View Document Here - Hanford Site

Quaaterra 6nmrr,naeri 

13,715 Rider Inc, Anmi 

Ea rth Cih, Miso:in ata4 1 

1 4 208-8i66 bienhanir 

314 208-875- j,, 

Bechtel Hanford Incorporated 

3350 George Washington Way 

Richland, Washington 99352 

Project Number 

SDG 

Number of Samples 

Sample Matrix 

Data Deliverable 

Date SDG Closed 

II Introduction 

CASE NARRATIVE 

550.184 

W02587 

Twenty (20) 

Water 

Summa ry 

November 10, 1998 

iiivanterra 

December 21, 1998 Ldta 

Attention: Joan Kessner 

t 

;.1516177 7\ 

_ hfvi 

On October 27, 1998 and October 28, 1998 a total of twenty "water" samples were received by 

Quanterra, Richland and transferred to Quanterra, St. Louis for chemical analysis. There were 

no comments or nonconformances associated with the shipping or receiving of the samples. 

Upon receipt, the samples were given the following laboratory ID numbers to correspond with 

the specific client ID's: 

St. Louis ID BHI ID SAF ID Matrix Date of Receipt 

19221-001 BOR494 C99-006 Water 27-OCT-98 

19221-002 BOR495 C99-006 Water 27-OCT-98 

19221-003 BOR4C7 C99-006 Water 27-OCT-98 

19221-004 BOR4C8 C99-006 Water 27-OCT-98 

19221-005 BOR499 C99-006 Water 27-OCT-98 

19221-006 BOR4 130 C99-006 Water 27-OCT-98 

19221-007 BOR4K9 C99-006 Water 27-OCT-98 

19221-008 BOR4LO C99-006 Water 27-OCT-98 

19221-009 BOR4 174 C99-006 Water 27-OCT-98 

19221-010 BOR4 1`5 C99-006 Water 27-OCT-98 

19221-011 B0R4D1 C99-006 Water 27-OCT-98 

19221-012 BOR4D2 C99-006 Water 27-OCT-98 

19221-013 BOR4 176 C99-006 Water 27-OCT-98 

19221 -0 14 BOR4L4 C99-006 Water 27-0C'r-98 

rl^ 

30C) oo ,^ 

. 

f /


December 21, 1998 

Project Number: 550.184 

SDG: W02587 

Page 2 

St. Louis ID BHI ID SAF ID Matrix Date of Receipt 

19254-001 BOR491 699-006 Water 28-OCT-98 

19254-002 BOR4131 C99-006 Water 28-OCT-98 

19254-003 BOR4132 C99-006 Water 28-OCT-98 

19254-004 BOR492 C99-006 Water 28-OCT-98 

19254-005 BOR4178 C99-006 Water 28-OCT-98 

19254-006 BOR4F7 C99-006 Water 28-OCT-98 

III. Analytical Results/ Methodology 

rrjuanterra 

The analytical results for this report are presented by analytical test. Each set of data includes 

sample identification information, analytical results and the appropriate detection limits. 

Analyses requested: ICP Metals by EPA method 6010A 

Mercury by EPA method 7470 

Anions by EPA method 300.0, (CL,FL,NO2,NO3.SO4) 

Deviation from Request: No Deviation from requested methods. 

IV. Definitions 

The following codes are used to denote laboratory quality control samples and can be found in 

the data summary section of this report: 

QCBLK- Quality Control Blank, Method Blank 

QCLCS- Quality Control Laboratory Control Sample, Blank Spike 

DUP- Laboratory Duplicate 

MS- Matrix Spike 

MSD- Matrix. Spike Duplicate 

O()OOD ?


December 21, 1998 

Project Number: 550.184 

SDG: W02587 

Page 3 

V. Comments 

C` uanterra 

Inorganics: A Laboratory Control Sample, Method Blank, Matrix Spike and Matrix 

Spike Duplicate were analyzed with each preparation batch per the 

protocol for this analysis. 

The percent difference for the Magnesium serial dilution (10.9) was 

greater than 10 which was indicated on the form ones by the "E" flag. 

Wet Chemistry : A Laborato ry Control Sample, Method Blank, Matrix Spike and 

Laborato ry Duplicate were analyzed with each preparation batch per the 

protocol for this analysis. 

There were no comments or nonconformances for the Anions analysis. 

I ce rtify that this Summary Package is in compliance with the SOW, both technically and for 

completeness, for other than the conditions detailed above. Release of the data contained in this 

hard copy data package has been authorized by the Laboratory Manager or a designee, as 

verified by the following signature. 

Reviewed and approved: 

h.^^l o -tq - JO fvtMe-` 

Shiela M. Louvier 

St. Louis Project Manager 

000cuy

erulec t. 143 n1) ger R. White 

Sample Lleader Tempi ate 

- 

Sample Nc. Client ID 

Comments 

U Container Type 

Data 

19221-001 13 OR494 

C99-006 

PN Plastic-500m1 

19221-OOIMS POR494 

C99-006 

ON - Plastic-SOOn:l 

19221-ODIMSD BOR494 

C99-006 

1 PH Plastic-500m1 

19221-002 BOR491 

C99-006 

1 

1 

13221-003 BHR.4^7 

99-OOE 

FN -clastic-50Wn1 

19221-004 BOR4C8 

C99-003 

1 

I 

1 

19221-005 BOR499 

C99-006 

j^^- ample Las uoL L. t.1 1au screened. 

C 

Cal 

Analysis 

ICAPD/6010/Q4. 

ICAPD/6010/Q4 

ICAPD/6010/Q4 

-L,', pU U/Q4 

FL/300.0/Q4 

TCAP/5010/Q4 

NO2/300-0/Q4 

N(1 3/300.0/Q4 

504/300-0/Q4 

TCAPD/6010/Q4 

—,10 qQ4 

00 /Q4 

I AP/6010/Q4 

NO2/300.0/Q4 

NO3/3U0 0/Q4 

50413 1)0 1,/Q4 

¢ranter 11) November 03, 1998 10:00 am 

Accountr 10722 Project: SSO.184 Quanterra -Richland OAS Nu. 551.184 Rev- 3 

Master Sample Login: 19221 

C-Matrix 

Water 

Water 

Water 

Water 

Water 

Water 

Water 

Reviewed by and Date: L• _-^ }.^3^v-^- 

(413192:100) 

(413192:100) 

(413192:100) 

cio as P7 

Date: Collected Received Due Shipper Rad Category Rad Sample No. 

Class Preservative Anal. Due Date Hold Date Site (Container Numbers :% Filled) 

27-OCT-98 10:22 27-OCT-98 14:09 25-NOV-98 AIRBORNE I 

S M03 18-NOV-98 25-APR-99 S11A 

27 OCT 98 10.22 27-OCT-98 14:09 25 NOV 98 AIRBORNE 1 

S IINO3 18-NOV- 98 25-APR-99 S11A 

27-OCT-98 10:22 27-DCT-98 14:09 25-NOV-98 AIRBORNE 1 

S M03 18-NOV-98 2S-APR-99 S11A 

27-CCT-98 10 22. 27-OCT-98 11:09 25-NOV-98 AIRBORNE 1 

S COLD 18-NOV-98 24-NOV -98 S11A (413194:100) 

S COLD 18-NOV-99 24-NOV -98 S11A (4131941100) 

S HNO3 18-NOV-98 25-APR -99 S11A (413193:100) 

.ti COLD 18-NOV-98 29-OCT-98 S11A (413194:100) 

COLD 18-NOV-98 29-OCT-98 S11A (4131941100) 

S COLA 18-NOV-98 24-NOV -98 S11A (413194:100) 

Screening not Required 




27 -OCT 98 09:19 2TOCT -98 14:09 25-NOV-98 AIRBORNE 1 Screening not Required 

S HNO3 18-NJV 98 2S-APR -99 S11A 1413200:100) 

27- OC1'-98 09:19 27- OCT-98 14:09 25-NOV-98 AIRBORNE i Screen;nq not. Required 

COLD 18-NOV 9t 24 NOV j8 S11A (413202:100) 

S COLD 18-NOV-98 24-NOV-98 S11A (413202:100) 

C HNO3 18-NOV-98 25 - APR - 99 S11A (413201:100) 

S COLD 18-NOV-98 29-OCT-98 S11A (413202:100) 

S COLD 18-NOV-98 29OCT 98 S11A (413202:100) 

S COLD 18-NOV-98 24 NOV-98 S11A (413202:100) 

27- OCT-98 11:D9 27- OCT-98 14:09 25-NOV-98 AIRBORNE 1 Screening not Required 

Page 1

p rol ect Manager R- White 

Sample Header 'template: 

---- - 

Qudcterra November 03. 1998 10:]0 am 

Account: 10722 Project: 550.184 Quanterra-Richland QAS No. `-5 0 .184 Rev. 3 


Reviewed by and Date: 

Sample No. Client I II 

Comment s 

C-Matrix Date: Collected Received Due Shipper Rad Category Rad Sample No. 

_ 4 

Data: 

Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:% Filled) 

1 PN P1a stir -500m1 ICAPD/6010/Q4 5 FB403 23-NOV-98 25-APR -99 S11A (413203:100) 

19221 -006 BOR4 11 0 Water 27- OCT-98 11:09 57-OCT-98 14.09 25-NOV-98 AIRBORNE 1 Screening not Required. 

C99-005 

l FN Pldst is 5 1111 ' 7 CL/300.0/Q4 S COLD 18-NOV-98 24-NOV -98 SIIA (413205:100) 

1 FL/300.0/Q4 S COLD 18-NOV-98 24-NOV -98 S11A (413205:100) 

1 ICAP/6010/Q4 S HNO3 18-NOV-98 25-APR -99 S11A (413204:100) 

I NO2/300.0/Q4 S COLD 18-NOV-98 29-OCT -98 SIIA (413205:100) 

1 NO3/300.0/Q4 S COLD 18-NOV-98 29-OCT -98 S11A (413205:100) 

1 SO4/300.0/Q4 S COLD 18-NOV-98 24-NOV -98 S11A (413205:100) 

19221 -007 BOR469 Water 27- OCT-98 08:35 27-OCT-98 14:09 25-NOV-98 AIRBORNE 1 Screening not Required 

C99-O0e 

I ^.+ -_^-__^- L OOmI :CAPD/6010/Q4 S HNO3 18-NOV 98 25-APR -99 SIM ( 4132(11:1011) 

11 !21 t'!! ,. ,,,. Wat ur 11 0 i-I'-)8 08:35 27-OCI'-98 19:09 25-NOV Id AIRBORNE 1 Screem nq not Required 

C99 0o, 

1 I-N - p lastic -SOOmI CL/300.O/Q4 COLD 18 NOV-98 24-NOV -98 511A .413206 .1001 

- FL/300.0/Q4 S COLD 18-NOV-98 24-NOV -98 SlIA (413208:100) 

1 ICAP/6010/Q4 a HNO3 18 NOV-98 25-APR -99 S11A 1413207:100) 

1 NO2/300.0/Q4 S COLD 18-NOV-98 29-OCT -96 S11A (413208:100) 

1 1403/300.0/Q4 S COLD 18-NOV-98 29-OCT -98 S11A (413208:100) 

1 SO4/300.0/Q4 S COLD 18-NOV-98 24-NOV-98 S11A (413208:100) 

19221 - 009 BOR414 Water 27- o("I-98 12:56 27-OCI-98 14:00 25-NOV-98 AIRBORNE 1 Screening not Required 

C99-005 

AN An6rer Glass 500ml HGD/7470/Q4 S HNO3 1.8- 140V-98 24-NOV-98 91IA f413210: 100) 

1 Pit Plastic -500 11 i ICAPD/6010/Q4 S HNO3 10-NOV-98 26-APR-99 Sl1A (413209:100) 

1-221 0 0 9015 HIIi Wat. ^r ,..I ,8 6 lr.au N..V-ii6 AIRBORNE 1 xreeni ng not Required 

C99-( 1 06 

lit , j,, H3P/7410/Q4 S IINO3 18-NOV-99 24 NOV-98 S11A 1413210:100) 

r y e21 -0 u9MaU B0R4F4 Water 27-OCT-98 12:56 27-OCT-98 14:00 25-NOV-98 AIRBORNE 1 Screening not Required 

C99-00t 

1 AN - Amber Gtass-500ml HGD/7470/Q4 S HNO3 1e-vnn_o8 __ ___ I_ ___„ X41321012.) 

f - 

1522.1-Bq9 M5U :.: ..ontiuued on next page. 

-'-S afyle I:. u: i..: it"n rad ";,,,I 

1. 

Page 2

Project Manage': R. White 

Sample Header 'Template 

Sample No Client ID 

Comments 

4 Container 'Type Analysis 

Data: 

19221-009ml) BOR4F4 

(Continued from previous page) C99-006 

'Il—se Cam tai r,e rs' have no assigned Products_ 

I PN - Plastic SOOml 

19221-010 B('R4F5 Water 

C99-006 

1 AN Class -500ml HG/7470/Q4 

1 PN - Plastic -500m1 CL/300.0/Q4 

` FL/300,0/Q4 

I ICAP/6010/Q4 

- NO2/300.0/Q4 

1 NO3/300.0/09 

504 /300.0/Q4 

19221-011 BOR4D1 Water 

C99-00F 

PG i —a r,u Souml ICAPD/6010/Q4 

19221 012 BOR4D2 Water 

C99-005 

1 PN _ p lastic-50 Cm1 _Li300.0/Q4 

1 FL/300.0/Q4 

1 ICAP/6010/Q4 

1 NO2/300.0/Q4 

1 NO3/300.0/Q4 

1 SO4/30n. 0/04 

i 121 01 :k4PC Water 

C99 -OOb 

PN Plastic 5 (1 0 ,111 CLi300.0/Q4 

1 i 300.O/Q4 

1 ICAP/6010/04 

1 _ NO2/300.0/Q4 

NO3/300.0/Q4 

1 i_ o. ., 300. a/Q4 

a.iilr hi. mI Lrr:: ri ,.. 'u .•d. 

( S 

Qua nterra November 03, 1998 10:00 am 

Account: 10 -/22 Prnj ect: X50.184 Quanterra-Richland QAS No, 550.184 Rev_ 3 


Reviewed by and Uate: 

C-Matrix Date: Collected Received Due Shipper Bad Category Bad Sample No. 

Class Preservative Anal. Due Date Hold Date Site (Container Numbers:} Filled) 

Water 27-OCT-98 12:56 27-OCT-98 1.4:00 25-NOV-98 AIRBORNE 1 Screening not Required 

HNO3 SIIA (413209:100) 

27-OCT-98 12:56 27-OCT-98 14:00 25-NOV-98 AIRBORNE 1 Screening not Required 

S HNO3 18-NOV-98 24-NOV-98 S 11 A 

5 COLD 18-NOV-98 24-NOV-98 SIIA 

S COLD 18-NOV-98 24-NOV-98 S11A 

S RNO3 18-NOV-98 25-APR-99 SlIA 

S COLD 18-NOV-98 29. OCT 98 S11A 

S COLA 18-NOV-98 29-OCT-98 S1IA. 

c COLD 18-NOV-98 24-NOV-98 SSIA 

27-OOT-98 10:15 27-OCT 98 1410, 25-NOV-98 AIRBORNE 1 

5 HNO3 18-NOV-98 26-APR-99 S11A 

27 07T-98 10:15 27-OCT-98 14;00 25-NOV-98 AIRBORNE 1 

(413213:100) 

!413212:100) 

(413212:1001 

(413211:100) 

(413212:100) 

^413e12:100) 

(413212:100) 

(413214:100) 

COLD 18-NOV-98 24- NOV -98 SIIA )413216:100) 

5 COLD 18- NOV -98 24- NOV -98 SIIA (413216:100) 

S HNO3 18- NOV-98 25-APR-99 S11A (413215:100) 

S COLD 18- NOV -98 29- OCT-98 SIIA (413216:100) 

S COLD 18- NOV -98 29- 0('' C -98 S11A (413216:100) 

n COLD 18- NOV -9? 24 NOV 98 SIIA !413216 , 100) 

Se reeving not Required 


CI-9S :.9:05 29-OCT -9n 14:00 25-NCV-9N AIRBORNE _u cai: my not Required 

d ('OLD 18-50' -38 24- NOV-98 SIJA (413219:100) 

S COLD 18- NOV -98 24- NOV-98 SIIA (413219:100) 

S HNO3 18- NOV-98 25- APR-99 SIIA (41321.8:100) 

S COLD 18- NOV-98 29- OCT-98 S11A (413219:100) 

S COLD -„ ..-O -38 2y. oCi-98 S11A (413219:100) 

S COLD 18- NOV-98 24 NOV 98 SIIA (433219:100) 

Page 3

Froject Manager: R White 

Sample Header 'Template: 

Sample No. Client ID 

Comments 

4 Container 'type 

Data: 

19221-013DUP bUR4F6 

C99-006 

l IN - Plastic-50otn1 

1 

1 

1 

1 

19221-013MS Hl1R4F6 

C99-006 

1 

1 

FN - Elastic-500m1 

19221 oll BOR4 114 

C99-006 

G 

l^ 

CN Elastic-5001x; 

3'-5 glll^le Ins not been r ad sr: eened. 

- - - 

Quanterra November _- - 03, 1998 

-- 

10:00 am 

-- -- 

Account: 10722 Froject: 550.184 Quanterra- Richland QAS No. 550.184 Rev. 3 

Reviewed by and Date: 


C-Matrix Date:. Collected Received Due Shipper Had Category Had Sample No. 

lnalysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:& Filled) 

Water 27-OCT-98 94:05 27-OCT -98 14 :00 25- NOV-98 AIRBORNE 1 Screening not .Required 

:L/300. 0/Q4 S COLD 18-NOV-98 24-NOV-98 S11A (413219:10D1 

'L/300.o/Q4 S COLD 18-NOV-98 24-NOV-98 S11A (413219:100) 

402/300.O/Q4 S COLD 18-NOV-98 29-OCT-98 S13A (413219:100) 

]03/300.0/Q4 S COLD 18-NOV-98 29-OCT-98 S11A (413219:100) 

SO4/300.0/Q4 S COLD 18-NOV-98 24-NOV-98 S11A ( 413219:100) 

Water 27-CCT-98 C9:05 27-OCT-98 14:00 25-NOV-98 AIRBORNE 1 Screening not Required 

1./300-O /Q4 S COLD 18-NOV-98 24-NOV-98 S11A (413219:1001 

L/300.O/Q4 c COLD 18-NOV-98 24-NOV-98 S11A (413219:100) 

102/300.0/Q4 S COLD 18-NOV-98 29-OCT-98 S11A (413219:100) 

103/300 -0/Q4 S COLA 18-NOV-98 29-OCT-98 S11A (413219:100) 

04/30,0. 0/Q4 .. COLD 18-NCV-98 24 -NOV-98 oi.n 1413219. 10 . 

Water 27-OC'I' 98 09'05 27-OCT-96 14:00 25-NUV-98 AIRBORNE 1 Screening not Required 

CAPD j o010 /Q4 S NNO3 18-NOV-98 2S-APR-99 S11A (413220:i001 

Page 4 

- 

-- -

Chain of 

Custody Record 

j ( t) ttO 

if7-7/ 

Returned to Client n, PINK - Field Gopy 

"( 

q 1C 

cult # a ilo7 ? 7 

QUA 4124 

Client 

0197 

ESC-h^C^^' 

Project Manager 

FA 

Dat 

ll^ 

Address Telephone Number (Area Co eJ/Fax tuber Lab Number 

City State Zip Code 

Project Name / 

Contract'Purchase OmeriOuole No. 

Sample I . No and Description 

(Conleers m for each sample may be combined on one line) 

_ 

1 

v- 4 9 

9 -- 

r--q — 

WIrl 

- - q u2 

F21 

ô 

r 3 tiK 

q Ncn Hazard q Flammable q Skin Irritant q Poison B \`^4 

Tutu Around Time Required 

24 Hours q 48 Hours q 7 Days q 1 ,;.D,^ys q 21 Days 

3. FIakS gwshed By 

—mmew,—.—___— 

Co 

re cet t q,4 

DISTRIBUTION: WHITE Stays with the Sample, 

Date Time 

Site Contact Lab Contact 

Carner/Waybdl Number 

Matrix 

a 

m 

a pre ulsposa, 

o 

= 

Containers & 

Preservatives 

o 

i i 

wl^- ^^^ 

- ^ ^ 

o 

= 2 

Return To Client q Disposal By Lab q A rchive For 

OC Requirements (Specify) 

,Time 3. Received By 

Analysis (Attach list if 

more space is needed 

Q%uanterra 

Chain of Custody Numb 

10 17 E 

Page of 

Special Instructions/ 

Conditions of Receipt 

(A lee may be assessed d samples are retained 

Months longer than 3 months) 

lj `M n9^s hed W 1, D /l , I „ / 1 Vl Q 

/ 

v ; ^{ Ti/m/e^(^5j\) 

1. Received By 

aic c 

/d;1p`jV ^ eYcb 

Date Time o Recci:cd By 

,^ 

, Time 

Date 

1—

PNNI, 

Colleclnr 

AF No. 

C.99-006 

— — — - ---- — 

CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST 

RR FOX (PIFTI) Contact/Reauester 

)IT Telephone No. MSIN FAX 

Sampline Oriein 

HANFORDSITE 

Purchase Order/Charee Code 

Protect Title Loebook No. Ice ChestTemp. 

Shipped To (Lab) Method of Shi pment Bill of Ladina/Air Bill No. 

Protocol Data Turna ro und OHske Property No. 

POSSIBLE. SAMPLE IIALARDS/REMARKS 

* ^ 

C.O.C. s 

SPECIAL INSTRUCTIONS Hold Time Imal A cl ivit y Exemption: 

FAX COPIES OF QES & I MA LOG-INTO DL STEW AR T (372 - 1704) 170T& IM DUNCAN (372-9052). 

C99-006-45 

Page 1 of 1 

Yes Lj No 

Sample No lah ID * Uaie Time No/Type Conlniner Sample Analysis 

Preservative 

BOR401 (F) W 1x500-mL Ge CP Metals - 6010A RCRA GW HNO3 to pH

PNNL 

- _ -- -- 


Collector 

RR FOX (R 'Af No. 

C99-W6 

Contac tlReauester 

1H KF.SSNFR 

'amaline Octal n 

HANFORDSITE 

Teleohone No. MSIN 

(5091172-9518 


FAX 

Protect Title 

hioued To (],a t)) 

Quan 

lAebook No. 

h 

Method of Shiomenl 

4 

tee Chest No. 

t- a^ 

Bill of Ladine/Air Bill No. 

'Team. 

3 C 

Protocol Data Turnaround Offshe Proaeriv No. 

POSSIBLE SAMPLE HAZARDS/REMARKS 

C.O.C. p 

SPECIAL INSTRUCTIONS Hold Time T'olal Activit y Exemption 

FAX COPIES OF QES & TMA 1-OO-INTO DI-STEWART (372-1700) & JM DUNCAN (372-9052) 

C99-006-61 

Page 1 01 i 

Yes Lg No 

Simple No. lab II) Dale TimeNo/Type Container Sample Analysis 

Prese rvative 

BOR4F6 W 1X500—col— GACr ICP Metals - 6010A RCRA GW ) HNO3 to pH Q 

BOR4F6 W 1 x500-m l- P IC Anions -300.0 (Chloride, Fluo ri de, Nitrogen In Nitrate, Nitrogen in Wells, Sulfate) / (TI 

6-6 ((d^ 

Cod 4C 

BOR4F6 W 1x1000-mL P Gross Alpha 8 Gross Bela HNO3 to pH ¢ 

9OR4F6 W 1x20 mL P Achvdy Scan None 

BOR4F-6 W !x400-mL Gn' Gamma Spec t roscopy(Wa te r) HNO3 to pH

9. Samês are: 

/ in good condition 

broken 

Figure 1 

S^•MPLE CHECK-{N LIST 

ratei7me Received: ^^>l/ .^^ /^J^G^/ 

; SGk: 

y / 

Work Order Number: ^^ 1C^ _ S A F 

leaking 

have air bubbles 

R 5 SH- 50 W-93 -0003 

?evision 5 

Shipping Container ID: y JJ^^! ^ Ct ain of Custcdy `'l - ^^^^^' `y ^^4 61 

1. Custody Seals on shippin g container intact? Yes . [ 

2. Custcdy Seals dated and signed? Yes LI-Wo ( 1 

3. Chain-of-Custody record present? a L Yes ij--t4c [ ] 

4. Cooler temperature 

r. Vermiculite,'packing mate ri als is Wet [) D ry [^ 

6. Number of samples in shipping container: 

i . Sample holding times exceeded? Yes [ j No [ ^' 

a. Sample 

= 

have: 

oe 

tody seals 

t 

h azard labels 

appropriate sample labels 

10. Where any anomalies icenti':ed in sam ple receipt? Yes (] No [jam 

11. Description of anomalies (inci::de sample numbers;: 

Sample Cust 

/^r3, C^ ^Dat^ /L/^/ ^ 

Y e 

eleehoned To: On Sy 

,^(IOCl12

LSAFNo. 

; K1H( Ft ConlacUReaaesler 


S 

IH 

feleuhone No. MSIN FAX 

smnline Orf rin Purchase Order/Charee Code 

Proiect TIBe Loebook No._ Ice Chest N 

- 36` 

Shipped To flab) Method of Shi pment Bill of Ladir it Bill No. 

Protocol 

A 

POSSIBLE SAMPLE IIALARUS/REMARKS 

SanipleNo LIE, ll) * Date 

Data Turnaround Offsific Propert y No. 

Time Noflype Container Sample Anafysis 

C.O.C.# - 

C99-006-57 

Temp. 

SPECIAL INSTRUCTIONS Hold Time Total Activit y Ezeanntion: 

FAX COPIES OF QES & TMA LOG 1 N TO DL STEW ART (372-1704) & JM DUNC AN (372-9052). 

Page t of 1 

;,< 

Yes No 

P reservative 

B0R4F4(F) W 1x500-mLG Mercu ry -7470-(CV) 

10 ^. I HNO3 to pH

Datei7me Received: 

Figure i 

SAMPLE CHECK-IN LIST 

RFSH-SOW-93-0003 - 

Revision 5 

Work Order Number. SAr x: (^—^^^p _ 

_ j 

Shipping pp g Container 1 4 : X241 Chain cf Custody # ^^^-^^^ ^ 

4 

_4 Custody Seals on shipping container intact? 

- 

Yes , NO [ ] ^C^^ 

i 

I Custody Seals dated and signed? Yes [ Ptc [I 

3. Chain-of-Custody record present? Yes [j No [ ] 


5. Vermiculite/packing materials is Wet [ ] Dry [ ] 

6. Number of samples in shipping container: ? 

7. Sample holding times exceeded? Yes [ ] No [ ]'^ 

8. Samples have: 

^pe ustody seals 

hazard !abets 

a ppropriate sample labels 

5. Samples re: 

n good condition leaking 

broken have air bubbles 

10. Where any anomalies identified in sample receipt? Yes [ ] No [ 

11. Desc ri ption of anomalies (include sample numbers): 

Sample Custodian/Laborato ry : 

Telephoned Sy 

+o oou14

PNNI. 

Collector 

m? r Ct.n d 065I7 7 

--- - 

CHAIN OF CUS'T'ODY/SAMPLE ANALYSIS REQUEST 

).R BREWINGT ON (RFS) 'ontact/Reauester Telephone No. MSIN FAX 

AF No. Sampling Origin Purchase Order/Charge Code 

Proieei Title Loebook No. Ice Chest No. '1'emo. 

Shipped To (Lab) Method of Shipment Bill of Ladine/Air Bill No. 

Protocol Data Turnaround Willie Propert y No. 


r^ 

--- 

C.O.C.s 

SPECIAL INSTRUC'T'IONS field Time Total Activitv Exemption: 

FAX COPIES OF QBS & TMA I. COG -INTO DI. STEW ART ( 372-17(14) & JM DUNCAN (172-9052) 

1 

C99-006-3 

Page I of I 

Yes Ej No 

Sample No- Lab 1D Datc To. No/Type Container Sample Analysis Preservative 

BOR494 (F) W - - 1x500-mL G457 ICP Metals - 6010A RCRA GW Ô D/C. 

I HNO3 to pH Q 

BOR495 W 1x500-mL G ICP Metals - 6010A RCRA GW `' - .1 HNO3 to pH

PNNI, 

CuIlerlufJ R DRE MM( )N (RFS) 


Con tact/Rcoucslcr 

III KF-"NFR 

C.O.C.# 

1'eleuhone No. MSIN FAX 

(5091177-9538 

SAN No. Sairmuling Oriein Purchase Order/Charee Code 

Proiect Title Loebook No. 

,J-5;- 11 1 

/l"y 

Ice Chest No. Temo. 

— _ 

Ji 

Shinned To (Lab) Method of Shtoment Bill of Ladine/Air Bill No. 

Protocol Data Turnaround Offsite Pronerl y No. 


^r 

SPECIAL INSTRUCTIONS Hold Time 7 oral Activit y Exem ption 

FAX COPIES OF QES & TMA FOG IN l O DL STEWAR I (372-171,1 & 1M DUNCAN (372-9052). 

C99-006-6 

Pugc I of I 

Yes W No 

Sample No Lab ID Date Time No/fype Container Sample Analysis 

Preservative 

BOR499 (F) W 1x500-mL 00 ICE Metals - 6010A RCRA GW HNO3 to pH

Sample CustcdianlLaboratory: 

Telephoned To: 

Figure 1 


^ 

Date/Time Received: IZ16 S, ô^587 

Work Order Number: Q^^ y ^ y ^^^_ SAF #: 

By 

RFSH-SOW-93-0003 

Revision 

Shipping Container I D: Cain of Custody # l (— ^y ^^v 

1. Custody Seals on shipping container intact? Yes [ Jwi^ ( } 

2. Custody Seals dated and signed? Yes ( ^-wc [ ] 

3. Chain-of-Custody record present? ô^ 

Yes ( ]Îd [ ] 


5. Vermiculitelpacking materials is Wet [ ] D ry []^^ 


7. Sample holding times exceeded? Yes I] No [ ]^^ 


=tape hazard labels 

___,,custody seals appropriate sample labels 

9. Sample^s -are: 

^n good condition leaking 


10. Where any anomalies identi fi ed in sample receipt? Yes [I No [ 

11. Description of anomalies (include sampie numbers): 

10001 7 

I

PNNL 

Collector ConlacUlIcauesler 


lH KF gSNF7,R_ 

'AF No. Samuline Oriein 

Proiecl Tillc 

10(1-K R4(l & 2 1 GW SAMELING OCTOBER I Q99 

HANFORDSITE 

C,O.C.# 

Telephone No. 

(IN) 372-953H 

MSIN FAX 

Purchase Order/Charec Code 

I,oebook No. ice Chest No. , -- Temo. c 

Mooed To (Lab) Method of Shinntenl Hill of Ladine7Air Bill No. x 

Protocol 

Data Turnaround 

017she Prouerl y No. 

CERCI A 

45 Days 

POSSIBLE SAMPLE IIAZARD.S/REMARKS SPECIAL INS 'I RUCTI0NS Hold Time 

Tolal Aclivil y Exemption: 

• ^• 

FAXCOPIF'_SOPQF..S&7MALUG-INIODLS'IEWARI'(17Z 1704)&IMDUNCAN(372-9052). 

C99-006-41 

Page 1 of I 

Yes Lj No 

Sample Nu. l.;lb ID * Dale 'lime Nolfype Container Sample Analysis Prese rvative 

80114C7 (F) W _I 1x500-mL GO ICP Metals - 6010A RCRA GW 

6 

i^ll 

/ 

HNO3 to pit 

BOH4C8 W Ix500-mL ICP Metals - 6010A RCRA GW . J . / HNO3 to pH

PNNL 


Colleclm- R (RF9T Conlacl/Renuesler Telephone No. MSIN FAX 

A F No. Sampline Oriein Purchase Order/Charee Code 

Protect Title Loebook No. Ice Chest No. Temp. - 

it 

Shipped To (Lab) Method of Shipment Bill or Ladine/Air Bill No.. 

Protocol Data Turnaround Off.0tc ProDert y No. 

