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EPICLON EXA-9710

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Phosphorus Modified Epoxy Resin<strong>EPICLON</strong><br />

R<br />

<strong>EXA</strong>-<strong>9710</strong> for<br />

Halogen-free Laminates<br />

<strong>EPICLON</strong><br />

R<br />

<strong>EXA</strong>-<strong>9710</strong><br />

<br />

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UL94V-0<br />

<br />

<br />

<br />

<strong>EPICLON</strong> <strong>EXA</strong>-<strong>9710</strong><br />

<br />

<strong>EPICLON</strong> <strong>EXA</strong>-<strong>9710</strong><br />

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<strong>EPICLON</strong> <strong>EXA</strong>-<strong>9710</strong><br />

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Table 1<br />

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<strong>EPICLON</strong><br />

<strong>EXA</strong>-<strong>9710</strong><br />

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<strong>EPICLON</strong> <strong>EXA</strong>-<strong>9710</strong><br />

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Table 2 <br />

DICY<br />

<br />

PHENOLITE LA-7054<br />

<br />

Table 1 Typical Properties of <strong>EPICLON</strong> <strong>EXA</strong>-<strong>9710</strong><br />

Appearance<br />

Liquid<br />

Color, Gardner 2-3<br />

Epoxy equivalent weight (g/eq) 496<br />

Viscosity (mPas) 1500<br />

Non volatile (wt %) 70<br />

Phosphorus content (wt %) 3<br />

Solvent<br />

Methyl ethyl ketone<br />

Table 2 Varnish Composition<br />

Parts by weight Formulation 1 Formulation 2<br />

<strong>EXA</strong>-<strong>9710</strong>, solid 100 100<br />

Dicyandiamide (DICY) 2.1 <br />

LA-7054, solid* 25<br />

2-ethyl-4-methyl imidazole 0.3 0.05<br />

Methyl cellosolve 20 20<br />

Dimethylformamide 20 20<br />

Gel time at 160 (sec) 500 360<br />

*Amino-triazine novolac resin, OH value 125<br />

64 DIC Technical Review No.8 / 2002


<strong>EPICLON</strong> <strong>EXA</strong>-<strong>9710</strong><br />

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Table 3<br />

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Table 3 Properties of Laminates<br />

Formulation 1 Formulation 2<br />

Laminate thickness (mm) 1.6 1.6<br />

Phosphorus content (%) 2.9 2.4<br />

Tg by TMA () 124 125<br />

Tg by DMA () 147 149<br />

Peel strength, 35Cu (KN/m) 2.2 2.2<br />

Inner layer cloth (KN/m) 2.5 2.4<br />

Water absorption, boil 2hrs (wt %) 0.35 0.38<br />

Solder heat resistance, 260<br />

30 sec dip after boil 2hrs<br />

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UL<br />

UL-94V-0 <strong>EPICLON</strong> <strong>EXA</strong>-<strong>9710</strong><br />

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<strong>EPICLON</strong> <strong>EXA</strong>-<strong>9710</strong><br />

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Ames<br />

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28NOEL=1,000 mg/kg/day<br />

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TEL:0436-41-9815<br />

DIC Technical Review No.8 / 2002<br />

65

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