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quality standards - Labicom

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METHOD 603 – ACROLEIN & ACRYLONITRILEMethod 603 is a purge and trap gas chromatographic (GC) method applicable for the determination of acrolein and acrylonitrile.ACROLEIN & ACRYLONITRILEEPA METHOD 603, 1624, 8030A Acrolein AcrylonitrileNeat compounds of each of the above - (2 component kit)PP-3N KIT5mL Solutions of each, in the appropriate solvent - (2 component kit)PP-3S KITEPA 600METHOD 604 – PHENOLSMethod 604 is a flame ionization detector gas chromatographic (GC/FID) method applicable to the determination of Phenol and certainsubstituted phenols in municipal and industrial discharges as provided under 40 CFR 136.1. This method describes analytical conditionsfor derivatization, cleanup, and electron capture detector gas chromatography (GC/ECD) that can be used to confi rm measurementsmade by GC/FID. Method 625 provides gas chromatograph/mass spectrometer (GC/MS) conditions appropriate for the qualitativeand quantitative confirmation of results for all of the parameters listed in the method, using the extract produced by this method.Method 604.1 is an HPLC method applicable for the determination of Hexachlorophene and Dichlorophene in industrial and municipal wastewaters.The liquid chromatographic conditions described permit the separation and measurement of the compounds in the extract by HPLC using anultraviolet detector.PHENOLSEPA METHOD 604, 625/1625, 8270B 4-Chloro-3-methyl phenol 2,4-Dimethylphenol 2-Nitrophenol Phenol 2-Chlorophenol 4,6-Dinitro-o-cresol 4-Nitrophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dinitrophenol PentachlorophenolPP-2NPP-2SNeat compounds of each of the above (11 component kit)5mL Solutions of each, in the appropriate solvent - (11 components kit)PP-2M Mixture at 100ug/mL in Methanol, 5mL - (11 components)PP-HC9 Mixture at 2000ug/mL in Methylene chloride, 5mL Ampule - (11 components)PP-HC9JM Mixture at 2000ug/mL in Methylene chloride, 1mL Ampule - (11 components)NOTE: 2,4-Dinitrophenol and 4,6-Dinitro-o-cresol are at a concentration of 1000ug/mL in the PP-2M mixture only.DERIVATIZING AGENTSEPA METHOD 604, 604.1, 8040AF2303 1g Pentafl uorobenzylbromideF2304 5g HexaoxacyclooctadecaneMETHOD 605 – BENZIDINESMethod 605 is a high performance liquid chromatography (HPLC) method applicable to the determination of the listed benzidines in municipaland industrial discharges. The final benzidine compounds are measured with an electrochemical detector.BENZIDINESEPA METHOD 605, 625/1625, 8270B, CLP Benzidine 3,3-DichlorobenzidineNeat compounds of each of the above (2 component kit)PPB-5N KIT5mL Solutions of each, in the appropriate solvent - (2 component kit)PPB-5S KIT2000ug/mL in Methanol - (2 components)PP-HC7 5mL AmpulePP-HC7JM 1mL Ampule 173

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