C99-006-70 

Page 1 of 1 

POSSIBLESAMPLE HAZARDS/REMARKS SPECIAL INSTRUCTIONS Hold 'Time Total Activity Exemption Yes No 

FAX COPIES OF QES & TMA LOG-IN TO DI. STEW ART (372-1704) & )M DUNCAN (1'72-9052)_ 

Sample No lab IU Umc Time No/Type Container Sample Analysis Preservative 

BOR4K9 (F) W 

_ 

_ - 1.500 .1- GO ICP Metals - 6010A RCRA G IN 4y J / 

( 

HNO3 to pH

Date, me Received: /^t^^%f^ l/ ^ 

9. Sampi are:: 

3in good condition 

broken 

Sample Custodian/Laboratory: 

Figure 1 


SGTM: LU^^S^ ^7 

leak;ng 


RFSi:-S0W-93-0003 

Revision 

Work Order Number_ 115" (! SAF n ^^ -!^^ J 7^ ^^Û 

S,iioping Container ID: Y IIL_ Chain of Custody 76 

1. Custody Seals on shipping container intact? ^ fas [, -Ko [ ] 

I Custody Seals dated and signed? Yes j-^N o [ ] 

3. Chain-cf-Custody record present? C Yes ^Nc [ ] 

C . Cooler temperature L+ 

Vermiculite/packing materials is Wet [ j Dry [ ]% 


7. Sample holding times exceeded? Yes [ ] No (]/^ 

110. 

B. Sampi shave, 

=ape 

ustcdy seals 

"^P 

hazard labels 


Where any anomalies identi fi ed in sanple receipt? Yes [ j No [ 


T elechcned To: 

/i% Z"j- 

1000.0

Con&wn Up= Receipt Variance Report 

St. IA um Laboratory 

tv^ r 

CL Date: /L -o? 7- q ;i Time: Ll ^t7d 

pft Initiated by: .IOC' -71) C m N AAA, 

Stu , pe 'I t.. E__ ^Fti, ^, L l g 7175193 2 1( RFA/COC Numbers: 

Coudiuon /V anancr C h'etk all that apply): 

4168/" 

I _ aatpie ; e_ewed b roken leaking. 8. q Sample ID on container does not match sample ID 

2. _ 'lample , e::eweti without p roper p reservative. on paperwork. Explain: 

Cooler temperature not within 4C t 2C 

Record temperature: 

q pH_ 9. q A ll coolers on airbi ll not received with shipment. 

q other: 10. q Other (explain below;: 

3. q Sample received in improper con tainer. 

4. q Sample received without proper paperwork. Explain: 

5. q Paperwork received without sample. 

6. q No sample ID on sample con tainer. 

7. q Cus tody ta 

pe dis turbed/b roken/missing. 

Notes: 

d 

No variances were noted during sample receipt. Cooler Temperature Upon Receipt: C- _ 

Correc tive Action: 

q Client' s Name: Informed verbally on: By: 

q Client ' s Name: Informed in writing on: By: 

q Sample(s) processed " as is". 

q Sample (s) on hold unt il 

: If released, notify: 

Sample Control Supe rvisor Review: (or designate) Date: le o?Y-`Yp _ 

Project Management Review: Date: ^^ — ^, - 

SL-ADMLN-0104, Revised 11/24/95 

SIGNED ORIG INAL MUST BE RETAINED IN THE PROJECT FILE 

x1000 11

Project Gla eager: R_ White 

Sample Header Template: 

Sample No. Client ID 

Comments 

q Container Type 

Data: 

19254-001 BOR491 

SAF C99-006 

1 E - Plastic-500ml 

19254-002 BOR4B1 

SAF C99-006 

1 FN - Plasti 1 -50011 

19254-003 BOR4B2 

SAF C99-006 

1 

1 

1 

l 

1 

PN P,dsza^ Dbllll 

19249- 11 n4 DJR492 

SAF C99-006 

1 PIN - FlasL i.0 SOU:n 

I 

1 

1 

1 

1 

19254 005 BOR4F8 

SAF C99-006 

AN :,n:bee :, .. nulM1nl 

1 PN Pla Stic^500ni1 

I 

1 

I 

1 

1 

V 

3 . S9, 

^- has not been rad screened. 

r^ 

r: 

Quanterra November 03, 1998 09;35 am 

Account 10722 Project: 550.184 Quanterra-Richland CAR No - 550.184 Rev. 3 


(^ 

Reviewed by and Date: , d /y^LSL.C^ 

C-Matrix Date: Collected Received Due Shipper Red Category Rad Sample No. 

Analysis Class Prese rv ative Anal, Due Date Hold Date Site (Container Numbers:% Filled) 

Water 26-OCT-98 11:30 28-OCT-98.12:54 25- 14OV-98 AIRBORNE 1 

ICAPD/6010/Q4 S IM03 18-NOV -98 26-APR-99 S13A 

Water 28- OCT-98 10:19 28-OCT-98 12:54 25-NOV-98 AIRBORNE 1 

ICAPD/6010/Q4 S M03 18-NOV -98 26-APR-99 S13A 

Water 28- OCT-98 10:19 28-OCT-98 12:54 25-NOV-98 AIRBORNE 1 

CL/300.0/Q4 S COLD 18-NOV -98 25 NOV-98 S13A 

FL/3D0.0/Q4 S COLD 18-NOV -98 25-NOV-98 S13A 

1CAP/6010/Q4 S HNO3 18-NOV -98 26-APR-99 S13A 

NO2/300. 0/Q4 

NO3/300.0/Q4 

S 

S 

'O'D 

COLD 

18 NOV 98 

16-NOV-98 

- - 8 S13A 

30-OCT-98 S13A 

SO4/300.0/Q4 S COLD 18-NOV-98 25-NOV-98 S13A 

Wa(_er 28- CCI-98 11:30 28-OCT-98 12:54 2S-NOV-98 AIRBORNE 1 

CL/300.0/Q4 S COLD 1-B NOV-98 2'i NOV 98 S13A 

h'1,/3110.0 1 Q4 S ('011 1) 18-NOV -98 25-NOV-98 S13A 

1CAP/6010/Q4 S I1NO3 18-NOV-98 26-APR-99 S13A 

NO2 1 300. 0/Q4 S COLD 18-NOV-98 30-OCT-98 S13A 

NO3/300. 0/Q4 S COLD 18-NOV-98 30-OCT-9B S13A 

S O4/300.0/Q4 S COLD 1B-NOV-9B 25-NOV-9B S13A 

Water 28- OCT -98 G8 42 28-OCT-98 12:54 25-NOV-98 AIRBORNE 1 

(413793:100) 

(413 7 94:100) 

(413796:99) 

(413796:99) 

(413]95:100) 

(413796 99) 

(413796:99) 

(413796:99) 

(41 3798 :99 ) 

(413798:99) 

(413997:100) 

(413798:99) 

(413798:991 

(413798:99) 

HG/ 7470/Q4 S HNO3 18-NOV-98 25- NOV-98 S13A (413801'1.00) 

CL/300-0/Q4 S FOLD 18-NOV-98 25- NOV-9B S13A (413800:99) 

FL/300.0/Q4 S COLD 18-NOV-98 25- NOV-98 S13A (413800:99) 

ICAP/6010/Q4 S HNO3 18-NOV-98 26- APR-99 S13A (413999:100) 

NO2%d00.01 Q9 S COLD 18-NOV-98 30-OCT-98 S13A (413800:99) 

NO3/300.0/Q4 S COLD 18-NOV-98 30- OCT-9B S13A (413800:99) 

SO4/300.0/Q4 S COLD 18-NOV-98 25- NOV-98 S13A (413800:99) 

Faye 1 





Screening not Required

Frele,'t Manager; R. White 

Sample Header Template: 

Qua nterra November 03, 1998 09 :35 am 

Account: 10722 Project: 550.184 Quanterra-Richland QAS Nc. 550.184 Re, 3 


Reviewed by and 

Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Rad Category Rad Sample No. 

Comments 

4 Container Type Analysis Class Preservative Anal. Due Date field Date Site (Container Numbers:% Filled) 

Data. 

19254-006 gnR4F7 Water 28-OCT-98 08:42 28-OCT-98 12:54 25-NOV-98 AIRBORNE 1 Screening not Required 

SAF C99-006 

- AN - Amber Glass-500 m1 HGD/7470/Q4 S HNO3 18-NOV-98 25-NOV-98 S13A. 1413804:1007 

1 IN - plastic-SOOml ICAPD/6010/Q4 S HNO3 18-NOV-98 26-APR 99 513A (413802:100) 

O 

i — Sa1hple has not beea xad xened_ 

W 

Page 2

Chain of 

Custody Record 

yOC 

OUAG124 0797 

Client Project Manager 

rte- _ 

Addoss Telephone Number (Area Coda) 'Fax Number Lab Number 

Dale 

1029 -Ilk 

CM State Zip Code Site Contact Lab Contact Analysis (Attach list 

mores ce is needed if 

Project Name ^7 / ^ 

'f 

(—) w U c/ L^ L^Q^ 

Contract Purchase OrderlQuote No 

Sample I.D. No. and Description 

(Conla ,ners for each sample may be combined on one line) 

)02d OX4ql 

2 tR2 

3 / 

-Z A5Z 

V 

!1F^ 

-- 

CarnerWaybill Number \ 

Date Time $ 

Matrix 

y h 

° 

j ° ^_" 

Containers & 

Preservatives 

o 

2 2 2 AS 

IN 

Qivanterra 

Chain of Custody Numbed 

^_ J13C 

Page of 

Special Instructions/ 

Conditions of Receipt 

russr ie nazaro identification 

q Non-Hazard El Flammable F1 Sk1n Initan f q Poison 8 Unknown 

Sa 1ple Disposal 

Retwn 7o Client q Disposal By Lab q Archive For 

(A lee may be assessetl i/samples are retained 

Months longer than 3 months) 

Turn Around Time Repurred 

q 2 H urs q aB Hours El Days [1 14 Days F1 9 r Da Other 

I pC Requirements (Specify) 

sly, 

,r l f ^ /J 

to U1 JO 

t. r q ishbdB a(e Time 1. Received By 

N/ 

Date Time 

2. FIokqquished By 

U 

mir Time Z. Received By Date 

ffl 30 

Time 

3. F!^3quished By Date Time 3. Received By I Date I Time 

Cor^vts --- -- --fee 

e l 3eA C^ y /A,/ /v 3a -9P 

DISTRIBUTION_ 'WHIT[ - Slays with the Sample: CANARY - Returned fc Client with Report. PINK - Field Copy

PNNI, 


Collector 

AF No. 

C99-" 

R DREWINGTON (RFS) 

onlact/Reauester 

IB KESSNER 

Sampling Orkin 

HANFEIRDSITE 

Telephone No. MSIN 

1") 372-9518 


FAX 

Protect Title Logbook No. 

r-5 ntL - ^>'^ 

Ice Chest No. 

ii"s "B6 - 

Temp. p. 

hipped To (Lab) Method of Shipment Bill of Ladine/Alr Bill No. 

Protocol Bata Turna round to Properiv No. 

POSSIBLE SAMPLE HAZARDS/REMARRS 

> 

r^ 

J „ 

C.O.C.# 

PECIAL INSTRUCTIONS Hold Time Total Activity Exemption: 

FAX COPIES OF QES & TMA LOG IN TO DL STEW ART (372-1704) & IM DUNCAN (372-9052). 

C99-006-1 

Page 1 of 1 

Yes No 

Sample No lab ID Date Time NofFype Container Sample Analysis Prese rvative 

BOR491 (F) W 1x500-mL Go ICP Metals - 6010A RCRA GW HNO3 to pH

A 

PNNL 

Collector 


R BREWINGTON (RFS) DontmelfReamester rellephome No. MIN FAX 

AF No. Wrossum Ori g in Imbase Older/Chatee Code 

Prefect Tide 

IMIKKAU &21 OW RAMP[ I 

Attlealk No. few L 

M • 

/^ ce Chest No. f/rte 3G 

T ^ 

Shipped To (Lab) dedwersmoment lH1IofLmdInWAhrBHINo. 

Protocol haft 1Ltmround Wrielle proper" No. 


« •• 

- 

C.O.C. IF 

C99-006-7 

Page 1 of I 

SIFECIAL INSTRUCTWNS Hold Tlme Tool Activity Exemption: Yes L9 No 

FAX COPIES OF QES R TMA LOO-IN TO DL SMWART (77 2- 1701) t IM DUNCAN (371-9051). 

Semple No. Lab ID • Dab Time No/Type Contalm Sansple Analysis Presesyetlye 

8OMBi(F) IN 1x6004"2- Ge ICPMSWS- 8010AFCRAGW 0 

HNO3 to pH -2 

8011482 W 1x60o-mL ICP Metals -B010A RCRA OW 1 Hta ID PH 

8OR4B2 W 1x600 -mL P IC Anions - 300.0 (CbbdOe, Fkorkle, N itrogen In Nkou. Nitrogen in NW b. StrBab( d) 

BOR4B2 W ix1000mL P Orom A l pha 6 Orom Bela d 

HNO3 b pH Q 

BOR4B2 W 1x20-mL P Ac6t Scan None 

BOR02 W IX4000-ML GIP Oer" Specooeoopy(Wa err) HNO3 to pH

Date iTime Received: ^, 

Figure 1 


// Z-/V /^ SG#: 

Mork Order Number /^^^ 2 ^ -`3 SAF J 

q 

Shipping Container lO _ ^/^^^^1 Chain of Custody # eq cl- 

Telephoned OnC /, 

By 

RFSH-sow- -0003 

Re,rision 

y 

# ^Q-GC6 

1. Custody Seals on shipping container intact? ^l^Yes L, -No ( ] 

2. Custody Seals dated and signed? Yes [ c} O [ I 

3. Chain-of-Custody record present? s Yes [L-No [ j 


P. Vermiculite/packing mate ri als is Vet [ ] C ry [ } 


7. Sample holding times exceeded? Yes (j No { j^ 


14 

l,_^tape h azard labels 

custody seals appropriate sample labels 

9. Samples are: 

cod condition leaking 


10. Where any anomalies identified in sample receipt? Yes [ ] No [ jif 

11, Desc ri ption of anomalies (include sample numbers): 

-- r- 

Sample CustodianiLaborato ry : C t 

C 

r o00 21 7

PNNL 

4,(—t do 9 O I 


r ,R. BREWINGTON(RFS) ° ekohone No. MIN FAX 

Orldo Order Clam a Code 

Title 

k No. a Chest Na Tern. s 

Sr 

Db[vDed To (Lobl ethod of Shlumenl dl of LadlodAlr RW No. 

f-PRr7 A 

" 

LR SAMPLE HAZARDSIREMARKS 

a Turnaround 

41 Dave 

aProperly No. 

1g, 

C-O.C.d 

SrEClAL INSTRUCTIONS Hold Time Total Ac tivity Exemodm: 

FAX COPIES OF QBS A TMA IOG-IN TO DL SfEWART (372-1704) At )M DUNCAN (372-9052). 

C99-006-65 

Page I of I 

Yes kg No 

Sample No. lab ID • Date Time Nodi'ype Container Sample Analysis Preservative 

80R4F7 (F) W 

D7 

x Y 1x600-mL O Mamrry - 7470 • (C 

v 0 

V) /ad 0/67/- I 

HNO3 to pH 12 

BOW7 (F) W 1x60DinL 00 K3' MMW • B01( kA RGRA GW I 

HNOS to pH 4 

BORVO W I x5OO-mL G Movoury - 7470 - (CV) HNO3 a pH Q 

BOR4F8 

W 7x5W-mL ICP McWa - OMA RCRA OW HNO3 to pH Q 

B0R4F8 - _- - W 1x50OmL P IC Mips - 300.0 (Chiodda, Flualde, N itrogen In Ndrate, Ndmgen In Mate, Sukte) 

BOBVII W 1xi000-mL P Grua Alpha g Gmes Ilea HNO3 10 pH


Figure 1 


JJ 

DateTme Received: /^^f y^ ^^f^^ SG#: fLJ/^-^S^/ 

Work Order Number: 'J 1 ^, 32 /- 6Z53 SAF # 

/ 

Shipping Cont ainer I a %L 511 Chain of Custody # 

RFSH-SOW 93-0003 

Revision 

1. Custody Seals on shipping container intact? Y es/^ Q[ ] 

2. Custody Seals dated and signed? 

Yes J] No [ ] 

3. Chain-of-Custody record present? 

J 

^J Yes [ [ ] 


5. Vermiculitefpacking mate rials is Wet [ ] Dry [^] 

6. Number of samples in shipping container. J 

7. Sample holding times exceeded? Yes (] No [^ 


gape hazard labels 

stody seals 

— Û 


9. SampLesare: 

f in good condition leaking 


10. Where any anomalies identified in sample receipt? Yes (j No (^ 

11. Description of anomalies (include sample numbers): 

Telephoned To:_ Cn_^ By 

^J 

,)m)023

vd1n e 

5 191M fl: !rat 

Ci a- -^ ^, s 

Prt 5: 'do:__--— bey 

SIL per'No :- Au binl',- 

Condi tion/Variance (Check all that apply): 

1 ::7 Sample received broke nileaking. 

2 ".:.1 Sample received without proper prese rvative. 

q Cooler temperature not within 4-C t 2-C 

q pH- 

q other: 

Record tempera ture: 

3. q Sample received in improper con ta iner. 

4. Sample received without proper paperwork. Explain: 

5. q Paperwork received without sample. 

6. q No sample ID on sample con tainer. 

7. q Cus tody tape dis turbed/broken/missing. 

Condition Upon Rec eipt Vzmce Report 

SL Louis Laboratory 

01699', 

Login No. fias 

Date: l4 --?q-q; Time: 6.236 

Initi ated by: Jse Ti6in* vnr 

RFA/COC Numbers: ^[l / 0 

8. q Sample M on con ta iner does not match sample ID 

on paperwork. Explain: 

9. q A ll coolers on airbi ll nor received with shipment. 

10. q Other (explain below): 

q No variances were noted during sample receipt. Cooler Temperature Upon Receipt: 7 ,C 

Notes: 66Cg1I - ice II-c.6 AI, -1 

St16tn{ 

Meggol - iepm .-l-al, ph°1 sa-DMT 

Corrective Ac tion: 

4916A .S 5'00 m p 

q Client's Name: Informed verba lly on: By: 

q Client's Name: Informed in writing on: By: 

q Sample(s) processed 'as is". 

q Sample(s) an hold unt il : If released. notify: 

Sample Control Supe rv isor Review: for desienate) lf!"C. (Ce Date: /0 -.2 91 

0 

Project Management Review: Date: d-;- 7 8 

SL-ADMTN- 0004, Revised l U24/95 

SIGNED ORIG INAL MUST BE RETAINED IN THE PROJECT FILE 

il)ill^ s U

Cl o 

r71,7171" M7 

Condition Upon Receipt Var mce Report 

St. Louis Laboratory 

016895 

Login No.:_ ^ 2 s 

f%C:c`l>^ Date: —^ Time: 0-73d 

Pv e- ". ' : - . . _ _. _ 1 / Initiated by: êC ! ieli AAr 

Sh per ,

Qna nterra itr thlanu 

3330 Georce wa sh vlg con way 

Richlanc, 'WA 991/52 

Pn:7 ecC 550.185 

lateaory: :CAP Metals - Cissolved Sample Date 10/27/95 

'l ethod. EPA 6010 Recerpt Date 10/27/98 

'4atr1z: LIQUID Report Date 12/07/98 

__rent ID BOR494 Quanterra ID 19221 0'.11 

Anal yte CAS NumbeY 

Blank Sample 

Name 

Irep- 

Gate 

Analyses 

Date 'e5ult Un1L Qual. 

Detection 

Llml Dilu[1c.^. 

Aiumrnum 7429 -90-5 QCBLK192982 -1 _1/23/98 11/24/98 39.6 BG/-LB 2]0 

I trmony 7440 -36-0 UCBLK192982-1 11/23/98 11/24/98 v -0 UG/L U 60.0 

Ear um 7440 39 3 QCBLK192982-1 11/23/98 11/24/98 i4-1 UG/L B 2]0 L 

Be ry '_llum 7440 -41-7 QCBLK192982 1 11/23/98 11/24/98 5.79 UG/L B 5.1/ 

Cadmram 7440 -43-9 QCBLK192982 -1 11/23/90 :1/24/98 2.9 'JG/L -, 5 O 1 

2almum 7440 -70-2 QCBLK192982-1 11'23/9B 11/24/98 47500 UG/L 5000 1 

Ch mmrum 7440 49 3 QCBLK192982 -1 11/23/98 11/24/98 440 L'G/L 10.0 L 

''obalt 7440 -48-4 QCBLK192982-1 _:/23/98 11/24/90 2-4 IIG/L U 50.0 1 

Copper 7440 -50-8 OCBLK192982 1 !1/23/98 11/24/98 `_.5 LC/L B 25.0 1 

iron 7439-89 -6 QCBLK192982-1 ._;23/98 11/24/98 39.2 IIG/L B 100 

Magnesium 7439-95 -4 QCBLK192982 1 _1'23/98 11/24/93 :0200 UG/L E 5000 

Manganese 7439 965 QCBLK192982 -1 11!23'90 11/24/98 4.6 IIG/L B 15.0 

Lic

Category: :CAP Metals - Diss Dl Ved 

Method: EPA 6010 

Matrix: LIQUID 

-Tent ID: BOR494 

Analyte CAS Number 

-lank sample 

Name 

^.:a s'^_ria Ei cblaud 

3eorge 'Rashrngton way 

'UA 39352 

`50 1&4 

?rep. 

:ate 

Analyses 

Date 

T.l uminum 9429 -90-5 vCBLK192982-^ /23/98 11/24/98 

Antimony 7440 -36-0 QOBLK192962 = :._/23/98 11/24/98 

Barium 7440 -39-3 QCBLK192982-1 :.1/23/98 11/24/98 

Beryllium 7440 -41-7 QCBLKI92982-- 13/23/98 11/24/98 

Cadmium 7440 -43 9 :-BLK192982-1 13/23/38 11/24/98 

Calcium 7440 -70-2 l28LK192982-1 11/23/98 :1/24/98 

Chromrum 1440 -47-3 QCBLK192982-1 11/23/98 11/24/98 

Cobalt 7440 48-4 < 713LK192982 1 11/23/98 :1/24/98 

Copper 7440 -50-8 JCBLK192982-1 11/23/98 11/24/98 

iron 7439 89 6 '-'BLK192982 1 .2/23/98 11/24/98 

Magnesium 7439 -95-4 1-SLK1929SL 1 11/23/98 11/24/98 

Manganese 7439 96-5 ;CBLKI92992 1 1./23/98 11/24/98 

Nickel 7440 -02-0 ]CBLK192982-: 11 /23/98 11/24/98 

Potassium 7440 -09 -7 ,D31,K192982-1 2/23/98 11/24/98 

Silver )440 -22-4 'CBLK192982 = 11/23 1/ 98 11/24/98 

Sodium 7440 -23-5 ^CSLK192982 1 2/23 1/ 98 11/24/98 

Vanadium '7440 -62-2 J-BLK192982 - 11/23/99 11/24/98 

Zinc 7440 -686 CBLK1929821 11/23/93 11/24/99 

Strontium 7440 -24-6 ,CRLK192 9 82-1 _1'23/93 -1/24/98 

Result 'Join Qual 

99 tREC 

103 ^REC 

99 tREC 

103 tREC 

101 lREC 

103 #REC 

100 4REC 

Lot 4REC 

99 #REC 

105 4REC 

103 tREC 

98 4REC 

100 1REC 

106 tREC 

105 BREC 

102 4REC 

100 4REC 

102 %REC 

37 4REC 

Sample Date 10/27/98 

Receipt Date 10/29/98 

Report Date 12/0'1/38 

Quanterra IC : 19221-301MS 

Detection 

Limit Dilution 

/1000314 

1 

1 

1 

1 

1 

1

Category rCAP Metals - :isswoed 



Client 1c 9OR494 


clank Sample 

Name 

iva me r-_a krch_and 


Richland, WA 99352 

Pr0'ect. 550-.84 

Pre, 

Date 

Analyses 

Date Result 'Jr.it veal 

Aluminum 1429 -90-5 QCBLK192982 1 11/23/96 11/24798 97 BREC 

Antimony 7440 -36-0 QCBLK192982 -L 11./23/118 11/24/98 _03 BREC 

Barium 

Beryllium 

Cadmium 

7440 -39-3 

7440 41 7 

9440 -43 9 

QCBLK192982 1 

QCBLK192982 -L 

QCBLK192982-1 

11/23/96 

11/23/98 

1'/23/98 

11/24/98 

11/24/98 

11/24/98 

90 

102 

100 

BREC 

iREC 

6REC 

Calcium 

Chromium 

Cobalt 

Copper 

Iron 

Magnesium 

Manganese 

Nickel 

Potassium 

Silver 

Sodium 

Vanadlum 

Z>nc 

Strontium 

7440 -70-2 

7440 47- 3 

744048 4 

7440 -50-6 

7439 89 6 

7439 -95 4 

7439 -96-5 

7440 02 0 

7440 -09 

7440 -22 4 

7440 23 r, 

7440 -62 2 

7440 66 6 

7440 24 d 

QCBLK192982-1 ',1/23/90 

QCBLK192982L 11/23/98 

QCBLK192982-1 11/23/90 

QCBLK192982-1 ll /23/98 

QCSLK192982 1 11/23/98 

2CBLK192982-1 .:/23/90 

JCBLK192982-1 1,'23/90 

1CSLK192902 3/ 9 

"`CBLK19 98 2 3/ 8 

CBLK192 ii 1 23 /'8 

3 1 1"B 2 

iCBLK192982 1 11/.3/98 

lCBLK192962 1 11/23/98 

QCBLK192982 1 11/23/98 

11/24/96 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/" 

1/24/38 

11/24/95 

11/24/90 

1/24/96 

11/24/98 

11/24/98 

96 

96 

1_00 

99 

104 

101 

96 

9 

i3 

:04 

99 

99 

:01 

96 

kREC 

BREC 

BREC 

BREC 

BREC 

tREC 

YREC 

/RE(- 

RE- 

1 RE_ 

:REC 

1REC 

IREC 

BREC 

Sample Date - 10/27/99 

ReceLpt Date - 10/27/90 

Report Date 12/07/9B 

Quanterra :2 19221 I;OIMSD 

Detection 

Limit D11Ut1Cn 

1 

1 

L 

L

Juanterra-Richland 

3350 Georg= Washington 

Richland, 'IA 99352 

=rol"^t. 184 

Category: CCP Metals -6010A !TALI Sample Date 10/29/95 

Method.- EPA 6010 Receipt Date : 10/27/9c 

Matrix: LIQU ID Report Date 12/09/98 

Client _D: BOR495 Quanterra ID 19221 CO2 

Blank Sample Prep 

- 

Analpaes Detection 

Analyte CAS Number Name Date Date Result Unat Qual. Limit Dilution. 

Aluminum 9429 -90-5 QCBLK192982 -1 11/23/98 L1/24/98 40.9 UG/L 5 200 

Autamony -,440 -36-0 QCBLK192982 1 '.1/23/98 11/24/98 33.0 UG/L U 60.1 

Barium "1440 -39-3 QCBLK192982 L 11/23/98 11/2:/98 33.-/ UG/L B 201 1 

Beryllium 7440 -41-7 QCBLK192982 -1 :1/23/98 L1/24 1 98 J . 57 UG/L B 5.) - 

Cadmium 7440 -43-9 QCBLK1 92 982-1 :1/23/98 1./24/99 X2.6 UG/L '1 5.0 

Calcium 7440 -70-2 QCBLK192982 1 :1/23/99 .1/24/98 46300 UG/L 5000 

Chromium 7440 -47-3 QCBLK192982-1 11/23/98 =1/24/98 432 U6/- 10.0 

Cobalt 7440 -48-4 QCBLK192982 -1 _1/23/98 :1/24/98 2.4 Up/L -.1 50 .'a 1 

Copper 7440 -50-8 QCBLK192982 1 11 1 23/98 11/24'98 2.9 UG/L U 25.0 1 

Iron 7439 -89-6 QCBLK192982 :1/23/98 11/24!98 121 UO/L 100 - 

Magnesium 7439 -95-4 QCBLK192982 -1 11/23/98 :1/24'99 9990 _ 5000 

Manganese 7439 96-5 ^CBLK192982-: _!/.-3/58 11," , d 4.9 U,'/L B 15.0 

Nickel 7440 -02 0 nJCBLK192982 1 ./,13/98 11/2a ''o 10.8 if,;/L 17 t 

Potassrmn 7440 -09 7 QCBLK192982 1 _,!x3/98 _1/2..98 2510 JG/L B 5000 

3 11 ver -?440 22 4 QCBLK192982 1 -1/.3/98 11/24.98 5-0 UG/L U 10.6 L 

Sodium 7440 -23-5 ZrBLK192982 ..!23/98 1114198 18900 UG/L 5000 

Vanadium 7440 62-2 QCBLK192982 1 ../G3/98 11/24/98 LJ.9 UG/L B 50.0 1 

'"Inc 7440 66 6 @CBLK192982 1 :1/[3/98 11/24,98 6-3 UG/L B 20-0 

Strontlum 7440 24-6 QCBLK192982 -1 :1/83/98 11/24/39 200 UC/L 50.0 1 

X00030

„can--erra-Richland 

335D George Washington 'dav 

4,C,I.rd, WA 99352 

Pro -eCt 550-164 

Category: :CAP Metals :l_asDlved Sample Date 10/2/98 

Method: EPA 6010 Receipt Date 10/27/98 

Matrix: LIQUID Report Date 12/08/98 

Client ID: E0R4C7 Quanterra 11) : 19221 J03 

Analyte 

Antimony 

Barium 

Beryllium 

Cadmium 

Calcium 

Chromium 

'cbalt 

Copper 

Iron 

Magnesium 

Manganese 

Nickel 

Potassium 

,river 

Sodium 

V,uiadium 

Zinc 

_,tront_um 

CAS Number 

7429-90-5 

7440-36-0 

7440-39-3 

7440-41-7 

7440-43-9 

7440-70 2 

7440-47-3 

7440-48 4 

7440-50-B 

7439-89-6 

7439-95-4 

7439-96-5 

7440 02 0 

7440-09-7 

7440-22-4 

7440-23 5 

7440-62-2 

7440-66-6 

7440-24 6 

Elan. Sample 

Same 

QCBLK132982-1 

,CBLK192982-1 

QCBLK192982-1 

QCBLK192982-1 

QCBLK192982-1 

QCBLK192982-1 

QCBLKi92982 1 

QCBLK192982 1 

QCBLK192982-1 

Q'CBLK192982 1 

QCBLK192982'_ 

]CBLK192982-1 

y7RLK 2_52982 1 

-CBLK_92982-1 

]CBLK:52982-1 

CCBLK_92982 1 

.CBLK--2982-1 

QCBLK_92982-1 

QCBLK_52982t 

Prep. 

Date 

11/23/98 

11/23/98 

11/23/98 

i. 1/23/98 

__/23/98 

/23/98 

_1/23/98 

11/23/98 

11/23/98 

11/23/98 

1'_/23/95 

_:/23/98 

__/23/98 

L/23/9H 

,/23/98 

L./23/98 

11/23/98 

11/23/98 

11/23/98 

Analyses 

Lace 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11-/24/98 

11/24/98 

11/24/98 

11/2.4/98 

11/24/98 

11/24/98 

24/98 

_1/24/98 

LL;24/98 

11;24/98 

11/24/98 

I1/24/9e 

Result Unit Qual 

20.6 UG/L U 

33.0 UG/L U 

26.2 UG/L 9 

0.56 UG/L 9 

2.6 UG/1, U 

59400 UG/L 

164 UG/L 

2.4 UG/L U 

2-9 UG/L U 

46.2 UG/L B 

10900 UG/L _ 

1.3 UG; L _ 

10.8 UG/L it 

_720 UG/1, E 

5.o UG;L i 

1520 UG/L 

5.6 UG/L E 

349 'Jr 'L 

289 UG/L 

Detection 

Lim,.t Dilute::n 

00 1 

60-0 1 

Category: LCP Metals-5010A !T'AL) 

Method: EPA 601.0 


Clisnt tD_ BOR4C9 

Analyte 

Aluminum 

Antimony 

Barium 

Beryllium 

âdmium 

Calcium 

Chromium 

Cobalt 

''upper 

Iron 

Magnesium 

'4anganese 

l,ckel 

-,tassium 

silver 

Sodium 

vanadium 

ain- 

3Lrontiuoi 

CAS Number 

]440-36-0 

1440-39-3 

7440-41-7 

-1440-43-9 

7440-70-2 

:'440-47-3 

"440-48 4 

440-50-8 

-1439-89-5 

7439-95-4 

7439-96 5 

7440 - 02 - 0 

7440-09-7 

7440-22 4 

7440 23 5 

7440 62 2 

7440-56 6 

)440-246 

51ank Sample 

Name 

QCBLK192982-1 

QCBLK192982-1 

QCBLK192962-1 

QCBLK192982-. 

QCBLK192982.I 

QCBLK192982 I 

QCBLK192982.I 

QCBLK192982-1 

QCBLK192982 1 

QCBLK192982-1 

OCBLK192982 -1 

QC9LK192982 1 

QC13LK192982-1 

QCBLK192982 1 

'CBLK192982 1 

2CBLK192982-1 

CCBLK192992 -1 

.CBLK192982 1 

)C9LK192982 1 

Guanwrla R_cc1and 

3350 GeOrQe Washington 'Kay 

Richlacd, IIA 99352 

-rojec=. 150-184. 

