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Chemistry of Materials<br />
Situ Probing of High-Temperature Quantum Dots Solution Synthesis.<br />
Nano Lett. 2015, 15, 2620−2626.<br />
(25) Liu, Q.; Gao, M. R.; Liu, Y.; Okasinski, J. S.; Ren, Y.; Sun, Y.<br />
Quantifying the Nucleation and Growth Kinetics of Microwave<br />
Nanochemistry Enabled by in Situ High-Energy X-<strong>ray</strong> Scattering. Nano<br />
Lett. 2016, 16, 715−20.<br />
(26) Karim, A. M.; Al Hasan, N.; Ivanov, S.; Siefert, S.; Kelly, R. T.;<br />
Hallfors, N. G.; Benavidez, A.; Kovarik, L.; Jenkins, A.; Winans, R. E.;<br />
Datye, A. K. Synthesis of 1 nm Pd Nanoparticles in a Microfluidic<br />
Reactor: Insights from in Situ X-<strong>ray</strong> Absorption Fine Structure<br />
Spectroscopy and Small-Angle X-<strong>ray</strong> Scattering. J. Phys. Chem. C 2015,<br />
119, 13257−13267.<br />
(27) van der Stam, W.; Rabouw, F. T.; Geuchies, J. J.; Berends, A. C.;<br />
Hinterding, S. O. M.; Geitenbeek, R. G.; van der Lit, J.; Prevost, S.;<br />
Petukhov, A. V.; de Mello Donega, C. D. In Situ Probing of Stack-<br />
Templated Growth of Ultrathin Cu 2‐x S Nanosheets. Chem. Mater.<br />
2016, 28, 6381−6389.<br />
(28) Mozaffari, S.; Li, W.; Thompson, C.; Ivanov, S.; Seifert, S.; Lee,<br />
B.; Kovarik, L.; Karim, A. M. Colloidal Nnanoparticle Size Control:<br />
Experimental and Kinetic Modeling Investigation of the Ligand-Metal<br />
Binding Role in Controlling the Nucleation and Growth Kinetics.<br />
Nanoscale 2017, 9, 13772−13785.<br />
(29) Cheong, S.; Watt, J.; Ingham, B.; Toney, M. F.; Tilley, R. D. In<br />
Situ and ex Situ Studies of Platinum Nanocrystals: Growth and<br />
Evolution in Solution. J. Am. Chem. Soc. 2009, 131, 14590−14595.<br />
(30) Cormary, B.; Li, T.; Liakakos, N.; Peres, L.; Fazzini, P. F.; Blon,<br />
T.; Respaud, M.; Kropf, A. J.; Chaudret, B.; Miller, J. T.; Mader, E. A.;<br />
Soulantica, K. Concerted Growth and Ordering of Cobalt Nanorod<br />
Ar<strong>ray</strong>s as Revealed by Tandem in Situ SAXS-XAS Studies. J. Am. Chem.<br />
Soc. 2016, 138, 8422−8431.<br />
(31) Lassenberger, A.; Grunewald, T. A.; van Oostrum, P. D. J.;<br />
Rennhofer, H.; Amenitsch, H.; Zirbs, R.; Lichtenegger, H. C.;<br />
Reimhult, E. Monodisperse Iron Oxide Nanoparticles by Thermal<br />
Decomposition: Elucidating Particle Formation by Second-Resolved in<br />
Situ Small-Angle X-<strong>ray</strong> Scattering. Chem. Mater. 2017, 29, 4511−4522.<br />
(32) Ortiz, N.; Hammons, J. A.; Cheong, S.; Skrabalak, S. E.<br />
Monitoring Ligand-Mediated Growth and Aggregation of Metal<br />
Nanoparticles and Nanodendrites by in Situ Synchrotron Scattering<br />
Techniques. ChemNanoMat 2015, 1, 109−114.<br />
(33) Sakamoto, N.; Harada, M.; Hashimoto, T. In situ and Timeresolved<br />
SAXS Studies of Pd Nanoparticle Formation in a Template of<br />
Block Copolymer Microdomain Structures. Macromolecules 2006, 39,<br />
1116−1124.<br />
(34) Harada, M.; Tamura, N.; Takenaka, M. Nucleation and Growth<br />
