Certificate of pesticide residue analysis cereals, cereal ... - Fytolab
Certificate of pesticide residue analysis cereals, cereal ... - Fytolab
Certificate of pesticide residue analysis cereals, cereal ... - Fytolab
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<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>residue</strong> <strong>analysis</strong><br />
<strong><strong>cereal</strong>s</strong>, <strong>cereal</strong> products and fatty products<br />
Multi-<strong>residue</strong> methods: all the mentioned substances will be searched for.<br />
The general reporting limit (RL) (mg/kg) is mentioned on the right side <strong>of</strong> each <strong>pesticide</strong>.<br />
The limit <strong>of</strong> quantification may vary depending on the matrix<br />
The abbreviated method name as used by the laboratory is mentioned in [brackets]. This<br />
certificate may only be used in correlation with this laboratory method code as mentioned on an<br />
<strong>analysis</strong>-report.<br />
New <strong>pesticide</strong>s or updates <strong>of</strong> the certificate are indicated in green<br />
For an up to date list <strong>of</strong> the accredited analyses or the current version <strong>of</strong> this document: check our<br />
website: www.fytolab.com.<br />
[CL2] Multi-<strong>residue</strong> method for the determination <strong>of</strong> organochlorine <strong>pesticide</strong>s in <strong><strong>cereal</strong>s</strong> and<br />
fatty products (milk, eggs, butter, oil,...) - to be used as babyfood ingredient- and some special<br />
matrices like spices and herbs.<br />
aldrin - 0.01 [0.001]<br />
chlordane (cis+trans+oxy-) - 0.02 [0.002]<br />
pp'-DDE - 0.01 [0.001]<br />
pp'-DDD (TDE) - 0.01 [0.002]<br />
pp'-DDT - 0.02 [0.002]<br />
op-DDT - 0.01 [0.002]<br />
DDT (sum) - 0.01 [0.001]<br />
dieldrin - 0.01 [0.001]<br />
α-endosulfan - 0.05 [0.002]<br />
endrin (sum) - 0.01 [0.002]<br />
RL for milk between [brackets]<br />
HCB - 0.005 [0.001]<br />
HCH (sum) - 0.005 [0.001]<br />
alfa-HCH - 0.005 [0.001]<br />
beta-HCH - 0.01 [0.002]<br />
heptachlor (sum) - 0.01 [0.001]<br />
lindane (gamma HCH) - 0.005 [0.001]<br />
nitr<strong>of</strong>en - 0.005 [0.002]<br />
pentachloraniline (PCA) - 0.01 [0.001]<br />
quintozene (PCNB) - 0.01 [0.001]<br />
quintozene (sum) - 0.01 [0.001]<br />
[GMS2] Multi-<strong>residue</strong> method for the quantification <strong>of</strong> <strong>pesticide</strong>s by GC-MSMS in vegetable oil<br />
(complementary to GMS3)<br />
aclonifen – 0.02<br />
alachlor – 0.01<br />
benalaxyl (including benalaxyl-M) - 0.01<br />
bifenazate – 0.05<br />
bifenox – 0.05<br />
biphenyl – 0.1<br />
bromophos-ethyl - 0.01<br />
bromopropylate - 0.01<br />
cadusafos – 0.01<br />
chinomethionate – 0.01<br />
chlordane (sum <strong>of</strong> cis + trans) – 0.01<br />
chlorfenson – 0.01<br />
chlorobenzilate – 0.01<br />
chlorothalonil - 0.01<br />
chlorpropham (chlorpropham + 3-chloroaniline) -<br />
0.01<br />
chlorpyriphos-ethyl - 0.01<br />
chlorpyriphos-methyl - 0.01<br />
chlorthal-dimethyl (DCPA) - 0.01<br />
chlozolinate - 0.01<br />
cyhal<strong>of</strong>op-butyl – 0.01<br />
DDD (o,p’) - 0.01<br />
DDE (o,p’) - 0.01<br />
DDT (sum <strong>of</strong> p,p´-DDT, o,p´-DDT, p-p´-DDE and p,p´-<br />