Prep. 

Date 

23/98 

11;23/98 

__:23/96 

023/98 

,1,21/9E 

123/98 

_1/23/98 

1!23/9E 

:1/23/98 

_1/23/98 

1/23/98 

1/23/98. 

X1/23/98 

183/98 

Lj 23/90 

1/23/98 

1L/23/98 

LL/ 3/98 

Analyses 

Date 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

L1/24/98 

11/24/98 

_1/24/98 

-1/24/9E 

11/24/98 

11/24/98 

11/24/90 

11/24/98 

/24/98 


20.6 UG/L J 

33.0 UG/L 

26.0 UG/L 

U 

J.83 UG/L e 

2.7 UG/L ._ 

57900 UG/L 

167 W/L 

2-4 U(3/L 

3.0 JG/L B 

83-0 UG/L o 

10700 UG/L 

7.6 1 G/L _ 

_0.8 UG/L 

3450 'JG/L - 

5.0 UG/L 

7400 UG/L 

16 9 UG/L 3 

351 U(3/1. 

293 UO/L 

SdmD.e Date 10/27/48 


-Report Date 12/07/98 

Qaanterra ID 19221 c04 

Detection 


2C0 

50.0 

200 

5.0 

5.0 1 

5000 

10.0 

50.0 I 

100038 

25.D 

10) 

500) 1 

15.0 

40.0 

5000 

10.0 

5000 

50.0 

20.0 _ 

50.0

,Lua:Iter ra Hacb'_and 

3350 George Washingten way 

RiclLalm. WA 99352 

?ro]ect, 150-]84 

Categarv: ICAP Metals - S^:SSolved Sample Gate 10/2119, 

Method: EPA 6010 Receipt Date 10/27/5' 

Matrix: LIQUID Report Date 12/07/9, 

Client :D: BOR499 Quanterra ID 19221 065 

3iank, Sample Prep Analyses Detection 

Analyte CAS Number Name Date Date Result Unit Qual. Limit Dilution 

Aluminum '1429-90 -5 QCBLK192982 -1 11;23/98 11/24/98 23.1 UG/L B 200 1 

Antimony '1440 -36-0 :22LK192982 1 11;2.3/98 11/24/99 33.0 UG/L 1 60-0 _ 

Barium ']440 -39-3 QCBLK192982 1 1;23/98 11/24/98 38-0 UG/L B 200 

Beryllium 7440 -41-7 QCBLK192982 -1 :;23/98 '_1/24/98 1 57 U3/L B 5-0 1 

Cadmium ')440 -43-9 QCBLK192982 -1 -:;23/98 11/24/98 3.7 UG/L B 5.0 - 

Calcium '7440 70-2 QCBLK192982 1 -23/98 11/24/98 61600 UG/L 5000 

Chromium '1440 -47-3 QCBLK192982 -1 _:;23/98 11/24/98 243 UG/L 10.0 

Cobalt 9440 48-4 QCBLK192982 -1 -_/23/9H 11/24/98 2.4 UG/L ] 50.0 

Copper 7440-50 -8 Q2BLK192982 1 L '../23/98 :1/24/98 19.2 UG/L B 25.0 

Iron ']439 -89-6 QCBLK192982 -1 _1;23/98 II/24/98 41.8 CG/L B 100 

Magnesium 9439-95 -4 QCBLK192982 1 !-,23/98 11/24/98 13300 UG/I. _ 5000 

Manganese 7439 -96-5 QCBLK192982 1 .:;23/98 :1/24/98 ;-6 CG/:. B i5.0 

Nickel 7440 -02-0 vCB LK192982-1 -;23/9E _1/24/99 1018 UC/:, 40-0 

Potassium 

Silver 

7440 -09-7 

7440-22 -4 

QCBLK!92982 

)CBLK!92982 

1 

1 

-:,'23/96 

_,'23/98 

-,/24/18 

=2/24/98 

6220 

5.0 

IIG/:. 

UG/L 

j 

5000 

10.0 

Sodium 9440 23 5 QCSLK192982 1 .L;23/9F. C/24/98 24600 UG/L 5000 1 

Vanadium 7440 62 2 Q"BLK192982 1 ._/21/9. -1/24/58 17-0 113/L B 50-0 1 

Zinc 1440 -66-6 QCBLK192982 1 0;23/99 11/24/98 7.2 UG/L 3 20.0 1 

Strontium 1440-24 6 "BLK192982-1 .-;23/98 :1/24/98 277 UG/I. 50-0 ,

Category: 

Method: 

Matrix: 

Client ID: 

ICP Metals 

EPA 6010 

LIQUID 

BOR490 

-6G10A (TAL) 

Quan C2xra R1Ch: aad 

3351 :3eorg e Washington Way 

Rll R:a 1[], .;A 99;'32 

-_:r • ecC -.50-t84 

Sample Date 

Receipt Date 

Report Date 

Quan[e rra ID : 

10/27/90 

10/27/9tl 

12/07/98 

19221-G')6 

Blank Sample Prep. Anaiyses Detect,on 

Analyte -AS Numher Name Cate Date Result Unit Qual. Limit Dilution. 

Aluminum 7429 -90-5 QCBLK192982 -1 11/23/98 11/24/98 20.6 '1G/L U 2CO 

Antimomi 7440 -36.0 QCBLK192982 1 11/23/90 11/24/98 33.0 UG/L U 60.0 1 

Barium 7440 -39-3 QCBLK192982 1 11/23/98 11/24/98 38.6 UG/L B 2CO - 

Beryllium '1440 -41-, QCBLK192982 I _1-/23/98 11/24/98 0.57 U,/:, R 5-0 1 

Cadmium 7440 -43 9 QCBLK192982 1 L1,23/98 11/24/90 2.6 U3/I. T, 5.0 

Calcium 7440 -70-2 QCBLK1929821 11/23/98 11/24/98 62600 UG/1, 5000 

Chromium 2440 -47-3 QCBLK192982 1 11/23/90 :1/24/98 318 UG/L 10.0 I 

Cobalt '1440 -48-4 QCBLK192982 1 11'23/98 11/24/98 2.4 TT U 50.0 

Copper '1440 -50-8 QCBLK192982 1 :L'23/98 11/24/98 4.1 UG/L, 9 25,0 

Iron '43989 -6 QCBLK192982 -1 11'23/98 11/24/98 260 UG/L 100 

Magnesium "439 -95-4 QCBLK192982 -1 _1'23/98 11/24/98 13600 Vd/I, .: 5000 

Manganese 7439 96-5 QCBLK192982 -1 _1;23/98 11/24/98 9.0 1:3/L B 15.0 1 

Nickel '/440 -02 L QCBLK192982 1 :1;23/98 11/24/98 26.8 U3/L R 40.0 

Potassium /440 -097 QCBLK192982-1 __;23/98 11/24/98 5680 CG/1. 5002 

Silver "1440 -22-4 QCBLK192982 1 __1-23/98 11/24/98 5.0 DG/L j 10.2 

Sodium 9440 23-5 QCBLK192982 -1 11,21/96 11/24/98 25600 U3/1. 5001 

Vanadium 7440 -62 2 QCBLK192982 1 -i,21/9F :1/24/98 16.0 1: 1/ 9 50-1 , 

Zinc 7440 -66-a QCBLK192982 -1 :1/21/98 11/24/98 5.7 UG/L B 20.0 - 

Stroutium 7440 -24 E QCBLK192982 1 _123 1 96 :1/24/98 282 U':/L 50.0 1

Client ID_ BOR4K9 

Analyte 

E1ank Sample 

CAS Number Name 

aL r2ê rr a Ri c!llancl 

350 George Washangton Way 

4A P93F2 

Prc,er- '0 1 8 4 

Category. :CAP Metals - Dissolved Sample Date 10/27/98 

Method. 2PA 6010 Receipt Date 10/27/98 

Matrix LIQUID Report Date 12/07/98 

Quanterra ID 19221 U:i7 

Pre p, Analyses Detect:.cn 

Cate Date Result Cn1t Qual_ Lim,[ Dilut,oe 

Aluminum 7429 -90-5 QCBLK192982-: 1' 23/90 11/24/98 20.6 CG/L ., 200 

Antimony 7440 -36-0 QCBLK192982-1 '._/23/98 11/24/98 33.G UG/L 60.0 1 

Barium 7440-39 -3 QCBLK192982-1 iI/23/99 11/24/98 0.63 UG/L B 200 1 

Beryllium 7440 -41-7 QCBLK192982 1 11/23/98 11/24/98 0.50 UG/L 'II 5.0 1 

Cadmium 7440 -43-9 QCBLK192982-: !1/23/98 11/24/98 2.6 CG(L _ 5.0 

Calcium 7440 -70-2 2CBLK192982 1 :1123/98 11/24/90 225 UG/1, H 5000 

Chromium 7440 -47-3 QCBLK192982 1 i1/23/9B 11/24/98 2.7 -,T I/ U 10.0 

Cobalt 7440 -48-4 QCBLK192982 1 11/23/98 11/24/98 2.4 1 3/L '3 50.0 

Copper 7440 -50-8 DCBLK192982-1 11/23/98 11/24/98 2.9 CG/ 1. 

25.0 1 

Iron 7439 -89-6 QCBLK192982 1 -1;23/98 -1/24/98 34.9 U3 /L H 100 i 

Magnesium 7439 95-4 QCBLK192902 1 11;23/98 11/24/98 150 UG/L BE 5000 1 

.Manganese '1439 96-5 QCBLK192982-_ 11;23/98 11/24/38 2.9 ... . B 15.5 

Nickel 7440 -02-0 QCBLK192982 1 _23/96 11 11 24/98 10.8 UJ/L 11 40.0 1 

Potass,um 7440 -09-7 QCBLK192982 I -'_/23/98 li/24/98 1220 -3/L 'J 5000 1 

Silver 7440 -22-4 QCBLK192982-1 ,1/23/9H 11/24/98 5 0 CG/- :1 10.0 

Sodium 7440-23 5 ^CBLK192982 1 __/23/98 11/21/98 440 R;/L I ;000 

Vanadium "1440 -62-2 QCBL"K192982-1 _:;23/9F 11/24/90 6 4 _ b SO.O L 

Zinc °440 -66-6 QCBLK192982 1 1/2 /9L !1/29/98 7.0 __, ., H 20.0 

Strontium '440 24-6 CCBLK192982-1 1,?^/98 11;24/98 2 7 SG/L 50.0 - 

'J 

t(),1041

Category: 1CP Metals 6010A ;TAL 



Client ID. BOR4LO 


Blank Sample 

Name 

Quan to r—_3Ric bland 

3350 Gecr.3e Washington Nay 

Rachia-i. ?'A 99352 

Fro g, -=C, lh4 

Prep. 

Date 

Analyses 

Date 

Aluminum 7429 -905 QCBLK192982 -1 123/98 11/24/98 

Antimony 9440 -36-0 QCBLK192982 1 1_'23/98 11/24/98 

Barium 7440 -39-3 QCBLK192982 -1 __l23/S8 11/24/98 

Beryllium 7440 -41 7 QCBLK192982 -1 _-723/98 11/24/98 

Cadmium 7440 43-9 QCBLK192982 1 __ 23/96 11/24/98 

Calcium 7440 70-2 QCBLK192982 1 _1.23/98 11 1 24 1 98 

Chramlum 7440 -47 3 QCSLK192982-1 __,23/98 11/24/98 

Cobalt 9440 48-4 QCBLK192982 -1 -_/23/98 11/24/98 

Copper 9440 -50-8 QCBLK192982 -1 __;23/98 11/24/98 

Iron 7439 -89.6 QCBLK192982 -1 _1,23/98 11/24/98 

Magnesium 7439 -95-4 QCBLK292982-1 __/23/98 11/24/98 

Manganese 7439 -96-5 QCBLK192982 1 _]l23/98 11/24/98 

Nickel 7440 -02-0 QCBLK192982 1 __l23/98 11 1 24 1 98 

P p taseium 7440 -097 QCBLK192982 -1 __-23/99 11/24/98 

Silver 7440 22-4 QCBLK192982 I -. 23/98 11/24/98 

Sodium 7440 -23-5 QCBLK192982 I __'23/93 _1/24/98 

Vanadium '7440 -62-2 QCBLK192982 '_ -1'23/98 11/24/98 

Zinc 7440 -66-6 QCBLK192582 1 __;23/98 11/24/95 

StrOntlum '7440 -24-0 QCBLK192982 -1 ._,'23/95 11/24/98 


20.6 UG/L U 

33.0 DG/L U 

0.60 :JG/L U 

0-50 IG/L U 

2-6 1IG/L 

204 '1G/L B 

1 -G/L ll 

2 4 ',IG/L i1 

1 DG/I. B 

17.8 JIG/L 8 

ill UG/L BE 

_.9 U3/L B 

10.0 [:G/L ',] 

1220 

S,0 UG/L 'J 

332 DG/L B 

c.4 'J3/1. B 

9 DG/L 3 

2.7 Ug /L i 


Receipt Date = 10/2'7/'30 

Report Date 12/07/?d 

Quanterra ID 19221-198 

Detection 


2)0 

60.0 1 

zoo 

5 1 

5 0 

5000 

10 C 

50 C 

25 0 

100 

5000 L 

15.0 

40,C 

5000 

10.0 

SOCO 

50.0 

20.0 

50.0 1 

7.100042

Aualyte 

Antimony 

Barium 

Beryllium 

Cadmium 

Calcium 

Chromium 

Cobalt 

Copper 

Iron 

Magnesium 

Manganese 

Nickel 

Potassium 

Silver 

Sodium 

Vanadium 

Zinc 

Strontium 

Blank Sample 

CAB Number Name 

7429-90-5 UCBLK192982 1 

1440-36-0 OCBLK192982 1 

7440-39-3 QCBLK192982-1 

7440-41-7 QCBLK1929821 

7440-43-9 QCBLK192982 1 

7440-)0-2 QCBLK192982-1 

7440-k7-3 QCBLK192982-i 

7440-48-4 QCBLK192982-i 

7440-50 8 OCBLK192982 1 

7439-89-6 QCBLK1929821 

7439 95-4 QCBLK192982-1 

7439-96-5 QCB1,K192982-1 

7440-J2 0 QCBLK192982 

7440-09-7 QCBLK192982 1 

7440 22-4 QCBLK1929B2 1 

7440-23 5 UCBLK192982 1 

7440-62 2 QCSLK192982 1 

"1440-66-6 QCBLK192982-: 

7440-24 6 QCBLK192982-L 

Q'.ia uce rra-kicCl and 

3350 Georoe Washington Way 

Rcchland. '.JA 99352 

P-o3 ect. 550.184 

Category: ICAP Metals - Dissoived Sample Date _0/2'/98 

Method: EPA 6010 Receipt Date :5/27/95 

Matrix: LIQUID Report Date 12/07/9B 

Client ID: BOR4F4 Quanterra I1) = 

P[ep. Analyses 

Date Date 

1/23/98 

_1/23/98 

1/23/9h 

/23/96 

11123/98 

_;23/9E 

1/23/96 

11/23/98 

ii/23/96 

_/2,3/98 

L/21/98 

;_/23/98 

/23/98 

_/23/98 

G/23/98 

L/2 3/95 

/23/98 

1/23/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

1/24/98 

_4/98 

1/24/98 

11/24/98 

11/24/98 

1/24/98 

11/24/98 

11(24/98 


20.6 UG/L U 

33.0 UG/L q 

68.5 UG/L 6 

...57 UG/L B 

2.6 UG/L D 

94700 qG/L 

249 UG/L 

2.4 UG/L U 

5.7 UG/L B 

132 U3/L 

23800 UG/L E 

12-0 UG/L B 

188 'JG1_ 

7000 U13/L 

5 0 UG/L U 

L9300 UG/L 

20.8 qG/L B 

7-0 UG/L B 

456 UG/L 

Deteci:i On 

Lim..t Dilution 

200 

60.0 

CC 

-0 

5000 

10.0 

50.0 

25.0 

]On 

5000 

1'.0 

40.. 

5000 

10.0 

5000 

5(-0 

2C.0 

5C.G 

1)nrl043 

19221 J(,9

]ategory: :CP Metals -e010A TALC 



-ient _1 BOR4F5 

analyze 

Anta mony 

Barium 

5eryllium 

Cadmium 

Calcium 

_::rom ium 

-chalt 

-cDper 

tron 

MaQneslulll 

I^.anganese 

Nickel 

coca ssi wo 

SiLrer 

:odium 

.'anadrum 

,.0 

Lt roll, lum 

(AS Number 

Blank Sample 

Name 

t ..hn CErla X21 C::^311d 

0 George Washrngmn Way 

R_c hiand, WA 99352 

._;. 

- ,n . 194 

Pren 

Date 

Analyses 

Date result Unit Qual 

".429 -90-5 QCBLK192982 1 L1 23/96 11/24/98 0-6 UG/L U 

9440 -36-G QCBLK192982 1 '.1/23/98 11(24/98 _-3.0 UG/L 

'440 -39-3 QCBLK192982-1 li/23/98 11/24/98 59.6 JG/L B 

-, 440 -41-7 QCBLK192982-1 11 11 23/98 11 /24/98 ).57 UG/L B 

7440 -43-9 QCBLK192982-1 11/211)8 11/24/98 2.6 UG/I. 

7440 -70-2 QCBLK192982-1 1;23/99 11/24/98 .4D00 'J3/L 

7440 -47-3 2CBLK192982 1 :1/23/98 _1/24/98 428 UG/L 

7440 -48-4 QCBLK192982-1 '.1/23/98 11/24/98 2.4 UG/1, U 

7440 -50-8 QCBLK1929821 _1/23/98 '_1/24/98 2-9 UG/L _ 

7439 -89-6 LC2LK192982 1 :1/23/90 11/24/90 778 U 3 /L 

7439 -95 4 QCSLK192982 _ :1/23/98 11/24/98 _3700 UG/L E 

7439 -96-5 iCBLK192982 1 :1/.:3/98 :1/24/98 __- 7 UG/L 

?440 -02-0 QCBLK192982-I _1/.:3/98 11/24/90 207 UG/1, 

7440 09 . 7 QCSLK192982 1 /:3/98 11/24/98 _s'_e 'JG/L 

7140 22 4 :2CBLK192982 1 11, 1 :3/98 11/24/98 5.0 UG/L U 

7440 -23-5 OCBLKL92982 1/:'.3/98 11/24/98 -3100 UG/1, 

7440 62 2 QCBLK192982 - _'_/23/98 .1/24/98 _[-4 UG/L B 

7440 66 6 ICBLK!92982 1 /1.3/98 11/24/98 7.6 U(;/ I , B 

714024 -6 1ICBLK192982-i ..i: 3!98 11/24/98 451 UG/L 



Report Date 12/07/58 

Quanterra ID 19221 0:0 

Detection 

Limit Dilutic3 

200 

60.0 

200 

5.9 

5000 

10.0 

50.0 

25.0 

100 

5000 

15.0 

40.0 

5000 

10.0 

5000 

50.0 

20.0 1 

50.0 

30C!v44

Category: ICAP Metals - Dissolved 


Matrix: LIQU ID 

!IIient .D: BOR4L1 


Blank Sample 

Name 

^_a-Cerra Ric nland 

---c George Washington Way 

___^'and. '11A 99352 

50-184 

9rep, 

Date 

Analyses 

Date Result Unit Qual, 


Receipt Date . 10/29/99 

Report Date - 12/07/98 

Quanterra ID : 19221 0.. 

Detection 

Limit Diluu on 

ASUmi num "'429 -90-S QCBLK192982 1 '23/98 11/24/98 31.3 G/L B 200 

Antimony :'440 36-U CC13LK192962 '_ 1/23/98 11/24/98 33.0 UG/L U 60.0 

Barium ^440 -39-3 QCBLK192982 -1 .1;23/90 11/24/98 48.2 UG/L B 20) 

Beryllium ]440 41- 1 QCBLK192982 1 .1/23/98 11/24/98 0.56 U( 3 /L B 5.D 

Cadmium 9440 -43-9 QCBLK192982 -1 11/23/90 11 1/ 24/90 2.6 UG/L J 5.) 

Calcium 9440 -70-2 QCBLK192982 1 _1/23/98 11/24/98 93000 U'-/L 5000 

Chromium 7440 -47-3 QCBLK192982 -1 11/23/96 11/24/98 7.2 UG/L B 10.0 1 

Cobalt 7440 -48-4 QCBLK192982 -i :1/23/98 11/24/98 2.4 UG/L " 50.0 

Copper 7440 -50-8 QCBLK192982 1 11/23/98 11/24/98 2.9 UG/L U 25.0 

Iron 7439 -89-6 QCBLK192982 -1 '1/23/90 11/24/98 34.8 UC/L B 100 1 

Magnesium 7439 -95-4 ^CBLK192982 1 it/23/98 11/24/98 21200 CG/L B 5000 - 

Manganese 7439 -96-5 -. BLK192982 1 :1/23/98 11/24/96 4.1 UC/L B 15.0 1 

Vickel 7440 -02 0 }CBLK192982 1 :1;23/?6 -1/29/913 10.8 Ul/L 40.0 _ 

BoCaesrcnl 7440 09 7 ]CBLK192982 . .`-/23/98 .1/24/98 5280 UG/L 5000 1 

S leer 7440 -22 4 ]CBLK192982 :1, 3/ 11 8 .1/24/98 5.0 UG/L ^ 10.( 

,odium 7440 23 5 )CBLK192982 : -!/23/98 11/24/98 :6500 UG/L 5000 1 

Vanadium 7440 62 2 QCBLK192982-_ .1/23/98 11/24/98 21.1 UG/L B 50.0 

g ive 7440 -66 6 1CBLK192982-1 .1/23/98 11/24/98 - 5 .7 UG/L B 20.0 I 

3trontiwn 7440 -24 6 .CBLK192982 '_ 11/23/98 11/24/98 460 UG/I. 50.0 

:nij^45

Category: 1CP Metals-6G10A !1'AL' 



Client :D BOR4D2 

Analyte 

Antimony 

Barium 

Beryllium 

Cadmium 

Calcium 

Chromrum 

Cobalt 

Coppez 

Iron 

Magne Slum 

Manganese 

Nickel 

Potassium 

Silver 

Sodium 

Vanadimc 

Zinc 

strontium 

Blank Sample 


7429-90-5 QCBLK192982-1 

7440-36-0 QCBLK1929821 

7440-393 QCBLK192982-1 

7440-41-7 QCBLK192982-1 

7440 43-9 QCBLK192982-1 

7440-70-2 QCBLK192982-'_ 

7440 47-3 QCBLK192982-1 

7440 48-4 QCBLK192982-1 

7440-50-8 QCBLK192982-1 

7439 89-6 QCBLK192982-1 

]439-95-4 QCBLK192982-1 

7439-96-5 QCBLK1929821 

1440-02-0 QCBLK192982-1 

1440-09-7 QCBLK1929821 

7440-22 9 ICBLK192982 1 

?440-23-5 QCBLK192982-1 

1 440-62-2 QCBLK192982-1 

1 440 6ti-6 jCBLK192982 1 

`440-24 9 QCBLKI92982 1 

Qu ancer ra R_ch lard 

A350 Se or 3e Washington Way 

Rich Mind, WA :9352 

— sect: 550-.94 

Prep. 

aLe 

23/98 

1:/23/98 

11/23/98 

11/23/98 

11/23/98 

11/23/98 

11/23/98 

1:23/98 

11'23/98 

.1/23/98 

11 1 2 3 / 99 

,.'23/93 

11 23/ 98 

11'23/94 

-:r 23/98 

11;23/98 

1/23/99 

23/911 

25/99 

Analyses 

Date 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/99 

11/24/98 

:_/24/98 

11/24/99 

11/24/98 

11/24/98 

'1/24/98 

11/24/95 


20.6 UG/L 

33.0 UG/L U 

45.9 UG/L B 

0 57 UG/L B 

2.6 UG/L U 

88500 l3G/L 

3.4 UG/L B 

2.4 4:G/L U 

2.9 UG/L J 

71.4 UG/L B 

20100 UG/L E 

4.6 UC/1, B 

10.8 :'G /11 , 

6850 UG/L 

5.0 .G/L 

:6000 TG/1 

21.9 OG/1. 

17.9 UG/L B 

440 11G/1 

sample Date 10/27/98 

Receipt Date : 10/27/98 


Quanterra :D 19221-112 

Detection 

Limi: Dilution 

200 1 

60.0 1 

200 1 

5 0 

5 C 

5008 1 

10 d 

50.8 

25 0 _ 

lco 1 

0c0 

15.0 

40.0 

5000 

0.0 

5000 

50.0 

0.0 

SO.G L 

100u46

Analyte 

Antimony 

Barium 

Beryllium 

Cadmium 

Calcium 

Chromium 

Cobalt 

Npper 

Iron 

Magnesium 

Manganese 

Nickel 

Potassium 

Silver 

Sodium 

Vanadium 

zinc 

Stroutlum 

Quanterra-Rich:and 

3350 George washina to r 

R1chlar,. WA 39352 

Fr o , ec.. 550.184 

Category: ICP Metals-6010A !'CAL? Sample Date 10/29/98 

Method: EPA 6010 Receipt Date 10/27/98 


Client ID. BOR4F6 Quin to rra L., 19221-"1 

CAS Number 

31ank Samp le 

Name 

ârep- 

Date 

An— _s 

..a__ 


7429 -90 5 9-BLK192982-1 72 3/98 '_1/I-:98 31.0 UG/L B 

7440 -36 0 -, CBLK192982-1 :_/23/98 __,I-98 33.0 UG/L '.1 

7440 -39 3 2CBLK192982-_ ;[/23/98 i-1 - 58 29-2 CG/L 9 

9440 -41-7 1CBLK192982 1 =-/23/98 __,__ 38 r.5C UG/.. .. 

9440 -43-9 .C9LK192982 : =-./23/98 1-,- X 38 2.6 UG/L 

7440 -70 2 ;CBLK192982-1 .:./23/98 'cl/: 4.38 44000 UG/L 

7440 -47-3 ^,:BLK192982 1 1./23/98 11/2. 58 81.8 UG/L 

7440 -48-4 ICBLK192982 1 1_/2/98 11/=4.38 2.4 UG/L U 

7440 -50 8 rC 21,K192982-1 _!./23/98 11/14,98 2.9 UG/L U 

7439 -89-5 '-BLK192982 1 -:./23/98 it _4 28 48.") 'JG/L B 

7439 -95-4 1CBLK192982 1 I /23/98 1 1 , __ +8 9860 UG/L 11 

7439 96 5 2_BLK192952-1 1./23/98 11,.. ?8 3.1 'JG/I. B 

7440 -02-0 ;CBLK192982 C li/23/98 __,_ _ 10 o UG/L '.; 

7440 09-7 ;I'BLK!92982 .1/23/58 __ -8 3660 JG/L B 

7440 -22 9 .CBLK192982-: _;./23/98 ..._. -8 --„ 1( ;/L .. 

7440 -23-5 '.-BLK192982 1 ';/23/98 __, _. -8 10300 'UG/L 

7440 -62 2 )t'BLK192982 '. 11/23/98 11/1- -8 21.7 qG/L B 

7440 66 6 ;;"BLKI 92982-1 1:/23/98 11!=9:38 -.^ UG/L B 

7440 -24-6 :CBLK192982-1 11/23/98 11;14 3B 224 'JG/L 

Detec ti on 

Limit Diluc l,ln 

200 i 

60 0 1 

200 1 

5 1 1 

5 0 1 

5000 1 

10 1 1 

50.1 

25.1 

100 

5000 

40.0 

5000 

10.0 

5000 1 

50.0 I 

20.0 _ 

50.0 

I1n00it7

Quanteri3 aich'_ann 

3350 George Washirgton Way 

R1 C1:is nG, >,A 99352 

Category _ 

Method: 

LCAP Metals 

EPA 6010 

Lissoived Sample Date 

Receipt Date 

10/27/9 11 

10/27/98 

Matrax: LIQUID Report Date 

_ 

12/07/98 

Client 1D: BOR4L4 Quanterra ID = 19221 -014 

Analyte CZAR Number 

Blank Sample 

Name 

-0.134 

Prep. 

Date 

Analyses 

Date 

Aluminum 7429 -90-5 QCBLK192982 -1 -23 /9 8 11/24/90 

Antimony 7440 -36-0 QCBLK192982 1 _1/23/98 11/24/98 

Barium 7440 -39-3 QCBLK192982 1 :./23/98 11/24/90 

Beryllium 7440 -41-7 QCBLK192982 -1 .1/23/98 11/24/98 

Cadmium 7440 -43-9 QCBLK192982 -1 .,/23/98 -1/24/98 

Calcium 7440 -70-2 QCBLK192982 -1 11 1/ 2]/90 L1/24/98 

Chromium 7440 -47-3 QCBLK192982 C .1 2s/98 11/24/98 

Cobalt 9440 48-4 QCBLK192982 -1 11/23/90 L1/24/98 

Copper 7440 -50-8 QCBLK192982 I : 1 /23/98 11/24/98 

Iron 9439 -89 6 QCBLK192982 L 21/23/98 11/24/98 

Magnesium 7439 -95-4 QCBLK192982 -1 ;1/:3/98 :1/24/98 

Manganese 7439 -96-5 ^CBLK192982-1 :1/:3/98 11/24/98 

Nickel 7440 02-0 QCBLK192982 -1 ._.23/98 :1/24/98 

potassium 7440 -09-7 QCBLK192982 -1 _L/23/98 11/24/98 

311ver 7440 -22.4 QCBLKI92982-I _./23/98 11/24/98 

Sodium 7,140 235 QCBLK1929821 _1/:.3/98 11/24/98 

Vanadium 9440 62 2 JCBLK192982 ;1/23/98 11/24/98 

Zinc 7,140 66-6 QCBLK192982 -L -1/23/98 11/24/98 

>trontiuni 7x40 -24 6 QCBLK192982 ^_ _/:?3/98 '-1/24/98 


22.9 UG/L B 

33.0 UG/L 

29.0 UG/L B 

0.72 UG/L. B 

3.3 UG/L B 

43400 UG/L 

75.2 UG/L 

2.4 UG/L U 

2.9 UG/L U 

33.0 UG/L B 

9780 UG/L E 

3 8 UG/L B 

10.8 UG/L U 

3020 UG/L ., 

5.0 UG 1 1 111 

-0200 UG/L 

22.3 UG/L B 

8.0 UG/L B 

222 UG/L 

Der ecti Dn 

L1m1t Dilutroî 

20D , 

60.] 

200 

5.0 

5.0 , 

5000 1 

10.0 

50 0 

25.0 

100 1 

5000 

15.( 1 

40.0 i 

5000 1 

10.0 

5000 1 

50.0 

20.0 1 

50 0 

I 10001

:anterro Richland 



Pro l cct 650.10+4 

Categor y : ICAP Metals - 019_Olved Samâ le Date 10/28/98 

Method: EPA 6010 Receipt Date : 10/28/98 


Client ID: BOR491 Quanterra ID : 19254 001 

Analyte CAS Numbei 

auk Sample 

fame 

Prep. 

