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Newsletter - Aachener Verfahrenstechnik - RWTH Aachen University

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parts etc. If you observe a cross section of a thixo<br />

formed part (or the starting material used for<br />

thixo casting process) through a microscope, the<br />

structure of the material may look like the picture<br />

below to the right. If you look at a material of the<br />

same chemical composition, but for a traditional<br />

pressure casting process it may look like the picture<br />

to the left (Fig.11.<br />

Fig.11: Samples of the aluminum alloy A356.<br />

Left: quenched from liquid, middle:<br />

sheared in the semi solid state for 5 minutes,<br />

right: sheared in the semi solid<br />

state for 3 hours.<br />

The thixo forming material goes through a process<br />

to obtain this desired structure, which results<br />

in completely different flow properties and<br />

hence product properties. As rheologists we are<br />

investigating the rheological (flow) properties of<br />

the material using a rheometer with an integrated<br />

oven shown in Fig.12.<br />

The material’s flow properties are changing due<br />

to the Ostwald ripening effect. We are working<br />

in the constitution of a model to describe this<br />

effect in the thixo forming material. The rate of<br />

the Ostwald ripening is influenced by temperature,<br />

amount and duration of shear and other<br />

chemical and physical parameters of the alloy.<br />

We are investigating these influences: The rheological<br />

properties are being measured, then the<br />

samples are quenched (shock frozen) to solid<br />

and investigated under a microscope. Through<br />

the rheological and optical investigations, we are<br />

coupling the parameter influence on the ripening<br />

process as well as the influence of the ripening<br />

process on the flow properties of the material.<br />

The results will be used to verify the model as<br />

the constitution of this proceeds.<br />

Fig.12: Measurement set-up for rheological<br />

preparation and measurements. Left:<br />

Rheometer with integrated oven, middle:<br />

rheometer cup and rotational body,<br />

left: aluminum sample after measurement.<br />

The AVT <strong>Newsletter</strong> Mechanical Process Engineering 14

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