Certificate of pesticide multi-residue analysis by MSMS ... - Fytolab
Certificate of pesticide multi-residue analysis by MSMS ... - Fytolab
Certificate of pesticide multi-residue analysis by MSMS ... - Fytolab
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<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>multi</strong>-<strong>residue</strong> <strong>analysis</strong><br />
<strong>by</strong> <strong>MSMS</strong> detection<br />
Multi-<strong>residue</strong> methods: all the mentioned substances will be searched for.<br />
The general reporting limit (RL) (mg/kg) is mentioned on the right side <strong>of</strong> each <strong>pesticide</strong>.<br />
The limit <strong>of</strong> quantification may vary depending on the matrix<br />
The abbreviated method name as used <strong>by</strong> the laboratory is mentioned in [brackets]. This<br />
certificate may only be used in correlation with this laboratory method code as mentioned on an<br />
<strong>analysis</strong>-report.<br />
New <strong>pesticide</strong>s or updates <strong>of</strong> the certificate are indicated in green<br />
For an up to date list <strong>of</strong> the accredited analyses or the current version <strong>of</strong> this document: check our<br />
website: www.fytolab.com.<br />
[GMS] Multi-<strong>residue</strong> method <strong>by</strong> GC-<strong>MSMS</strong> for 145 compounds, isomers and<br />
degradation products - quantification <strong>of</strong> <strong>pesticide</strong>s in fruit, vegetables and potatoes.<br />
(for cereals and cereal products use GMS4, for tobacco RL’s are doubled, other commodities<br />
on request)<br />
aclonifen – 0.02<br />
acrinathrin - 0.01<br />
alachlor – 0.01<br />
benalaxyl (including benalaxyl-M) - 0.01<br />
benfluralin – 0.01<br />
bifenazate – 0.05<br />
bifenox – 0.05<br />
bifenthrin - 0.01<br />
biphenyl – 0.1<br />
bromophos-ethyl - 0.01<br />
bromopropylate - 0.01<br />
butralin - 0.01<br />
cadusafos - 0.01<br />
carbophenothion - 0.02<br />
chinomethionate – 0.01<br />
chlordane (sum <strong>of</strong> cis +trans) - 0.01<br />
chlorfenapyr ** - 0.01<br />
chlorfenson – 0.01<br />
chlorobenzilate - 0.01<br />
chlorothalonil - 0.01<br />
chlorpropham (chlorpropham & 3-chloroaniline) – 0.01<br />
chlorpyriphos-ethyl - 0.005<br />
chlorpyriphos-methyl - 0.01<br />
chlorthal-dimethyl (DCPA) - 0.01<br />
chlozolinate - 0.01<br />
cyfluthrin (sum <strong>of</strong> isomers) - 0.01<br />
cyhal<strong>of</strong>op-butyl - 0.01<br />
cyhalothrin (lambda) - 0.01<br />
cypermethrin (sum <strong>of</strong> isomers) - 0.01<br />
DDD (o,p’) - 0.01<br />
DDE (o,p’) - 0.01<br />
DDT (sum <strong>of</strong> p,p´-DDT, o,p´-DDT, p-p´-DDE and p,p´-TDE<br />
(DDD) expressed as DDT) - 0.01<br />
deltamethrin - 0.01<br />
diazinon - 0.01<br />
dichl<strong>of</strong>luanid - 0.05<br />
