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Conditions<br />
Applications<br />
Organotin Compounds<br />
Column: <strong>ACE</strong> 3 C18, 150 x 2.1mm<br />
Part Number: <strong>ACE</strong>-111-1502<br />
Mobile Phase: 65:23:12:0.05<br />
MeCN/H 2O/CH 3CO 2H/TEA<br />
Flow Rate: 0.2ml/min<br />
Detection: ICP-MS<br />
App. No. 1018<br />
Reproduced with kind permission of LGC Ltd., Middlesex, UK<br />
Pilocarpine<br />
Conditions<br />
Column: <strong>ACE</strong> 5 C18, 150 x 4.6mm<br />
Part Number: <strong>ACE</strong>-121-1546<br />
Mobile Phase: 15:85 MeCN/2mM<br />
tetrabutylammonium<br />
dihydrogen phosphate<br />
Flow Rate: 1.0ml/min<br />
Detection: UV, 254nm<br />
1<br />
Time - Minutes<br />
Compounds<br />
1. Dibutyltin<br />
2. Tributyltin<br />
Compounds<br />
1. Isopilocarpine<br />
2. Pilocarpine<br />
44<br />
Peptide Test Mix<br />
Conditions<br />
Column: <strong>ACE</strong> 5 C18-300, 250 x 4.6mm<br />
Part Number: <strong>ACE</strong>-221-2546<br />
Mobile Phase: A. 0.1% TFA in H 2O<br />
B. 0.1% TFA in MeCN<br />
Flow Rate: 1.0ml/min<br />
Gradient: T(mins) %A %B<br />
0 90 10<br />
25 60 40<br />
Temperature: Ambient<br />
Detection: UV, 220nm<br />
App. No. 1019<br />
Polyamines<br />
Conditions<br />
Column: <strong>ACE</strong> 5 C18, 150 x 4.6mm<br />
Part Number: <strong>ACE</strong>-121-1546<br />
Mobile Phase: 90:10 MeOH/TRIS buffer<br />
(pH 7.0)<br />
Flow Rate: 1.2ml/min<br />
Detection: Fluorescence - λex 340nm<br />
λex 450nm<br />
App. No. 1020 2<br />
App. No. 1021<br />
Time - Minutes<br />
1<br />
2<br />
Compounds<br />
1. Gly-Tyr<br />
2. Oxytocin<br />
3. Angiotensin II<br />
4. Neurotensin<br />
2<br />
Compounds<br />
1. Putrescine<br />
2. Cadaverine<br />
(as OPA derivatives)<br />
Reproduced with kind permission of Controlled Therapeutics, Scotland, UK Reproduced with kind permission of Centre for Chemical Sciences, Royal Holloway University of London, UK<br />
1<br />
Time - Minutes<br />
1<br />
2<br />
Time - Minutes<br />
3<br />
4
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