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National Primary Drinking Water Standards

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EPA Method 1600 Series<br />

1600<br />

Method 1658 Phenoxy-Acid Herbicides<br />

Method 1658 consolidates several EPA wastewater methods used to determine Phenoxy-Acid Herbicides & Herbicide esters associated with the<br />

CWA, RCRA, & CERCLA; & other compounds amenable to extraction & analysis by wide-bore capillary column GC/ECD.<br />

M-1658-CAL-SET<br />

$ 75 / 3 x 1 mL<br />

All solutions in Isooctane<br />

12 comps.<br />

Components Low Medium High<br />

(units in ng/mL) ( 1X ) ( 10X ) ( 100X )<br />

2,4-D 100 1,000 10,000<br />

Dalapon 50 500 5,000<br />

2,4-DB 200 2,000 20,000<br />

2,4-Dichlorphenylacetic acid 10 100 1,000<br />

(Surrogate)<br />

Dicamba 20 200 2,000<br />

Dichlorprop 100 1,000 10,000<br />

Dinoseb 50 500 5,000<br />

MCPA 5,000 50,000 500,000<br />

MCPP 5,000 50,000 500,000<br />

Picloram 50 500 5,000<br />

2,4,5-T 20 200 2,000<br />

2,4,5-TP 20 200 2,000<br />

Method 1658-1665<br />

Method 1659 Dazomet in Municipal & Industrial Wastewater by NPD<br />

Method 1659 is used to determine Dazomet by base hydrolysis to Methyl Isothiocyanate (MITC) and subsequent determination of MITC by wide-bore<br />

fused-silica capillary column gas chromatography with a Nitrogen Phophorus Detector (NPD).<br />

Recovery & Precision Solution<br />

M-1659-RPS $ 10 / 1 x 1 mL<br />

25 µg/mL inAcetone<br />

Methyl isothiocyanate (MITC)<br />

Matrix Spiking Solution<br />

M-1659-MS $ 10 / 1 x 1 mL<br />

25 µg/mL inAcetone<br />

Dazomet<br />

Calibration Solutions<br />

M-1659-CAL-SET<br />

$ 25 / 3 x 1 mL<br />

M-1659-CAL-1X 0.2 mg/mL in Acetone 1 mL<br />

M-1659-CAL-5X 1.0 mg/mL in Acetone 1 mL<br />

M-1659-CAL-25X 5.0 mg/mL in Acetone 1 mL<br />

Methyl isothiocyanate (MITC)<br />

Method 1664 See Petrochemical or Inorganic Sections<br />

Method 1665 Semi-Volatile Organic Compounds Specific to the PMI by Isotope Dilution GC/MS<br />

The following method series is designed to meet PMI (Pharmaceutical Manufacturing Industry) methods promulgated in 40 CFR part 136. It is used<br />

to monitor the discharge of pollutants into surface waters. It can also be used to identify and measure purgeable and non-purgeable volatiles, semivolatiles,<br />

and certain organic pollutants specific to PMI discharge in water, soils, and municipal sludges.<br />

PMI Semi-Volatile Set<br />

M-1665-SET<br />

GPC Calibration Solution<br />

M-1618-GP-5ML<br />

At stated conc.inAcetone<br />

$ 35 / 1 x 5 mL<br />

5 comps.<br />

$ 320 / 5 x 1 mL<br />

(M-1618-GP-5ML, M-1653-TS, M-625-07-10X, M-1665, M-1665-LAB)<br />

PMI Stock Standard<br />

M-1665 $ 60 / 1 x 1 mL<br />

2000 µg/mL each in CH 2 Cl 2 6 comps.<br />

Corn oil<br />

bis(2-Ethylhexyl)phthalate<br />

Pentachlorophenol<br />

(300.0 mg/mL)<br />

(15.0 mg/mL)<br />

(1.4 mg/mL)<br />

Perylene<br />

Sulfur<br />

(0.1 mg/mL)<br />

(0.5 mg/mL)<br />

Aniline<br />

N,N-Dimethylacetamide<br />

N,N-Dimethylaniline<br />

Dimethylformamide<br />

2-Picoline<br />

Pyridine<br />

Instrument Performance Check Solution<br />

M-1653-TS<br />

$ 20 / 1 x 1 mL<br />

50 µg/mL inAcetone<br />

PMI Labeled Stock Standard (Not for individual sale)<br />

M-1665-LAB<br />

1 x 1 mL<br />

500 µg/mL each in CH 2 Cl 2 5 comps.<br />

DFTPP<br />

PMI Internal Standard<br />

M-625-07-10X<br />

2.0 mg/mL in CH 2 Cl 2<br />

2,2'-Difluorobiphenyl<br />

$ 20 / 1 x 1 mL<br />

Aniline-d 7<br />

2-Picoline-d 7<br />

N,N-Dimethylaniline-d 11 Pyridine-d 5<br />

Dimethylformamide-d 7<br />

Tel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • Web AccuStandard.com 205

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