dichlorvos - 0.01<br />
dicloran - 0.01<br />
dic<strong>of</strong>ol (sum <strong>of</strong> isomers) - 0.01<br />
dieldrin (sum <strong>of</strong> aldrin + dieldrin) - 0.01<br />
diphenylamine - 0.05<br />
ditalimfos - 0.01<br />
endosulfan (sum alfa + beta + -sulfate) - 0.01<br />
endrin - 0.05<br />
EPN - 0.01<br />
ethion - 0.01<br />
eth<strong>of</strong>umesate - 0.01<br />
ethopr<strong>of</strong>os - 0.008<br />
ethoxyquin - 0.01<br />
et<strong>of</strong>enprox - 0.01<br />
etrimfos - 0.01<br />
famoxadone - 0.02<br />
fenchlorphos - 0.01<br />
fenitrothion - 0.01<br />
fenpropathrin - 0.01<br />
fenpropimorph - 0.01<br />
fenvalerate (sum <strong>of</strong> isomers) - 0.01<br />
fipronil - 0.01<br />
flucythrinate (sum <strong>of</strong> isomers) - 0.01<br />
fludioxonil - 0.01<br />
flumetralin - 0.01<br />
fluvalinate-tau (sum <strong>of</strong> isomers) - 0.02<br />
formothion - 0.01<br />
HCH (sum <strong>of</strong> alfa + beta + delta + epsilon) - 0.01<br />
hexachlorobenzene (HCB) - 0.003<br />
iprodione - 0.02<br />
isocarbophos - 0.01<br />
is<strong>of</strong>enphos(-ethyl) - 0.01<br />
is<strong>of</strong>enphos-methyl - 0.01<br />
lindane (gamma HCH) - 0.01<br />
malathion (sum <strong>of</strong> malathion + malaoxon) - 0.01<br />
mecarbam ** - 0.01<br />
mepronil - 0.01<br />
methacrifos - 0.01<br />
methidathion - 0.01<br />
metrafenone - 0.01<br />
metribuzin - 0.01<br />
mevinphos (sum <strong>of</strong> isomers) - 0.01<br />
Date: 07 June 2010 G:\web\pdf\gms_lms_v24.doc<br />
1/6
mirex - 0.02<br />
nitr<strong>of</strong>en - 0.01<br />
nitrothal isopropyl - 0.01<br />
oxadiazon - 0.01<br />
oxychlordane - 0.01<br />
oxyfluorfen – 0.01<br />
paraoxon-ethyl - 0.05<br />
parathion-ethyl - 0.01<br />
parathion-methyl (sum <strong>of</strong> parathion-methyl + paraoxonmethyl)-<br />
0.01<br />
pendimethalin - 0.01<br />
pentachloroanisol - 0.01<br />
permethrin (sum <strong>of</strong> isomers) - 0.01<br />
phenylphenol (ortho-) - 0.05<br />
phorate - 0.01<br />
phosalone - 0.01<br />
phosmet ** - 0.01<br />
phoxim – 0.02<br />
piperonyl butoxide - 0.01<br />
pirimiphos-ethyl - 0.01<br />
pirimiphos-methyl - 0.01<br />
procymidone - 0.01<br />
pr<strong>of</strong>luralin - 0.01<br />
prometryn - 0.01<br />
**: not in tobacco<br />
<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>multi</strong>-<strong>residue</strong> <strong>analysis</strong><br />
<strong>by</strong> <strong>MSMS</strong> detection<br />
propargite ** - 0.01<br />
propyzamide - 0.01<br />
prothi<strong>of</strong>os - 0.01<br />
pyrazophos - 0.01<br />
pyridaben - 0.01<br />
pyriproxyfen - 0.01<br />
quinalphos - 0.01<br />
quinoxyfen - 0.01<br />
quintozene PCNB (sum <strong>of</strong> quintozene + pentachloroaniline)<br />
- 0.01<br />
silthi<strong>of</strong>am - 0.01<br />
