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Using APEX2 to Analyze Twinned Crystals - Bruker AXS Support

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Types of twins –<br />

Non-merohedral twin<br />

• Twin opera<strong>to</strong>r is arbitrary but often<br />

a rotation of 180°<br />

• no exact overlap of reciprocal<br />

lattice points<br />

• Close, split and overlapping<br />

reflections<br />

• Special <strong>to</strong>ols for cell determination<br />

• Data integration requires more<br />

than one orientation matrix<br />

• Structure solution not difficult after<br />

“de-twinning”<br />

05.05.2011 4

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