TDE (DDD) expressed as DDT) - 0.01<br />
diazinon - 0.01<br />
dichl<strong>of</strong>luanid - 0.05<br />
dichlorvos - 0.01<br />
dicloran - 0.01<br />
dic<strong>of</strong>ol (total) - 0.01<br />
dieldrin (sum <strong>of</strong> dieldrin + aldrin) - 0.01<br />
diphenylamine - 0.05<br />
ditalimfos – 0.01<br />
endosulfan (sum <strong>of</strong> alfa +beta + -sulfate) - 0.01<br />
endrin - 0.05<br />
EPN - 0.01<br />
ethion - 0.01<br />
eth<strong>of</strong>umesate - 0.01<br />
ethoprophos - 0.01<br />
ethoxyquin - 0.01<br />
et<strong>of</strong>enprox – 0.01<br />
etrimfos - 0.01<br />
famoxadone – 0.02<br />
fenchlorphos - 0.01<br />
fenitrothion - 0.01<br />
fludioxonil - 0.01<br />
formothion - 0.01<br />
HCH (sum <strong>of</strong> alfa + beta + delta + epsilon) - 0.01<br />
hexachlorobenzene - 0.01<br />
iprodione - 0.02<br />
isocarbophos - 0.01<br />
is<strong>of</strong>enphos(-ethyl) - 0.01<br />
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is<strong>of</strong>enphos-methyl - 0.01<br />
lindane - 0.01<br />
malathion (malathion + malaoxon) - 0.01<br />
mecarbam - 0.01<br />
mepronil - 0.01<br />
methacrifos – 0.01<br />
methidathion - 0.01<br />
metrafenone – 0.01<br />
metribuzin – 0.01<br />
mevinphos (sum <strong>of</strong> isomers) - 0.01<br />
mirex - 0.02<br />
nitr<strong>of</strong>en - 0.01<br />
oxadiazon – 0.01<br />
oxyfluorfen – 0.01<br />
paraoxon-ethyl - 0.05<br />
parathion-ethyl - 0.01<br />
parathion-methyl (sum <strong>of</strong> parathion-methyl +<br />
paraoxon-methyl) - 0.01<br />
pendimethalin - 0.01<br />
pentachloranisol – 0.01<br />
phenylphenol (ortho-) - 0.05<br />
phosalone - 0.01<br />
phosmet - 0.01<br />
phoxim – 0.02<br />
<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>residue</strong> <strong>analysis</strong><br />
<strong><strong>cereal</strong>s</strong>, <strong>cereal</strong> products and fatty products<br />
piperonyl butoxide - 0.01<br />
pirimiphos-ethyl - 0.01<br />
pirimiphos-methyl - 0.01<br />
procymidone - 0.01<br />
prometryn - 0.01<br />
propyzamide - 0.01<br />
prothi<strong>of</strong>os – 0.01<br />
pyrazophos - 0.01<br />
pyriproxyfen - 0.01<br />
quinalphos – 0.01<br />
quinoxyfen - 0.01<br />
quintozene PCNB (sum <strong>of</strong> quintozene + pentachloroaniline)<br />
- 0.01<br />
silthi<strong>of</strong>am – 0.01<br />
spirodicl<strong>of</strong>en – 0.01<br />
spiromesifen – 0.01<br />
sulfotep - 0.01<br />
tecnazene - 0.01<br />
terbuthylazine – 0.01<br />
tetrachlorvinphos - 0.01<br />
tetradifon - 0.01<br />
tolcl<strong>of</strong>os-methyl - 0.01<br />
tolylfluanid (sum <strong>of</strong> tolyfluanid + DMST) - 0.05<br />
vinclozolin - 0.01<br />
[GMS3] Multi-<strong>residue</strong> method for the quantification <strong>of</strong> <strong>pesticide</strong>s (mainly pyrethroids) by GC-<br />
MSMS in fatty products like oils, cacao, babyfood, meat, milk, ... (complementary to GMS2)<br />
acrinathrin - 0.01<br />
benfluralin – 0.01<br />
bifenthrin - 0.01<br />
butralin - 0.01<br />
carbophenothion – 0.02<br />
chlorfenapyr – 0.01<br />
cyfluthrin total - 0.01<br />
cyhalothrin (lambda) - 0.01<br />
cypermethrin (sum <strong>of</strong> isomers) - 0.01<br />
deltamethrin - 0.01<br />