spirodicl<strong>of</strong>en - 0.01<br />
spiromesifen ** - 0.01<br />
sulfotep - 0.01<br />
tecnazene - 0.01<br />
tefluthrin - 0.01<br />
terbuthylazine - 0.01<br />
tetrachlorvinphos - 0.01<br />
tetradifon - 0.01<br />
tolcl<strong>of</strong>os-methyl - 0.01<br />
tolylfluanid (sum <strong>of</strong> tolylfluanide + DMST) - 0.05<br />
trifluralin - 0.01<br />
vinclozolin (vinclozoline + 3,5-dichloroaniline) - 0.01<br />
[GMS4] Multi-<strong>residue</strong> method <strong>by</strong> GC-<strong>MSMS</strong> for 136 compounds, isomers and<br />
degradation products - quantification <strong>of</strong> <strong>pesticide</strong>s in cereals and cereal products<br />
(other commodities on request)<br />
aclonifen – 0.02<br />
acrinathrin - 0.01<br />
alachlor – 0.01<br />
benalaxyl (including benalaxyl-M) - 0.01<br />
benfluralin – 0.01<br />
bifenazate – 0.05<br />
bifenox – 0.05<br />
bifenthrin - 0.01<br />
biphenyl – 0.1<br />
bromophos-ethyl - 0.01<br />
bromopropylate - 0.01<br />
butralin - 0.01<br />
cadusafos - 0.01<br />
carbophenothion - 0.01<br />
chinomethionate – 0.01<br />
chlordane (sum <strong>of</strong> cis + trans) - 0.02<br />
chlorfenapyr - 0.01<br />
chlorfenson – 0.01<br />
chlorobenzilate - 0.01<br />
chlorothalonil - 0.01<br />
chlorpropham (chlorpropham & 3-chloroaniline) - 0.01<br />
chlorpyriphos-ethyl - 0.005<br />
chlorpyriphos-methyl - 0.01<br />
chlorthal-dimethyl (DCPA) - 0.01<br />
chlozolinate - 0.01<br />
cyfluthrin (sum <strong>of</strong> isomers) - 0.01<br />
cyhal<strong>of</strong>op-butyl - 0.01<br />
cyhalothrin (lambda) - 0.01<br />
cypermethrin (sum <strong>of</strong> isomers) - 0.01<br />
DDD (o,p’) - 0.01<br />
DDE (o,p’) - 0.01<br />
DDT (sum <strong>of</strong> p,p´-DDT, o,p´-DDT, p-p´-DDE and p,p´-<br />
TDE (DDD) expressed as DDT) - 0.01<br />
deltamethrin - 0.01<br />
diazinon - 0.01<br />
dichlorvos - 0.01<br />
dicloran - 0.01<br />
dieldrin (sum <strong>of</strong> dieldrin + aldrin) - 0.025<br />
diphenylamine - 0.05<br />
ditalimfos - 0.01<br />
endosulfan (sum <strong>of</strong> alfa +beta + -sulfate) - 0.01<br />
endrin – 0.05<br />
EPN - 0.01<br />
ethion - 0.01<br />
eth<strong>of</strong>umesate - 0.01<br />
ethopr<strong>of</strong>os - 0.008<br />
Date: 07 June 2010 G:\web\pdf\gms_lms_v24.doc<br />
2/6
ethoxyquin – 0.01<br />
et<strong>of</strong>enprox - 0.01<br />
etrimfos - 0.01<br />
famoxadone – 0.02<br />
fenchlorphos - 0.01<br />
fenitrothion - 0.01<br />
fenpropathrin - 0.01<br />
fenpropimorph - 0.01<br />
fenvalerate (sum <strong>of</strong> isomers) - 0.01<br />
fipronil - 0.01<br />
flucythrinate (sum <strong>of</strong> isomers) - 0.01<br />
fludioxonil - 0.01<br />
flumetralin - 0.01<br />
fluvalinate-tau (sum <strong>of</strong> isomers) - 0.02<br />
formothion - 0.01<br />
HCH (sum <strong>of</strong> alfa + beta + delta + epsilon) – 0.01<br />
