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PG580RM Potentiostat-Galvanostat - Andreescu Labor & Soft

PG580RM Potentiostat-Galvanostat - Andreescu Labor & Soft

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<strong>PG580RM</strong><br />

<strong>Potentiostat</strong>-<strong>Galvanostat</strong><br />

Multi-Channel<br />

The Uniscan <strong>PG580RM</strong> is a high quality, digital scanning<br />

multi-channel potentiostat system. The design provides<br />

a user-configurable instrument for demanding research<br />

applications.<br />

Research laboratory performance<br />

From 2 channel to 14 channel operation<br />

System configurations up to 98-channels<br />

USB connection<br />

User programmable techniques via powerful macroprogramming<br />

language<br />

Ultra-low noise, low current performance<br />

Multi-channel and multiplexing capabilities<br />

Powerful Windows TM software with full suite of<br />

electrochemical and corrosion techniques<br />

The design of the <strong>PG580RM</strong> makes it an ideal choice for<br />

use in the following application areas<br />

Materials characterisation<br />

Electrochemical sensors<br />

Combinatorial electrochemistry<br />

Screening of fuel-cell catalysts<br />

Microbial influenced corrosion studies<br />

Multichannel measurements of pH and chloride<br />

concentrations in corrosion studies<br />

uniscan instruments<br />

www.uniscan.com


Features<br />

High throughput combinatorial<br />

micro electrochemistry<br />

Electrosynthesis is an effective way to produce<br />

chemical transformations by utilising redox reactions.<br />

Libraries of specific ions can be generated in the<br />

wells of microtitre plates by potentiostatic electrolysis<br />

under the computer control of the <strong>PG580RM</strong><br />

multichannel electrochemical system. As an online<br />

technique the multi-channel system allows a very fast<br />

assessment of the redox state during the electrolysis.<br />

The <strong>PG580RM</strong> has unique features which makes<br />

it an ideal choice where high sample throughput is<br />

a requirement. The <strong>PG580RM</strong>’s modular concept<br />

means it can be configured to create a user defined<br />

system from a 2-channel up to a 14-channel system<br />

within the same chassis. By connecting a 14-<br />

channel chassis to other RM units an extended<br />

system is created. A ninety-eight sensor array can<br />

be individually addressed by ‘chaining’ together<br />

seven 14-channel systems. The software treats the<br />

combined units as one system.<br />

Multiplexing Capabilities<br />

Where high throughput is not essential but high<br />

productivity needs to be achieved the user can make<br />

use of the multiplexing capabilities of the RM system.<br />

Each individual channel can, with the appropriate<br />

cable set, sequentially address up to five working<br />

electrodes making a cost effective solution to working<br />

with multiple electrodes.<br />

The system can also be configured to have one<br />

counter electrode, one reference electrode but<br />

multiple working electrodes. This feature makes the<br />

instrument suitable for applications such as multipoint<br />

corrosion monitoring applications or fundamental<br />

research of potential variations along a polarised ribbon<br />

electrode.<br />

Autosequencing<br />

The software permits auto-sequencing of experiments.<br />

Experiment chains such as E CORR<br />

vs. Time, LPR, Tafel<br />

and Potentiodynamic scans can be accomplished<br />

without the need to manually start the next<br />

experiment. You can also include loops so that a<br />

group of experiments is repeated a number of times.<br />

Data is automatically transferred to the computer for<br />

subsequent analysis.<br />

Analogue Triggering<br />

Capability<br />

The <strong>PG580RM</strong> modules have a real time analogue<br />

triggering facility. The triggering can be configured to<br />

execute on high or low thresholds of current, potential<br />

or auxiliary voltage. The triggering provides sub<br />

millisecond timing accuracy and can offer both pre and<br />

post trigger data as required.<br />

A typical application would be an electrochemical<br />

sensor where a small initial potential is set between<br />

the electrodes to detect the point when an analyte<br />

comes into contact with the electrodes. The trigger<br />

facility allows the instrument to apply waveforms and<br />

measure with precision timing relative to such an<br />

event.<br />

2


<strong>Soft</strong>ware<br />

The software supplied with the<br />

<strong>PG580RM</strong>, either UiEChem TM or<br />

UiECorr TM , is a comprehensive<br />

and fully featured package which<br />

encompasses a wide selection<br />

of standard electrochemical<br />

techniques. All this is combined<br />

with an easy-to-use graphics<br />

interface. After a technique<br />

has been selected a waveform diagram is displayed<br />

showing the structure of the experiment. At the<br />

same time the user can enter in the experimental<br />

parameters, set the sampling rate, number of cycles<br />

and current autoranging. The software automatically<br />

configures itself to the number of potentiostat<br />

channels installed in the <strong>PG580RM</strong> unit.<br />

A standard graphics display is provided for each<br />

technique and we have added the ability for the user<br />

to define their preferred format for each technique<br />

from a simple template. A right-mouse click on the<br />

plot gives access to the graph properties. From here<br />

you can choose from a selection of line sizes, colours<br />

and styles and overlay multiple data files.<br />

Advanced waveform generation<br />

The <strong>PG580RM</strong> modules are capable of generating<br />

complex and repetitive waveforms with precision timing.<br />

The instrument has a sequenced waveform generator<br />

which generates waveforms based on a sequence of<br />

steps. Each step may comprise a waveform which<br />

includes pulses, linear sweeps and arbitrary waves.<br />

The waveform generator has a timing resolution of<br />

125 microseconds and will seamlessly sequence<br />

from one step to the next. Other events such as Cell<br />

On/Off and WE number can also be programmed<br />

into a sequence. The sequencing supports loops and<br />

advanced functionality such as analogue triggering. The<br />

sequencing is used to create the standard experiments<br />

in the UiEChem TM or UiECorr TM software packages and<br />

both these applications support macro programming<br />

for unique experiments. The sequencing facilities may<br />

also be used in your own programming language via the<br />

optional ActiveX ® control.<br />

A configurable autosequencing routine provides an easy<br />

solution to starting and stopping long term experiments.<br />

Extended monitoring of the corrosion state of metals by<br />

LPR or sensors by chronoamperometry is now a ‘handsoff’<br />

operation.<br />

3


Specifications<br />

General<br />

Slots taken<br />

2 minimum in base unit<br />

Cell connections<br />

2 or 3 and earth<br />

Floating measurements<br />

Yes with isolation option<br />

Maximum ADC sample rate<br />

100 kHz<br />

Maximum time record<br />

Unlimited*<br />

Scan rate<br />

1 µV/s to 10 V/s<br />

Minimum pulse duration 125 µs<br />

*Subject to max 131k data points.<br />

Counter Electrode<br />

Voltage polarisation range<br />

Current polarisation range<br />

Maximum compliance<br />

Rise time<br />

± 2 V with factory option to<br />

± 8 V<br />

±20 mA<br />

±8 V<br />

1 V/µsec into 1 kΩ<br />

Reference Inputs<br />

Connections<br />

Differential Electrometer<br />

Maximum voltage measurement<br />

± 2 V with factory option to<br />

± 8 V<br />

Maximum resolution 61 µV<br />

Input impedance<br />

10 11 Ω II 5pF<br />

Input bias current<br />

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