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Cycling Studies Dehydrogenation: Ramp from 25 o C to 200 o C, 15 psia H 2 Hydrogenation: 170 o C, 1200 psia H 2 N-ethylcarbazole CH 3 N Cycle 1 Cycle 2 Cycle 3 Rapid hydrogenation and cycling stability 14 © Air Products and Chemicals, Inc, 2006
Understanding the Mechanism - 2H 2 -2H 2 - 2 H 2 N + 2 H 2 N + 2 H 2 N + 2 H 2 N (11.3)* (12.4)* (12.8)* ( )* : ∆H calc. (B3LYP/G-311G**) in Kcal/mol H 2 ∆H exp. (overall) = 12.2 kcal/mole H 2 15 © Air Products and Chemicals, Inc, 2006
Page 1 and 2: © Air Products and Chemicals, Inc,
Page 3 and 4: Air Products’ Hydrogen Experience
Page 5 and 6: An Integrated Production, Storage a
Page 7 and 8: Partial List of Organic “Liquid C
Page 9 and 10: Fundamental Energetics for Containi
Page 11 and 12: Enthalpies of Hydrogenation as Func
Page 13: Flow Measurement of Hydrogen Genera
Page 17 and 18: Dehydrogenation Flow Reactor Test S
Page 19 and 20: H 2 Purity from Continuous Flow Deh
Page 21 and 22: Perhydro-Nethylcarbazole Conformers
Page 23 and 24: Increasing Capacity: Hydrogen Gener
Page 25 and 26: Phenanthrolene Dehydrogenation N N
Page 27 and 28: Summary and Conclusions ‣ Liquid
Page 29 and 30: Thank you © Air Products and Chemi

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