Date 

Analyses 

Uate Result Unit Qu il l 

Detec: ion 


Aluminum 7429 -90 5 yCBLK192982-'_ :_/23/98 11/24/98 24.5 UG/L B 200 - 

Antimony 944036 0 ;CBLK192982-1 1./23/90 11/24/90 33.J UG/L U 61.0 i 

Barium 7440 -39-3 CCBLK192982 1 11/23/90 11/24/90 27.3 UG/L B 200 

Beryllium 7440 41 7 ^CBLK192982- 1 11/23/98 11/24/98 0.64 UG/L B 5.0 

Cadmium 7440 -43-9 GCBLK192982-1 11/23/98 11/24/98 4.1 UVI, B S.0 

Calcium 7440 -70-2 ICBLK192982 1 11/23/90 11/24/90 54000 UG/L 5100 - 

Chromium 7440 -47 3 QCBLK192982-1 11/23/90 11/24/98 14-8 UVI, 11.0 i 

Cobalt 7440 -48-4 ;CBLK192982-1 11/23/90 11/24/98 2.4 UG/L U 51.0 

Copper 7440 -50-8 QCBLK192982 1 11/23/90 11/24/90 2.9 UG/L U 25.0 

Iron 7439 -89 6 =BLK192982 1 11/23/98 11/24/98 40.8 UG/L B L00 

Magnesium 7439 -95-4 iCBLK192982-1 11/23/98 11/24/98 10500 UG/L E 5]00 

Manganese 7439 -96-5 ,CB LK192982 1 11/23 11 98 11/24/98 4-1 UCIL B 15.0 

Nickel 7440 02 0 COBLK192982 1 1/23j58 11/24/98 10.8 UG/L U 41.0 

Potassium 7440 -09-7 "1_BLK192982 '_ _1/23/99 11/24/98 3690 UG/L B 5]00 

Silver 7440 -22-4 ;;-BLKI92982 1 [1/23/98 11/24/98 5.0 UG/L 1 11.0 

Sodium 7440 -235 GCB LK192982 1- /23/98 11/24/98 14000 UG/L 5100 

Vanadium 7440 62 2 UCBLK192982 1 ':/23/98 11/24/98 '_5-9 UVI, B 51.0 

Zinc 7440 -66-6 C9 K192982 1 1./23/90 11/24/98 8.4 UG/L B 21.0 - 

Strontium 7440 -24 6 ;:-BLK192982 1 11/23/98 11/24/98 220 UG/L ID .0 

1300)43

Category: !CAP Metals 

Method EPA 6010 


Client ID: BOR4B1 

Analyte 

Antimony 

Barium 

de ryl liven 

'admrum 

Calcium 

chromium 

Cobalt 

.topper 

lion 

14agne9lnm 

Manganese 

Fickel 

I-otasslum 

6r I v e r 

5'odlum 

%anadium 

zinc 

Strontium 

J1s601VEd 

CAS Number 

7429-90-5 

7440-36-0 

7440-39-3 

7440-41-7 

7440-43-9 

7440-70-2 

7440.49-3 

7440-48-4 

7 , 1 40 50-8 

7c39 . 89-6 

7439-95-4 

7439 96-5 

7440 02-0 

7440 09-7 

7440-22 4 

7440-23-5 

7 440-62 2 

/440-66-6 

7440-24-6 

Blank Sample 

Name 

QCBLK192982-1 

QCBLK192982 1 

QCBLK192982 1 

']CBLK192982-1 

QCBLK192982 -1 

QCBLK192982-i 

QCBLK192982 -1 

QCBLK192982 -1 

QCBLK192982-1 

QCSLK192982-1 

QCBLK192982 -1 

QCBLK192982 -1 

UCBLK192982-i 

QCBLK192982 -t 

QCBLK1929B2-1 

QCBLK192982-'. 

QCBLK192982 - : 

QCBLK192982 1 

,^ CBLK192982 1 

)conterra -.n c11 arc 

3350 George Wasn-,ton Way 

Ri chianti, wA 991c2 

9ro;ect ':50.164 

l-rep. 

Date 

1/23/98 

/23/96 

,1/23/98 

11/23/98 

11/23/98 

1111 - 3/98 

11/-3/98 

1:/23/98 

11/23/98 

11/23/98 

11/23/98 

11/23/98 

1_ /23/98 

"_/23/93 

1/23/9x` 

1/ 91 

1/98 

23/98 

l 112 ;/98 

Analyses 

Date 

-1/24/98 

_1/24/98 

_1/24/98 

11/24/98 

]1/24/98 

1/24/98 

-1/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

:1/24/98 

1/24/98 

11/24/98 

:/24/98 

_1/24/98 

1-/24/98 

=124/98 

__/24/98 

Result Unit Qua 

20.6 UG/L U 

33.0 UG/L U 

46-2 UG/L B 

0.57 UG/L B 

2.6 UG/L U 

878JO UG/L 

3-0 UG/L B 

2.4 UG/L U 

2.9 UG/L U 

46.0 UG/L B 

19800 UG/L E 

7.6 UG'L B 

30-0 UG/L 8 

408" UG;L B 

5.0 UG/L U 

7650 t1G/L 

18.2 'JG/L B 

6.2 UG/L B 

177 T TG / L 




Quanterra ID : 19254 Oft 

Detection 


^noo,)o 

20(1 1 

60.0 

200 

5.( 1 

5.0 _ 

5000 

10.0 

50.0 1 

25.0 1 

100 

5000 1 

15,0 

40.0 

soon i 

1c.o _ 

5000 

50.0 

20.0 

50.0

Quanterxa-Rich_and 

3350 Geor

Category :CP Metals 6010A 'CAL' 

Method -PA 6010 

Matrix: :IQUID 

Client L3 SOR492 

AnalyCe CAS Number 

Biank Sample 

Name 

Quanteraa Rtct-and 

3350 3eorge Washington Way 

Sian_and, WA 99152 

[-ro'ect. -,0._84 

S tep, 

Date 

Analyses 

Date 

Aluminum 7429 -90-5 QC13LK192982 L 11/23/98 11/24/98 

Antimony 7440 -36 0 QCBLK192982 1 11/23/98 11/24/98 

Barium 7440 -39-3 QCBLK192982 1 11/23/98 11/24/98 

Bery llium 7440 41- -, QCBLK192982 -1 _1/23/98 11 /24/98 

Cadmium 7440 43-9 OCBLK192982-1 11.'23/58 11/24/98 

Calcium 744070 -2 QCBLK192982 -1 11/23/98 _1/24/98 

Chromium 7440 47-3 QCBLK192982-1 Li/23/98 11/24/98 

Cobalt 7440 48-4 QCBLK192982-1 11/23/90 11/24/98 

Copper 7440 -50-8 QCBLK192982-1 1,/23/98 11/24/98 

Iron 7439 89-6 QCBLK1929821 11/23/98 11/24/98 

Magnesium 7439 -95-4 QCBLK192982 -'1 .1 23;98 11/24/98 

Manganese 7439 -96-5 QCBLK192982 1 11/23/98 11/24/98 

Nickel 7440 02-0 QCBLK192982-: 1123;98 11/24/98 

Potasslum 7440 -09 7 QCDLK192982-1 _1-23/91 11/24/98 

Silver 7440 22-4 QCBLK192982 1 1 123/98 11/24/98 

Sodium 7440 -23-5 QCBLKI92982 1 _:'23/98 1_1/24/90 

Vanadium 7440 62-2 QCBLK192982 1 LL '23/98 11/24/90 

Zinc '7440 -66-6 QCBLK192982 L :1'23/9!! 11/24/98 

Btrontinm 7440 -24-6 QCBLK192982 -1 11,'23/98 11/24/98 

Sample Date 10/28/j8 


Report Date 12/07/9- 

Quanterra ID 19254 J04 

Detection 

Result Uni t Qual Limit Dilutloe 

64.3 '1G/L B 

33-0 l;G/L D 

26.2 13/L B 

0.57 .'G/L B 

...6 

53400 

_G/L 16 

21.1 ,:G/L 

2.4 JG/L U 

2.9 CG/L U 

131 DG/L 

10400 T ., .. 

6.1 J3!1. 3 

10-8 .'C/L I 

2340 '3/L B 

.0 ; 33/1 T 

13500 C1/L 

20.1 C3/L B 

6.5 'S3/L B 

2 13 ; :' /L 

230 

60.0 1 

210 

5-0 1 

5.0 1 

5000 

10 0 1 

50 0 1 

25 0 

10C 

5000 

15.0 1 

40.0 

5000 

10.0 

loco 

50.0 

20.0 

50.0 1 

OO^J^

Quante sa Rici)land 

3350 Seorce Washington Way 

F,h'_and. AA 39352 

Pro , ect .=C -'b4 

Category: ICP Metals 6010A 1'CALi Sample Date 10/28/98 

Method EPA 6010 Receipt Date 10/28/98 


Client 1D: BOR4F9 Quanterra IL 1925410'5 

Analyte 

=_ink Sample 


?rep 

:ate 

Analyses 

Date 

Result unit Qual 

Detection 


7429-90-5 Q7BLK192982 1 

x/29/98 20.6 'JG/L U 

200 1 

Antimony 

944036-D YCBLK192982 1 

c/23/99 11/24/98 33.0 JG 1- 

60.) 

Barium 

Beryllium 

7440-39 3 

7440-41-7 

-,CBLK1929B2-1 

QCBLK192982-1 

__/2S /98 

/23/94 

11/24/98 

11/24/98 

29.9 

0.57 

UG/L 

'JG/L 

B 

B 

200 _ 

Cadmium 

7440-43 . 9 1CBLK192982 

/23/96 11/24/98 2-8 JG/L 

5.. 

Calcium 

hromium 

7440-70 2 

7440-473 

Q2BLK192982 

1CBLK192982 . 

23/98 

23/98 

11/24/98 

11/24/98 

3880(, 

46.0 

CG/L 

JG/L 

5000 

10.0 

Cobalt 

744048-4 ^7BLK192982-1 

/23/98 13/29/98 2.4 'JG/L U 

50.0 1 

Copper 

7440-50 . 8 CRLK192982-1 

on 

7439-89-6 iCBLK192982-1 

Magnesium 

7439-95-1 lRLK192982-1 

Manganese 

7439-96-'3 ,3CBLK192982 t 

Nickel 

40.0 7440-02 0 ,CELK192982 1 

Potassium 

7440-09-7 CCBLK1929821 

Silver 

7440-22-4 Q(BLK192982-: 

Sodium 

7440-23 5 1BLK192982 

Vanadium 

7440-62-2 ';('BLK192982 1 

zinc 

7440-66 3 'CBLK192982 1 

Strontium 

7440-24 1i 3LK192962 1 

/23/98 

/23/98 

/23/98 

t3) 90 

_/9a 

..:;23/98 

§8 

_3/98 

_;23/58 

u; 98 

:1/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

11/24/98 

_1/24/98 

_1/24/98 

11/24/95 

11/24/98 

3-2 

208 

10800 

7-4 

.6.5 

4610 

5 C 

13906 

29.3 

6-5 

q 

'JG/L 

'JG/L 

UG/L 

UG/L 

qG/L 

JG)L 

'J L 

T1/1.. 

JGiL 

'IG/L 

'lG/L 

B 

e 

B 

B 

B 

' 1 

B 

R 

25-0 

100 

5000 

15_ C 

5000 

10.0 

5000 

50,) 

20.0 

50-0 

1 

1 

I 

1 

1 

1

':uanterra Richland 

.358 George Nashiagcon way 

NA 99352. 

.:.._. -50-04 

Category . CLAP Metals -90111 V eu Sample Date 10/28/98 

Method: -PA 6010 Receipt Date : 10/28/98 

Matrix : LIQUID Report Date _ 12/07/98 

Client 1D BOR4P7 Quanterra ID 19254 ]06 

Analyte 

Antimony 

Barium 

Beryllium 

Cadmium 

Calcium 

Chromium 

Cobalt 

Copper 

Iron 

Magnesium 

Manganese 

Nickel 

Potassium 

Silver 

Sodium 

Vanadium 

Zinc 

Strontium 

CAS Mims, 

]429-90-5 

7440-36-0 

7440-39 3 

7440-41-7 

9440 439 

7440-70-2 

7440-47-3 

7440-48 4 

7440-50-8 

7439-89 6 

7439-95 4 

7439-9 ; iS 

7440 C2-0 

7440.097 

'440-22 4 

7440 2s 5 

'440 62 

7440-66 0 

7440 24-a 

Blank Sample 

Name 

QCSLK192982 

QCDLK192982.1 

QCBLK192982 1 

QCBLK192982 

OCBLK192982-_ 

QCBLK192982 -1 

QCBLK192982 1 

OCBLK192982 

QC13 LK192982-. 

QCBLK192982 1 

QCBLK192982 -_ 

QCBLK192982 

QCBLKI9 2 992-1 

QCBLK192982 -1 

QCBLK192982 _ 

QCBLK192982-: 

QCBLKI91982-1 

QCBLK192982 1 

QCBLK292982 - 

Prep, 

Date 

,/23/98 

L 1/23/98 

C,/21/98 

L 1/23/90 

L' '21/9H 

LL/23/98 

1_/'23/98 

/23/90 

1 123 /98 

/23/98 

/23/98 

1:/23/98 

11/23/98 

11/23/98 

.1/23/96 

11/::3/^8 

1;2]/98 

23/9g 

Analyses 

Late 

1/24/98 

11/24/98 

11/24/98 

11/24/98 

1'_/24/98 

11/24/98 

11/24/98 

11/24/98 

-1/24/98 

11/24/98 

11/24/98 

11/24/98 

_1/24/98 

11/24/98 

L1/24/98 

11/24/98 

1i/24/98 

11/24/98 

11/24/98 

Result Umt Qual 

20.6 'JG/L U 

33.0 '7G/L U 

29.9 UG/L B 

0.56 UG/L B 

2.6 JG/L U 

39400 7G/L 

12.8 UG/L 

2.4 JG/L U 

2_9 UG/L U 

50.2 UG/L B 

11000 UG/L R 

4.2 'JG/L B 

11.8 7G/L e 

3240 '.lG/L 

;.0 'lG/L U 

L4200 11G/L 

2'0.3 JG/L 0 

1 .3 UG/L B 

100 13/L 

Detection 


200 

60.0 

200 

5.0 

S) 

5000 _ 

10 0 

50.0 

25.0 

110 1 

5070 

15.. 

40.0 _ 

50)0 

10.0 

5000 

SO.i. 

20 C 

50 C

Quanterra-Richland 

3350 Geoz ge Washington Way 

RLet:!aIId, WA 99352 

er,eC , _ ' SO.la4 

Category: MERCURY Sample Date 10/27/96 

Method: EPA 7470 Receipt Date,_0/27/98 

Matrix: LIQUID Report Date 12/C9/99 

Client Quanterra dank Sam p le Prep, Analyses Detect o:: 

ID ID Anal-':e ^_AS Number Name Date Date Result Unit Qua:. Limit __.. 

BOR4F5 19221-010 Mercer: 7439-91 6 QGBLK192313-L 11/17/98 11/17/98 0.10 UG/L U 0.2C 

BOR4F8 19254-005 Mercer-. 7439-97 6 QC13LF,19231 -L _1/17/98 11/17/98 0.10 UG/L U 0.2J 

-Inno57

Category Mercury - Dissolved 

Method EPA 7470 


Quancerra E.-cnianI 

3350 Gecroe Washin g ton Way 

Richland, 99352 

Prole__ _._94 

Sample Date - 10/29/99 



Client Quanterra 5;arx Sample Prep. Analyses Detection 

1D ID Analyte CAS Numbor _.ame Cate Date Result Unit Quai. Limit D11, 

SOR4F4 19221-009 Merc ury 7439 -97 c rCE. 8:92313 1 11/17/98 11/17/95 0.10 'SG/L U 0 2C 1 

BOR4F4 19221 009MS Mercury 7439 97 c ,CEL K _92_1: 1 . 1 /17/95 11/17/95 102 BREC _ 

BOR4F4 19221-009MSD Mercury 7439 -97 CBLK-92313 1 11/17/95 11/17/99 100 4REC 

BOR4F7 19254 006 Mercury 7439 -97 E ^ 1 11/17/99 11/17/95 0.10 'Id/L U 0 20 1 

ooQ59

U.S. EPA - 'LP 

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE 

Lab Name: QUANTERRA MO 'ontract: 519.184 

Lab Code: ITMO Case No.: SAS Nc.: SDG No.: WD2587 

SOW No.: SW846 

EPA Sample No. Lab Sample ID 

_BOR4130 19221-006_ 

_BOR481 _19254 -002 

_BOR4132 19254-003 

9OR4C7 19221-003 

_BOR I&C8 L9221-004 

80R4D1 19221-011_ 

_BOR4D2 L9221-012 

_BOR4F4 19221-009 

BOR4F4SD _192, ?1-009SD_ 

_BOR4F4S 19221-009S 

B0R4F5 :19221-010 — 

90R4F6 __i9221 -013 

30R4F7 __9254 -006 

30R4F8 I 92`-4-005 

_BOR4K9 19221-007 

_BOR4LO 19221-008 

_BOR4L4 __19221-014_ 

BOR491 19254-001 

_BOR492 19254-004 

BOR494 19221-001 

Were ICP interelement corrections applied ? 

Were ICP background corrections applied ? 

If ves - were raw data generated before 

application of background corrections ? 

Comments 

Yes/No YES 

Yes/No YES 

Yes/No NO 

I certify .hat this data package is in compliance with the terms and 

conditions of the contract, both technically and for completeness, for 

or:her than the conditions detailed above. Release of the data contained 

in this hardcopy data package and in the computer-readable data submitted 

on floppy diskette has been authorized b y the Laboratory Manager or the 

Manager's designee, as verified by the òllowing signature. 

Signature: Name: 

Date ._.tle. 

COVER PAGE - IN SW--..5

Lab Name: QUANTERRA MO 

U.S. EPA - --LP 

COVER PAGE - INORGANIC ANALYSES DATA. PACKAGE 

"ontra = 519.=34 

Lab Code: ITMO Case No.: SAS No.: SDG No.: S^70258? 

SOW No.: SW846 

EPA Sample No. 

_BOR494SD 

_BOR494S 

BOR495 

BOR499 

Were ICP interelement corrections applied ? 

Were ICP background corrections applied ? 

If yes - were raw data generated before 

application of background corrections ? 

Comments: 

Lab Sample ID 

19221-OO1SD 

19221-OO1S 

19221-002 

1.9221-005 

Yes/No YES 

Yes/No YES 

Yes/No NO- 

1 certify that this data package is in compli ance with the terms and 

conditions of the contract, both technically and for completeness, for 

ether than the conditions detailed above. Release of the data contained 

in this hardcopy data package and in the computer-readable data submitted 

on floppy diskette has been authorized b ry the Laboratory Manager or the 

Manager's designee, as verified by the following signature. 

S_anature: Name: 

Date Title: 

COVER PAGE - 1N SW-846 

n(1fiQ^ j

Color Before: 

Color After: 

Comments: 

CAS No 

7429-90-5 

7440-36-0 

7440-39-3 

7440-41-7 

7440-43-9 

7440-70-2 

744C-47-3 

744C-48-4 

744C-50-8 

7439-89-6 

7439-95-4 

7439-96-5 

7439-97-6 

7440-02--0 

7440-09--7 

7440-22 -4 

7440-23-5 

7440-62-2 

7440-66-6 

7440-24-6 

U.S. EPA - CLP 

1 EPA SAMPLE NO. 

INORGANIC ;VALYSES DATA SHEET 

BOR4B0 

Lab Name: QUANTERRA MO _ontract: 519.184 

Lab Code: ITMO Case No.: SAS No.: SDG No.: W0258-1 

Matrix !soil/water): WATER —aE Sample ID: 19221-006 

Level (low/med): LOW Date P.eceived: 10/.'.7/98 

Solids: 0.0 

Concentration Units (uc/L or mg/kg dry weight): LTG/L_ 

Analyte Concentration C Q M 

Â T minuet u 

20.6 U 

SIP 

Antimony_ 

33.0 U 

P_ 

Barium 

38.6 B 

Beryll um.'_ 

_C . 57 B 

^P– 

Cadmium 

2.6 U 

^P . 

Calcium _02600 P' 

Chromium_ _ 

318 P 

Cobalt 

^2.4 U 

( Copper_ ^4.1 B 

!Iron 

260^ 

Magnesium 

13600( 

Manganese 

9.0 B 

Mercury_ 

—E--! 

P 

P 

P_I! 

P 

'P 

NR 

Nickel 26.8 B P 

Potassium 5680( 

P– 

Silver _ 5.O, U 

P 

Sodium 

25600' 

P 

Vanadium 

1 6.O^B 

^P–I 

Zinc – —_ - 5.'7ÎB P i 

Strontiur _ 

282 P 

Clari Before: Texture: 

Clar-_}r After: Artifacts: 

–I 

I 

SW-846


1 EPA SAMPS_E NO. 

INORGANIC ANALYSES DATA SHEET 

3 0 R43' 


Lab Code: ITMO Case No.: 

Matrix (soil/water ) : WATER 

Level (Low/med): LOW 

Sol_ds: 0.0 

Contract: 

SAS No.: 

519.184 

SDG No.: 

Lab Sample :D: 

Date Received: 

W02587 

19254-002 

1 0/28/98 

Color Before: 

Color After: 

Comments: 

Concentration Units (ug/L or mg/kg dry weight): UG/'- 

CAS No Analvte Concentration C _QM l 

7429-90 -5 

7440 -36-0 

7440 -39-3 

7440 -41-7 

7440 -43-9 

7440 -70-2 

7440 -47-3 

7440 -48-4 

7440 -50-8 

7439 -89-6 

7439 -95-4 

7439 -96-5 

7439 -97-6 

7440 -02-0 

7440 -09-7 

7440 -22-4 

7440 -23-5 

7440 -62-2 

7440 -66-6 

7440 -24-6 

A Tum num um _2 0 . 6 

Antimony _33.0 

Barium 46.2 

Beryllium —__0.57 

Cadmium 2.6 

Calcium 87800 

Chromium_ __ _3.0 

Cobalt 

2.4 

Copper_ ---- --2.9 

Iron 46.0 

Magnesium 19800 

Manganese 7.6 

Mercury_ 

__ 

Nickel 

_30.0 

Potassium] 4080 

Silver 1 5.0 

Sodium I _ _7650 

Vanadium_ _18.2 

Zinc 6.2 

Strontium 377 

Clarity Before: 

Clarity After: 

i 

P 

P 

P_ 

P-i 

P 

P 

F -_- 

P 

P 

E a– 

P 

NR 

P_ 

F_ 

P- 

_ Texture: 

Artifacts, 

F 

I 

^:W-846 

-in00 63 

I

CAS No 

7429-90-5 

7440 -36 -0 

7441-39 -3 

744C -41 -7 

7440-43 -9 

7440 -70 -2 

7440 -47 -3 

7440 -48 -4 

7440 -50 -8 

7439 -89 -6 

7439 -95-4 

7439 -96 -5 

7439 -97-6 

7440 -02 -0 

7440 -09 -7 

7440 -22 -4 

7440 -23 -5 

7440 -62 -2 

7440 -66 -6 

7440 -24 -6 

U.S. SFA - --LP 


Analyte ConcentrationiC^ Q M 

A Tu num 132 3 P 

Antimony_ 33.OiU P 

Barium 48 .013 P --^ 

Beryllium `_ 0.80 !i 3 P_ 

Cadmium 

2.6101 

ICalcium I, P- 

910001_ 

P 

Chromium , 21.'2, 

^P_^ 

,Cobalt 2.41J! 

K oppe r 

3.3 3 P 

Iron — ^^' — —331' p- 

Magnesiuml 20100, E P_ 

Manganese 14._;31 P 

Mercury_' NR I 

(Nickel 34.313 P li 

Potassium) _4930'3 

Silver 

Sodium 78501 P 

Vanadium 27.8 3 , nlZinc 

- - - 8._'31 P 

Strontium _379 P_i 

EPA SAMPLE NO. 

BOR492 



Matrix (soil/water;: WATER 

Level (low/med): LOW 

Contract: 

SAS No.: 

519.184 

SDG No.: 

-an Sample ID: 

-7 ate Received: 

W02587 

19254-003 

10/28/98 

s Solids: 0.00 

Concentration Units (ug/L or mg/kg dry weight): UG/L 

Color Before: Clarity Before: Texture: 

Color After: Claritv After: Artifacts: 

Comments: 

3W-846 

ino(164

Color Before: 

1'olor After: 

Comments: 

J.S. EPA CLP 

i 


INORCANIC ANALYSES DATA SHEET 

Lab Name: QUANTERRA, MO 


Matrix (soil/water): WATER 


° Solids: 0.0 

Contract: 

SAS No.: 

519.184 

SDG No.: 

Lan Sample In: 


9OR4C"' 

W02567 

19221-003 

10/27/98 

Concentration Units (ug/L or mg/kg dry weighti: UG/L 

CAS No Analvte Concentration CI Q M 

7429 -90 -5 

7440 -36 -0 

7440 -39 -3 

7440 -41 -7 

7440 -43 -9 

7440 -70 -2 

7440 -47 -3 

7440 -48 -4 

7440 -50 -8 

7439 -89 -6 

7439 -95 -4 

7439 -96 -5 

7439 -97 -6 

7440 -02 -0 

7440 -09 -7 

7440 -22 -4 

7440 -23 -5 

7440 -62 -2 

7440 -66 -6 

7440 -24 -6 

A u^num 20.6 

Antimony_ i 33.0 

Barium 

Beryllium) 

Cadmium 

Calc'_um ! 

Chromium 

_26.2 

0.56 

2.6 

_59400 

164 

CobaIt 

Copper_ ,- 

Iron _ 

Magnesiuml 

Manganese) 

Mercary_ 

Nickel 

Potassiumi 

Silver 

Sodium 

Vanadium_ 

Zinc 

Strontium. 

2.4 

2.9 

46.2 

10900 

7.3 

— 

10.8 

1720 

5.0 

7520 

349 

289 

Clarity 3etore^. 

Claritl :After: 

U 

U BBU 

U 

U B 

B 

U 

B 

U 

B 

iP P 

P_I 

P 

P 

P p– 

I^ – 

E —Ip 

NR', 

PP–, 

P - 

P 

P_ 

P_' 

I_ 

i 

_i 

Texture: 

Artifac,-s: 

Sig-846 

^0006S

Color Before: 

Color After: 

Comments: 


1 EPA SAMPLE NC. 

'INORGANIC ANALYSES DATA SHEET 

30R4C8 

Lab Name: QUANTERRA MO Contract: 519.184 

Lab Code: ITMO Case No.: SAS No.: SDG No.: W02587 

Matrix !soil/water): WATER Lam Sample ID: 7-9221-004 

Level (low/med) LOW Date Received: 10/27/92 

% Solids: 0.1 

Loncentration Units (ug/L cr mg/kg dry weight): UG/-- 

CAS No Analyte (,Concentration ICI 4 lul 

7429 -90 -5 

7440 -36 -0 

7440 -39 -3 

7440 -41 -'7 

7440 -43 -9 

7440 -70 -2 

7440 -47 -3 

7440 -48 -4 

7440 -50 -8 

7439 -89 -6 

7439 -95 -4 

7439 -96 -5 

7439 -97 -6 

744J -02 -0 

7440 -09 -7 

7440 -22 -4 

7440-23 -5 

7440 -62 -2 

7440 -66 -6 

7440 -24 -6 

!A uminum , 20.6 

Antimony— 33.0 

Barium _26.0 

Beryllium _0.83 

Cadmium 2.7 

Calcium 57900 

Chromiva_ 167 

(Cobalt --2.4 

Copper_ I_ 

3.0 

Iron _ 83.0 

Magnesium _i 10700 

(Manganese __7.6 

,Mercury_ 

( Nickel 10.8 

Potassium _ 

U 

P- I 

U 

P 

B P 

B — P 

BI 

P 

P' 

7-J 

P 

P- 

BI 

P_ 

E P 

9 

P— 

NR 

U 

P 

_3450 B 

P— 

Silver_ _ 5.0 U P 

Sodium _7400 

p_ 

Vanadiun 16.9 C 

'I pP_. 

(Zinc —! _ _351 

Strontium) 283 



I— I 

I 

— 

Texture: 

Artifacts: 

SW-846

Color Before: 

Color After: 

Comments: 

U.S. EPA - C T 





BOR4D1 





o Solids: 0.0 

Contract: 

SAS No.: 

519.184 

SDG No.: 

Lan Sample -D: 


W02587 

19221-011 

10/27/98 

Concentration Units (ug/L or mg/k g dry weight): UG/^_ 

CAS No Analyte Concentration C1 Q n 

7429 90 -5 

7440 -36 -0 

7440 -39 -3 

7440 -41 -7 

7440 -43 -9 

7440 -70 -2 

7440 -47 -3 

7440 -48 -4 

7440 -50 -8 

7439 -89 -6 

7439 -95 -4 

7439 -96 -5 

7439 -97 -6 

7440 -02 -0 

7440 -09 -7 

7440 -22 -4 

7440 -23 -5 

7440 -0'2 -2 

7440 -66 -6 

7440 -24 -6 

A Tminum u 

Antimony 

Barium 

Beryllium 

Cadmium 

calcium— 

Chromium 

Cobalt 

Copper_ 

Iron 

Magnesium 

Manganese 

Mercury_ 

Nickel 

Potassium 

Silver 

Sodium 

Vanadium 

Zinc 

Strontium 

IB 

33.0 U 

48.2 B 

0.56 B 

2.6 U 

93000 

.2 B 

2.4 U U 

4.8 B 

21200 

4.1 !B 

_0.8IU 

6280 

_ 5.OI 0 

____16500 

_ 21.4 B 

_ 15.7 B 

460' 

P ' 

P 

P_ 

P 

P- 

P_1 

P - 

P - 

p- 

E - P 

— ! P- 

NR' 

P- 

P li 

P 

-P_' 

P 

P - 

P 

Texture: 

Artifacts: 

SW-846 

^ 00 e67

Color Before: 

Color After: 

Comments: 


1 EPA SAMPLE N0. 


BOR4D2 





o Solids: 0.0 

Contract: 519.184 

SAS No.: SDG No.: 

----L--al5 Sample ID: 


W02587 

19221-012 

10/27/98 


CAS No. 

7429 -90-5 

7440 -36 -0 

7440 -39 -3 

7440 -41 -7 

7440 -43 -9 

7440 -70 -2 

744J -47 -3 

744 -48 -4 

744D -50 -8 

7433 -89 -6 

7439 -95 -4 

7433 -96 -5 

7433 -97 -6 

7440 -02 -0 

7440 -09 -7 

7440 -22 -4 

7440 -23 -5 

7440 -62 -2 

7440 -66 -6 

7440 -24 -6 

Analyte 

AA umminum 

Antimony 

Barium 

Beryllium 

Cadmium 

Calcium 

Chromium_ 

Cobalt 

Copper_ 

Iron 

Magnesium 

Manganese 

Mercury_ 

Nickel 

Potassium 

Silver 

Sodium 

Vanadium 

Zinc 

Strontium 

Concentration 



20.6 

33.0 

45.9 

_0.57 

2.6 

88500 

- 3.4 

-- 2 .4 

2.9 

71.4 

20100 

4.G 

_6850 

5.0 

16000 

21.9 

17.9 

440 

C 

U 

U 

B 

B 

U 

B 

U 

U B 

"I 

U 

U 

B 

B 

Q 

E 

101 

P_ 

P_ 

P 

P 

P 

P_ 

P 

P_ 

P 

P_ 

P_ 

P 

NR 

P 

P 

P 

P 

P_ 

P 

P 

Texture: 

Artifacts: 

^W-846 

-Inn068 

I 

l

Color Before: 

Color After: 

omments: 


INORGANIC ANAL'SES DATA SHEET 



EPA SAMPLE NC. 

