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ice formation around a horizontal tube in a rectangular vessel

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Waterglycolsolution410 mm 500 mm 500 mm 470 mm 580 mm 480 mm 500 mm 560 mmFigure 2. Measurement stations along test <strong>tube</strong>Tw4Tw4Tw3Tw3Tw3Tw6 Tw5Tw2Tw1Tw7 Tw813 10 1 1 10 135 14324275Tw2Tw1143242755Tw6 Tw5Tw2Tw1Tw7 Tw813 10 1 1 10 131 8323975a) x/L= 0.1 b) x/L= 0.47 c) x/L= 0.86Figure 3. Temperature measurement locations with<strong>in</strong> the waterAll the thermocouples used were K type, teflon<strong>in</strong>sulated thermocouples. An <strong>ice</strong>-bath was employed asthe reference junction for all the thermocouples used.Outputs of the thermocouples were monitoredcont<strong>in</strong>uosly with a sampl<strong>in</strong>g rate of 30 read<strong>in</strong>gs/s, us<strong>in</strong>ga computer-controlled data logg<strong>in</strong>g system.Due to the experimental nature of the present work, carewas given to the uncerta<strong>in</strong>ty <strong>in</strong> measurements. The fluidflow rate is measured by means of a calibratedrotometer with accuracy of ± 4%. To performcalibration of the rotometer, water was pumped from asupply reservoir to a constant head reservoir. Fromthere, water flowed to a weigh<strong>in</strong>g tank through themeasur<strong>in</strong>g section with the rotometer under test. Theflow rate was adjusted with a control valve situated atthe downstream end of the test section. The rotometerwas calibrated by measur<strong>in</strong>g the volume of water thatpasses the rotometer dur<strong>in</strong>g a certa<strong>in</strong> measur<strong>in</strong>g time.Table 1. Uncertanity and range for different parametersParameter Range Uncerta<strong>in</strong>ityTube <strong>in</strong>ner radious (mm) 6 ± 0.1 mmTube outer radious (mm) 8 ± 0.1 mmTube length (m) 0 − 4 ± 0.5 cmFlow rate (l/h) 0 − 1000 ± %4Temperature (ºC) -7 to 30 ± 0.3 ºCIce thickness (mm) 0 − 20 ± 0.1 mmHereto the water was collected <strong>in</strong> the weigh<strong>in</strong>g tank,whereby the volume <strong>in</strong>crement was measured andaverage flow rate was computed by divid<strong>in</strong>g the volumeby the time. Temperatures of water and transfer fluidare measured by means of K type teflon <strong>in</strong>sulatedthermocouples with accuracy ± 0.3 ºC. Thethermocouples were calibrated aga<strong>in</strong>st a plat<strong>in</strong>umresistance thermometer <strong>in</strong> a stirred liquid bath whosetemperature was adjusted with the help of atemperature-measur<strong>in</strong>g bench. Thickness of the <strong>ice</strong>formed <strong>around</strong> the <strong>tube</strong> is measured with ± 0.1 mm.Table 1 shows the range and uncerta<strong>in</strong>ity of parametersfor the experiments. Thickness of the <strong>ice</strong> formed on the<strong>tube</strong> was determ<strong>in</strong>ed us<strong>in</strong>g a visual technique. Icethickness was measured at the same stations wheretemperature measurements were made. Smallobservation w<strong>in</strong>dows are opened through the <strong>in</strong>sulationmaterial at the measur<strong>in</strong>g stations to be able to make <strong>ice</strong>thickness measurements. Photographs of the <strong>ice</strong> weretaken with a digital camera (Nikon Coolpix 8700, 8MP,10x optic zoom) from the front and the top of the<strong>vessel</strong> at each station to be able to detect circumferentialchanges <strong>in</strong> <strong>ice</strong> thickness. Different light sources andpositions were tested dur<strong>in</strong>g the prelimenary experimetsto determ<strong>in</strong>e the best light<strong>in</strong>g arrangement. A travers<strong>in</strong>gmechanism was designed to be able to detect the <strong>ice</strong><strong>formation</strong> along the <strong>tube</strong> with a short period of timebetween the stations. The time period between any twomeasur<strong>in</strong>g station was 20 s at maximum. Allphotographs were taken <strong>in</strong> close-up mode with 5 MPresolution. Figure 4 shows two images of solidificationtaken at two different times at the first measur<strong>in</strong>gstation (x/L=0.1) for an <strong>in</strong>let temperature of -5.8 ºC,flow rate 900 l/h as an example to the images takendur<strong>in</strong>g the experimets. At the end of experiments, thephotographs taken were transferred to an image analysisprogram (Image-ProPlus 4.5) for post process<strong>in</strong>g. Us<strong>in</strong>gsome of the techniques offerred by the program, brightimages that clearly <strong>in</strong>dicate the boundaries of the <strong>ice</strong>formed <strong>around</strong> the <strong>tube</strong> were obta<strong>in</strong>ed. From the imagesprocessed, thickness of the <strong>ice</strong> was determ<strong>in</strong>ed for thetop and bottom of the pipe separately (left and rightsides of the pipe for the photographs taken from the topof the pipe) us<strong>in</strong>g the pipe diameter as a referencedimension.78

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