fenpropathrin - 0.01<br />
fenvalerate (sum <strong>of</strong> isomers) - 0.01<br />
flucythrinate (sum <strong>of</strong> isomers) - 0.01<br />
flumetralin - 0.01<br />
fluvalinate-tau total - 0.02<br />
nitrothal isopropyl - 0.01<br />
oxychlordane - 0.01<br />
permethrin (sum cis+trans) - 0.01<br />
phorate - 0.01<br />
pr<strong>of</strong>luralin – 0.01<br />
propargite - 0.01<br />
pyridaben - 0.01<br />
tefluthrin - 0.02<br />
trifluralin - 0.01<br />
[GMS4] Multi-<strong>residue</strong> method by GC-MSMS for 136 compounds, isomers and<br />
degradation products - quantification <strong>of</strong> <strong>pesticide</strong>s in <strong><strong>cereal</strong>s</strong> and <strong>cereal</strong> products<br />
(other commodities on request)<br />
aclonifen – 0.01<br />
acrinathrin - 0.01<br />
alachlor – 0.01<br />
benalaxyl (including benalaxyl-M) - 0.01<br />
benfluralin – 0.01<br />
bifenazate – 0.05<br />
bifenox – 0.01<br />
bifenthrin - 0.01<br />
biphenyl – 0.1<br />
bromophos-ethyl - 0.01<br />
bromopropylate - 0.01<br />
butralin - 0.01<br />
cadusafos - 0.006<br />
carbophenothion - 0.01<br />
chinomethionate – 0.01<br />
chlordane (sum <strong>of</strong> cis + trans) - 0.01<br />
chlorfenapyr - 0.01<br />
chlorfenson – 0.01<br />
chlorobenzilate - 0.01<br />
chlorothalonil - 0.01<br />
chlorpropham (chlorpropham & 3-chloroaniline) - 0.01<br />
chlorpyriphos-ethyl - 0.005<br />
chlorpyriphos-methyl - 0.01<br />
chlorthal-dimethyl (DCPA) - 0.01<br />
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chlozolinate - 0.01<br />
cyfluthrin (sum <strong>of</strong> isomers) - 0.01<br />
cyhal<strong>of</strong>op-butyl - 0.01<br />
cyhalothrin (lambda) - 0.01<br />
cypermethrin (sum <strong>of</strong> isomers) - 0.01<br />
DDD (o,p’) - 0.01<br />
DDE (o,p’) - 0.01<br />
DDT (sum <strong>of</strong> p,p´-DDT, o,p´-DDT, p-p´-DDE and p,p´-<br />
TDE (DDD) expressed as DDT) - 0.01<br />
deltamethrin - 0.01<br />
diazinon - 0.01<br />
dichlorvos - 0.01<br />
dicloran - 0.01<br />
dieldrin (sum <strong>of</strong> dieldrin + aldrin) – 0.01<br />
diphenylamine - 0.05<br />
ditalimfos - 0.01<br />
endosulfan (sum <strong>of</strong> alfa +beta + -sulfate) - 0.01<br />
endrin – 0.05<br />
EPN - 0.01<br />
ethion - 0.01<br />
eth<strong>of</strong>umesate - 0.01<br />
ethopr<strong>of</strong>os - 0.008<br />
ethoxyquin – 0.01<br />
et<strong>of</strong>enprox - 0.01<br />
etrimfos - 0.01<br />
famoxadone – 0.01<br />
fenchlorphos - 0.01<br />
fenitrothion - 0.01<br />
fenpropathrin - 0.01<br />
fenpropimorph - 0.01<br />
fenvalerate (sum <strong>of</strong> isomers) - 0.01<br />
fipronil - 0.004<br />
flucythrinate (sum <strong>of</strong> isomers) - 0.01<br />
fludioxonil - 0.01<br />
flumetralin - 0.01<br />
fluvalinate-tau (sum <strong>of</strong> isomers) - 0.01<br />
formothion - 0.01<br />
HCH (sum <strong>of</strong> alfa + beta + delta + epsilon) – 0.01<br />
hexachlorobenzene (HCB) - 0.003<br />
iprodione - 0.01<br />
isocarbophos - 0.01<br />
is<strong>of</strong>enphos(-ethyl) - 0.01<br />
is<strong>of</strong>enphos-methyl - 0.01<br />
lindane (gamma HCH) – 0.01<br />
malathion (malathion + malaoxon) - 0.01<br />
mecarbam - 0.02<br />
mepronil - 0.01<br />
methacrifos - 0.01<br />
