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CERTIFICATE Cenificd tu s4l.!q !I4L quj!44 !!4t brr c'ried ou his rcs€lrch rd exD€rimdf.l work oo thc topic cntid.d ts'QUAiTrATrvE All^rysts ot soME t'EG!rA!L! O[!l tY |tc NMt AND Cltroil^rolcR^llllc METttot s" llnder out g0id.{Ee rnd sw€rvision in lhe labor'ton$ ofNational Cen' re of Excllldc€ in Antb4icrl Chedlarv, Utivenity of Sindlq Jaftshoro Paki$n H$ rcs.€rEh wo* is origfu! ddircr nd hi! tn sis is wodty of FB"iatiotr to tbe Universiry ofsindh for thc rwed ofd.gr.c of Doctor of Pttilosphy itr Anibriol chemsary. Protulor and Supervisor Natiodl Cefi. of frx.illdc. in AEMic.l Ch.tnify Univdsity of Sirdh, Jmhoro. ffimr !d c}$?.wiror Nrin l C.d!r ofEcclbr. ir Adyli..l Crrdrry UaEty of Sd! Jdo.o
QUANTITATIVf, <strong>BY</strong> 'JC NMR ANALYSIS OF SOME VEGETABLE OILS AND CHROMATOGRAPHIC METHODS ABSTRACT CC ,r,ni" Uo t-t €"ii out o lo v's'.rlb oil o!9|| in dd'r io "C Xm ",,a find oul qu.miritct 6. tut, eid @nF!'nn in rh€' oik sds e{inis ofs'db Aoh Shdh AgrFultui.l R6arch lsrndc Taldoi'r! P'lnur bv' bar ldfz'd in rhn tndv Oib ht b.€o *tEd.d from fi* t*ds bv 3Ltd'rd ndt@d Thc oil si'pl€! '|v' ben ul'n trom bdl d.kd Tn. 3-& wde d'o rdtad fo' 6orgi td|6' misture oil onr'nt fr4 nnv icid.nd D.oGn (Ml) @it.I gtl 'dqn| of fooign 'd6 9s grsan it @noE 'd trd liBc.d Mo6lur. us hish in cottos"4 tunno6 (HOl) rnd lis€td' Cotto6*d' iunflowd IHG|l. !i li!..r| o*d htrb oil d|an FF tutv @irL in t[ oih we h'low d' Fnsi bh lini. Ts $)d-n wi.i6 ro'd s Et-L 'd \vilin lbe'd biSh Fo&n @nE od. drcl.d.dl oh.i"d @dsc'lv €"|o dlv'd for @bu itd'( tc 6ltv rcd, iodi v.t!. (Iv) dd stoni66rio rbt (sv) Hi'n ndiE dE 6' obtd'd i'r "fno*.r .nd lro4d o'lt naih 60dcd rhMd rh' lowtr !'potrIfioton vtlu' Stin'Lri@ ELriion tine T' of@rdn"t rrc @' obt'in'd for oilt to fld th! 'll 1im. ..out.d for 'rC Nrfl aslFir' t!8nd Tr {hF of i' o$ of cD ' l sd4e 8 'ound atuo. of liB..d oil For qq|nintiw ulvtit tP'dr OoD G3? ppn w' rcqui"d tnd th' che s'liot@ of oih oro tm sm'rF s G4tv GrolP (i) ilvonEd ot t'6o6 t'n 6nc Gd o'hrddt Gt of oik b€bns.d to ctow {ii) v'ticn 4lnii'd &nb witlt tbc do{th bo'i fu66) 6 .dditio. to lh. &ids fou'i li Gtu[' (') Nat oil gnp!* wse u'd without |nv lolvat iD NMR aEltsit wing Ertdrl Der.riun t ct r3c NMR qNtiLiiv' 'dvsis showod h!! lmut of srw't'd inv ad! r
Page 1 and 2: QUANTITATM ANALYSIS oF soME vncnres
Page 6 and 7: cottoB.€d ed sorab.{a oih. Acid w
Page 8 and 9: 3.2 U€ ofv.lrtbb ot! 3.3 EdibL F.
Page 10 and 11: 5, v.!t b Ol lDryri nz.l F.w AcA (M
Page 12 and 13: I r Us6 of lrious v.sd.bL otu LIST
Page 14 and 15: (6.10) tR $.q@ C.alc€t Pto{otr Dd
Page 16 and 17: ACKNOWLEDGEMENT I wiln to €4r* ny
Page 18 and 19: l-1 Iniroduction CHAPTER. I INTRODU
Page 20 and 21: s|wh.r re.6itic. Tlit pir@ w$ &!Fd
Page 22 and 23: suggor.d lbd indnidot tirbeid.! on
Page 24 and 25: It.l9l Bred.nd F@L€l J- Aa Cban S
Page 26 and 27: {l.6sl S. Sbr|Lt Ai od A. w. K Kb@d
Page 28 and 29: 2.2.1 rnpuritica Adoinu.* flcis! st
Page 30 and 31: @ctroiaa with th. o@ dryine rctoo@
Page 32 and 33: .ll th€ triEo3a n! f.eding sruf,
Page 34 and 35: 6DD rtic, bron p'rtL or rcd S..d w'
Page 36 and 37: LmSEED! MUSTARD SEEDr it 25-35% oft
Page 38 and 39: .rd @y .lF b. usd $ fiEl .nd fcnili
Page 40 and 41: SAFFLOWER SEEDST lr ir ofotb.B st p
Page 42 and 43: SUN'IIIWER SEEDS. Hdidu.dN Lin.4 Ar
Page 44 and 45: 12.f?l Orlord Arvic.f b^rrF,ltltd,M
Page 46 and 47: J.l Introduction CHAPTER-3 VEGETABL
Page 48 and 49: Ahour 20% of id€dibk oib .r. a.d
Page 50 and 51: !..tiutrd d.ry tury slt re6 & &r ba
Page 52 and 53: J.a Strrcarr. .f Fr[y Aci- 1s-.dlt/
Page 54 and 55:
t5.l.2 t Ediv! l.d.! Th. r.n crre h
Page 56 and 57:
AMbrial i-pttur Th. eoooift.in. v.l
Page 58 and 59:
lL t- ftry.dild i. tdor !rf!.t h..