hexachlorobenzene (HCB) - 0.003<br />
iprodione - 0.02<br />
isocarbophos - 0.01<br />
is<strong>of</strong>enphos(-ethyl) - 0.01<br />
is<strong>of</strong>enphos-methyl - 0.01<br />
lindane (gamma HCH) – 0.01<br />
malathion (malathion + malaoxon) - 0.01<br />
mecarbam - 0.01<br />
mepronil - 0.01<br />
methacrifos - 0.01<br />
methidathion - 0.01<br />
metrafenone - 0.01<br />
metribuzin - 0.01<br />
mevinphos (sum <strong>of</strong> isomers) - 0.01<br />
nitr<strong>of</strong>en - 0.01<br />
nitrothal isopropyl - 0.01<br />
oxadiazon – 0.01<br />
oxychlordane - 0.01<br />
oxyfluorfen – 0.01<br />
paraoxon-ethyl - 0.05<br />
parathion-ethyl - 0.01<br />
<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>multi</strong>-<strong>residue</strong> <strong>analysis</strong><br />
<strong>by</strong> <strong>MSMS</strong> detection<br />
parathion-methyl (sum <strong>of</strong> parathion-methyl +<br />
paraoxon-methyl) - 0.01<br />
pendimethalin - 0.01<br />
pentachloranisol - 0.01<br />
permethrin (sum <strong>of</strong> isomers) - 0.01<br />
phenylphenol (ortho-) - 0.05<br />
phorate - 0.01<br />
phosalone - 0.01<br />
phosmet - 0.01<br />
phoxim – 0.02<br />
piperonyl butoxide - 0.01<br />
pirimiphos-ethyl - 0.01<br />
pirimiphos-methyl - 0.01<br />
procymidone - 0.01<br />
pr<strong>of</strong>luralin - 0.01<br />
prometryn - 0.01<br />
propargite - 0.025<br />
propyzamide - 0.01<br />
prothi<strong>of</strong>os - 0.01<br />
pyrazophos - 0.01<br />
pyridaben - 0.01<br />
pyriproxyfen - 0.01<br />
quinalphos - 0.01<br />
quinoxyfen - 0.01<br />
quintozene PCNB (sum <strong>of</strong> quintozene + pentachloroaniline)<br />
- 0.01<br />
silthi<strong>of</strong>am - 0.01<br />
spirodicl<strong>of</strong>en - 0.01<br />
spiromesifen - 0.01<br />
sulfotep - 0.01<br />
tecnazene - 0.01<br />
tefluthrin - 0.01<br />
terbuthylazine - 0.01<br />
tetrachlorvinphos - 0.01<br />
tetradifon - 0.01<br />
tolcl<strong>of</strong>os-methyl - 0.01<br />
trifluralin - 0.01<br />
vinclozolin (vinclozolin + 3,5-dichloroaniline) - 0.01<br />
[LMS] Multi-<strong>residue</strong> method <strong>by</strong> LC-<strong>MSMS</strong> for 250 compounds, isomers and<br />
degradation products - quantification <strong>of</strong> <strong>pesticide</strong>s in fruit, vegetables, potatoes and<br />
cereals (for tobacco RL’s are doubled, other commodities on request)<br />
6-benzylaminopurine – 0.01<br />
acephate - 0.02<br />
acetamiprid - 0.01<br />
acibenzolar-S-methyl - 0.01<br />
aldicarb (sum <strong>of</strong> aldicarb + -sulfon + -sulfoxide) - 0.01<br />
allethrin – 0.01<br />
ametryn – 0.01<br />
amidosulfuron – 0.01<br />
atrazine – 0.01<br />
azaconazole – 0.01<br />
azadirachtin – 0.01<br />
azamethiphos - 0.01<br />
azimsulfuron - 0.01<br />
azinphos-ethyl - 0.01<br />
azinphos-methyl - 0.01<br />
