (100 µg/mL) N-Nitrosodi-n-propylamine (100 µg/mL) Pyrene (100 µg/mL) 1,2,4-Trichlorobenzene (100 µg/mL) AccuStandard has found that benzidine degrades in multi-component semivolatile solutions. For this reason, the benzidine in any calibration curve should be used as a qualitative retention time marker. Reported hits for benzidine should be quantitatively determined by analyzing a single benzidine solution or by using the benzidine response observed in the Daily GC/MS tuning solution. Method 8275A (Thermal Extraction/GC/FID/MS) Semi-Volatiles by Thermal Chromatography Semi-Volatiles M-8275 $ 60 / 1 x 1 mL 1.0 mg/mL each inAcetone 17 comps. Aldrin Benzo[k]fluoranthene Benzo[a]pyrene Carbazole 4-Chloro-3-methylphenol 1-Chloronaphthalene 2-Chlorophenol Dibenzothiophene 2,4-Dichlorophenol Internal Standard 2,4-Dinitrotoluene Diphenylamine Fluorene Hexachlorobenzene 4-Methylphenol Naphthalene Phenanthrene Pyrene Z-014J $ 80 / 1 x 1 mL Z-014J-PAK SAVE 37% $ 250 / 5 x 1 mL 4.0 mg/mL each in CH 2 Cl 2 6 comps. Naphthalene-d Acenaphthene-d 10 1,4-Dichlorobenzene-d 4 Phenanthrene-d 10 Chrysene-d 12 8 Perylene-d 12 Alternate Source Line For complete listing of competitive 8270 see the QC Section Tel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • Web AccuStandard.com 247
EPA Method 8000 Series Method 8280-8310, Canadian, FL Method 8280A Dioxins & Furans by HRGC/LRMS Dioxin Mixture M-8280A $ 150 / 1 x 1 mL M-8280A-PAK SAVE 20% $ 600 / 5 x 1 mL 5 µg/mL each inToluene 5 comps. 2,3,7,8-Tetrachlorodibenzo-p-dioxin 1,2,3,7,8-Pentachlorodibenzo-p-dioxin 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin Furan Mixture M-8280B $ 150 / 1 x 1 mL M-8280B-PAK SAVE 20% $ 600 / 5 x 1 mL 5 µg/mL each inToluene 5 comps. 2,3,7,8-Tetrachlorodibenzofuran 1,2,3,7,8-Pentachlorodibenzofuran 1,2,3,4,7,8-Hexachlorodibenzofuran Column Performance Check M-8280-CPC $ 200 / 1 x 1 mL 5 µg/mL each inToluene 7 comps. 1,2,3,4-Tetrachlorodibenzo-p-dioxin 2,3,7,8-Tetrachlorodibenzo-p-dioxin 1,2,3,4,7-Pentachlorodibenzo-p-dioxin 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin Octachlorodibenzo-p-dioxin 1,2,3,4,6,7,8-Heptachlorodibenzofuran Octachlorodibenzofuran 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin 2,3,7,8-Tetrachlorodibenzofuran Canadian Environmental Method Multi-Component Dioxin Mixtures CustomWindow Defining Mixture D-WD 20,000 ng/mL in Toluene $ 1,100 / 1 x 1 mL D-WD-2.5X 50,000 ng/mL in Toluene $ 2,000 / 1 x 1 mL 7 comps. 1,2,4,6,8/1,2,4,7,9-Pentachlorodibenzo-p-dioxin (Isomer pair) 1,2,3,8,9-Pentachlorodibenzo-p-dioxin 1,2,4,6,7,9/1,2,4,6,8,9-Hexachlorodibenzo-p-dioxin (Isomer pair) 1,2,3,4,6,7-Hexachlorodibenzo-p-dioxin 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin 1,2,3,4,6,7,9-Heptachlorodibenzo-p-dioxin Octachlorodibenzo-p-dioxin Custom Calibration Mixture D-CAL 20,000 ng/mL in Toluene $ 900 / 1 x 1 mL D-CAL-2.5X 50,000 ng/mL in Toluene $ 1,600 / 1 x 1 mL 6 comps. 1,2,3,7,8-Pentachlorodibenzo-p-dioxin 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin Octachlorodibenzo-p-dioxin Column Performance Check M-8280-CPC $ 200 / 1 x 1 mL 5.0 µg/mL each inToluene 7 comps. 1,2,3,4-Tetrachlorodibenzo-p-dioxin 2,3,7,8-Tetrachlorodibenzo-p-dioxin 1,2,3,4,7-Pentachlorodibenzo-p-dioxin 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin 2,3,7,8-Tetrachlorodibenzofuran Formulations atHighest Concentration for Economical Prices Method 8310 PAHs by HPLC PAH Mixture M-8310 $ 75 / 1 x 1 mL M-8310-PAK SAVE 20% $ 300 / 5 x 1 mL 0.5 mg/mL each inAcCN 16 comps. Acenaphthene Acenaphthylene Anthracene Benz[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Surrogate Standard M-8310-SS M-8310-SS-PAK 0.1 mg/mL inAcetonitrile Decafluorobiphenyl Chrysene Dibenz[a,h]anthracene Fluoranthene Fluorene Indeno[1,2,3-cd]pyrene Naphthalene Phenanthrene Pyrene PAH Quality Control Calibration Mixture M-610-QC At stated conc.inAcCN Acenaphthene (0.1 mg/mL) Acenaphthylene (0.1 mg/mL) Anthracene (0.1 mg/mL) Benzo[a]anthracene (0.01 mg/mL) Benzo[a]pyrene (0.01 mg/mL) Benzo[b]fluoranthene (0.01 mg/mL) Benzo[g,h,i]perylene (0.01 mg/mL) Benzo[k]fluoranthene (0.005 mg/mL) $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL Internal Standard Post Supercritical Fluid Extraction M-8310-SFE-IS-100X M-8310-SFE-IS-100X-PAK 20,000 µg/mL inAcCN:THF (1:1) Biphenyl Florida Method PAH Mixture $ 35 / 1 x 1 mL 16 comps. Chrysene (0.01 mg/mL) Dibenz[a,h]anthracene (0.01 mg/mL) Fluoranthene (0.01 mg/mL) Fluorene (0.1 mg/mL) Indeno[1,2,3-cd]pyrene (0.01 mg/mL) Naphthalene (0.1 mg/mL) Phenanthrene (0.1 mg/mL) Pyrene (0.01 mg/mL) $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL Z-014G-FL $ 85 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 :Benzene 18 comps. Acenaphthene Acenaphthylene Anthracene Benz[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene Dibenz[a,h]anthracene Fluoranthene Fluorene Indeno[1,2,3-cd]pyrene Naphthalene Phenanthrene Pyrene 1-Methylnaphthalene 2-Methylnaphthalene Standards of Interest For more Canadian Methods see the Regional Section of this catalog, pages 256-258. 248 AccuStandard is accredited to ISO/IEC 17025 and certified to ISO 9001
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EPA Method 8000 Series

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