EOR4F4 

Lab Name: QUANTERRA MO Contracts: 519.184 


Matrix (soil/water): WATER — a Sample 1D: 19221-009 

Level low/med): LOW Date Received: 10/27/98 

Solids: 0.0 

Concentration Units (ug/L or mg/kg dry weight;: UG/L 

I 

^ 

, 

CAS No. Analyte Concentration C Q M 

7425-90 -5 

744C-36 -0 

744C-39 -3 

744C-41 -7 

744C-43 -9 

7440-70 -2 

7440-47 -3 

7440-48 -4 

7440-50 -8 

7439-89 -6 

7439-95 -4 

7439-96 -5 

7439-97 -6 

7440-02 -0 

7440-09 -7 

7440-22 -4 

7440-23 -5 

7440-62 -2 

7440-66 -6 

7440-24- 6 

A uminum 20.6 U 

Antimony _33.0 U 

Barium 68.5 B 

Beryllium _ _0.57 B 

Cadmium 2.6 U 

Calcium 94700 

(Chromium 249 

'Cobalt -' -- —2.4 U 

—5 .7 

Toppe'-_ 

g 

,Iron 1321-11 

'Magnesium 23800 

Manganese 12.0 B 

',Mercury_ 0.10 U 

'Nickel - -- 188 

Potassium 7000 

'( Silver S.O,U 

Sodium _1.9300 

Vanadium 20.8 W 

(Zinc 7.O,B, 

Strontium _ _456 

E 

iP 

P_ 

F 

P 

P 

P 

F 

P- 

f- 

^P P - 

P 

CV', 

P 

P 

P-_' 

P 

P 

I 

Texture: 

Artifacts: 

SW-646 

I OO(G9



Concentration I C I 4 M 

U 

U BB 

U 

E 

P- 

P 

P 

P 

P 

P - 

P - 

P 

P 

P_ 

P 

P 

Cv 

P 

P 

P 

P P 

P - 

P 

EPA SAMP'-E NO 

30R4F5 




Level !;low/med): LOW 

% Solids: 0.0 

a ract: 

SAS No.: 

519.184 

SDG No.: 

Lai Sample ID: 


W02587 

19221-010 

10/:7/98 

Color Before: 

Color After: 

Comments: 


CAS No 

7429-90-5 

7440-36-0 

7440-39-3 

7440-41-7 

7440-43-9 

7440-70-2 

7440-47-3 

7440-48-4 

7440-50-8 

7439-89-6 

7439-95-4 

7439-96-5 

7439-97-6 

7440-02-0 

7440-09-7 

7440-22-4 

7440-23-5 

7440-62-2 

7440-66-6 

7440-24-E 

Analyte 

AA u 

Antimony 

Barium 

Beryllium 

Cadmium 

Calcium 

Chromium 

Cobalt 

Copper 

Iron 

Magnesium 

Manganese 

Mercury 

Nickel 

Potassium 

Silver 

Sodium 

vanadium 

Zinc 

Strontium 

_ 20.6 

33.0 

_69.6 

0.57 

_ — 2.6 

94000 

- 428 

2.4 

2.9 

778 

23700 

16.7 

0.10 

207 

6310 

5.0 

19100 

21.4 

7.6 

454 



i- 

i_ 

_ Texture: 

Artifacts, 

'W-846 

il000170

CAS No. Analyte Concentration 

7429-90-5 A uminum u 

31.0 

7440-36-0 Antimony — 'I _33.0 

7440-39-3 Barium 29.2 

7440-41-7 Beryllium) 0.50 

7440-43-9 Cadmium , 

_ 2.6 

7440-7C-2 I Calcium 

44000 

7440-47-3 ichrcmium_I 81.8 

7440-48-4 (Cobalt 

2.4 

7440-5 0 -8 .Copper_ _ 2.9 

l - V l - V 

7439-95-4 

7439-96-5 

7439-97-6 

7440-02-0 

7440-09-7 

7440-22-4 

7440-23-5 

7440 -62-2 

7440-66-6 

7440-24-6 

Magnesium 

Manganese 

Mercury_ 

Nickel 

Potassium 

Silver 

Sodium 

Vanadium 

Zinc 

Strontium 

U.S. EPA - (-LP 


9860 

_ 3 .1 

10.8 

3660 

5.0 

_10300 

---21.7 

5.3 

_224 

_ 

C Q M 

B P_ 

U P_' 

B P_ 

U P 

U P— 

P ^ 

U P 

U a— 

B I P 

i 

' 

B ENRI 

U 

B 

U 

P_I 

IP 

P 

IB 

F' 

P 

IB I P P 


20R4F6 

Lab Name: QUANTERRF, MO Contract: 519.184 1 I 


Matrix (soil/water): WATER Lam Sample ID: 19221-013 

Level (low/med): LOW Date Received: 10/27/98 

% Solids: 0.0 



Color After: Clarity After: Artifacts: 

Comments: 

SW-846 

i(;0071

CAS No. Analyte Concentrationic 

7429-90-5 

7440-36-0 

7440-39-3 

7440-41-7 

7440-43-9 

7440-70-2 

7440-47-3 

7440-48-4 

7440-50-8 

7439-89-6 

7439-95-4 

7439-96-5 

7439-97-6 

7440-02-0 

7440-09-7 

7440-22-4 

7440-23-5 

7440-62-2 

7440-66-6 

7440-24-6 

A uminum 

Antimony 

Barium 

Beryllium 

Cadmium 

Calcium 

Chromium 

Cobalt 

Copper_ 

Iron 

Magnesium 

Manganese 

Mercury_ 

Nickel 

Potassium 

Silver 

Sodium 

Vanadium_ 

Zinc 

Strontium 


I . EPA SAMPLE NO. 

INORGANIC ANALI'SES DATA SHEET 

OR4F" 

Lab Name: QUANTERRA MO Contract: 519.184 i 


Matrix (soil/water): WATER LaE Sample ID: 19254-006 

Level (low/med) LOW Date Received: 10/28/98 

c Soiids: 0.c 

Concentration Units (ug/L or mg/kg dry weigt): UG/L- 

_20.6 

_33.0 

29.9 

-_ _0.56 

2.6 

39400 

L2.8 

2.4 

----2 .9 

50.2 

11000 

4.2 

5.10 

__ 11.3 

_3240 

U 

U 

B 

B 

U 

U 

U B 

B 

U BB 

5.01U 

1 142G0 

_26.3 

7.3 

- 180 



Comments: 

B 

B 

Q 

5 

P 

P 

P 

P 

IP- 

P_ 

P_ 

P - 

P 

P_ 

P 

CV 

P 

P 

P 

P_ 

P 

P_ 

P 

^W-846





% Solids: 0.0 

CAS No 

742'3 -90 -5 

7440-36 -0 

7440 -39 -3 

7440-41 -7 

7440 -43 -9 

7440-70 -2 

7440-47 -3 

7440-48 -4 

7440-50 -8 

7439-89 -6 

7439-95 -4 

7439 -96 -5 

7439-97 -6 

7440-02 -0 

7440-09 -7 

7440-22 -4 

744C-23 -5 

7440-62 -2 

744C-66 -6 

744C-24 -6 



INORGANIC =1IALYSES DATA SHEET 

30R4F8 


SAS No.: SDG No.: W02587 

LaE Sample ID: 19254-005 

Date Received: 10/28/98 

Concentration Units (ug/L or mg/kg dry weight): UG/L_ 

Analyte -OncentrationlC'. 

A uT minum 20.6 U 

Antimony_ _33.0 U 

Barium 29.9 

Beryllium) _ _0.57 11 B 

Cadmium i _ 2.8 B 

Calcium 38800 

Chromium,_ V_ 46.0 

Cobalt 2.4 U -J 

Copper_ _ J3.2 B 

Iron - i208 

Magnesium J 10800 

1, 

_ 

Manganese _ _ 7.4 B 

Mercury_ ___O.10,U 

Nickel 16.5B 

Potassiumi _4610 B 

Silver_ 5.0 U 

i Sodium 13900 

Vanadium' 25.3 B 

(Zinc -- - 6.5 B 

Strontium' _ _179 

Q 

M 

P - 

P 

P P 

P 

P-' 

P_ 

Pp 

P 

P 

P 

CV 

P 

P 

P- 

P 

P 

P 

P_ 

Color Before: Clarit,3 Before: Texture: 

Color After: Clarit ,,° After: Artifacts: 

Comments: 

SW-846 

1no1 -1 r 3

Color Before: 

Color After: 

Comments: 




BOR4K9 




Level g low/med): LOW 

% Solids: 0.0 



—LYE Sample ID: 


W02587 

19221-007 

10/27/98 

Concentration Units (ug/L or mg/kg dry weight-): UG/L_ 

CAS No Analyte Concentration C 4 M 

7429 -90 -5 

7440 -36 -0 

7440 -39 -3 

7440 -41 -7 

7440 -43 -9 

7440 -70 -2 

7440 -47 -3 

7440 -48 -4 

7440 -50 -8 

7439 -89 -6 

7439 -95 -4 

7439 -96 -5 

7439 -97 -6 

7440 -02 -0 

7440 -09 -7 

7440 -22 -4 

7440 -23 -5 

7440 -62 -2 

7440 -66 -6 

7440 -24 -6 

A uminum 

Antimony_ 

Barium 

Beryllium 

Cadmium 

Calcium 

Chromium_ 

Cobalt 

Copper_ 

Iron 

Magnesium 

Manganese 

Mercury_ 

Nickel 

!Potassium 

Silver 

Sodium 

Vanadium_ 

Zinc 

IStrontium 

_ 20.6 

33.0 

0.63 

_0.50 

2.6 

-- —225 

------2 . 7 

---- —2 .4 

-- —2.4 

34.9 

150 

—2.9 



1220 

5.0 

440 

6.4 

7.0 

-2.7 

U 

U BUUBUU 

U 

B 

B B 

U 

U 

U 

B 

B 

B 

iT 

E 

P_ 

P_ 

P 

PP 

P_ 

P 

P- 

IP P- 

PNR 

P 

P 

P_ 

IP 

IP-- 

F 

i 

Texture: 

Artifacts: 

zW-84F 

0nu74

Color Before: 

Color After: 

Comments: 

CAS No 

7429-90 -5 

7440 -36 -0 

7440 -39 -3 

7440 -41 -7 

7440 -43 -9 

7440 -70 -2 

7440 -47 -3 

7440 -48 -4 

7440 -50 -8 

7439 -89 -6 

7439 -95 -4 

7439 -96 -5 

7439-97 -6 

7440 -02 -0 

7440-09 -7 

7440-22 -4 

7440 -23 -5 

7440 -62 -2 

7440--66 -6 

7440--24 -6 


i EPA SAMPLE NO. 


BOR4LC 





% Solids: 0.0 

Contract: c^_._84 


=ao Sample ID: 

,ate Received: 

W025F' 

19221-008 

10/27/98 


Analyte 

A um i nnum 

Antimony 

Barium 

Beryllium 

Cadmium 

Calcium— 

Chromium 

Cobalt 

Copper_ 

Iron 

Magnesium 

Manganese 

Mercury_ 

Nickel 

Potassium 

Silver 

Sodium 

(Vanadium_ 

Zinc 

Strontium 

ConcentrationiC 

Clarit y Before: 


20.6'1U 

33.0 Tj 

0.60U 

0.50 U 

2.6 J 

_ 204 3 

17.SIB 

_117 B 

10.8'U 

1220 

S.OIU 

332 B 

_6.4 3 

5.9 B 

2., J 

Q 

E 

i 

M 

P 

P—' 

P 

P_' 

P 

E) 

P 

P 

P__ 

P 

rdR ! 

p I 

I^ 

h_ 

P_ 

P 

t= I— 

I 

Texture: 

Artifacts: 

SW-846 

^-,00075

U.S. EPA - --LP 

1 EPA SAME:Ê NO 


1 

BOR4L4 





% Solids: 0.0 

Contract: 519.184 1 

SAS No.: SDG No.: W02587 

Lab Sample ID: 19221-014 



CAS No Analyte lConcentration C X 0 

7429-90 -5 

7440 -36 -0 

7440 -39 -3 

7440 -41 -7 

7440 -43 -9 

7440 -70 -2 

7440 -47 -3 

7440 -48 -4 

7440 -50 -8 

7439 -89 -6 

7439 -95 -4 

7439 -96 -5 

7439 -97 -6 

7440 -02 -0 

7440 -09 -7 

7440 -22 -4 

7440-23 -5 

7440-62 -2 

7440-66 -6 

7440-24 -6 

A Timm um 

22.9 B 

Antimony ___33.0 U 

Barium 29.0 B 

Beryllium _0.72 B 

Cadmium 3.3 B 

Calcium _43400 

Chromium_' 75.21 _ 

Cobalt 2.4 U 

Copper_ ,_ 2.9 U 

Iron 

3 3.012 

Magnesium 

Manganese 

Mercury_ 

Nickell 

Potassium 

Silver 

Sodium 

vanadium 

9780 

_3.82 

10.8 U 

3020 B 

5.0 U 

_10200 

_22.3 B 

Zinc 8.0 

1 

B 

Strontium 222 

P— 

P PPPP 

—E- P P 

olor Before: Clarity Before: Texture: 

Color After: Clarit y After: Artifacts: 

^cmments: 

P 

P' 

P 

PR 

P' 

P 

P 

P 

SW-846 

l00(-,!'7F


_. EPA SAMPLE NO. 


BOR49=_ 





Contract: 

SAS No.: 

519.184 

SDG No.: 

LaE Sample ID: 


54025£37 

_9254-001 

10/28/98 

% Solids: 0-0 

Concentration Units (ug/L or mg /kg dry weighti: UG/L 

CAS No. Analyte (Concentration 

7429-90-5 AA uT inum 24.5 

7440 -36 -0 Antimony 33.0 

7440 -39 -3 Barium _27.3 

7440 -41 -7 Beryllium 0.64 

7440 -43 -9 Cadmium _ 

4.1 

7440 -70 -2 Calcium— 54000 

7440 -47 -3 Chromium_ 14.8 

7440 -48 -4 Cobalt ---2.4 

7440 -50 -8 Copper 2.9 

7439 -89 -6 Iron 40.8 

7439 -95 -4 Magnesium _ L0500 

7439 -96 -5 Manganese', 4 . 1 

7439 -97 -6 Mercury_ 

744C -02 -0 Nickel 1 10.8 

744C -09 -7 Potassium) 3690 

744C -22 -4 Silver 5.0 

744C -23 -5 Sodium 14000 

744C -62 -2 !Vanadium ! 15.9 

744C -66 -6 'Zinc –' 8.4 

7440 -24 -6 ^Strontiuml 220 

C 

B 

U 

B B 

B 

– 

U 

B 

B 

U 

B U 

B 

3 

Q M 

U- 

E 

P_I 

P 

P 

P 

P P 

P- 

P 

P 

P_ 

P 

NR 

P 

P 

P 

p – 

P- 

P 

'P 



Comments: 

.I(10U 

SW-846





Solids: 0.0 

Color Before: 

Color After: 

Comments: 

U.S. EPA. - CLP 

INORGANIC ANALYSES BATA SHEET 



ki 


308492 


SAS No.: SDG No.: '402587 

Lam Sample ID: 19254-004 _ 


Concentration Units (ug/L or mg/'kg dry weight): UG/-- 

CAS No 

7429 -90-5 

7440 -36 -0 

7440 -39 -3 

7440 -41 -7 

7440 -43 -9 

7440 -70 -2. 

744 -47 -3 

7440 -48 -4 

7440 -50 -8 

7439 -89 -6 

7439 -95 -4 

7439 -96 -5 

7439 -97 -6 

7440 -02 -0 

7440 -09 -7 

7440 -22 -4 

7440 -23 -5 

7440 -62 -2 

7440 -66 -6 

7440 -24 -6 

Analyte 

A uminum 

Antimony_ 

Barium 

Beryll,um 

Cadmium 

Calcium 

Chromium_ 

Cobalt 

Copper_ 

Iron 

Magnesium 

Manganese 

Mercury_ 

Nickel 

Potassium 

Silver 

Sodium 

Vanadiwn_ 

Zinc 

Strontium 

ConcentrationlC 

i 64.3 B 

33.0 U 

--- 2 6 .2 B 

—_0.57 B 

_ 2.6 U 

i X3400 

-— 21. i - 

-— 2 . 4 U 

-- ---— _ .9 U 

_ 

131 

10400 

—^_ 5.18 

_i0.8 U 

2340 B 

_ 5.0 U 

_ 13500 

__20.1 B 

0'.5 B 

--l--213 

Q IM 

1 p I 

P 

P 

P—! 

P 

P 

—' P__ 

E P P - 

I Nff 

P 

P--; 

P -p 

P ^- I 

- P-I 

Texture: 

Artifacts: 

Ss'-846

Color Before: 

Color After: 

Comments: 

CAS No. Analyte Concentration lc 

7429-90-5 A unum I ^ 

7440-36-0 !,Antimony_; ^ 

7440-39-3'9arium 

7440-41-7 'Beryllium ) — 

7440-43-9 ( Cadmium 

7440-70-2 'Calcium 

7440-47-3 Chromium 

7440-48-4 'Cobalt i ^ 

7440-50-8 Copper 

7439-89-6 Iron 

7439-95-4 (Magnesium _ 

7439-96-5 Manganese 

7439-97-6 Mercury_ 

7440-02-0 Nickel 

7440-09-7 Potassium 

7440-22-4 ;Silver 

7440-23-5 (Sodium 

7440-62-2 ,Vanadium 




39.6 B 

33.0 U 

34.1 B 

0 79 B 

2.9 B 

47500 

440 

2.'I 

L.S^B1_ 

39.2 B 

10200 

Q 

E 

M 

P-I P 

P_i 

P 

P-I 

P 

P_ 

P-' 

14R 

P 

P 1,- 

p 

SOR49^. 


Lab Code: ITMO Case No.: SAS No.: SDG No.: W025E7 

Matrix (soil/water): WATER — Lam Sample ID: ;9221-00'_ 

Level (low/med): LOW Date Received: LO/27/98 

Solids: 0.0 

Concentration Units (ug/L or mg/kg dry weight;: UG/L_ 

7440 

7440 -66 

-24 -6 

-6 

I Zinc 

( Strontium 

10.8Û 

385013 

5.0 U 

_19100 

20.6 .3 

10.v'BI 

__ 204 

_ I 

1 - 



i 

Texture: 

Artifacts: 

i nnu7a 

SW-846

CAS No. Analyte Concentration 

7429 -90 -5 Aluminum _40.9 

7440 -36 -0 Antimony_ 33.0 

7440 -39 -3 Barium 33.7 

7440 -41 -7 Beryllium 0.57 

744C-43 -9 Cadmium 2.6 

744C -70 -2 Calcium ___ 16300 

744C -47 -3 

,Chromium 432 

7440 -48 -4 Cobalt _2.4 

7440 -50 -8 Copper 2.9 

7439 -89 -6 Iron 121 

7439 -95 -4 Magnesium, _9990 

7439 -96 -5 1 

M 



anganese 4.9 

7439 -97 -6 Mercury_' — 

7440 -02 -0 Nickel 10.8 

7440 -09 -7 Potassium ) 2510 

7440 -22 -4 Silver 5.0 

7440 -23 -5 ,Sodium !8900 

7440 -62 -2 !Vanadium 17.9 

7440 -66 -6 (Zinc 6.3 

7440 -24-6 ,Strontium _200 

C Q M 

B F 

U P 

B P 

B P 

U P pip 

i 

U 

P 

E P 

B — P–, 

NR 

U P 

BU PP_' 

B 

P- 

P– 

P 


BOR495 



Matrix ,soil /water): WATER Lab Sample ID: 19221-002 

Level ow/med) LOW Date Received: 10/27/98 

Solids: 0.0 

Concentration Units (ug/L or mg/kg dry weight,: UG/L 



Comment::: 

^-^nn08n 

SN-34 6

Color Before: 

Color After: 

Comments: 

CAS No 

7429-90-5 

7440-36-0 

7440-39-3 

7440-41-7 

7440-43-9 

7440-70-2 

7440-47-3 

7440-48-4 

7440-50-8 

7439-89-6 

7439-95-4 

7439-96-5 

7439-97-6 

7440-02-0 

7440-09-7 

7440-22-4 

7440-23-5 

7440-62-2 

744C-66-6 

7440-24-6 


EPA SAMP_iE NO. 






I 

BOR499 

Contract: 519.184 ^^ -^ 

SAS No.: SDG No.: W05587 _ 

LaE Sample ID: 19221-005 

Date Received: 10/::7/98 

s Solider: 0.0 


Analyte Concentration C Q M 

AA Tinum um 

23.1 B P 

Antimony- U P-_' 

Barium _38.0 B P 

Beryllium 0.57 B P 

Cadmium 3.7 B P 

Calcium 61600 _ 

P 

Chromium— 

Cobalt 

Copper - 

2.4 

- 19.2 

U 

B 

-P- 

-'P_ 

Iron -_--- 41.8 BI 

Magnesium 13300 

Manganese! — _5.6 B 

Mercury_ 

Nickel 10.8 U 

Potassium, 6220 

Silver 15.0 U 

Sodium24600 

P 

E iP 

J !P 

NR' 

P 

,P 

P 

P- 

Vanadium_ 17.0 B P_I 

ilinc 7.2 B P 

Strontium: 2771 ,-i P_ 

Clarity Before: 'Texture: 

Clarity After: Art_facts: 

-I 

P 

SW-846 

0001SI

,ivanterra Richland 



Pro3ecc 550.184 

Category: Anions Sample Date 10/29/98 

Method: EPA 300.0 ReCelpt Date 10/27'98 

Matrix: LIQUID Report Date 12/07!98 

Client ID: BOR495 Quauterra :D :9221 002 

Blank Sample Prep. Analyses Detection 

Analyte CAS Number Name Gate Date Result Unit Qual. Licit Dilution 

Fluoride 16984-48-8 QCBLK189945-1 10/28/98 10/28/98 0.26 MG/L 0.10 

Nitrate NO3 -N QCBLK189945-1 10/28/96 10/28/98 6.61 MG/L 0.20 ., 

Nitrite MO2 -N QCBLK189945 1 .0/28/98 10/28/98 0-020 ?1G/L U 0-C20 

.-in(^090

Quanterra- Richland 

3350 Geor ge Washing ton Fay 


Project. 550.:84 

Category- Anions Sample Date - 10/29/98 

Method: EPA 300.0 Receipt Date 10/21/98 


Client I0: BOR4C8 Quanterra ID 19221-(.04 

Blank Sample Prep. Analyses Detection 

Analyze CAS Number Name Date Date Result Unit Qual. Limit Dilution 

Fluoride 16984-48-8 QCBLK189945-1 1[/28/98 10/28/98 0.15 MG/L 0.10 1 

Chloride 16887-00-6 QCBLK189945-1 1C/28/58 10/28/98 12.2 MG/L 2.00 10 

Sulfate 14808-79-8 QCBLK189945-1 1C/28/98 10/28/98 -18.5 MG/L 5.GO 10 

Nitrate NO3-N QCBLK189945-1 lc/28/9B 10/28/98 5-54 MG/L 0.20 l0 

Nitrite NO2-N QCBLK1899451 1[/28/98 10 1 28 1 98 0.020 MG/L U 0.020 1 

11)n(:93

@ua nêrr.^ EiChlan. 

3350 Geozge Washing ton Way 

Ricn-and. WA 99352 

P ro^nct. 350.184 

cate gor y : ;lions Sample Date 10/29/98 

Method: EPA 300.0 Recei p t Date 10/27 96 

Matrix: LIQUID Report Date - 12/07:98 

Client i3: BOR4B0 Quanterra ID 19221 .06 

Blank Sample Frep. Analyses Detection 

Analyte CAS Numoei Name Gate Date Result Unit Qual. Limit Dilut_cn 

Fluoride 16984-4E-8 QCSLK189945-1 10/26/98 10/28/98 0.28 MG/L 0.10 

Nitrate NO3 N QCBLK189945 1 :0/28/98 10/28/98 9.61 MG/L 0.40 2 

Nitrite NO2 N QCBLK189945 1 10/28/98 10/28/98 0.( 1 20 MG/L U 0.)20

Category: A1111ne 

Method: EPA 300.0 

Yatrrx: LIQUID 

Client 1D: 13 OR4L0 

Quae^tex ra are hlard 

3350 Geox.ie Washington Way 


?rol eaL 550-'.84 

Blank Sample Prep. Analyses 

An,l e CAS Number Name Date Date 

Fl uorrde 16984-48-8 QCBLK189945-1 10/28/58 10/28/98 

Chlorvde 16889-00-6 QCBLK189945-1 1C/28/98 10/28/98 

Sulfate 14808-79-8 QCBLK1899451 10/28/98 10/20/98 

NiL_ate NO3 -N QCBLK1899451 10/28/98 10/28/98 

Nitr.Le NO2-N QCBLK189945 1 10/28/98 10/28/98 

Resul- 'Unit Qual 

0.19 MG/L G 

0.20 MG/L U 

0 5D MG/L C 

0.020 MG/L U 

0.020 MG/L 


RecelpC Date 10/27/98 


Quanterra IL 1922'_-.:08 

Detection 

Limit Dilntrcn 

0.10 

0.20 1 

osu _ 

0.020 1 

0.020 1 

4o(I(JJ

Category. Anions 

Method: =PA 300.0 

Matrix. LIQUID 

Client ID. ROR4F5 

Blank Sample 

Analyte CAS Number Name 

Fluoride 16984-48-8 r7BLK189945-1 

Nitrate NW -N QCBLK189945 1 

Sulfate 14808-99-8 kCBLK129945-1 

_—ntenra RLchland 

Ceorce Washington way 

. __. _and, NA X9152 

Samp..e Date :0/29 / Se 

Receipt Date - 10/27/98 

Report Date 12/09/9b 

Quan Cerra ID 19221 ) 1 J 

Prep- Analyses Detection 

mace Date Result knit Qual. Limn: Dil ut i:;n 

1C/28/98 10/28/98 0.28 MG/L O.LO _ 

1Cl28198 LO/28/98 8-51 MG/L 0.30 1 0 

10/28/98 10/28/98 88-2 MG/L 5-00 :C 

O C (19 ^'

uanterra R'Chland 

3350 3emrge Washington way 

Rich and, 'OA 39352 

_ .. 150.184 

Category: Anions samp, Date .012 a198 

Method: EPA 300"0 Receipt Date 10/27/98 

Matrix, LIQUID Report Date 12/07/99 

Client LC_ BOR4D2 Q - 

uanterra _v 19221 -:Ql 

Blank Sample Prep. Analyses Detect-on 

Analyte CAS Number Name Date Date Result Unit Qual. Limit Dilution 

Fluoride 16984-48-8 QCBLK189945 1 10/28/99 10/28/98 0.20 MS/L 0.1.0 1 

Nitrate NO3 -N QCBLK189945 1 10/28/90 10/28/98 39.5 M3/1, L.cO 40 

Nitrite ,102-N UCBLK189945-1 10/28/99 10/28/98 O.C20 MG /11 J.020 

.nit

:]uancerza Richland 

3350 George Washicgtdn Way 

Richland, NA 09952 

211 ,, ect- 50.134 


Method: EPA 300.0 Receipt Date : 10/27/98 


Client :D: BOR4F6 Guanterra ID 19221 -C.i 

Blank Sample Prep. Analyse= Detection 

Anal yce CAS Number Name Date Date Result Omt Qaal. Limit Dilution 

Fluoride :,6984-48-8 QCDLK189945-1 1D/28/98 LO/28/53 0.22 M3/., 0.10 

Chlorade 1,6889-00-6 QCBLK189945 -1 l0/28/9F 10/28/95 11.2 MG/L 1.00 l 

Sulfate 14808-79-8 QCBLK189945 1 10/28/98 10/28/3- 47.7 MG/L 2.50 

Nitrate NO3 N QCBLK189945 1 10/28/98 10/28/9_' 2.75 MG/L 0.10 

Nitrite NO2 N QCBLK189945 1 1C/28/98 10/28/3_ 0.020 M./L U 0.020 

1-100095

Quancer ra Richland 



550.194 


Method: EPA 300.0 Receipt Date 10/29/98 


Client ID- BOR4F6 Quante rra ID - 1922_-u I30UP 

Blank ?amole Prep. Analyses Detection 

Analyte CAS Number Name Date Date Result Unit Qual. Lim,; Dilution 

Fluoride 16984-48-8 QCBI.KI89945-1 x/28/98 10/28/98 0.22 MG/L O.10 1 

Chloride 16887-00-6 QC2LK189945 1 1-/28/98 10/28/98 10-6 MG/L 1-00 

Sulfate 14808-79-8 QCBLK189945 1 1[/28/98 10/20/98 47.3 MG/L 2.30 3 

Nitrate NO3-N QCBLK189945-1 1,1'28/98 10/28/98 2-75 MG/ T, 0...C - 

Nitrite NO2 -N QC21K185945-1 1C/28/98 '_0/28/98 0.020 MG/L ., 0.0:70 _

Quanterra R ich: and 

3350 Ieurye Washington way 

Richland. WA 99352 

1 1 11 ,'t 550.:84 

Category: Anions Sample Date 10/29/'8 

Method: EPA 300.0 Recelnt Date = 10/27/98 

Matrix- LIQUID Report Date 12/071`8 

_Lent '.:D: 60R4F6 Quancerra _E : 19221 -::_]MS 

Blank Sample prep. Analyses Detection 

Analyte CAS Number Name Date Date Result qelt Qua l. Limit Oil ut Ior. 

Fluoride 16984-48-8 QCBLK189945-: 10/28/98 10/28/98 97 3REC 1 

Chloride 16889 00-6 QCBLK189949 1 10/28/98 10/28/98 ll' sREC _. 

Sulfate 14808 79-8 QCBLK189941 1 10/28/98 10/28/98 95 4REC 10 

Nitrate NO3-N QCBLK1899451 10128198 i0/28/98 124 SREC 

Nitrite NO2 QCBLK189945 -1 Lo /28/98 10/28/98 118 REC .. 

,,oo1". 4

"anterri -R,cnlanp 

i35o beanie Wasfnrp ton ', 

dA '93'2 

F . o-sr . , 350.189 

Category. Anions Sample Cate :0/29/98 

Method: ?PA --0-0 Peceipt Date 10/27/90 

Matrix: :IQUID Report Date 12/07/90 

:lent :... 30R495 puanterra :D 19221 :02 

31 a:.R Sampie Prep Anaiy see Detection 

Analyte CAS Number ::a me Date Cate Result Unit Gual. Limit Dil ut:cn 

Chloride 16887-00-6 QCBLK -.91239-1 0/29/98 10/29 98 8-92 M3/1, 0.40 

Sulfate 14808--9-8 'CBLd:x1239 1 _9/29/98 ;0!23/53 16.6 MS/L L 00 

1-. 1 3

;uancerr a-Rlchl ana 

3350 George Washington way 

Rtch_ana. 'WA 99352 

:'ro-,1-c-t 550.184 

Category era ons -ample Date 10/2798 

Methcd EPA 300 0 Recerpt Date 10/27!98 

Matr,. _ ;UID Report Date 12/08/98 

_lienc :. ?0R490 U,anterra ID 19221 006 

Blank samnie Prep. Analyses Detection 

Analyte CAS Number Name Date Date Result Unit ]nal. Lirtit Dilution 

Chloride 16889-00-6 vCBLK191239-1 10/29/98 10/29/98 7 -22 MG/L 1.00 

Sulfate 14808-79-8 QCBLK1912 1 91 '.0/29/98 -0/29/98 45.8 MG/L 2.50 9 

14

,uanterr -sac.--na 

335C George wasnrnaton way 

3_ch:a^.n. wA 39352 

?z Ode^: _5-._'4 

Cateao ry : Anicns a'ample Cate - !0/2 7 ;98 

Method: -FA 500.` Recelct Date 10/27/98 

.Matrix: LIQUID Report Date 12/08/98 

Client L. 30R4F5 Quan terra ID 19221 :.0 

21ank Sample arec. Anaiysee Detection 

Anaiyte CAS Number Name Date Date Result unit Quai. Lim..t Dilution 

2hlorlae 16887-00-6 QCSLK191239- 1 LS/29/98 10/29/98 83.3 .MG/L 5 00 25 

Nit ri te NO2 N ^^_BLK191239-1 :J/29/95 10 1/ 20/98 D.10 MG/L 1 0 10 -

35C let. rae wasnrrcrin >:av 

_. ^... Inc. "dA -1332 

Ca to gory Anrcrs Sample Date 10/2"'/98 

Methca --PA 300.0 ReCe1Dt Da' :e = 10/27/98 

Matrix. LIQUID Report Date 12/07/90 

:Bent L. 30R4D2 Quanterra q? : 19221 012 

Blank Sa moie ?rep. A..laiyses Detect ion 

Analyte CAS Numder game ;;ate gate Result Unit Qual. Limit Dilutlon 

Chlorl de 16807-3:-_ QCBLK191239-1 :0/29/9B _3/29/98 13. 7 MG/L _.00 

Sulfate -4808-'9-_ ', CSLKt9]239 : -'/29/FB LJ/29/9B 49.4 I'VL 2.50 

-1nnl1- r'

2uanterra Ricn.and 

-1350 3ecrge Washington Way 

want eâ - RiU land 

-350 .i,r::e wasninocon wav 

Rl!n[ : " 4A 79352 

Categoryr -:nicns damole Date 10/2E/',' 

Method .2A 300.6 Decelpt Dare 10/28/93 

Matrix. :-:QUID Report Date 12/05/53 

]:ient :1. SGR492 ^.uanteira IC : 19254 -.:,-4 

31anx Sample ?rep. Analyses Detection 

Analyte CAS Number Name Date Date Result 9mt :oal. Limit Dilutacn 

Fluoride 16984-48-8 ^CBLK191239-1 /29/98 10/29/98 0.20 MG/L 0.10 

Chloride 16887-00-6 QCBLK191239-1 =`/29/98 22/29/99 3.64 MG/L 0.29 

Sulfate 

Nitrate 

Nitrite 

14808-79-8 

NO3-N 

NO2-N 

QCBLK191239-1 

;-CBLK191239-1 

2CBLK191239-1 

::/29/98 

'2/29/98 

-',29/98 

10/29/98 

10/29/98 

_0/29/98 

23.7 

7.69 

0-020 

MG/L 

MG/L 

11G/L 

_ 

1-00 

0.20 

0.020 

2 

:Q 

_

Category, Amcns 

Method: :PA 3 11 0.0 

Matrix. ;,SQUID 

Client 30R4F2 

Analyte 

-:Intern, -Cniana 

3350 :;eo ree 'dashington Way 

Sic h.. ^:^tl. _ :9352 

E ... -E: Leo 

Sample Date 1 0/28/98 

Receipt Date _0/28/98 


Quanterra L. . /9254005 

31ank Sample 'rep. Analyses Detection 

CAS Number Name :ate Date Result Onit veal. Limit Dilution 

Fluoride :6984-48-8 Q-BLK191239 1 ../29/98 10/29/98 0.24 MG/L 0.10 

Chloride 16881-00-6 QCBLK191239 1 L29/98 10/29/98 2.39 MG/L 0.40 .. 

