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Data Collection and Data Reduction Techniques for ... - Bruker

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<strong>Data</strong> integration<br />

• The q–vector is written to<br />

APEX2’s database <strong>and</strong> part of<br />

the p4p file<br />

• SAINT automatically switches<br />

to “incommensurate mode”<br />

<strong>and</strong> generates a hklf 6 type<br />

output file with a .ram<br />

extension<br />

• Specify the Maximum Satellite<br />

Index in the integration<br />

options dialog<br />

• SAINT refines the q-vector<br />

during data integration<br />

• The q-vector refined to about<br />

0.238 <strong>for</strong> all pseudoephedrine<br />

data sets<br />

2/27/2013<br />

31

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