of Metal Nanoparticles during Photoreduction Using In Situ Time-<br />
Resolved SAXS Analysis. J. Phys. Chem. C 2011, 115, 14081−14092.<br />
(35) Manocchi, A. K.; Seifert, S.; Lee, B.; Yi, H. In Situ Small-Angle<br />
X-<strong>ray</strong> Scattering Analysis of Palladium Nanoparticle Growth on<br />
Tobacco Mosaic Virus Nanotemplates. Langmuir 2011, 27, 7052−<br />
7058.<br />
(36) Wang, J. A.; Winans, R. E.; Anderson, S. L.; Seifert, S.; Lee, B.;<br />
Chupas, P. J.; Ren, Y.; Lee, S.; Liu, Y. Z. In Situ Small-Angle X-<strong>ray</strong><br />
Scattering from Pd Nanoparticles Formed by Thermal Decomposition<br />
of Organo-Pd Catalyst Precursors Dissolved in Hydrocarbons. J. Phys.<br />
Chem. C 2013, 117, 22627−22635.<br />
(37) Sun, Y.; Zuo, X.; Sankarana<strong>ray</strong>anan, S.; Peng, S.; Na<strong>ray</strong>anan, B.;<br />
Kamath, G. Quantitative 3D Evolution of Colloidal Nanoparticle<br />
Oxidation in Solution. Science 2017, 356, 303−307.<br />
(38) Kim, S. W.; Park, J.; Jang, Y.; Chung, Y.; Hwang, S.; Hyeon, T.;<br />
Kim, Y. W. Synthesis of Monodisperse Palladium Nanoparticles. Nano<br />
Lett. 2003, 3, 1289−1291.<br />
(39) Cargnello, M.; Doan-Nguyen, V. V. T.; Gordon, T. R.; Diaz, R.<br />
E.; Stach, E. A.; Gorte, R. J.; Fornasiero, P.; Mur<strong>ray</strong>, C. B. Control of<br />
Metal Nanocrystal Size Reveals Metal-Support Interface Role for Ceria<br />
Catalysts. Science 2013, 341, 771−773.<br />
(40) van Embden, J.; Chesman, A. S. R.; Jasieniak, J. J. The Heat-Up<br />
Synthesis of Colloidal Nanocrystals. Chem. Mater. 2015, 27, 2246−<br />
2285.<br />
1134<br />
Article<br />
(41) Wu, L.; Willis, J. J.; McKay, I. S.; Diroll, B. T.; Qin, J.; Cargnello,<br />
M.; Tassone, C. J. High-Temperature Crystallization of Nanocrystals<br />
into Three-Dimensional Superlattices. Nature 2017, 548, 197−201.<br />
(42) Cargnello, M.; Jaen, J. J. D.; Garrido, J. C. H.; Bakhmutsky, K.;<br />
Montini, T.; Gamez, J. J. C.; Gorte, R. J.; Fornasiero, P. Exceptional<br />
Activity for Methane Combustion over Modular Pd@CeO 2 Subunits<br />
on Functionalized Al 2 O 3 . Science 2012, 337, 713−717.<br />
(43) Cargnello, M.; Wieder, N. L.; Montini, T.; Gorte, R. J.;<br />
Fornasiero, P. Synthesis of Dispersible Pd@CeO 2 Core-Shell<br />
Nanostructures by Self-Assembly. J. Am. Chem. Soc. 2010, 132,<br />
1402−1409.<br />
(44) Jin, T.; Guo, S. J.; Zuo, J. L.; Sun, S. H. Synthesis and Assembly<br />
of Pd Nanoparticles on Graphene for Enhanced Electrooxidation of<br />
Formic Acid. Nanoscale 2013, 5, 160−163.<br />
(45) Xi, Z.; Erdosy, D. P.; Mendoza-Garcia, A.; Duchesne, P. N.; Li, J.<br />
R.; Muzzio, M.; Li, Q.; Zhang, P.; Sun, S. H. Pd Nanoparticles<br />
Coupled to WO 2.72 Nanorods for Enhanced Electrochemical<br />
Oxidation of Formic Acid. Nano Lett. 2017, 17, 2727−2731.<br />
(46) Liu, Q. S.; Bauer, J. C.; Schaak, R. E.; Lunsford, J. H. Supported<br />
Palladium Nanoparticles: An Efficient Catalyst for the Direct<br />
Formation of H 2 O 2 from H 2 and O 2 . Angew. Chem., Int. Ed. 2008,<br />