Sulfate 14808 -29-8 QCBLK191239 1 _9/29/98 10/29/98 30.1 MG/L 1.00 

Nitrate NO3 -N QCBLK191239 1 LJ129/98 _0/29/98 2.58 MG/L 0.10 

Nitrite '102-N CCBLK191239 : .3129;98 _0/29/98 ).020 MG/L 1 0.020

_ateaory: Anacns 

Methoa'. EPA 3JO.0 


-lien[ 1L. NA 

;aanêz ra -:u ::^.l ar:a 

3,50 ie,j"e 4asnlnjton Wav 

.c c[_ana, '.iA 93352 

rc'e ._.194 

Blank Sample Prep. Analyses 

Analyte CAS NU si Name Date Date 

Fluoride 16984-48-8 QCBLK191239-1 .0/29/98 10/29/99 

^hloride 16889-GO-6 QCBLK191239-1 10/29/98 10/29/98 

Sulfate 14808-99-8 QCSLK191239-1 10/29/98 10/29/98 

Nitrate NO3-N QCBLK191239- 1 10/29/98 10/29/98 

NiCrlte NO2-N' QCBLK191239-1 :0/29/98 10/29/98 


0.10 MG/L U 

0.20 MG/L C 

0.50 MG/L U 

J.020 MG/L U 

).020 -IG/L U 

Sampie Date - NA 

Receipt Date NA 


Quancerra 1D QCBLF..91239-1 

Detection 


0.10 1 

0.20 

9 so 

0.020 

0.020 

i L L ^1

Analyte 

Chloride 

Sulfate 

Nitrate 

Nitrite 

2uantex'ra Richland 

3350 George Washington Wav 

?ic.^.lint. 4A ;9352 

:ro , eci. -SC--64 

:ateooty: Anions Camo+e Dace NA 

Mechoa. EPA 300.0 Receipt Dale NA 

Matrix: LIQUID Report Date 12/090 

- liens :D. NA Quanterra '.D -. QCL:B13.23)-'. 

Blank Sammie 


16984-48-8 QCBLK191239 

16887-00-6 QCBLK191239-- 

14808-79-8 QCBLK191239 -1 

NO3-N ]CBLK191239-- 

NO2-N (=LK191239 -1 

Step. 

Date 

.0/29/98 

0/29/98 

-0/29/98 

^/29/96 

0/29/90 

Analyses 

Data 

10/29/98 

10/29/96 

10/29/98 

10/29/99 

10/29/98 

Result Unit Qua.. 

92 %REC 

+REC 

%REC 

103 %REC 

1.0 %REC 

,il(l1l i 

Detection 

Linit Dilution

Bechtel Hanford, Inc. 



January 17, 1999 

A ttention: Jo an Kessner 

SAF Number 

Date SDG Closed 

Number of Samples 

Sample Type 

SDG Number 

Data Deliverable 

I. Introduction 

CERTIFICATE OF ANALYSIS 

C99-006 

November 10, 1998 

Ten 

Water 

W02587 

45-Day Summary 

^.raanterra 

y^ 

r,, ^•^ 1993 

Between October 27, and October 28, 1998, ten water samples were received by the Quanterra 

Environmental Services Richland Laboratory (QTESRL) for radiochemical analysis. Upon 

receipt, the samples were assigned the following laboratory ID numbers to correspond with the 

Bechtel Hanford (BHI) speci fic IDs: 

QTESRL ID# BHI ID# MATRIX DATE OF RECEIPT 

81050601 BOR495 Water 10/27/98 

81050602 BOR4 130 Water 10/27/98 

81050603 BOR4C8 Water 10/27/98 

81050604 BOR4D2 Water 10/27/98 

81050605 BOR4F5 Water 10/27/98 

81050606 BOR41`6 Water 10/27/98 

81050607 BOR41-0 Water 10/27/98 

81053301 BOR492 Water 10/28/98 

81053302 BOR4132 Water 10/28/98 

81053303 BOR4F8 Water 10/28/98 

11. Analytical Results/ Methodology

Bechtel Hanford Inc. 


Page 2 

%%uanterra 

The analytical results for this report are presented by laboratory sample ID. Each set of data 

includes sample identification information; analytical results and the appropriate associated 

statistical errors. 

The requested analyses were: Gamma Spectroscopy 

Gamma Scan by method RICH-RC-5017 

Gas Proportional Counting 

Gross Alpha by method RICH-RC-5014 

Gross Beta by method RICH-RC-5014 

Liquid Scintillation Counting 

Tritium by method RICH-RC-5007 

Carbon-14 by method RICH-RC-5022 

III. Quality Control 

The analytical results for each analysis performed under SDG W02587 include a minimum of 

one Laboratory Control Sample (LCS), one method (reagent) blank, and one duplicate. Any 

exceptions have been noted in the "Comments" section. Quality control sample results are 

reported in the same units as sample results. 

IV. Comments 

Gamma Spectroscopy 

Gamma Scan by method RICH-RC-5017 

The initial LCS was spiked with a Sr-Yt90 spike vial, therefore, the LCS was reprocessed. 

The LCS, batch blank, sample and sample duplicate (BOR495) results are within contractual 

requirements. 

Gas Proportional Counting 

Gross Alpha by method RICH-RC-5014 


requirements. 

Gross Beta by method RICH-RC-5014 


requirements. 

C 0-0

Bechtel Hanford Inc. 


Page 3 

%%%uanterra 

Liquid Scintillation Counting 

Carbon-14 by method RICH-RC-5022 


requirements. 

Tritium by method RICH-RC-5007 


requirements. 

I certify that this Certificate of Analysis is in compliance with the SOW, both technically and 

for completeness, for other than the conditions detailed above. Release of the data contained 

in this hard copy data package has been authorized by the Laboratory Manager or a designee, 

as verified by the following signature. 

Reviewed and approved: 

Doug Swenson 

Project Manager 

I) " It

SAMPLE RESULTS 

)Ouanterra 

LAB NAME: QUANTERRA, Richland SDG: /RPT GRP: W02587 / 6871 

LAB SAMPLE ID: 81050601 MATRIX: WATER 

CLIENT ID: BOR495 DATE RECEIVED: 10/27/98 1:30:00 PM 

COUNTING TOTAL REPORT METHOD 

ANALYTE RESULT Q ERROR (2s) ERROR (2s) MDA/IDL UNIT YIELD NUMBER 

CO-58 -1.80E-01 U 5.3E+00 5.3E+00 9.65E+00 pCi/L N/A RICHRC5017 


CS-137 -5.87E-01 U 2.4E+00 2.4E+00 4.15E+00 pCi/L N/A RICHRC5017 

EU-152 1.56E+00 U 6.3E+00 6.3E+00 1,13E+01 pCi/L N/A RICHRC5017 

EU-154 -1.24E+00 U 7.6E+00 7.6E+00 1.41E+01 pCi/L N/A RICHRC5017 

EU-155 2.90E-01 U 6.2E+00 62E+00 1.07E+01 pCi/L N/A RICHRC5017 

FE-59 5.87E+00 U 1.5E+01 1.5E+01 2.92E+01 pCi/L N/A RICHRC5017 

ALPHA 2.18E+00 J 1.4E+00 1.4E+00 1.39E+00 pCi/L 100.00% RICHRC5014 

BETA 9.42E+01 4.8E+00 9,7E+00 2.84E+00 pCi/L 100.00% RICHRC5014-8 

TRITIUM 9.92E+02 1.9E+02 2.6E+02 2.99E+02 pCi/L 8810% RICHRC5007 

Number of Results: 10 

Result = IDL When Not Detected Quanterra Analytical Se rvices, Inc 

(Q)Uahfiers: U = Analyte result < MDA/IDL, rptChemRadSample; v3.41 

J = No U qualifier and result < I., ^ , J


i-manterra 





ANALYTE RESULT Q ERROR(2s) ERROR(2s) MDA/IDL UNIT YIELD NUMBER 

CO-58 1.02E-01 U 3.9E+00 3.9E+00 7.47E+00 pCi/L N/A RICHRC5017 

CO-60 -1.05E+00 U 1.5E+00 1.5E+00 2.55E+00 pCi/L N/A RICHRC5017 

CS-137 4.42E-01 U 1.7E+00 1.7E+00 3 53E+00 pCi/L N/A RICHRC5017 

EU-152 -3.73E-01 U 6.0E+00 6.0E+00 1.07E+01 pCi/L N/A RICHRC5017 

EU-154 1.56E-01 U 5.1 E+00 5.1 E+00 1 08E+01 pCi/L N/A RICHRC5017 

EU-155 -6.66E-01 U 4.1 E+00 4.1 E+00 7.31 E+00 pCi/L N/A RICHRC5017 


ALPHA 2.80E+00 J 1.7E+00 1,8E+00 1.64E+00 pCi/L 100.00% RICHRC5014 

BETA 9.44E+00 1.9E+00 2.1E+00 2.76E+00 pCi/L 100.00% RICHRC5014- 6 

C-14 3.66E+03 4.3E+01 1.8E+02 1.56E+02 pCi/L 100.00% RICHRC5022 

TRITIUM 4.05E+02 1.5E+02 2.2E+02 2.99E+02 pCi/L 88.10% RICHRC5007 



(Q )ualifiers: U = Analyte result < MDA/IDL, 

J = No U qualifier and result < 

rptChem RadSample; v3.41 I. `^ n 

v Q


%%uanterra 



CLIENT ID BOR4C8 DATE RECEIVED: 10/27/98 1:30:00 PM 


ANALYTE RESULT Q ERROR(2s) ERROR(2s) MDAIIDL UNIT YIELD N U MBER 



CS-137 2.30E-01 U 2.2E+00 2.2E+00 4.26E+00 pCi/L N/A RICHRC5017 



EU-155 -1.20E+00 U 3.9E+00 3.9E+00 6.99E+00 pCi/L NlA RICHRC5017 


ALPHA 1.35E+00 U 1.2E+00 1.2E+00 1.62E+00 pCi/L 100.00% RICHRC5014 

BETA 2.13E+01 2.5E+00 3.1E+00 2.77E+00 pCi/L 100.00% RICHRC5014-B 

TRITIUM 6.23E+02 17E+02 2.4E+02 2.99E+02 pCi/L 88.10% RICHRC5007 


Result = IDL When Not Detected Quanterra Analytical Services, Inc 

(Q)ualifiers: U = Analyte result < MDAIIDL, rptChemRadSample; v3.41 r _ ^'•. 

J= No U qualifier and result < C, U v


f uanterra 



CLIENT ID: BOR4D2 DATE RECEIVED: 10/27/98 1.30:00 F'M 



CO-58 -1.10E-01 U 4.1 E+00 4.1 E+00 7.77E+00 pCi/L N/A RICHRC5017 



EU-152 2.03E+00 U 5.7E+00 5.7E+00 1.06E+01 pCi/L N/A RICHRC501- 



FE-59 6.54E+00 U 1.3E+01 13E+01 2.73E+01 pCi/L N/A RICHRC5017 

ALPHA 3.14E+00 1.9E+00 1.9E+00 1.74E+00 pCi/L 100.00% RICHRC5014 

BETA 1.00E+01 2.0E+00 2.2E+00 2.74E+00 pCi/L 100.00% RICHRC5014-B 





(Q)ualifiers: U = Analyte result < MDA/IDL, rptChemRadSample; v3.41 i t- J = No U quallfier and result < 

J


Abanterra 



CLIENT ID BOR4F5 DATE RECEIVED: 10/27198 1:30:00 PM 





CS-137 5.31 E-01 U 1.9E+00 1.9E+00 3.81 E+00 pCi/L N/A RICHRC5017 


EU-154 9.49E-01 U 4.9E+00 4.9E+00 1.08E+01 pCi/L N/A RICHRC5017 


FE-59 -1.60E+01 U 1.4E+01 1.4E+01 2.02E+01 pCi/L N/A RICHRC5017 

ALPHA 4.75E+00 2.6E+00 2.7E+00 2.40E+00 pCi/L 100.00% RICHRC5014 

BETA 8.99E+00 2.0E+00 2.2E+00 3.02E+00 pCi/L 100.00% RICHRC5014-8 




(Q)ualifiers: U = Analyte result < MDA/IDL, rptChemRadSample; v3.41 

J = No U qualifier and result < 

C 0 C, r 

v ^


o%%uanterra 


LAB SAMPLE ID 81050606 MATRIX: WATER 

CLIENT ID: BOR4F6 DATE RECEIVED: 10/27/98 1:30:00 PM 


ANALYTE RESU LT Q ERROR(2s) ERROR(2s) MDA/IDL UNIT YIELD NUMBER 


CO-60 3.94E-01 U 3.0E+00 3.0E+00 5.66E+00 pCi/L N/A RICHRCS017 

CS-137 1.40E+00 U 2.5E+00 2.5E+00 4.85E+00 pCi/L N/A RICHRC5017 

EU-152 6.29E-01 U 6.1 E+00 6.1 E+00 1.08E+01 pCi/L N/A RICHRC5017 

EU-154 1.83E+00 U 7.2E+00 7.2E+00 1.43E+01 pCi/L N/A RICHRC5017 



ALPHA 1.28E+00 U 1.1 E+00 1,1E+00 1.54E+00 pCi/L 100.00 0/, RICHRC5014 

BETA 1.83E+01 2.3E+00 2.8E+00 2.61E+00 pCi/L 100.00 0/, RICHRC5014-B 




(Qlualifiers: U = Analyte result < MDAIIDL, rptChemRadSample; v3.41 I) ^^ 

J = No U qualifier and result


%%%uanterra 



CLIENT ID: BOR41-0 DATE RECEIVED: 10/27/98 1 30:00 PM 


ANALYTE R ES ULT Q ERROR (2s) ERROR (2s) MDA/IDL UNIT YIELD N UMBER 

CO-58 1.17E+00 U 3.9E+00 3.9E+00 7.89E+00 pCi/L N/A RICHRC5017 


CS-137 4.16E-01 U 2.0E+00 2.0E+00 3.97E+00 pCiiL N/A RICHRC5017 





ALPHA -1.12E-01 U 2.2E-01 2.2E-01 9.59E-01 pCi/L 100.00% RICHRC5014 

BETA 1.10E+00 U 1.2E+00 1.2E+00 2.55E+00 pCi/L 100.00% RICHRC5014-8 

TRITIUM 6.01E+03 3.6E+02 6.2E+02 2.99E+02 pCi/L 8810% RICHRC5007 


Result = IDL When Not Detected Quanterra Analytical Se rv ices, Inc 


J = No U qualifier and result < 1 ^.


►1manterra 














BETA 6.51E+01 4.0E+00 6.4E+00 2.68E+00 pCi/L 100.00% RICHRC5014-8 





(Q)ualifers: U = Analyte result < MDA/IDL, rptChemRadSample; v3.41 r 

J = No U qualifier and result


Airanterra 








CS-137 -3.71 E-01 U 2.3E+00 2.3E+00 4.25E+00 pCi/L N/A RICHRC5017 






BETA 1.04E+04 2.9E+02 8.4E+02 7.21 E+01 pCi/L 100.00% RICHRC5014-B 





J = No U qualifier and result < ^^ 1 J


x, imanlerra 

LAB NAME: QUANTERRA, Richland SDG: /RPT GRP: W02587 If 6871 


CLIENT ID: BOR4F8 DATE RECEIVED: 10/28/98 3:05:00 FM 







EU-154 4.79E-01 U 5.3E+00 5.3E+00 1.12E+01 pCi/L N/A RICHRC5017 




BETA 1.11 E+Ol 2.0E+00 2.2E+00 2.74E+00 pCi/L 100.00% RICHRC5014-B 




(Q)ualifiers: U = Analyte result < MDAIIDL, rptChemRadSample; v3.41 0 

J = No U qualifier and result < I, i -) I "t

LAP NAME: 

LAB SAMPLE ID: 

CLIENT ID: 

ORIG LAB SAMPLE ID: 

DUPLICATE RESULTS 

QUANTERRA, Richland 

D1050601 

BOR495 

81050601 

SDG: /RPT GRP: 

MATRIX: 

DATE RECEIVED: 

A,96anterra 

W02587 / 6871 

WATER 

10/27/98 1:30:00 P 

DUP COUNTING TOTAL MDA/ REPORT METHOD ORIG 

ANALYTE RESULT Q ERROR( 2 s) ERROR (2 s) IDL UNIT YIELD NUMBER RESULT RPD 

CO-58 -8.52E-01 U 5.3E+00 5.3E+00 9.79E+00 pCi/L N/A RICHRC5017 -1.80E:-01 130.23% 

CO-60 6.84E-01 U 3.1E+00 3.1E+00 6.17E+00 pCi/L N/A RICHRC5017 -8.42Ei-01 1927.66% 

CS-137 7.24E-01 U 2.3E+00 2.3E+00 4.54E+00 pCi/L N/A RICHRC5017 -5.87E.-01 1915.08% 

EU-152 2.02E+00 J 5.9E+00 5.9E+00 1.11 E+01 pCi/L N/A RICHRC5017 1.56E+00 25.80% 

EU-154 4.62E+00 J 8.7E+00 8.7E+00 1.82E+01 pCi/L N/A RICHRC5017 -1.24E+00 347.23% 

EU-155 2.21E+00 U 4.7E+00 4.7E+00 9.10E+00 pCi/L N/A RICHRC5017 2.90E-01 153.61% 

FE-59 -3.49E-01 U 1.5E+01 1.5E+01 2.83E+01 pCi/L N/A RICHRC5017 5.87E+00 225.30% 

ALPHA 1.67E+00 IJ 1.3E+00 1.3E+00 1.98E+00 pCi/L 100.00% RICHRC5014 2.18E+00 26.13% 

TRITIUM 9.73E+02 1.8E+02 2.6E+02 2.99E+02 pCi/L 88.10% RICHRC5007 9.92E+02 1.94% 


Result = IDL When Not Detecte Quanterra Analyticall services, Inc 

(Q)ualifiers: U = Analyte result < MDAML, 

rptChemRadDup; v3.41 

J = No U qualifier and result < RDL. I- L-) ^- J


%%%uanterra 


LAB SAMPLE ID: D1050602 MATRIX: WATER 

CLIENT ID: BOR495 DATE RECEIVED: 10/27/98 1:30:00 P 

ORIG LAB SAMPLE ID: 81050602 

DUP COUNTING TOTAL MDA/ REPORT METHOD ORIG 

ANALYTE RESULT Q ERROR( 2 s) ERROR (2 S) IDL UNIT YIELD NUMBER RESULT RPD 

BETA 1.16E+01 2.1 E+00 2.3E+00 2.75E+00 PCi/L 100.00% RICHRC5014-B 9.44E+00 20.38% 

TRITIUM 4.43E+02 1.5E+02 2.2E+02 2.99E+02 PCi/L 88.10% RICHRC5007 4.05E+02 9.01 3„ 


Result = IDL When Not Detects Quanterra Analytical) Se rvices, Inc 

(Q)ualiflers: U = Analyte result < MDAIIDL, 

J = No U qualifier and result < RDL. 

rptChemRadOup; v3.41 

l^ 1 U


0h%luanterra 

LAB NAME: QUANTERRA, Richland SDG: IRPT GRP: W02587 / 6871 

LAB SAMPLE ID: D1053301 MATRIX: WATER 

CLIENT ID: BOR492 DATE RECEIVED: 10/28/98 3:05:00 P 

ORIG LAB SAMPLE ID 81053301 

OUP COUNTING TOTAL MDAI REPORT METHOD ORIG 

ANALYTE RESULT Q ERROR( 2 s) ERROR (2 s) IDL UNIT YIELD NUMBER RESULT RPD 

C-14 3.92E+03 1.5E+02 2.7E+02 1.56E+02 pCi/L 100.00% RICHRC5022 4.53E+03 14.37% 


Result = IDL When Not Detecte Quanterra Analyticall Services, Inc 

(Q)ualifiers: U = Analyte result < MDAIIDL, 

rptChernRadDup; v3.41 

q _ 

r 

J - No U qualifier and result < RDL i_ I 1

BLANK RESULTS 

%'%uanterra 

LAB NAME: QUANTERRA, Richland SDG /RPT GRP: W02587 / 6871 

LAB SAMPLE ID: J105061 MATRIX: WATER 





CS-137 1.55E+00 U 2.0E+00 2.0E+00 4.19E+00 pCi/L N/A RICHRC5017 





ALPHA 1.17E-01 U 3.1E-01 3.1E-01 7.58E-01 pCllL 100.00% RICHIRC5014 

BETA 6.95E-01 U 1.2E+00 1.3E+00 2.67E+00 pCi/L 100.00% RICHRC5014-6 



(Q)ualifiers: U = Analyte result < MDA/IDL, rptChemRadBlank; v3.41 

J = No U qualifier and result < RDL r S

BLANK RESULTS 

%%%uanterra 


LAB SAMPLE ID: J105061X MATRIX: WATER 



TRITIUM 8.59E+01 U 1.3E+02 2.0E+02 2.99E+02 pCi/L 88.10% RICHRC5007 



(Q)ualiflers: U = Analyte result < MDA/IDL, rptChemRadBlank; v3.41 

J = No U qualifier and result < RDL 

L (^ J

BLANK RESULTS 

%%%uanterra 


LAB SAMPLE ID: J105331X MATRIX: WATER 



C-14 2.66E+00 U 3.4E+00 5.2E+00 1.56E+02 pCi/L 100.00% RICHRC5022 


Result = IDL When Not Detected Quanterra Analytical Se rv ices, Inc 

(Q )ualifiers: U = Analyte result < MDA/IDL, rptChem RadBlank; v3.41 

J = No U quali fier and result < RDL 

t J L^ i^

LABORATORY CONTROL SAMPLE 

%%%uanferra 


LAB SAMPLE ID: J105061M MATRIX: WATER 

COUNTING TOTAL MDA/ REPORT 

ANALYTE RESULT Q ERROR(2s) ERROR(2s) IDL UNIT YIELD EXPECTED RECOVERY 

TRITIUM 2.87E+03 2.6E+02 3.9E+02 2.99E+02 pCi/L 88.10% 2.72E+0:3 105.52% 


Result = IDL When Not Detecte Quanterra Analytical Services, Inc 

(Q)ualifers: U = Analyte result < MDAIIDL, rptChernRadLcs; v3.41 l., 0 .:. 1 

J - No U qualifier and result < RDL.


VP anterra 


LAB SAMPLE ID: J105061S MATRIX: WATER 

COUNTING TOTAL MDA/ REPORT 

ANALYTE RESULT Q ERROR (2 s) ERROR(2s) IDL UNIT YIELD EXPECTED RECOVERY 

CO-60 4.25E+01 8.5E+00 8.5E+00 4.37E+00 pCi/L N/A 3.84E+01 110.65% 

CS-137 2.84E+01 7.3E+00 7.3E+00 5.21E+00 pCi/L N/A 2.50E+01 113.63% 

EU-152 7.73E+01 1.6E+01 1.6E+01 1.20E+01 pCi/L N/A 7.66E+01 100.82% 

ALPHA 1.95E+01 2.9E+00 3.5E+00 8.39E-01 pCi/L 100.00% 2.26E+01 86.084/o 

BETA 2.30E+01 2.5E+00 3.2E+00 2.61 E+00 pCi/L 100.00% 2.27E+0'1 101.30% 

TRITIUM 2.91E+03 2.6E+02 4.0E+02 2.99E+02 pCi/L 88.10% 2.72E+03 107.16% 


Result = IDL When Not Detects Quanterra Analytical Services, Inc 

Qlualiflers: U = Anal a result < MDAIIDL, 

YtrptChemRadLcs; v3.41 

J = No U qualifier and result < RDL.


C19banterra 

LAJ NAME: QUANTERRA, Richland SDG: IRPT GRP: W02587 / 6871 

LAB SAMPLE ID: J105331S MATRIX: WATER 

COUNTING TOTAL MDAI REPORT 

ANALYTE RESULT Q ERROR(2s) ERROR(2s) IDL UNIT YIELD EXPECTED RECOVERY 

C-14 1.74E+03 1.8E+02 2.7E+02 1.56E+02 pCi/L 100.00% 1.82E+03 96.03% 


Result = IDL When Not Detects Quanterra Analytical Se rvices, Inc 

(Q)ualifiers: U = Analyte result < MDA/IDL, rptChemRad l-cs; v3.41(^ (1; 

J = No U qualifier and result < RDL. `'

`watt Creer,u fsi: `6'IC SCCo ^S'IC 53 

Clan ro: Q R --z— 

Oue Cate i a - a s -^t $ 

Lab Satttnte vumcc a SDO: LA_' q 

Medwd ôn ?aametax C 4 nA m C`- 

Maestz G'}P 

A. cslbrustm. 

1. 4 the olihrmm doomtanum waded w aopiable7 

a Semple Aae/yeie 

1. Am ft ra=mie + " -,ttan ammta.0a etnmia? 

Qaa►sars Data Racvinv C 

RIDIOCI E OSI'RY 

aeweer iu= I Yes (J) (Ne(J} I tilA(J) 

I I I 

I I 

I 

Were ali sample mwiag teas ma? I I I i 

7. [a We s=am=e Nittitmsm Caeaaoie Am

Project ID: 

Sample Numbers: 

Tests: 

Matrix: 

QUANTERRA LABORATORY NONCONFORMANCE MEMO (NCB 

PACE 1 OF 2 

LAG M: 9 ^CJ S 

6 S 

NCM Initiated by: 

Analvticai Area (check aooroo riate area ) : 

• Sample control q GC q Wet chemist ryO Data review 

• Organic prepara ti on q HPLC Cl Metals PQadioclermstry 

• Inorganic prepara ti on q GCIMS q Repor ting q Bioassay 

Nonconformance (check anorooriate area): 

Holding 17rne Violations (exceeded by days) Quality Assurance/Quality Control 

Category l Laboratory Independent O 17. QC data repo rted outside of controls 

O 1. Holding time expired in transit q 18. Incorre ct procedure used 

q 2. Sample received > 48 hrs. or 112 holding time has q 19. SOP inten tiona lly modified with QA and Tech. approval 

expired 

q 3. Test added by c lient after expiration O 20. Invalid instrument calibra tion 

Categoryll. Laboratory Dependent O 21. Insufficient sample received for proper analysis 

q 4. Instrument failure 

5. Analyst er ror 

01? 

Incorrect or Incomplete Client Deliverable 

q 22. Hardcopy deliverable error 

Cl 6. Login error O 23. Electronic de liverable error 

q 7. Miscommunication 

Reported detecdon limits elevated due to: 

q 8. Other (complete descrip tion required) O 24. Sample matrix 

Category III: Analysis Reruns (QA/QC) O 25. Insufficient sample volume 

q 9. Surrogates O 26. Other (complete description required) 

O 10. I nt ernal Standards 

O 11. Spike Recoveries 

O 12. Blank Contamination 

Category IV. Analysis Reruns (Confirmation) 

q 13. Second column 

O 14. Contamination check 

q 15. Confirmation of matrix effects 

O 16. Other (complete description required) 

No tification (check aooroo riate area ) : 

O 27. Other (specify): 

Comments/E: lanation: 

Cliff notified by (name and date): C lient's name and response: 

q in writing C i,J q by facsimile q process "as is" O re-sample 

^ f 

Y,740 

O by telephone q other (explain) O on hold until q other (explain) 

Project Manager (signature and date): / O 49

Corrective Action 

Roan Caxre 

C ^^^^(y^^,^7( A 

IFcGlri r 

^ 

tom= 

RC PUV4 DCL 

QUANTERRA LABORATORY NONCONFORMANCE MEMO (NCM) 

PALS 2 or 2 

ca ^ 

v^ `' 

WA ^V I z I' 

Responsibi lity for performing CA assigned to: 

S 

V1,/ 

Actions to prevent recurrence 

C^Q^- +IN\-a_ 00- Lr.?_ I 

First Level Supervisor. 

Responsible Manager: 

Ouality Assurance Review 

• Anomaly 

• Further ac tion required: 

Assigned to 

r Q 

_Xc 

Initial and 

Initial and Date: 

Initial and Date: - 

LOG#: RD-99- 

Date: 

Date: 

4 'r ^'Y 

Deficiency q Rerun 

QA signattue. Date:; 

Corrective Action Ve rification 

Verified 

q Cannot Verify (specify reason): 

N nconform ce Mem Closure 

QA signature) [e: 

=k^ 

j 4 rl; 

A/^ 

14

4,t ci .^^tee2 

Q=mwm D ram Review Ckddiu 

RADIOCEM S Y 

went Ceete-uattpQrac ^s'16 50 '^_ 10 57 3 3 

Ciea fn: BNz_ cl-o06 

} 

Oue Date: 1 ^- - a s - s `p ' 7 c! 

Lzb Satsmle vu,n,er,r SDG: 

Mcdmd Tea?y ? ( h 

Waamc tj,i 4 

^w ^ a 5 a '7 

( —^ 

davtew item I Yee( ) (No (.!) ( mA(.o 

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c aw 

1.la the Weak vidd twlhin mtene i I 1 1Î 

L gym. dtmD..^h^ ^=r,e, ^Q ê1^5^.en 

L:tmt7 I x I I l ^. 

7. la we eWc newt < IA u o C.>^Ca -%"m Limu7 I "^ 

a. [a the clan,, > 11-:ho CseQaa 1,1- o I.i= to < Caeraa Deacons Lit=? 

^. Ls dIC Manx .'L9ali> Itz L:nnt'aa Oanxm L J= hm du soapte maid

Wcnc Ordarmer fdh 

Diem In! ^• 

D" Dalian. t 2 a $ - ^7 

Lab samele Vmnbe• or SDC: t a 5 S 

Meddod Ten?anm . Z 

Nauss I c'ê. 

A. 

Qnamma Dua RCACW QseddLst 

RADIOCSFIrr, OTMY 

iieetew Um I Ye(J) I 'l°(J) Â(J) 

Is the ddm m dammaaadm Neh:dd rhea=puoMd I I I 

_ 

I Ra+iatetJl 

^ I / 

1. . Am the s mulsr ds mboa aec000moi camas I I I 

^/ 

,V I /. 

Wem all sale holding torte tne7 I ( I ^^ 

-- 

7. 4 the ammle Metitmm Detamols Amv 

C QC Sample 

L Is tJt. dlanlc ,"W tvhhin aecmrsto atteta 

WmCaeaa Deama lim>^ I A I 

` 

I 

I 

1^ 

f 

^ 

^' 

Is t)m to;.:..,,.^ Detmole Aatvtry Corte hiaanetaa 5 t• Caeaes Deem 

Litmt7 

7. G UW olatu'. ;mtt < Ir me C^ .^.a®m Law? 

a, Is to diem( > it the C. DCCCian LSch de < r^ OdUsummi [i®t7 

!. v to dlanit ttRLt > dfe catraG 'Jaeam i :^.. dm to mtspte natty

I 

Work C+dn,umacrsL' (J^^ 3 

clan :n 

Due Due. 

L.Lb Samote Number or SDO: 

Method Tet Parmmeax 

Mm= 

A. Ca0radea 

1. Is the d'bewW dttamemavW itdudad wtas aeglicbl.t 

1; Saple laelpb 

1. Are the amends vidda vrtddp ara:mram anatm? 

Z. Wee all sample holding tame ma? 

Qaamun Data Review Checklist 

RADIOCEM USTRY 

Ramtm It® I Yea (1) I No (1) NIA(1) I V LAM 

Ravier/Jl 

I 1 I / 

7. Is the sample Miaiontm Dascabla A asvny < ftC.aaaa 00,0M l,imQ I I I I _.I 

c— QCsamm*cm 

1. Is the block vidd .7dun sozmam moms 

Z IS the Minimum Daeaahla .la Vny fW%U almo st m-, S the Clashes Daeoium 

LIMA? 

7. Is the bloat thud < Ir :!u C.atraa Daem on lot? 

a, fa the olamc > V: Uu Cu Deumm La but < Cavan Daaam Lao? 

J. is the biotic ,sett > the c m Daeeton Lad boa the saanle teaad < the Coevaes 

Deeaean L=t? 

I 1 

J I I I ^.. 

6. Is Ne i.CS fault wksm •^--- mtmat I ,^ I I ^ ^ I 

T. Is the LCS Ln bid •.vuhm arrernanta anau I I ( `^ % 

S. G the LCS Minunum Deter sble Amvtty 5 the Camas Daecom iat? .^ 

9. MS/MSD tauln and vteid meet •^'^•rt•- anaat 

1 0. Duplin sampteressla.tna"eid:eceet •--•^^•— anma7 t% 

D. Other 

I. Are all Nonmetiomunm utcluded aetd nmed7 

2 Are all requued fa tten til ed out? 

1. Curtct methodology used? 

a. Trutsmpuon cyntxed7 

I ^ ^ I I 

MT 

]. Were all nlmlauaen ch=td u a WmtmW tmleatcv? I ,j 

6. Umu Contemn? I I I I l 

Commen ts an any -No' response: 

First Lore! R=nv- i^l.^ll f C ^ ^ GG^ Î^CC CGE L C- Date: `t 

Seond Lzvei Date: 

Farm d- LS-738,. /96. Rev.4 

1 Y 91 

^^ 

î

clew 1D• 

Qumwr a Data Review CBeckditt 

RADIOCHE1rIISTRY 

Due Date - 

(sb Santale ^lumtter ar SIJG: 

Mcdwd Ten ?sremeters 

Mat a: 

,L CiYbreCan 

^-^'-+ 

1. s the oltltruian doaunaaaaon in cluded where equable? 