azoxystrobin - 0.01<br />
beflubutamid – 0.01<br />
bendiocarb – 0.01<br />
benfuracarb * - 0.01<br />
benthiavalicarb-isopropyl - 0.01<br />
bitertanol – 0.02<br />
boscalid (nicobifen) - 0.02<br />
bromacil – 0.02<br />
bromfenvinphos-methyl – 0.01<br />
Date: 07 June 2010 G:\web\pdf\gms_lms_v24.doc<br />
3/6
omuconazole - 0.01<br />
bupirimate – 0.01<br />
bupr<strong>of</strong>ezin – 0.01<br />
carbaryl ** - 0.01<br />
carbendazim (sum <strong>of</strong> carbendazim + benomyl) - 0.01<br />
carbetamide – 0.01<br />
carb<strong>of</strong>uran (sum <strong>of</strong> carb<strong>of</strong>uran + 3-hydroxy-carb<strong>of</strong>uran)<br />
– 0.01<br />
carbosulfan – 0.05<br />
carboxin – 0.01<br />
carfentrazone-ethyl - 0.01<br />
chlorantraniliprole – 0.01<br />
chlorbromuron - 0.01<br />
chlorfenvinphos – 0.01<br />
chlorfluazuron – 0.01<br />
chloridazon - 0.01<br />
chloroxuron - 0.01<br />
chlorsulfuron – 0.01<br />
chlortoluron - 0.01<br />
cl<strong>of</strong>entezine - 0.01<br />
clomazone – 0.01<br />
cloquintocet-mexyl – 0.01<br />
clothianidin - 0.01<br />
cyaz<strong>of</strong>amid - 0.01<br />
cymiazole - 0.01<br />
cymoxanil – 0.01<br />
cyproconazole - 0.01<br />
cyprodinil – 0.01<br />
demeton-S-methyl- 0.006<br />
dichl<strong>of</strong>enthion – 0.01<br />
dicrotophos - 0.01<br />
dieth<strong>of</strong>encarb – 0.01<br />
difenoconazole - 0.01<br />
diflubenzuron - 0.01<br />
dimethenamid – 0.01<br />
dimethoate (sum <strong>of</strong> dimethoate & omethoate) - 0.01<br />
dimethomorph - 0.01<br />
dimoxystrobin - 0.01<br />
diniconazole - 0.01<br />
disulfoton (sum <strong>of</strong> disulfoton + -sulfone + -sulfoxide) -<br />
0.01<br />
diuron - 0.01<br />
dodemorph – 0.01<br />
dodine - 0.02<br />
epoxiconazole - 0.01<br />
ethi<strong>of</strong>encarb - 0.01<br />
ethi<strong>of</strong>encarb-sulfon – 0.01<br />
ethi<strong>of</strong>encarb-sulfoxide – 0.01<br />
ethirimol - 0.01<br />
etoxazole - 0.01<br />
fenamidone - 0.01<br />
fenamiphos (sum <strong>of</strong> fenamiphos, -sulfone & -sulfoxide) -<br />
0.02<br />
fenarimol – 0.01<br />
fenazaquin – 0.01<br />
fenbuconazole - 0.01<br />
<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>multi</strong>-<strong>residue</strong> <strong>analysis</strong><br />
<strong>by</strong> <strong>MSMS</strong> detection<br />
fenhexamide - 0.01<br />
fenobucarb – 0.01<br />
fenoxaprop-P-ethyl – 0.01<br />
fenoxycarb - 0.01<br />
fenpropidin – 0.01<br />
fenpyroximate - 0.01<br />
fensulfothion – 0.01<br />
fensulfothion-sulfon – 0.01<br />
fenthion (sum <strong>of</strong> fenthion + -sulfon + -sulfoxide) – 0.01<br />
fenuron - 0.01<br />
florasulam – 0.01<br />
flazasulfuron – 0.01<br />
flonicamid - 0.01<br />
fluazifop-P-butyl (sum <strong>of</strong> fluazifop-P-butyl + free acid) –<br />
0.01<br />
fluazinam - 0.02<br />
