Multiwave PRO

More documents

Recommendations

Info

$Abbemat Refractometer Se$

Large-scale & HighperformanceSynthesis➤ Scale-up rotors for large-scaleparallel synthesisThe large-scale rotors for Multiwave PRO meet therequirements of multigram applications and highperformancesynthesis. The vessels used for largescalesynthesis are modular and interchangeable,using the same vessel caps and liners. Opening andsealing Multiwave PRO’s rotors, vessels and sensorsis quick and simple - just use your hands. This toolfreehandling is unique to Anton Paar and simplifiesthis frequently repeated work step.Precisely tooled fluoropolymer liners and sealsallow the processing of various chemical reactionsin solution and in solid phase. Thick-walled quartzvessels are available which withstand extremeconditions up to 300 °C and 80 bar. These aresuitable even for near-critical water chemistry.➤ Precise reaction controlAn immersing temperature probe in a referencevessel combined with infrared sensors monitoringthe external vessel temperature provide utmostaccuracy in the control of reaction conditions. Anadditional hydraulic pressure system simultaneouslymonitors the pressure in all vessels of Rotor 8N.The sensors are already installed and ready for use.For convenient handling, the sensors transfer data tothe Multiwave PRO controller wirelessly, so you donot need to connect cables before loading the rotor.➤ Safe and smooth operationMultiwave PRO’s high overpressure toleranceprovides trouble-free operation even under extremeconditions. To ensure a safe working environment,pressure is released and noxious vapors areexhausted automatically before you open the rotor.
Efficient Scale-up➤ Direct scalability up to themultigram rangeAll methods developed in the high-throughputrotors can be directly transferred to the scale-uprotors. With a capacity of about 15 g per vessel aproductivity of approximately 200 g product per runcan be achieved.➤ Scale-up with low-absorbingsolventsTo enable scale-up of methods utilizing low-absorbingsolvents Multiwave PRO uses passive-heatingelements made from silicon carbide. Adding theseto the vessels enables efficient heating of mixturescontaining non-polar solvents.➤ Create a gas atmosphere in eachvesselAn ingeniously simple gas loading system enablesyou to create a reactive or inert gas atmosphereindividually in each vessel. Pressures up to 20 barcan be applied prior to reactions for safe andeffective syntheses with sensitive substrates andgaseous reagents.Rotor 48MF50 16MF100 16HF100 8NXF100 8NXQ80No. of vessels 48 16 8ReactioncontrolOne reference vessel with immersing temperatureprobe and pressure sensorRemote IR control in 16 positionsOne reference vessel withimmersing temperature probeRemote IR control in all positionsLiner material PFA PTFE-TFM n/aPressure jacket PEEK Ceramic QuartzVolume 50 mL 100 mL 80 mLOperationparametersMax. designpressureTypicalapplications200 °C @ 20 bar (290 psi)60 bar(870 psi)240 °C @ 40 bar(580 psi)115 bar(1670 psi)Multigram library generation, parallel scale-up,synthesis of key intermediates, nanomaterials260 °C @ 60 bar(870 psi)Pre-pressurizedreactions,nanomaterials140 bar(2000 psi)300 °C @ 80 bar(1160 psi)Near-criticalwater chemistry,nanomaterials
Page 1 and 2: Multiwave PROMicrowave Reaction Sys
Page 3 and 4: Excellence in Microwave SynthesisVa
Page 5: A Quicker Route toYour ResultsMicro

Multiwave PRO

You also want an ePaper? Increase the reach of your titles

Delete template?

Save as template?