IL Seeswle Analysis 

I. Ate the samois yields wrdsm accounta nt anarm? 

L Were all saemle holding tma me7 

Bone[. It® I Yea(.!) I No (1) I CUA(1) 

_ 

I r,LAVI/ll 

( I I I / 

I ` 

I / 

7. s the saamtt 4f -nntm Daecaoie Aeavny < the Caerae Deemm LimW I X I I I ^" 

c QC Seaapls 

t. s the black ^dd within esamtafo crit eria 

L s the Stimtnum Dceteaale A=MTy fartht blot[ tsma S the Cato: Detect, 

7. Ls uta olatu[ :tun < I,_ to C_- Dexetm Land? / 

i 

4. s No alai > I r' an C^ '.?ersam Lou bm < Caaaa 0e eam LiaW 

I 

i 

3. Is the Mani::cwt > dte C Zane 2x 

D-o-ion (:mst7 

m L bm tta samWe rzmd < the Carman I I \/ 

^7 

6. Ls the LCS mutt •xnh= tCC.ast¢ e:sena7 I 

'. s the L= ;nad •+vthin ,—__.._ rya / ,( 

S. is the L= Minunum Ca Ic A=a 5 Lhe Camae Daacam Lamm? X 

9. M&MSD =ulta ant yteid am aass`weaz -•tau7 I " 

IO. Dugiiete3ttmte n=ulna ant .arid ^:x •^------^t7 X 

D. Other 

I A— .11 _....o I I I X 

L Am ail reautrud foam tiled oua' 

J. Csreasahocoiogy wsm7 

i. Ttaaserivuon the 7 

S. Wrv7 l t I ^/ 

4 

I 

p 6. Lima atec mc7 

Commcnts on any -No natant: 

Fiat Lzrei Raitrv- Date _ I 147-2 

Send Lc:e: Rc.•tov 

Daze / y 79 

Form' LS-733.5 i95, 3c: 

z 

/

CHAIN OF 

CUSTODY FORMS 

roo0

PNNI, 

CollectorR UREWINGTON (RFS) 

- 


C.O.C. IJ 

onlact/Reoueslar Teleplione No. MSIN FAX 

'AF No. 

(1994" 

amoline Origin 

"ANFORnSITF 

Purclialse Order/Cbarae Code 

Prolect Title Loubook No. Ice Chest No. _ 

s sC 7 

Temm. 

Shinned To (Lab) Method of Sblomenl Bill of Ladino/Air Bill No. 

Proto co l Data Turnaround Offille Properly No. 

POSSIBLE SAMPLE HAZARDS/REMARKS i 

^/ 

f_ A 

=FP 

INSTRUCTIONSHo ld Thoe TrialActivityExemp tion: 

ES OF QBS @ TMA LOG-INTO DL STEW ANT ( 371-1704) A JM DUNCAN ( 372-9052). 

C99-006-1 

Page 1 of 1 

Yes No 

Semple No. Lab ID • Date Tim Noaype Container Sample Analysis Preservative 

BOR491 (F) W /6, _,< 

r 1 x500-m l- G(P ICP Metals - 601 OA RCRA G IN ) - ` .-r HNO3 to pH

PNNI, 

Collector 

Ft. gREWINOTON (RFS) 


'ontact/Reouesler 

]it 

'AF No. Samplinz Oriein 

C.O.C.# 

Telephone No. MSIN PAX 


C99-006-7 

Page L of 1 

Prolect Title Losibook No. 

i 1l- s •^< - ^^ 

Ice Chest No. 

f/nL 3G'^ 

Temp. - 

r 

Tipped To (Lab) Method of Shipment Bill of LadlpdAir Bill No. 

Protocol Data Turnaround Offafte Proneriv No. 

IBLE SAMPLE HAZARDS/REMARKS SPECIAL INSTRUCTIONS Hold Time Total Activity Exemption: Yes L9 No 

FAX COPIES OF QFS & TMA LOG-IN TO DL STEW ART (372-1704) & IM DUNCAN (372-9052). 

Sample No. LAb ID • Date Time Norl ype Container Sample Analysis Preservative 

BOR4B1 (F) W 1 x500-mL GIP ICP Metals - 6010A RCRA GW^ n ) HNO3 to pH Q 

BOR4B2 W 1x500-mL G/P ICP Metals - 6010A RCRA GW p / 

HNO3 to pH

PNNL 

' llector 


D R RREWINGTON (RFS) 

III 

tact/Reauester 

eleohone No. MSIN FAX 

'AF No. Semolina Origin Purchase Order/Charge Code 

rolect TIBe Lelzbook No. Ice Chest No. Temp. 

Shinned To (Lab) Method of Shlomm nt Bill of Ladino/Air Bill No. 

Protocol ala Turna ro 

und Rslle Property No. 

POSSIBLE SAMPLE HALARDS/REMARKS 

" 

SPECIAL INSTRUCTIONS Hold Time Total Activitv Exemotion: 

FAX COPIES OF QES & TMA LOG-IN TO Dl. STEWART (372-1700 & IM DUNCAN (372-9052). 

C99-006-65 I 

Page 1 of 1 

Yes 0 No 

Sample No. Lab ID • Date Tint Nol1'ype Container Sample Analysis Preservative 

BOR4F7 (F) W Ix500-mL G Mercury - 7470 (CV) / I 

HNO3 to pH

Figure 1 


DateMme Received: ^l^^^d ^^ SG#: `C.En/^-279 1 

Work Order Number: ^^Qr^2 -7; SAF # C 1/f-0^ 


Revision 5 

Shipping Container D ^/^ ^(^ Chain of Custody # 0161-Cr.Yo" 

QP-e lDf2^ 

1. Custody Seals on shipping container intact? Yes LI-No [ ] 

2. Custody Seals dated and signed? Yes [^ I 

3. Chain-cf-Custody record present? e Yes [Lyo I] 


5. Vermiculite/packing mate rials is Wet [ ] D ry 

6. Number of samples in shipping container: J 

7. Sample holding times exceeded? Yes [ ] No [ r 

S. Samples have: 

l tape h azard labels 

ê0stody seals appropriate sample labels 

9. Samples-are: 

good condition leaking 


10. Where any anomalies identified in sample receipt? Yes [] No [ ]C 

11. Desc ription of anomalies (include sample numbers): 

Sample Custcdian/Laborato ry : ^- 

Telephoned To: .On 

34 

( OJ'

Figure 1 


DatvTime Received: /^^fy^ Î SG#: ^^J 2S^/ 

Work Order Number: 91 92 7L 3 SAF #: 

RFS H-SOW-93 -0003 

Revision 5 

Shipping Container I ^LS Chain of Custody #` ^^"LAS _ 

1. Custody Seals on shipping container intact? Yes/^Nc [ ] 

2. Custody Seals dated and signed? 

Yes U. 140 [ j 

3. Chain-cf-Custody record present? 

// 

L/ Yes (^ ( ] 


5. Vermiculite/packing mate ri als is Wet [ ] D ry [ ]i 

6. Number of samples in shipping container. 

7. Sample holding times exceeded? Yes [ ] iNc [L= 


gape hazard labels 

stody seals 

— Û 



-^ in good condition leaking 


10. Where any anomalies identified in sample receipt? Yes (] No I^ 


Sample Custodian/Laborato ry : eDate: 

Telephcned To:_ On By 

34 

I 

CU35

0 

W 

C) 

CLIENT C ODE ID NL\TRIK RECEI VED DETECTOR ACQ DA7 E SAMPLE MINUTES CNTS A NET CPNI A CNTS B NET CPNI B 

POW BOROP4 10 1 28/98 10.15M PM QUAD22D 10/3 1/98 9:34:16 ANI BOROP4 30 4 0.03904762 70 1.0819048 

LIQUID Bkg; 103 1/98 5:53:37 AM BKG 700 66 0.09428571 876 1.2514286 

AN Dale: 10/31/98 Tot Sa, Alq: 1.00E+00 1.00E+01 Alp; (Dpm/ 8.27E-0 2 (uCU 3.73E-06 (pCU 3.73E+00 ± 2.3E+01 CAT 6. 7E+00 Lab 

Ppl mg: 3.2 / Units: L ^, ml Bel; Alq): 2.02E+00 So): 9.10E-05 1.Ig): 9.10E+01 + 2.4E+01 I ^ 5.5E-01 

Alq 

POW BORIN 13 10/28/9812.54: 00 PM QUAD22B 10/31/9810:1125AN1 BORIN1 3 30 4 0.03476190 45 0.0471429 

LIQUID Bkg: 10/31/98 5:53:37 ANI BKO 700 69 0.09857143 1017 1.4528571 

AnI Date: 10/31/98 "Lot Sa,Alq: 2.00E+00 1.00E+01 Alp; (Dpm/ 1.03E-01 (uCU 9.30E-06 (pCU 4.65E+00 +2.4E+01 CAT 5.4E+00 Lab 

Ppt mg: 0 Unlit: L /, n il Bet; Al it ): 6.79E-02 So): 6.12E-06 Llg): 3.06E+00 + 2.0E+0I I i 1.6E+01 Alq 

POW BORINI8 1028/9812.54:00 PNI QUAD22C 10/31/9810: I1: 25 AM BORI NIB 30 9 0.21428571 52 0.6461905 

LIQUID Bkg: 1031/985- 53:37 ANI BKG 700 60 0.08571429 761 1.0871429 

Anl Dale 10'31/98 Tot Sa„Uq: 300E-00 IOOF'01 Alp; (UpnU 6.41F-01 (uCU 8.66[-05 (p( V 2.89E+01 +2.3E+01 CAT 8.7F.-01 Lab 

Ppl mg: 7.7 / Units: 1, /, n il 110;Alq) : 1.08E+00 So): 1461:04 LIg): 4.88E+01 + 2.0E+0I 

1 

^11 .0E+00 

9 

LIg 

POW BOR3K9 1027 198 1:30.00 Pit QI3AD22D 10/31 198 10:1125 AM BOR3K9 30 4 0.03904762 43 0.1819048 

LIQUID Bkg: 1031 %98 5:53:37 AM 13KG 700 66 009428 5 71 876 1.2514286 

,W Dale: 10/31/98 Tot Sa,Alq: 4.00F+00 IOOE+01 Alp; (DpnJ I.13E-01 (uCU 2.04E-05 (pCU 5.11E+00 +2.3E+01 CAT 4.9E+00 Lab 

Ppt mg: 21 1 Units: 1., 

e-^ ml Her; Alq): 3.20E-01 So): 5.76E-05 LIg): 144E+01 +1.9E+01 I -3.5E100 lJq 

PGW BOR31.3 1027199130:001'NI QUAD23C 10/31/9810: 11:33 AM DORM 30 3 802714286 60 0-8857143 

LIQUID Bkg: 1013 1/98 5:53 . 44 AM BKG 700 51 0.07285714 780 1.1142857 

.Anl Date: 10 3 1 9 8 Tot So, Alq: 5.00E+00 I.00F+01 Alp; (DpnJ 5.64E-02 (uCU 127E-OS (p( I/ 2.54E+00 + 2AE+01 CAT 9-8E+00 Lab 

1 Alq 

1'pl mg: 19 llnite: L nil Beq Alq): I.70EfOO So): 3.841:04 I.Ig): 7.68E+01 +23E+01 6.51101 

^ 1•I[ 

PGW BOR492 102898 12:54.00 Phi QUAD23 1) 10/31/98 10:11 33 AM BOR492 30 29 0.90666667 495 15.525714 

LIQUID Bkg: 10'11,99 5 1144 ANI BKG 700 42 006 682 0.9742857 

AnIDate: 10 , 3 199 T'ot So, Alq: 7.00L,00 IOOE,01 Alp; (Dpm/ 237F 4 00 (uCU 7.46E"04 (p(I/ 1.07E+02 +27E+01 CAT 23E-0 1 Lab 

Pplmg: 2.2 / Units: I nil Bel; Alq): 2.916:01 So): 9181:01 Llg): I IIF-03 +63F+01 1 

Alq 

3.8E-02 

I •le 

PGW BOR495 1027'98 2:09.00 Phi QUAD24A 1031/98 10:11'.28 ANI BOR495 30 5 0.07952381 70 1.1833333 

IrQulf) Bkg: 1031/985: 53: 25 AM BKG 700 6! 0 087!4286 805 ,5 

An) Dale-. 10 , 3 1 198 1 o So, Alq: 600E+00 I.00E+01 Alp; (Dpm/ 2 14E-01 ("Cl/ 5.7811-05 (p( 'U 9.63E+00 + 2.3E+01 CAT --"2.6E +00 Lab 

Ppt mg: 1.2 Anita: 1. / ml Bet; Alq): 226E+00 So): 6.IOE 04 Idg): 1.02E+02 + 2.5E+0I 1 4.9E-01 

Alit lg 

3 1 -0cl- 98 Quanterra Em ironment Services, SCP V2. 03 2

7 

G 

^.J 

Ê 

CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQDATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCP6IB 

PGW BOR4B0 10 27/982:09:001'M Q(b11)24D IO111/98 10:1 1,28 AM BOR4 130 30 26 0.79380952 496 14.93 

LIQUID Bkg: 1013 1/98 5-..53:25 Ap l BKG 700 51 0.07285714 889 1.27 

Anl Date 10/3 1/98 Tot Sa, Alq: 7.00E+00 1.00E+01 Alp; (Dpnd 1.94E+00 (uCU 6.12E-04 (PC[/ 8.74E+01 ± 2.9E+ 01 CAT 2.9E-0 1 Lab 

p ill mg: 3.4 links: 1, all Bet; AIq): 84E40 2 Sa): 8.97E-03 Lig): 1.28E+03 + 6.3E+01 I ' 3.9E-02 AN 

IL 

PGW BOR4B2 

(()^, 

10/28/9812:54:00 PAI QUAD2 1 C 10/31/981110:09 AM BOR4B2 30 31 0.94619048 2607 85.932857 

LIQUID Bkg: 10/31/98 5:53:29 AM BKG 700 61 0.08714286 677 0.9671429 

.W Date: 10/31/98 Tot Sa, Alq: 6.00E+00 I.00 F+01 Alp; (D ion/ 1.47E-01 (uC I16.69E-05 (pCV LlIE+01 ±2AE+01 CAT 2.2E+00 Lab 

Ppl mg: 3.6 / Unib: 1, all Bet; AI 1,69E+02 Sa : 4.57E-02 

9): ) L I1/: 

7.62E+03 ± 1,5E+02 I ^ 6.6E-03 Alq 

LIg 

PUW 110R4C8 10/27M 2.09,00 PAI Q(1AD22A 10/ 31/9811. 1O 16 AN] BOR4C8 30 5 008095238 43 02161905 

LIQUID Bkg: 10'W98 5:53 77 AM BKG 700 60 0.08571429 852 1.2171429 

AM Date: 10'31/98 Tot Sa,Alq: 6.00F+00 LOOF'01 Alp; (D ian/ 2.33E-01 (uCU 6.30E-05 (P ( V 1,05E+01 +2.2E+01 CAT 24E+00 Lab 

Pill mg: 2 5 / IInIh: L / ml Bel; ,1/y): 3 55E-131Sa): 9.611,-05 LIg): 1,60E+01 + 1.9E+01 

I 

3.1E+00 

A Alq 

Llq ig 

PGW BOR4D2 10'271982: 09: 00 PKI QUAD22 13 10'31/9811:10:16.-1/I BMW 30 79 2.53476190 1944 60.01381 

AM Dale: 10131 198 

P Pt m C: 5 

I Rkg: 1091/98 5 51 17 A p t BKG 700 69 0.09857143 1017 1452857i 

Tot Sa, Alq: 7.00E+00 

Units: L 

1.00E'01 

all 

Alp; (Dpnd 6.37E+00 (uCU 2.01E-03 

Bet; Alq): 113E+1/2 Sa): 3.38E-02 

(pCU 2.87E+02 +4.IE E+01 

LIg): 3.11E+03 ± 1,2E+02 

CAT 8.7E -0 2 Lab 

1 AI 

9.8E -0 3 

14S 

PGW B0 11 4 1` 5 10/27/98 2:00:00 P pl QUAD2 1 C 1031/98 8:56:56 A p l 130 114 1`5 30 3 0.01285714 58 0.9661905 

AM Dale: 10/31/9R 

P l m 5.8 

P 8^ ^ 

LIQUID Bkg: 1001/985: 53: 29 AM BKG 700 61 0.08714186 677 0.9671429 

ToISa, AIq: 6.00E+00 

units: I. / , 

IOOF+01 

m1 

Alp; (Dpnd 983E-03 (uCU 2.66606 

Bet; M 1 91 F+00 Sa : 3 15604 

Alq): ) 

(pCU 443E-0 1 +2.IE+01 

Lig): B 8.59E+01 + 2.3F+01 

CAT 56E01 Lab 

I 

5 RE-01 

Alq 

LIL 

PGW BOR4F6 10/27/98200: 00 P p 1 QUAD22A 10/31/98856:59A,51 BOR4 1`6 30 3 0.01428571 53 05495238 

IIQIID Bkg: 10'31/985.53.37;"1 BKG 700 60 0.08571429 852 1.2171429 

AM Date: 1031/98 TotS., Alq: 6.00E r 00 1 00L10 Alp; (Dpnd 263602 (uCk 7.12E -06 (P(1/ 1.19E+00 +2.IE+01 CAT 21E+01 Lab 

P r. tmg: 21 Units; I. ml BM Alq): 1.02F,'00 Sal: 275F-04 I.^g): 459E+01 +2.I F, 01 

- 

I 

-^ 

1.1E+00 

Alq 

Ng 

PGW B9R4 1 8 ^ 10/27/98200: 00 PM QUAD22B 10 : 31/98856: 59 Ap t BOR4 1`8 30 5 0.06809524 50 02138095 

J41)GO IIQIID Bkg: 1011/985: 5117 A8t 13AG 7u0 69 0098`.7.43 M" i452857i 

Anl Date: 1091/98 Tot Sa, Alq: 6.00E+O0 I 00 F+01 Alp; (Dpnd 1.05E-01 (uCU 5.54605 (pCV 9.23E+00 + 2.5E+01 CAT 2.7E+00 Lab 

p ill P mG 2.1 ^ 

Units: L / ml Bet; AI9) 3.66601 Sa ) : 9.9UF: 05 L Ugh 1.65E+01 + 2.1 F,+01 I /3.OE +00 

Ûq 

Lig 

? 1-0, 9t QDanterra Environment Scnices, SCP V2.03 3

W 

00 

PNNI, 


Collector R 13REWINGTO N (RFS) ontact/Repuester Telephone No. MSIN FAR 

-951% 

_ISM%372 

'AF No. Sampling Origin Purchase Order/Charee Code 

10.C.N 

C99-006-3 

Page j of I 

Prolect Title Logbook No . Ice Chest No. Temp. { 

'hipped To (Lab) Method of Shipment Bill of Lading/Air Bill No. 

Protocol Data Turnaround Offshtc Property No. 

POSSIBLE SAMPLE: HAZARDS/REMARKS SPECIAL INSTRUCTIONS H eld Time Total Activity Exemption: Yes No U 

FAX COPIES OF QES & TMA LAG-IN TO DL STEWART (372-1704) & )M DUNCAN (372-90il). 

Sample No lab ID • Date Time NwType Container Semple Analysis P rese rvative 

1 x500-mL G/P ICP Metals - 6010A RCRA GW I o 

BOR494 (F) W ^3.' jam' 

X, % ^— 

l V. 

BOR495 W 1x500-m l_ GP ICP Metals - 601 OA RCRA GW ^^'` 

5 / , 5b HNO3 to pH

PNNI, 


'olleclo9 R . BREWINGTON (RFS) ContactMeauester Telephone No. MSIN FAR 

SAN No. Semolina Odeln Puirchase Order/Churee Code 

Proiecl 1111e 

Losibook No. 

Ice Chest No. Tema 

Inn-KR4(1 

i-5'- N/ 

i / 2- •_^ C `^ 

'hipp ed To (Lab) Method of Shipment Bill of Ledina/Air Bill No. 

Protocol eta Turnaround Offaite Property No. 

C.O.C.# 

C99-006-6 

Page 1 of 1 

POSSIBLE SAMPLE HAZARDS/REMARKS PECIAL INSTROCPIONS H old Time Total Activit y ExemMion Yes Lj N., L 

FA% COPIES OF QES & TMA I.OG IN TO DL S7l EW ART (372-1704) & 1M DUNCAN (372-9052). 

Sample No. Lab ID Date Time No/Type Container Sample Analysis Presc rvtaive 

BOR499 (F) W 1X500-ML GIP ICP Metals - 6010A RCRA GW J / -- HNO3 to pH

U 

PNN 1, 


Collector onlact/Reuaes/er Telephone No. MSIN FAX 

'AF No. Sannollne Ordain Purchase Order/Char¢e Code 

Prolecl Title Logbook No. yin ,^.•% N/s , ce Chest No. Tema. 

.5 -.4 43/ 4 r 

hiotKd To (Lab) Method of ShionteLL Bill of Ladina/Alr Bill No. 

otocol as Turnaround be Progeny No. 

POSSIBLE SAMPLE HAZARDS/REMARKS SPECIAL INSTRUCTIONS Hold Time Total Ac ti vity Eaemodon: 

FAX COPIES OF QES R TMA LAG-IN TO DL STEWART (372-1704) A 1M DUNCAN (372-9052). 

C.O.C.tr 

C99-006-41 

Page 1 of 1 

Yeso No 

Sample No. Lab ID • Date Time No/Type Container Satnple Analysis Preservative 

BOR4C7 (F) W 1 x500-mL G/P ICP Metals - 6010A RCRA GW 

Q 

BOR4C8 W 7x500-mL G/P ICP Metals - 6010A RCRA GW /1^ 

(L r 

BOR4C8 W 1 x500-m l- P IC Anions - 300.0 (Ch lor ide, Fluodoe, Nitrogen in Nitrate, Nitrogen in Nit rite, Suaate) Cod 4C 

HNO3 to pH

..7 

N+ 

PNNI. 

Collector Ft (FtFy) -ontac 

III 

t/Reuuester 


Telephone No. MSIN FAX 

F No. amdina Orkin 

VTV 

Pu rchase Order/Char ee Cude 

Prolml Title Loebook No. Ice Chest 

-,t a 

learn. 

S 

Mooed To (Lab) Method of Shipment Bill of Ladina/Air Bill No. 

Protocol a Turnaround Offsh e Prouertv No. 

POSSIBLE SAMPLE ILAZAR WREMARKS 

" 

SPECIAL INSTRUCTIONS Hold Time TOW Activit y Exemolion: 

FAX COPIES OF QES & TMA TOG INTO D I- STEWART (372-1704) & IM DUNCAN (372-9052). 

C99-006-45 

Page j of I 

Yes No 

Sample No. Lab II) • Date Time Nc/I'ype Contai ne r Sample Analysis Prese rvative 

BOR4DI (F) W 1x500-mL G/P ICP Metals - 6010A RCRA GW 

77-70 

HNO3 to pH

.a' 

PNNL 

— — 


Collector . vs F"A ( ontact/Reuuater Telesshone No. MSIN FAX 

'AF No. 

'amolina Orivin 

(199-11116 

HAISIR)RDSITE 

srolect Title Loullsock No. 

_ 

..O.C.II 

Purchase Order/Chartre Code -^ 

6 Ice Cheat N 3E. Temp. 

'hipped To (Lab) Method of Shipment Bill of Lading/Air Bill No. 

P ro to co l Data Turna round Offidtir Propertv No. 

C99-006-57 

Page 1 of 1 

POSSIBLE SAMPLE HAZARDS/REMARKS SPECIAL INSTRUCTIONS Hold Th ise Total Activitv Exemtkion: Yes W No 

FAX COPIES OF QES & TMA LOG IN TO DL STEWART (772-1700) & 1M DUNCAN (772-9052). 

Sample No lab ID Date Time NwType Container Sample Analysis Preservative 

BOR4F4(F) W 

is 

\ 1x500-mL G Mercury -7470-(CV) nC/ 

HNO3 to pH .2 

B0R4F4 (F) W - 4500-m l- GIP ICP Metals - 6010A RCRA GW )C 

HNO3 to pH

PNNL 


C ollect or Rq ^-0X(R 'ontact/Reautater Telealsom No. MSIN PAX 

'AF No. Sarroallne Orlein Purchase Order/Charve Code 

Protect Title Lovistank No. 

c 

ce Chest No. 

4 . î 

Temo. 

-9 L 

Shinned To (Lab) Method of Shloment Bill of Ladine/Air BIB No. 

Protocol Data Turnaround Offshe Prooertv No. 

POSSIBLE SAMPLE HA ZARDS/REMARKS 

' 

C.O.C. it 

C99-006-61 

Page 1 of 1 

SPECIAL INSTRUCnONS Hold Time Toud Activit y ExemuOon: Yes LQ No 

FAX COPIES OF QFS & TMA LOGAN TO DL STEWART (372-1704) & JM DUNCAN (372-9052). 

Sample No. lab IU ' Date Time NarFype Container Sample Analysis Preservative 

BOR4F6 

W I l> ^ °>t. C^ CS 

1 x500-mL G/P ICP Metals - 6010A RCRA GW (; D ` / HNO3 to pH

PNNL 


Collector D R BREWINGTON (R FS) ontact/Reamesler Telephone No. MSIN FAX 

'AF No. Samr,lbut Orleln Purrhane Order/Charee Code 

Protect Title 

- 

Logbook No. ,/ in -if it 

Ice Chest No, ! 

iin c- 

hipped To (Lab) Method of Shipment Bill of Ladins/Alr Bill No. 

Pirrolocal Data Turnaround Offshe P roocrt y No. 

C.O.C. p 

Termp. c 

POSSIBLE SAMPLE HAZARDS/REMARKS SPECIAL INSTRUCTIONS Hold That Taal Activit y Exemaion: 

FAX COPIES OF QES k 1'MA LOG-IN 10 DL STEWART (372-1704) 81M DUNCAN (372-9052). 

C99-006-70 

Page 1 of 1 

Yes L9 No 

Sample No. Lab ID a Date Time No/Type Container Semple Analysis P reservative 

BOR4K9 (F) W - 1x500-m l- G(P ICP Metals -6010A RCRA GW /ì D ? HNO3 to pH


r good condition 

broken 


Telephoned T 

Figure 1 

SAMPLE CHECK-IN LIS T 

/ ^ o 

Date/Tme Received: ^/ IZ16^ f SG#: (C^Q 

p 

leaking 



Revision 5 

Work Order Number: 0 ^^ ^ 

n 

SAF #: l^ /q! 

- ' 

Shipping Container ID: 

/^n 

0( 

^^^ 1 Chain of Custody # lam` q - c t1-3 t^_ 

1. Custody Seals cn shipping container intact? Yes ( }'b1a ( ] 

2. Custody Seals dated and signed) Yes [ ],Nb [ ] 

3. Chain-of-Custody record present? 


o 

Yes ( ]]"NC'( ] 

5. Vermiculite/packing mate rials is Wet [ j D ry [ L^ 

1 


7. Sample holding times exceeded? Yes [ ] No (]^^ 


3tape h azard labels 

',oastody seals appropriate sample labels 

10. Where any anomalies identified in sample receipt? Yes [I No [ 

11. Desc ription of anomalies (include sample numbers): 

34 

X045

Figure 1 

SAMPLE CHECK-IN LI 

Date>Tme Received: SG»: 

Work Order Number: 0 ^ f! C t/i SAF 4: ^ 

f 

ST 

/ l Gn 

^ / -G^(p 

Shipping Container IQ:(' ^^^ Chain of Custody # ^ (/ _ C^^ 

RFSH-SO`; ^'-93-0003 - 

Revision 5 

1. Custody Seals on shipping container intact? Yes jr-j-'N o [ jj 7/^^ 

2. Custody Seals dated and signed? Yes Nc [ j 

3. Chain-cf-Custody record present? Yes [ ] No [ ] 


5. Vermiculite/packing mate rials is Z_ / Wet [I Dry [ ]i 


7. Sample holding times exceeded? Yes [ ] No [ j"— 


___,,,Liape 

ustody seals 

h azard labels 



n good condition leaking 

_broken have air bubbles 

10. Where any anomalies identified in sample receipt? Yes (] No [ 


Sample Custodian/Laborato ry : L

Figure 1 


Date,Tme Received: ^^^! / 0 ^Y^`"^ 

SGT ^0 5^^ 


Revision 

1 

/ (^ 

Work Order Number: ^^^/^S^.F T ^^^^^- C3^^ Y^ / -C%'^L


3n good condition 

broken 

Figure 1 


leaking 


RFSH-sow-9;-0003 

Revision 

DateTme Received: ^^^lElf 

/ 

Q / 

ICY SG:: L(^YJo2^^ / 

Work Order Number: 0 ` f SAF 

c G 

—!,rJ 9 J^ l "^^^ 

Shipping Container ID' L Chain of Custcdv Ct -C( ^! 76 

SCI-rte'/; 

1 . Custcdy Seals on shipping container intact? files 1^t6 o[ 

l 

2. Custcdv Seals dated and signed? Yes P'Nc [ ] 

3. Chain-cf-Custody record present? Q ^-- Yes (.j^Nc [ ] 


5. Vermiculiteipacking materials is Wet [ j D ry [ ^% 

6. Number of samples in shi p ping container: 

7. Sample holding times exceeded? Yes (] No [ ^% 

8. Sampl s have: 

ape h azard labels 

custody seals approp riate sample labels 

10. Where any anomalies identified in sample receipt? Yes I No [j/ 


Sample CUStC62.,i/Laborato ry : 

Telephoned To'. 