47, 6221−6224.<br />
(47) Niu, Z. Q.; Peng, Q.; Gong, M.; Rong, H. P.; Li, Y. D.<br />
Oleylamine-Mediated Shape Evolution of Palladium Nanocrystals.<br />
Angew. Chem., Int. Ed. 2011, 50, 6315−6319.<br />
(48) Man, R. W. Y.; Brown, A. R. C.; Wolf, M. O. Mechanism of<br />
Formation of Palladium Nanoparticles: Lewis Base Assisted, Low-<br />
Temperature Preparation of Monodisperse Nanoparticles. Angew.<br />
Chem., Int. Ed. 2012, 51, 11350−11353.<br />
(49) Lv, T.; Wang, Y.; Choi, S. I.; Chi, M. F.; Tao, J.; Pan, L. K.;<br />
Huang, C. Z.; Zhu, Y. M.; Xia, Y. N. Controlled Synthesis of<br />
Nanosized Palladium Icosahedra and Their Catalytic Activity towards<br />
Formic-Acid Oxidation. ChemSusChem 2013, 6, 1923−1930.<br />
(50) Mazumder, V.; Sun, S. H. Oleylamine-Mediated Synthesis of Pd<br />
Nanoparticles for Catalytic Formic Acid Oxidation. J. Am. Chem. Soc.<br />
2009, 131, 4588−4589.<br />
(51) Liu, Y.; Wang, C.; Wei, Y. J.; Zhu, L. Y.; Li, D. G.; Jiang, J. S.;<br />
Markovic, N. M.; Stamenkovic, V. R.; Sun, S. H. Surfactant-Induced<br />
Postsynthetic Modulation of Pd Nanoparticle Crystallinity. Nano Lett.<br />
2011, 11, 1614−1617.<br />
(52) Ortiz, N.; Skrabalak, S. E. Manipulating Local Ligand<br />
Environments for the Controlled Nucleation of Metal Nanoparticles<br />
and their Assembly into Nanodendrites. Angew. Chem., Int. Ed. 2012,<br />
51, 11757−11761.<br />
(53) Cargnello, M.; Doan-Nguyen, V. V. T.; Mur<strong>ray</strong>, C. B.<br />
Engineering Uniform Nanocrystals: Mechanism of Formation and<br />
Self-assembly into Bimetallic Nanocrystal Superlattices. AIChE J. 2016,<br />
62, 392−398.<br />
(54) Zhang, F.; Ilavsky, J.; Long, G. G.; Quintana, J. P. G.; Allen, A.<br />
J.; Jemian, P. R. Glassy Carbon as an Absolute Intensity Calibration<br />
Standard for Small-Angle Scattering. Metall. Mater. Trans. A 2010, 41,<br />
1151−1158.<br />
(55) Zheng, H. M.; Smith, R. K.; Jun, Y. W.; Kisielowski, C.;<br />
Dahmen, U.; Alivisatos, A. P. Observation of Single Colloidal Platinum<br />
Nanocrystal Growth Trajectories. Science 2009, 324, 1309−1312.<br />
(56) Wang, F. D.; Richards, V. N.; Shields, S. P.; Buhro, W. E.<br />
Kinetics and Mechanisms of Aggregative Nanocrystal Growth. Chem.<br />
Mater. 2014, 26, 5−21.<br />
(57) Mourdikoudis, S.; Liz-Marzan, L. M. Oleylamine in Nanoparticle<br />
Synthesis. Chem. Mater. 2013, 25, 1465−1476.<br />
(58) Gallagher, P. K.; Gross, M. E. The Thermal-Decomposition of<br />
Palladium Acetate. J. Therm. Anal. 1986, 31, 1231−1241.<br />
(59) Amatore, C.; Jutand, A.; M'barki, M. A. Evidence of the<br />
Formation of Zerovalent Palladium from Pd(OAc) 2 and Triphenylphosphine.<br />
Organometallics 1992, 11, 3009−3013.<br />
(60) Stephenson, Ta; Morehouse, Sm; Powell, A. R.; Heffer, J. P.;<br />
Wilkinson, G. Carboxylates of Palladium Platinum and Rhodium and<br />
Their Adducts. J. Chem. Soc. 1965, 0, 3632−3640.<br />
DOI: 10.1021/acs.chemmater.7b05186<br />
Chem. Mater. 2018, 30, 1127−1135