flufenacet - 0.01<br />
flufenoxuron - 0.01<br />
fluopicolide – 0.01<br />
fluoxastrobin - 0.01<br />
flupyrsulfuron-methyl-Na – 0.01<br />
fluquinconazole - 0.01<br />
flurochloridone – 0.01<br />
fluroxypyr - 0.02<br />
flurtamone – 0.01<br />
flusilazole - 0.01<br />
flutolanil – 0.01<br />
flutriafol – 0.01<br />
fon<strong>of</strong>os – 0.01<br />
foramsulfuron* – 0.01<br />
forchlorfenuron - 0.01<br />
fosthiazate - 0.01<br />
fuberidazole - 0.01<br />
furalaxyl – 0.01<br />
furathiocarb - 0.01<br />
haloxyfop-methyl (sum <strong>of</strong> haloxyfop-methyl + free acid)<br />
– 0.01<br />
heptenophos – 0.01<br />
hexaconazole - 0.01<br />
hexazinone – 0.01<br />
hexythiazox - 0.01<br />
imazalil (=enilconazole) - 0.01<br />
imazamox *** – 0.01<br />
imidacloprid - 0.01<br />
indoxacarb (sum <strong>of</strong> S & R isomers) - 0.01<br />
iodosulfuron-methyl-sodium - 0.01<br />
iprovalicarb - 0.01<br />
isoprothiolane – 0.01<br />
isoproturon - 0.01<br />
isoxaben - 0.01<br />
kresoxim-methyl – 0.01<br />
lenacil – 0.01<br />
linuron - 0.01<br />
lufenuron - 0.02<br />
mandipropamid – 0.01<br />
mefenpyr-diethyl – 0.01<br />
Date: 07 June 2010 G:\web\pdf\gms_lms_v24.doc<br />
4/6
mepanipyrim – 0.01<br />
metaflumizone – 0.01<br />
metalaxyl (sum <strong>of</strong> metalaxyl & metalaxyl-M) - 0.01<br />
metamitron - 0.01<br />
metazachlor – 0.01<br />
metconazole - 0.01<br />
methabenzthiazuron - 0.01<br />
methamidophos - 0.01<br />
methiocarb (sum <strong>of</strong> methiocarb + -sulfon + -sulfoxide) -<br />
0.01<br />
methomyl (sum <strong>of</strong> methomyl + thiodicarb) - 0.01<br />
methoxyfenozide - 0.01<br />
metobromuron - 0.01<br />
metolachlor - 0.01<br />
metoxuron - 0.01<br />
metsulfuron-methyl - 0.01<br />
molinate - 0.01<br />
monocrotophos - 0.01<br />
monolinuron - 0.02<br />
myclobutanil – 0.01<br />
napropamide – 0.01<br />
nicosulfuron - 0.01<br />
nitenpyram – 0.01<br />
novaluron – 0.01<br />
nuarimol – 0.01<br />
<strong>of</strong>urace – 0.01<br />
omethoate - 0.003<br />
oxadixyl – 0.02<br />
oxamyl - 0.01<br />
oxydemeton-methyl<br />
(oxydemeton-methyl + demeton-S-methylsulfone) -<br />
0.006<br />
paclobutrazol - 0.01<br />
penconazole – 0.01<br />
pencycuron – 0.01<br />
pethoxamid – 0.01<br />
phenmedipham ** - 0.01<br />
phenthoate ** - 0.01<br />
phosphamidon - 0.01<br />
picolinafen - 0.01<br />
picoxystrobin - 0.01<br />
pinoxaden – 0.01<br />
pirimicarb (sum <strong>of</strong> pirimicarb + pirimicarb-desmethyl) -<br />
0.01<br />
prochloraz - 0.01<br />
pr<strong>of</strong>en<strong>of</strong>os – 0.01<br />
promecarb – 0.01<br />
propachlor – 0.01<br />
propaquizafop – 0.01<br />
propham – 0.01<br />
*: not in acidic matrices<br />
**: not in tobacco<br />
***: not in cereals<br />
<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>multi</strong>-<strong>residue</strong> <strong>analysis</strong><br />