34 

1`045 

^ :J

n I 

^S I U'^`^ lvt ^S I Ur^Co L4J 

4L , ( l zl q s 

LIENT CODE: ID p 1AIRIX RECEIVED DF,TECIOR A ( Q DAl F. SAMPLE -^ -MINUTES ( , N'FSA NETCPbIA CNTSB NETC'i'NIH 

HAV 1101201 14 1028/9811WOOITI QEV122 1)10:11/989.34.16A61 80120)'4 30 4 003904762 - 

1.)(1 11 1 1) Bkg: 10 131/985.5397AAI BKG 700 66 0.09428571 876 1.25 1 4286 

A ni Date: 10/3 1 /98 "1'nt So, Alq: I.00E+00 1.00E+01 Alp; (Dpn t/ 8 27E-02 (uC'V 3.73E-06 (pCV 3.73E+00 + 2.3E+01 CAT 6.7E+00 Lab 

P i ll mg: 3.2 1^ Units: L ^, n il Bet; Alq): 2.02E+00 So): 9.IOE-05 Leg): 9.I(1E+01 + 2.4E+01 I 5.5E-01 Alit 

PG(V BORIN13 10'28/98)2:54-.00P I QUAD221i 10/3)/98)0;)1.25 AM B0R1613 30 4 003476190 45 0.0471429 

1_IQUID Bkg: 10'3 1/985.53Y17 ATI BKG 700 69 0.09857143 1017 1.4528571 

AW Dole: 103 1/98 1'ut So, Alq: 2.00E+00 I OUE+01 Alp; Q)pm/ 1 03E-01 (u('1/ 9.301 06 (pCV 4.65E+00 + 2.4E+01 CAI 5.4E+00 Lab 

p ill P m g ^ 0 / Units: 1. /, ml Ilel; AIq): 6791.02 So): 6.121:06 Leg): 3061.+00 +201- 1111 

1 

^ 1.6E+01 

Alq 

IIg 

PGIV HORINIR 10/28/9812: 5400 PKI QUAD22C 10131 ,9810 It 25 A p t BORI 1,I8 30 9 0.21428571 52 0.6461905 

LIQUID Bkg: 10711985: 5337 :%NJ BKG 700 60 008571429 761 10971429 

AidDete: I 01 1 /98 'FntSa„AIq: 3.00E+00 100001 Alp; ( I)pn ,/ 6AIG01 (uC1/ 8.661[-O s 

1/ (p(' 289E+01 +2.31-+01 CAT 8.7E-0 1 Lnh 

1 

^'l .UE Alq 

+00 

Leg 

P ill mg: 3.7 / Ilnlln: I nil I{el; ,AIq): 1.081-11)0 S o): 1 .4604 1- L I t ): 488E+01 +2001 1-1 

P(Ak' 130R3K9 10' 27/ 981: 30:001' p l QUAD22D 10/31/98 10 11 2 5 Apt BOR3K9 30 4 003904762 43 0.1819048 

1.1(lIOD Bill: i 1'98 5:53 it ANi i3K(I 700 66 0.09428571 876 1.2514286 

AM Dote: 1 0/31 198 Tot So, A Il i : 4.00 F , 00 IOOE+01 Alp; (Dpnd I-13E.-01 (u( 'V 204L05 (pCV '.IIE+00 ?231-+01 CA IF 49Ei00 Lib 

P ill mg: 2.1 1 Iinite: ^- n il Bet; Alq): 3.2OF-01 So): 5.761.05 (-Ig): IA4E+01 + 1.9E+01 I ---3.5E.00 

PG%V BOR319 1 027/98 1:30:00 J I M QUAD23C 10/31,98 10_11.33 r1)( BOR319 30 3 0.02714286 60 0.8857143 

LIQUID Bkg: 10/31/98 5:53.44 AAI HKG 700 51 0.07285714 780 1_) 142857 

Aid Dow 10/31/98 1 utSn„1)q: 500E+00 I.00E101 ,Up; (I)pnd 5.64E-02 (,CV 1171.-OS (pCV 254E+00 +2_IE+01 CAT' 9.8E+00 Lob 

1 - pt nrg: 1.9 Unils: I. nil Iteq ,AIq): 1 70F 100 So): 1 811>04 Lig): 7 68E+01 + 2.3E+01 

I 

6 51;-01 

Ale 

^ LIg 

POW 801(492 10'28/78 12.54:00 J IM QUAD23 1) 10/31,98 10.11 31 ,1)I 1 1OR492 30 29 0.90666667 495 15.525714 

1 [Oum Ilkg: 10:31 . 9R 5 51 41 A p l 11K6 7110 42 006 682 09742857 

-Anl D.w 10 1198 1 o So, AIli 7 001 100 I OOE 1 01 Alp; (Opnd 2. 171;+00 (u('1/ 7.46 1:04 (p( V 1.07E+02 + 2.7 1-101 CAI 2 R-Ul Lab 

Ppt mg: 2 2 / 11n11: I n1l It,[; :1)q): 2911- 1 01 So). 9.18E-03 1.1g): 1.310+03 + 69E 1 01 I J.8F-02 

PGs(' HOR495 X ^(^) 10'27'98 2 0900 FIN QUAD24A 10/11,98 10.11.28 AAI 13OR495 30 5 0.07952381 70 I_IR33333 

0 _ n l 1101 ID Mg: x.,.,,:98 553.25 ,Ni um, 700 61 0.08714286 R05 115 

AM Dole: 10/31/98 lot So, Alq: 6.00E-00 IOOE101 Alp; (D ion 3 214E-OI (it( I/ I7RE-OS (p('1/ 9.63E+00 +23E+01 C'A'I ^6F 100 Lob 

1 

4.91;01 

Alq 

1.1g 

M^ Ppl mg: 11 Ilnll_r L^ ud Bel; ,AIg ) : 22(,10100 Se): 6 111I.-W L I gl: 10211@ +2511 1 01 

3l- Oct-98 Quan(ci t a Em h immen( Sen ices, SCP V2.03 2 

Leg 

1.g

7 

)1^7^18 

CLIENT C(/DE IIl MATRIX REC'EI5"Ei/ DE I ECI OR U Q D.\ IT,SAIIIPLE MINUTES CNTS A NET CPI11 A C'NTS R NET CPM B 

PGW BOR4BO LO W27/982:0900PAI QIAVD24D 10/3 1,9810:11:28 AN[ BOR4BO 30 26 079380932 486 14.93 

.^ I.IQIIIU Bkg: 10/31/985.53:25 AAI BKG 700 51 0.07285714 889 1.27 

Ant Date: 10/31 198 T,a Sa,Al 7.00E+00 

q: I.00F,01 - - 51 p; (1/pnJ 1.94E+UO (uCU 6.120-04 fOl 

(pC'V 8.74E+OI + 291101 CAT 2.9GU1 Lab 

Ppt mg: 3.4 11-, Units: L ml Ret;, Alq): 2.84E+01 So): 8.97E-03 LIg): 1, 28E+03 + 6.3E+01 1 3.9E-02 LIg 

POW B0 114 132 10/2 8 /98 12:54:00 PM QUAD2IC 10/31/98 1110:09 AAI BOR4 13 2 30 31 0.94619048 2607 85.932857 

1.1(lIIID Ilkg: 1091/98 5:53 29 AAI BK6 700 61 0.08714286 677 0.9671429 

Ant Date: 10/31/98 Tut So, A19: 6.00E+00 IOOL'01 Alp; (DpnJ 2.47E-01 (uCV 6.69E-05 (pCU 1.11E+OI +2.IE+OI CAT 2.2E+00 lab 

Ppl mg: 16 / IIn11s: I. / nd Rel; Alq): 1,69E+02 So): 4.57F.-02 Llgl: 7.62E+03 + 1.5E,02 1 i 6.6E-03 

Alq 

PGW BOR4C8 ^7 W,3 10'27/982°.09DOPkI QUAD22A 10/31/9811: 10: 16 AAI BOWS 30 5 0.08095239 43 0.2161905 

C)^ /A I.IQUIU likg: 10/31/985.57. 37 AAI IIKG 700 60 0.08571429 852 1.2171429 

Ant !late 10/31/98 I'M So, Alq: 60(71100 1OOEMI Alp; (Dp,N 2.33E-01 (uCU 670E-05 (p( I/ 1.05E+01 +22E+OI CAT 2AE100 lab 

F 1 en 2.5 

P R :/ Unl1s: I, / nil Rai; AU 3 55IF Of Sa : 

II: ) 9611, OS LIg): 1.60E 101 ± 1,9E H71 

1 , Alq 

111+OU 

I.^g 

POW 11OR41J)2 X /. ' I 10'27/98 2 09.00 1'kl QU AD2213 10'7198 11.10 M AM I30R4D2 30 79 2.53476190 1844 6401381 

n {nV /\ 

1 

3_ - ___ 000. 

IlQlgp 

- __. 

Aul Dolc 10/71 1 98 

' 1 u1 So, Alq: 7.OU1'l10 

Blig 

1.001/'01 

!!P7!-98•._1 " ,'AI ilk(./ 

- __ -_ 

__. 

-_ _- __. 

_ _ 

Alp; (I)p,.,/ 637F100 (u('U 201103 

100 

(pCU 

69 0, 09857143 1017 1.4529571 

-_ - 

- 

_.__ __.__ 

2.871102 +4.IL1111 l'A 8 7L 01 L.I. 

Ppt mg: 5 / th lls: I. nd 110; ,\bU: 113E.02 5a): 7581: u2 IJg): 5.111107 +1.21+112 

1 

9.8E-03 

Alq 

I•Ig 

PGW BOR4F5 Qj 10,27/982:00,00 I'M QUAD2IC I OA 1 /989: 56 56 AM BOR4 1` 5 30 3 0.01285714 58 0.9661905 

0^7 "4 114: 1091/98 5.5329 AAI BKG 700 61 0.08714286 677 0.9671429 

Ant Dole: 1091/98 IM So, Alq: 6.00E+00 LOOS101 Alp: (DpnJ 9.83E-03 (uUU 2.66E-06 (p(' 1/ 443E-01 +2.1E+01 CA'F 561+OI Lab 

Ppt mg: S8 Units: I- ml Ilrt; -AIq): 1 91F'00 So): 5.151:04 LIg): 8.591,01 ± 2.3E+01 I 

---- 

5 8E-111 

Alq 

Leg 

POW BOR4F6 ^ ^Î^p 1027/982.00,001'kl QUAD22A 10/31/98856.59 AAI BOR4F6 30 3 001418571 53 05495138 

IIQI g U Illkg: M3t,9835117 M BKG 700 60 0.08571429 852 12171429 

Ant Dow 10'11/99 1w So, Alq; 6.000 1 01 1001.MI Alp; (I)pm/ 267E-02 (uCU 712L-06 (p( I/ 1.19E4OO +2.1E101 (A1 2.11'01 Lab 

Ppt mg: 2 3 Onlls: L 1111 Bel; 41g) 102E'00 So). 2 751-04 LIE): 4.59 1, 1 01 + 21E101 I " 1.11100 Atq 

PGW BOR41'8 10/27/98 2'.00:00 1'M QUAD22R 1091 198 8:56:59 AM BOR4F8 10 5 006809524 50 0.2138095 

LIQI IU ! !kg: .-, AM i3KG 700 69 00985714 3 11117 /,4528371 

Ant Dale: 10 131/98 1 n1 So, Alq: 6 001 1 00 1 00E+01 Alp; (I )pnJ 203E-01 (uCt/ 5.54E-OS (pCU 9.23E+00 + 2.5E+0I CAI ' j 7E+0O Lab 

Ppl mg: 21 I1ni1s: 1- 110 Rel; AIq): 3.66F.01 So): 99OF-05 LIg): 1.65E101 +2AE'01 

I / Alq 

3. 0 1100 

LIg 

^^ Jl-Orl-Y3 Quanicrra Emirunment Senices, SCP V2.03 3

`lam 11ILI98 

CLIENT CODE Ill AIATRIX RECEIVED DETECLOR ACQ DATE SAMPLE MINUTES CNTS A NET CPAs A CNTS B NET CPAt B 

POW 13OR4^10 k 

1. 

3 

^^ 102 7/982:0900PAI 

C 

QUAD2 1 C 10'31/989-.34:12 AAI BOR410 30 3 0.01285714 34 0.1661905 

-F l /J \ I,IQI qD Ilkg: 1011 1/9 8 5:53:29 AAI BKG 700 61 008714286 677 0.9671429 

AM Date: 10/31/98 TM So, Alq: 600E 100 I.00Ef01 Alp; (Dpm/3.24E-02 (uCi/ 877E-06 (pCl/ 1.46E+00 +1.9E40I CAT 1.7E+01 Lab 

Ppt mg: 0.2 

1^ 

finite: I. ^, od Bel; Alq): 3.191:01 S o): 9.611.05 LIg): IA4E401 + I. IJ E101 I -- 3.51400 Alq 

I•Ig 

POW BOR4X7 10127/981.00:00 PM QUAD22C 10/31/988:56:59 AAI BOR4X7 30 11 0.28095238 176 47795238 

1 -IQ1 1 1 1) MR: 103 398 5:53:37 AM BKG 700 60 0.,39571429 761 1.0871429 

AnlDdc 10 /3 1/98 lot So, Alq: 1.601 : f01 1.(831. 01 Alp; (UpnJ 7091:01 (u('1/ 5.HE:04 (PCB 3391:101 + 2.41:101 C'A'P 781.01 Lab 

Ppl mg: 31 Units L ml Itel; Alq): 8.851;100 So): 6.38603 I.Ig): 3.99EfO2 +17E401 

I 

1.31(-0 1 

Alq 

LIg 

POW 60R4X9 10/27/98 2:40:00 PAI QUAD22D 10/31/98 8:5659 AAI BOR4X9 30 7 U. 13904762 42 0.1485714 

LIQUID Bkg: 10111/985: 5377 AM BKO 700 66 00942R571 876 1.2514286 

AM Dale: 1031/98 Tot Sa,Alq: 1. 60Ef01 I.(JOE, 01 AIp; (Dina/ 4.091:- 0 1 (uCL/ 2.95104 (pCU IB4E+01 +23E401 CAT -^ I.4E40U Lab 

Ppt mg: 0 ^ Ilnlb: I. nJ Bel; ,A111 ) : 196.01 So): 1 41 04 1-g): 9.819.100 + 1.91401 

I 

571400 

A1 

1. ^ g 

POW 13OR419 10 27/98100.00 PAI QUAD23C 10 1 31/988: 57: 03 AM BOR4F9 30 3 002714286 75 1.3857143 

1 IQUID llkg. 10 31,98 5:53 44 AM BKG 700 51 007285714 780 1.1142857 

AnIDole: 10/31198 1ot So. Alq; 1.60E-01 100E-01 Alp; (UpnJ 441E-02 (uCl/ 3.19E-05 (p( 1/ 1.9915+00 +2IF401 (At I3E101 Lab 

Ppl mg: 1F Unite: L /, nd Uet; ,\111 ) : 2.68E+00 So): 1.93E- 0 3 I,Ig): 1.21 1402 +261401 

I 

4.1E-0 I 

Alq 

POW BOR103 1027/981: 00.00 PAI QUAD23D 1011/988:57:03 AAI 13OR503 30 8 0.20666667 47 0.592381 

LIQUID Blig: 10'31199 5:53 44 AAI BKG 700 42 006 682 09742857 

Anl Date: 10 , 3 1/98 lot Sn„\Iq: 1.601;401 1OOE-01 Alp; (UpnJ 598E-01 (uCV 4.31E-04 (PCP 2.69E+01 +2.1E+01 CA'L 9.3E-01 Lab 

Ppt mg: 0 Units: L / nd I1e 1 ; ,A1111'. 9.94E-0 I Sa): 7.161: 1 4 LI L[& 4A8E+01 +201+(31 

1 _/ 

I_I 1 

Alq 

1.16 

P(iq' 11OR510 1047/98 1:00:00 PAI QI 1 AU24,A 10 11198 8:5652 AAI 13OR510 3 0 11 0.27952381 40 0.1833333 

i Igl4U Bkg: 10 31.99 5 5715 AAI BKG 700 61 008714286 805 1.15 

,No] Dow IW31,98 Tot Sa„AIq: 2.001:-132 1.001101 ,kip; (Dpm/ 9 .63 1-01 (it( 1/ 7 79F 07 (p(V 3.89E-01 4 2.5E-401 CA '1 64E-0I Lab 

Pptmg: 02 

/ 

IIn11e: I. / nd Itel; AI q): 1.91601 Sa ) 1.721>07 1. jg): 9.61E 1(30 + 191:101 I ^.8H 430 Alq 

1.18 

PGR' 11OR511 10-171981.(10(30 PAI QUAD24 1) 10/31/998: 56.52 AM BOR511 30 5 009380952 49 03633333 

I IQUID Ilkg: 1001198 5:51.2S ,Ut BKG 700 51 0.07285714 889 1.27 

Anl Dale: 10/31/98 Tot So, Alq: 2 OOL-02 100E-01 Alp; (Dpnd 259E-01 (oC l/ 234607 (p( 'U 117E.401 + 2 3E+01 CAT 2.1E+00 Lab 

- PPtmg: 02 ^' Unlb: I. nd 11et: Alq)! 649E-01 Sa): 584E-07 Idg): 292E401 +2.IEN)1 I 171`100 

Alq 

F + i 1-0(r/-98 Quanlerra Environment Seniecs, SCP V2.03 4

Quanterra 

E^..l 

S^ 

CUSTO ME R - 6 FI--L— 

*** REANALYSIS REQUEST *** 

CHAIN-0F-CUSTODY BATCH ANALYSIS RECORD 

DUE DATE I, L/^ 

ANALYSIS ^Gd m wyd 

MATRIX a j;2 SAMPLE DELIVERY GROUP bV 0 25 19 

I) INITIATED 15&--l 3 

SOP(S) # ( +RL A e 

ACTIONS (Initial & Date) 

BATCHNUMBER 53 1 ,0 5D ô. 

4) SEPARATION LAB RECEIVED 

SOP(S) # C XJO 

5) COUNTING/N EASUREMENT 

2) PREP LAB RECEIVED / ^l^ LAB RECEIVED 

SOPS) # , I -7t57/7/ SOP(S) # 

6) DATA REVIEWED AND 

3) SAMPLE REMAINDER STORED FPS I / ANALYTICAL PREP STORED -6-6- - (I Î 

SOP(s) # n^/^+ SOP(s) # 614 p- v2, 

RC-048 I 0/96 REV 3 

CUB

I 

1 n i I 

BATCH SUMMARY/CHAIN OF CUSTODY 

w,11-(!;IS y _MATRIX DUE DATE 

** 

OR { CRDER SEQUENCE # CLIENT COMIvIENiS 

1 _ _ 

-IB QC BATCH REAGENT BLANK 

-IX QC BATCH MATRIX BLANK 

-IM 1S 

(circle) 

-2M or 2S 

(circle) 

QC BATCH MATRDUREAGENT 

SPIKE 

QC BATCH MATRDUREAGENT SPIKE 

DLD Ô (O ^' — Duplicate of Sample # O T^ 

P P 

Batched and QC updated by Qa on 1 7 

Recd in Prep Lab by ICK on 1 Sop# - d -^-SQ /7/ Rev# 

Recd in Sep Lab by_ on Sop# Rev# 

Recd in Sep lab by on Sop# Rev# 

ED/CPPT by on Sop# Rev# 

Rec d in C.R. byon ^^ Sop# /C (C l7'tb , C 7 Re v# 

Data Reviewed by ?t on {SCl Sop# 9l Z I^ 6ecC ` Rev#.^^_ 

Original batch sheet and complete calculation file to be fi led with the FIRST listed work order number 

FORM NO.. RC-52 I/98 Rev. 8 

^

CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 28-Oct-1993 

Q Page 1 

CUSTOMER: BHI // SAMPLE DELIVERY GROUP /U^r 

MATRIX WATER ^^ ^ - bu- BATCH NUMBER I _ 

CUSTOMER 

GES ID DUP ACCOUNT ID COMMENTS 

=-aa=eaaeaaaaaaco.a.easvaaaas-aa-asaaaa=aaaaneaa=ana=avaa==a.ase.ô_ao.s 

1 ) 81050601 BHI BOR495 

3IO -s-060 4 

2 ) 81050602 o BHI BOR4BO 

1 

3 ) 81050603 BHI B0R4C8 

4 ) 81050604 BHI BOR4D2 

5 ) 81050605 BHI BOR4F5 

6 ) 81050606 BHI BOR4F6 

7 ) 81050607 BHI BOR4LO 

eaa=aeaaaesysa-aa=aaaaaaa=a..aaao=m...ca.casaasaacs=oeaasa=aeasaaaas=asl 

I / ACTIONS (Initial & Date) 

1) INITIATED — ClÔ^(C^^ 5) COUNTING/MEASUREMENT LAB 

SOP(S) # J'J SOPS) # 

( 7 9 

2) PREP LAB RECEIVED 9j0 

f 

SOPS) #/QICt/^C,7D^b+sd^/'/ 

3) SAMPLE REMAINDER STORED 

SOPS) # 


SOPS) # 


ANALYTICAL PREP STORED 

SOPS) # 

r'UJì

CUSTOMER: BHI 


Page 1 

( 

SAMPLE DELIVERY GROUP UÛ^ 

MATRIX WATER - ^ BATCH NUMBER 

CUSTOMER 

DES ID DUP ACCOUNT ID COMMENTS 

1 ) 81053301 BHI BOR492 

2 ) 81053302 BHI BOR4B2 

3 ) 81053303 BHI BOR4F8 

TI orb 6 ( B 

=cs--sss-assns=as---sa-.ssa--ss ----as sasa--av-ssss--as---ss---sa --s--s. 


1) INITIATED ^^ /^c '^ 5) COUNTING/MEASUREMENT LAB 

SOPS) # SOP (S) # 

2) PREP LAB RECEIVED / , 6) DATA REVIEWED AND 


SO PS) 

SOPS) # 


^^ 

/^/ 

SOP (S) # (^ 


SOP (S) # 

L'^JJ

uanterra 


ANALYSIS of MATRIX IS O DUE DATE / )-S 

WORK ORDER SEQUENCE # CLIENT COMMENTS 

J I OSDC^ IB QC BATCH REAGENT BLANK 

J -1X QC BATCH MATRIX BLANK 

J I QSD^ -1M IS 

J 

D Q-1) 06o 

(circle) 

-2M or 2S 

(circle) 

I bÔ^D 07 

ID53301 03 

Batched and QC updated by r -5 on t 7 c 

QC BATCH MATRIX/REAGENT 

SPIKE 

QC BATCH MATRDUREAGENT SPIKE 

Duplicate of Sample # $ 10S060 

Recd in Prep Lab by f18- on i 9 Sop#S^/^ l a S`D 1 y D Rev# 

Recd in Sep Lab by_ on Sop# Rev# 

Recd in Sep lab by on Rev g 

ED/CPPT by on 

y 

Recd in C.R. by on 1 r 

Sop# Rev# 

Sop# g(C E(12 (ÔOo 3 Rev -4 C 

Data Reviewed by on 1 ^/ Sop# Rle0K 66'0o 2- Rev# Z 

Original batch sheet and complete calculation file to be filed with the FIRST listed work order number. 

FORM NO.: RC-52,1/98, Rev. 8 

GU:;o

1) 

2) 

3) 


Page 1 

CUSTOMER: BHI 

MATRIX : WATER 

r- SAMPLE DELIVERY GROUP ^ ^^J 

1 

DOCK BATCH NUMBER w /"JO& 

CUSTOMER 


====c=========v=a=a-aaa===a=a===c=_.=====caa=====a==aa==-^---==c====a=== 

1 ) 81050601 BHI BOR495 

.p 1 o 5-0(oo1 

2 ) 81050602 BHI BOR4B0 

3 ) 81050603 BHI BOR4C8 

4 ) 81050604 BHI BOR4D2 

5 ) 81050605 BHI BOR4F5 

6 ) 81050606 BHI BOR4F6 

7 ) 81050607 BHI BOR4L0 

ACTIONS ( Initial & Date) 

jtj 

INITIATED ^cl 3 5) COUNTING/MEASUREMENT LAB 

SOP(S) # V SOPS) # 

PREP LAB RECEIVED - 

44^ 

SOPS) 

# RI^f^FC5Î6,^ 

SAMPLE REMAINDER STORED ^/'S 


SOP(s) # 07^ 

SOPS) # 



SOPS) #

CUSTOMER: BHI 

CHAIN—OF—CUSTODY BATCH ANALYSIS RECORD 29-•Oct-1998 

Q Page i 

SAMPLE DELIVERY GROUP I^D^` 3 ^ 

MATRIX WATER CI -DC BATCH NUMBER D 

CUSTOMER 


1 ) 81053301 BHI BOR492 

2 ) 81053302 BHI BOR4B2 

3 ) 81053303 BHI BOR4F8 

.5 '1 C ,5-0 (o ( 8 

So50615 


1) INITIATED ^c13 5) COUNTING / MEASUREMENT LAB 

SOP(S) # To SOP(S) # 

2) PREP LAB RECEIVED 6) DATA REVIEWED AND 

U ANALYTICAL PREP STORED 

SOP(s) # (R C ^SO^7. G 

3) SAMPLE REMAINDER STORED 7 Q 

SOS) P # _ 

1 

SOP (S) # N/^ 


SOPS) # 

C'0Jii

C%%uanterra 

`r„In ;nr 


ANALYSIS b _MATRIX U^_Q^DUE DATE 

WORK ORDER SEQUENCE # CLIENT CO S 

1 OS^J C^ 1B QC BATCH REAGENT BLANK 

J /asoG -1M r1S 

-1X QC BATCH MATRIX BLANK 

(circle) 

1 -2M or 2S 

D 0_ SCE b O _ 

(circle) 

G7 

Batched and QC updated by on1/ 71?,^7 

Recd in Prep Lab by EPS on ^^11 

^ 

QC BATCHMATRDGREAGENT 

SPIKE 

QC BATCH MATRIXIREAGENT SPIKE 

Duplicate of Sample # Oct 

Sop# 544,1 Rev# 

Recd in Sep Lab by on Sop# Rev# 

Recd in Sep lab by on Sop#_ Rev#__ 

ED/CPPT by 

7 

^7 

Recd in C.R. by I 7 /^ on 19 i 

on 

Sop# Rev# 

Sap# K I C (-1 /2 19 000 -5 — Rev# 

—V 

Data Reviewed by —4L = on Sop# IC ) C t^ )Z ICCO Z- Rev#_ 

Original batch sheet and complete calculation file to be IDed with the FIRST listed work order number. 

FORM NO.'. RC-52,1/98, Rev 8 

C-0

CHAIN-OF-CUSTODY BATC^ ANALYSIS RECORD 28-•O[t-1998 

Page i 

CUSTOMER: BHI SAMPLE: DELIVERY GROUP U , 

MATRIX WATER O 

BATCH NUMBER 

CUSTOMER 


1 ) 81050601 BHI BOR495 

2 ) 81050602 BHI BOR4B0 

SID SO&O- 

3 ) 81050603 BHI BOR4C8 

4 ) 81050604 BHI BOR4D2 

5 ) 81050605 BHI BOR4F5 

6 ) 61050606 BHI BOR4F6 

7 ) 81050607 BHI BOR4L0 

a-xa-x-x----xc-xx=-xx-v-xxx-=-xx-=o----x=x--o=x==xx==xax---=--xv x:o--x axx 


1) INITIATED ÌCI 5) COUNTING/MEASUREMENT LAB 

SOP (S) # SOPS) # 

2) PREP LAB RECEIVED C 

l / 

/ / 7 6) DATA REVIEWED AND 

( 

P5 ^/ 

/ 

ANALYTI CAL PREP STORED 

SOP(S) 

# R^CI^QCI 7D ^6 ^^J(/^T• 

3) SAMPLE REMAINDER STORED C 

SOPS) # 


SOP (S) # 

SOPS) # 

l 0 PU

CUSTOMER: BHI 

CHAIN-OF-CUSTOD" B%TCi- ANALY!.;IS RECORD 

SAMPI-E CELIVEF''v' GROUP 

MATRIX WATER BATCH NUMBER 

N-Y)b 

CUSTOMER 


1 ) 81053301 BHI BOR492 

2 ) 81053302 BHI BOR4B2 

3 ) 81053303 BHI BOR4F8 

s osoh i8 

î czsa r, ^S 


1) INITIATED 5) COUNTING/MEASUREMENT LAB 

SOP(s) # 5 SOP(s) # 

2) PREP LAB RECEIVED ! b) DATA REVIEWED AND 


SOP(s) # 

SOP(S) # 

3) SAMPLE REMAINDER STORED 7 9^ 


SOPS) # N _ 

SOPS) # 

29-Oct-1999 

Page 1 

n 06 4

_ 7 ^ 

w. 


nra.^ _rsls C-/L/ MATRIX 14j4 fR DUE DATE_z 

W 

11K041)1:H SEQUENCE I CLIENT COMMENTS 

/Al 2 11 QC DATCI I REAGENT BLANK 

I^t-)1-7,_^y^_ •IX QC DATCIIMATRMBLANK 

f^ IM OF S 

— 

) --— 

(circ le) 

IM or 1S 

(circk) 

QC BATCH MATRDUREAGENT 

SPIKE 

QC DATCH MA7 ME-AGENT SPIKE 

DvpllceteofSmnple0 

/6)- 533 0 S 

//- ) ^^^ c62 aN 

Uatched and QC updated by Diva.•- on yg _ 0 

Reed in Prcp Lab by on Sop# Zk'#o6C SZ â2 Rev# 

Itcc'd in Sep Lab by on Sop# Rev# 

Rcc'd in Scp lab by on Sop# Rev# 

ED/CPPT b y i on SopA RovN 

Rcc'd in C R. by o Sop# k I( j Rev# C^ 

Data KcAmcdby X11; ^^ on )t1 î Soo# ^C I L'l {(c c'CC^ a Rev# 

Original batch sheet and cowpk el calculation file to be filed with die FIRST listed work order number. 

FORM NO.: RC-51. Ilya, Rev., g 

a_1 

C. 06

CHAIN—OF —CUSTODY BAT(F' ANAL N '.:S RECORD 29—Oct-1998 

Page 1 

CUSTOMER: BHI SAMPLE DELIVEP) GROUP 

Q 

MATRIX WATER l BATCH NUMBER 

CUSTOMER 


^lDS^3/ S 

1 ) 81093301 BHI BOR492 

3 9 ^^ ^J ^J 


1) INITIATED 5) COUNTING/MEASUREMENT LAB 

SOP(S) # 

t{^ 

'^ SOPS) # 


^p 

SOP() ) # /1 I^.^.P^ ^,^2 



SOP (S) # 

SOPS) # 


SOPS) # 

f^06

n yyl(, CHAIN-OF-CUSTOD" BATCH ANALYSIS RECORD 28-Oct-1998 

I^ Page 1 

CUSTOMER: BHI SAMPLE DELIVERY GROUP DDD,^3yl^ 1 J 

MATRI), WATER 001 - DOD BATCH NUMBER D - 3(/& 

CUSTOMER 


1 ) 81050602 BHI BOR4B0 

2 ) 81050604 BHI BOR4D2 

==-o=-xmmm-ox--oxxovv---=oxo=m==cc=-x = - ==cvo--xxxooc=vx-xvxc= ^-==-o. 

ÂCTIONS (Initial & Date) 

y 

1) INITIATED w'3 D 5) COUNTING/MEASUREMENT LAB 

\ 

SOP(S) # D ^J SOPS) # 

2) PREP LAB RECEIVED G / S i'^ 6) DATA REVIEWED AND 



90P(S) # 


SOP(S) # 

SOPS) # 

C0E4

(l %'uanterra 

^' 6'mimnm^^nral 

h•rrir us 


ANALYSIS -_.,MATRIX f„ î^^ DUE DATE /a • s- F8 

(O S o G 

WORK ORDER SEQUENCE # CLIENT COMMENTS 

— 

-tB 

3 ^v 

13 Hr 

w zs^7 

QC BATCH REAGENT BLANK 

/ 0 5 O 4 -IX QC BATCH MATRIX BLANK 

1 /050 6 15 

yH 

D 105e) (F o I 

/0 5C 0Z 

S/ o 5o 0/ 

Io 53 3 01 

(circle) 

-2M or 2S 

(circle) 

- 

o 

03 

Batched and QC updated by on /-.Z- 

Recd in Prep Lab by N on N h 

Recd in Sep Lab by_ on 

Recd in Sep lab by on 

ED/CPPT by on 

Rec'd in C.R. by on l L^ y 

QC BATCH MATRIX/REAGENT 

SPIKE 

QC BATCH MATRD{/REAGENT SPIKE 

Duplicate of Sample # k/ 0 5 6 (¢ m / 

" / ^t F1/o So loo i 

Sop#k I eN g Q 5 007 Rev# / 

Sop# .v Rev #^!P_ 

Sop# Rev# 

Sop# Rev 

Sop# 9l ( HR D6^r c / Rev# 

Data Reviewed by 6 Y' on ` ` Sop# _ lC-^C E b G Z Rev# Z, _ 

Original batch sheet and complete calculation file to be filed with the FIRST listed work order number. 

FORM NO.: RC-52, 1/98 Rev. 8 

j 

i

CUSTOMER: HHI 

CHAIN—OF —CUSTOljY BA1CH Q',AL"'.'i S RECORD 28--Oct-1998 

Page 1 

` : Iir^hIP L-li I)E:IH 

MA 

T I X WATER C1^^ - 

NUMBER /Y 3^4TC 

CUSTOMER 


jr )o Sob^.+i 

1 ) 81050601q BHI BOR495 

DIo5 c, uo^ _4» k 

2 ) 81050602 1 BHI BOR4BO 

3 ) 81050603 BHI B0R4C8 

4 ) 81050604 BHI BOR4D2 

5 ) 81050605 BHI BOR4F5 

6 ) 81050606 BHI BOR4F6 

7 ) 81050607 BHI BOR4LO 

Jo 


1) INITIATED lLllC 5) COUNTING/ MEASUREMENT LAB 

SOPS) # Ko )^T SOP(S) # 

2) PREP LAB RECEIVED 

/' 

SOP(S) #RAP ke 5007 



3) SAMPLE REMAINDER STORED 4-e 

SOP (S) # 

SOPS) # 


SOPS) # 

710 50 4 1 X p 

J 

10 5 0 ( s 

10 0 

(p0, 90 r a. 5 9 Ì dlo . bzo 

/ 0 Y,2-- 

C0cJ

CHAIN—OF —CUST01 c. BoOGH . o \. AL" ! ; S RECORD 29—Oct-1998 

CUSTOMER: BHI /^ ':;ANPL_i:' DE:L IVEF • `' GROUP 

Page 1 

' ' 1 (^ J 

WJ,2)5b 

1 

MATRIX WATER IJ BATCH NUMBER 

I 

^^ 

CUSTOMER 


1 ) 81053301 BHI BOR492 

2 ) 81053302 BHI BOR4B2 

3 ) 81053303 BHI BOR4F8 

---------- 

ACT 

IONS (Initial & Date) 

---- ------- 

1) INITIATED 

/ V 

O 5) COUNTING/MEASUREMENT LAB 

SOP(s) # OJ?JJ^J SOP(s) # 



SOP(S) # 

SOP(S) # 


SOP(5) # 


SOPS) #

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