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The Soils of Middlesex County - Agriculture and Agri-Food Canada

The Soils of Middlesex County - Agriculture and Agri-Food Canada

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ANALYTICAL METHODS<br />

Many <strong>of</strong> the methods used for soil analyses are<br />

outlined in the Manual on Soil Sampling <strong>and</strong><br />

Methods <strong>of</strong> Analysis (1) . <strong>The</strong> appropriate section<br />

numbers are indicated in parentheses after the soil<br />

analyses, as follows:<br />

a) Particle size analysis by pipette method, after<br />

pretreatment (2 .11)<br />

b) pH CaC12 (3 .11), pH water (3 .13)<br />

c) Organic carbon by wet oxidation, using<br />

ortho-phanathroline-ferrous sulfateasindicator<br />

(3 .613)<br />

d) Calcium carbonate equivalent, using 6N HCl<br />

<strong>and</strong> some glassware modifications (3 .41)<br />

e) Cation exchange capacity (3 .34)<br />

f) Electrical conductivity (4.12)<br />

g) Bulk density by core method (2 .21)<br />

h) Water retention by pressure-plate extraction<br />

(2 .43)<br />

i) Shrinkage was determined by a modification<br />

that used the COLE rod method (2 .13)<br />

Analytical methods not outlined in the Manual<br />

for Soil Sampling <strong>and</strong> Methods <strong>of</strong> Analysis (1), with<br />

their appropriate references indicated in<br />

parentheses, are as follows :<br />

a) Saturated hydraulic conductivity followed<br />

procedures used by U.S. salinity lab U.S.D.A .<br />

(2)<br />

b) Calcite-dolomite ratio determined by a<br />

gasometric procedure using the Chittick<br />

apparatus (3)<br />

c) COLE rod method for determining shrinkage<br />

limit (4)<br />

Volume <strong>of</strong> woody material, <strong>and</strong> von Post<br />

Decomposition values, for organic soils, were<br />

estimated from guidelines outlined in the CanSIS<br />

Manualfor Describing <strong>Soils</strong> in the Field (5) .<br />

Engineering test data for selected soils is<br />

presented in Table 1 . All tests, except for bulk<br />

density, porosity, free swell <strong>and</strong> COLE rod, were<br />

completed using American Society for Testing<br />

Materials (ASTM) methods (6). <strong>The</strong> test<br />

procedures <strong>and</strong> their ASTM numbers are as<br />

follows:<br />

a) United classification D2487-69<br />

b) AASHO classification D3282-73<br />

c) Atterberg limits (LL - liquid limit, PL - Plastic<br />

Limit, PI - Plasticity Index) D423-4-72<br />

d) Mechanical Analysis (Grain size analysis)<br />

D422-72<br />

e) Compaction (Maximum dry density <strong>and</strong><br />

percent optimum moisture) D698-70<br />

f) Free swell was determined from a method<br />

outlined by Holtz <strong>and</strong> Gibbs (7)

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