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DETERMINATION OF THIN FILM'S MECHANICAL PROPERTIES

DETERMINATION OF THIN FILM'S MECHANICAL PROPERTIES

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27<br />

of a blunt punch indenting an elastic solid (Loubet et al, 1984, Doerner and Nix,<br />

1986 ). They obtained:<br />

Figure 3.4 Characteristic region of load-depth diagram<br />

S<br />

dP A<br />

= = 2Er<br />

(3.2) and where<br />

dh π<br />

s<br />

2<br />

1 1−ν<br />

1−ν<br />

0<br />

= + (3.3)<br />

E E<br />

r<br />

E o<br />

2<br />

Er is called reduced modulus or combined modulus, S=dP/dhs is the<br />

experimentally measured stiffness of the upper portion of the unloading data, which<br />

is the slope of the curve fitted straight line of the initial part of unloading, A is the<br />

projected contact area of the indenter at maximum loading condition, E and ν are<br />

Young’s modulus and Poisson’s ratio for the specimen, and E o and νo are the same<br />

parameter for the indenter.<br />

The substitution of reduced modulus in Equation (3.2) for indentation test data is<br />

valid (A.C. Fischer-Cripps, 2001). Because of the utilization of the slope or<br />

unloading stiffness, it makes no difference whether or not the deflection of the<br />

indenter is accommodated explicitly or transferred to that occurring within the

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