methidathion - 0.01<br />
<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>residue</strong> <strong>analysis</strong><br />
<strong><strong>cereal</strong>s</strong>, <strong>cereal</strong> products and fatty products<br />
metrafenone - 0.01<br />
metribuzin - 0.01<br />
mevinphos (sum <strong>of</strong> isomers) - 0.01<br />
nitr<strong>of</strong>en - 0.003<br />
nitrothal isopropyl - 0.01<br />
oxadiazon – 0.01<br />
oxychlordane - 0.01<br />
oxyfluorfen – 0.01<br />
paraoxon-ethyl - 0.05<br />
parathion-ethyl - 0.01<br />
parathion-methyl (sum <strong>of</strong> parathion-methyl +<br />
paraoxon-methyl) - 0.01<br />
pendimethalin - 0.01<br />
pentachloranisol - 0.01<br />
permethrin (sum <strong>of</strong> isomers) - 0.01<br />
phenylphenol (ortho-) - 0.05<br />
phorate - 0.01<br />
phosalone - 0.01<br />
phosmet - 0.01<br />
phoxim – 0.02<br />
piperonyl butoxide - 0.01<br />
pirimiphos-ethyl - 0.01<br />
pirimiphos-methyl - 0.01<br />
procymidone - 0.01<br />
pr<strong>of</strong>luralin - 0.01<br />
prometryn - 0.01<br />
propargite – 0.05<br />
propyzamide - 0.01<br />
prothi<strong>of</strong>os - 0.01<br />
pyrazophos - 0.01<br />
pyridaben - 0.01<br />
pyriproxyfen - 0.01<br />
quinalphos - 0.01<br />
quinoxyfen - 0.01<br />
quintozene PCNB (sum <strong>of</strong> quintozene + pentachloroaniline)<br />
- 0.01<br />
silthi<strong>of</strong>am - 0.01<br />
spirodicl<strong>of</strong>en - 0.01<br />
spiromesifen - 0.01<br />
sulfotep - 0.01<br />
tecnazene - 0.01<br />
tefluthrin - 0.01<br />
terbuthylazine - 0.01<br />
tetrachlorvinphos - 0.01<br />
tetradifon - 0.01<br />
tolcl<strong>of</strong>os-methyl - 0.01<br />
trifluralin - 0.01<br />
vinclozolin - 0.01<br />
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<strong>Certificate</strong> <strong>of</strong> <strong>pesticide</strong> <strong>residue</strong> <strong>analysis</strong><br />
<strong><strong>cereal</strong>s</strong>, <strong>cereal</strong> products and fatty products<br />
[P2] Multi-<strong>residue</strong> method for the determination <strong>of</strong> organophosphorus <strong>pesticide</strong>s in <strong><strong>cereal</strong>s</strong><br />
and cerea products - to be used as babyfood ingredient. This method is also applicable (and<br />
validated) for seeds. milk, oil, meat, liver, ... with matrix-dependant RL’s (all in the same order <strong>of</strong><br />
magnitude <strong>of</strong> <strong><strong>cereal</strong>s</strong>)<br />
chlorpyrifos - 0.01<br />
chlorpyrifos-methyl - 0.01<br />
diazinon - 0.01<br />
dichl<strong>of</strong>enthion - 0.01<br />
dichlorvos - 0.01<br />
ethion - 0.01<br />
ethopr<strong>of</strong>os - 0.01<br />
etrimfos - 0.01<br />
fenchlorfos - 0.01<br />
fenitrothion - 0.01<br />
hepten<strong>of</strong>os - 0.01<br />
malathion - 0.01<br />
methidathion - 0.01<br />
mevinphos - 0.02<br />
parathion - 0.01<br />
parathion-methyl - 0.01<br />
pirimiphos-ethyl - 0.01<br />
pirimiphos-methyl - 0.01<br />
sulfotep - 0.01<br />
Specific individual methods for the determination <strong>of</strong> <strong>residue</strong>s <strong>of</strong> <strong>pesticide</strong>s in fatty products<br />
and tobacco.<br />
benzo[a]pyrene - 0.01<br />
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