<strong>by</strong> <strong>MSMS</strong> detection<br />
propiconazole - 0.01<br />
propoxur – 0.01<br />
proquinazid – 0.01<br />
prosulfocarb - 0.01<br />
prosulfuron - 0.01<br />
pymetrozine * - 0.01<br />
pyraclostrobin – 0.01<br />
pyraflufen-ethyl – 0.01<br />
pyridaphenthion - 0.01<br />
pyrifenox - 0.01<br />
pyrimethanil – 0.01<br />
quinclorac – 0.01<br />
quizal<strong>of</strong>op-ethyl – 0.01<br />
quizal<strong>of</strong>op – 0.01<br />
rimsulfuron – 0.01<br />
rotenone - 0.01<br />
simazine – 0.01<br />
spinosad (sum <strong>of</strong> spinosin A & D) - 0.01<br />
spirotetramat – 0.01<br />
spiroxamine - 0.01<br />
sulfosulfuron – 0.01<br />
tebuconazole - 0.01<br />
tebufenozide - 0.01<br />
tebufenpyrad - 0.01<br />
tepraloxydim – 0.01<br />
terbufos – 0.01<br />
tetraconazole - 0.01<br />
tetramethrin – 0.01<br />
thiabendazole - 0.01<br />
thiacloprid - 0.01<br />
thiamethoxam (sum <strong>of</strong> thiametoxam + clothianidin) -<br />
0.02<br />
thifensulfuron-methyl - 0.01<br />
thiophanate-methyl - 0.05<br />
triadimefon + triadimenol (sum) - 0.01<br />
triasulfuron - 0.01<br />
triazophos – 0.01<br />
tribenuron-methyl – 0.02<br />
trichlorfon - 0.01<br />
tricyclazole – 0.01<br />
tridemorph - 0.01<br />
trifloxystrobin - 0.01<br />
triflumizole - 0.01<br />
triflumuron – 0.01<br />
triflusulfuron-methyl – 0.01<br />
triforine - 0.01<br />
trinexapac-ethyl - 0.01<br />
triticonazole – 0.01<br />
vamidothion - 0.01<br />
zoxamide - 0.01<br />
Date: 07 June 2010 G:\web\pdf\gms_lms_v24.doc<br />
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<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>multi</strong>-<strong>residue</strong> <strong>analysis</strong><br />
<strong>by</strong> <strong>MSMS</strong> detection<br />
[LMS2] Multi-<strong>residue</strong> method, <strong>by</strong> LC-<strong>MSMS</strong> in negative mode for 22 compounds,<br />
isomers and degradation products - quantification <strong>of</strong> selected <strong>pesticide</strong>s (majority<br />
acidic herbicides) in fruit, vegetables, potatoes and cereals (other commodities on<br />
request)<br />
2,4-D - 0.01<br />
2,4-DB - 0.01<br />
4-CPA - 0.01<br />
2,4,5-T - 0.01<br />
bentazone - 0.01<br />
bromoxynil - 0.01<br />
clopyralid (3,6-DCP) - 0.2<br />
dicamba - 0.01<br />
dichlorophen - 0.01<br />
dichlorprop (2,4-DP) - 0.01<br />
dinocap - 0.1<br />
* : only on pear, LOD value<br />
dithianon – 0.25 *<br />
hexaflumuron - 0.01<br />
ioxynil - 0.01<br />
MCPA - 0.01<br />
MCPB - 0.01<br />
mecoprop (MCPP) - 0.01<br />
picloram - 0.05<br />
prohexadione-Ca - 0.2<br />
sulfentrazone - 0.01<br />
teflubenzuron - 0.01<br />
triflumuron - 0.01<br />
Date: 07 June 2010 G:\web\pdf\gms_lms_v24.doc<br />
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