Page 60 and 61:
CHAPTER - 4 THF',OR"ETICAL PRINCIPL
Page 62 and 63:
slErc 6H is i!. lire si&h. tC lit.
Page 64 and 65:
d2"2 G$ Lhuid Chronriogr.phy Crs cn
Page 66 and 67:
Thc blu@ Vr My b. ohlt dbydr.flow .
Page 68 and 69:
REFERENCES l1.rl G. D. a.da, Eigh R
Page 70 and 71:
(D) v...!.01. Oilr...l! (i) c.ttoD.
Page 72 and 73:
6 tI c jr i t t t 3 + 5 .E I : I+ r
Page 74 and 75:
Fig(s.4) Fl (s.2) r-3-F- rrtit r',2
Page 76 and 77:
g::i$;: !:ji !! !. 'E:l*i::::g?!:::
Page 78 and 79:
6l !t I 5E d B'. I .a it ! .I F{ i!
Page 80 and 81:
t61.22 G.t cttontqr.*b @.ltt s rrun
Page 82 and 83:
5,6.4 DeterniElion of SrDonificrtio
Page 84 and 85:
5.7.2 PROTEIN Wds[r ot.+dii.s r l0o
Page 86 and 87:
6.1 Oilseed Amlvsis CHAPTER - 6 RES
Page 88 and 89:
2. t. 5 3. (Ihori-78) (HGr) (Ebn90)
Page 90 and 91:
E E 4 -€:t€:en;:n:;Eit:E: ! !:d
Page 92 and 93:
n :;:€::::i*;;!;i gs g = i': .? i
Page 94 and 95:
E a : .x t .n 3
Page 96 and 97:
t : 79 'c F n I a I .E! Y> !E .E.!
Page 98 and 99:
8l e, .t E tf
Page 100 and 101:
h b s.m Aon Tlbk 6,3 tbrl th. hiS!.
Page 102 and 103:
.bb Ga AdF..ot of O.Dh.l 8llito .f
Page 104 and 105:
Qddi.tiv€ u|l6n of hoth srorp of
Page 106 and 107:
t9 , I a 6 F o IE .3tr IF Eg ta I
Page 108 and 109:
62LL2 c.tst tiN 4 G@p (4 oi,. TrEo.
Page 110 and 111:
(iv) s.tur6 96slnr$- = lo0 -(ri6E +
Page 112 and 113:
i 'I rt I T .€ - t6 6 t cE I 9
Page 114 and 115:
vl ,[; I I 5 I ! I , , I I
Page 116 and 117:
lL lD a !! E 'I ,2 .Ig. 5 t 6 t
Page 118 and 119:
Th. 16r|13 of p@tige @nD@nion of to
Page 120 and 121:
For GC. th€ lesa.bL oil ynrpLs ws
Page 122 and 123:
T.bl. 6? P.tk tu{r, fi.ighr of P..l
Page 124 and 125:
- g-. a- :! ct u3 F3 F; I I f I i I
Page 126 and 127:
TAII 6.' P.rc.ot gr Frtty Acid CooD
Page 128 and 129:
T.t{.6.10 gic.6ob of tb. rtre. util
Page 130 and 131:
Trblc 6.t2 to 6.rJ br @q.nriv. c!|.
Page 132 and 133:
T.bk 6.14 lbts th. onprtltirc 3tudy
Page 134 and 135:
REFERENCES l6.U C.dd Ari!.dliu C.|@
Page 136 and 137:
Prot bly str ofth6. t.v€ inctas.d
Page 138 and 139:
.1rds Scrors. Co ir nim{rseisN &grd
Page 140 and 141:
6hos hrs! d.sice of lNtulbn in rn6
Page 142 and 143:
! 3a ptr It io clar rt t iios @npLl
Page 144 and 145:
ootld .rd wB regridcd $ . h6ln h..r
Page 146 and 147:
%), For lld. ro$6, tlo @ncd id of .
Page 148 and 149:
CHAPTER - 8 CONCLUSION AND FUTURE P
Page 150 and 151:
APPENDIX. 1 (P.rk A,3lgrn.lo rtrd o
Page 152 and 153:
cAtBola No CHAN PPM (I) PEAXS cl :'
Page 154 and 155:
(] l'..k A$tgntrfrr ot !ioJ!b..n oi
Page 156 and 157:
'iOf..f f.g"-r,nf .con)Ol (.otrel.L
Page 158:
'--.' PCrrf rd:m-* fCsBlroli (5si)
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