CHEMICAL PREPARATIONMechanical preparation of vertebrate fossilsfrom the hard limestones (Kalken) of theUpper Lias beds is not a very satisfactorymethod. Acetic acid preparation is not newbut has seldom been practised in Germaninstitutions, although, when it is doneproperly, the risk is very slight and theresults are very good. In July 1971 oneauthor had the opportunity of visiting thelaboratory of the British Museum (NaturalHistory) where a method developed there wasbeing very successfully practised by A. E.Rixon and R. Croucher. Knowledge of thisEnglish method is indispensable:Prerequisites(a)(b)(C)Suitability of a specimen for acidtreatment: as the size of the objectincreases, so does the cost ofmaterials; above all, the time spenton the job can be tremendous; and theneed for special technical equipmentbecomes greater. With objects abovethe size of, say, an ichthyosaur skull(40-50cm). it is better not to use thismethod unless special equipment andfacilities are available.The calcium carbonate content must behigh.The inner structure of the matrix isimportant. Badly weathered, eroded, orfissured material is not suitable.Also unsuitable are more compactmatrices in which the larger hollowshave been filled with diageneticcalcite e. g. limestone with shell-bedlayers, or grown-over ammonite chambers.Preliminary treatmentSome preliminary mechanical treatment may benecessary. In the case of very thickconcretions it is worth chiselling away thematrix until close to the bone, so that theacid can work equally all over. Parts not tobe dissolved should be varnished, as aprotective measure, then enveloped in rubberand epoxy resin (Rixon 1968). The specimenshould be suitable for setting up, with asolid base and in particular with pointswhere it can be grasped.PreparationIt must be decided in advance how far theacid treatment will be taken, and which boneswill be freed. Unlike material fromSolnhofen or the Muschelkalk, it is necessaryto remove the undissolved sludge from allareas - not just the bone - of the washed anddried specimen, so that acid dissolution cango on equally. This can take up much time inthe case of complex and large specimens. Thefirst general rule is never to leave thespecimen too long in the acid, but rather tocheck it often. Excessive haste isinadvisable.The acid often acts uncontrollably. Finefissures or transversely or verticallyembedded thick mollusc shells can lead acidto the interior where it can act injuriouslyFig.7. A, ichthyosaur fragments in slab fromthe Unteren Stein, Holzmaden, before aceticacid preparation. B, close up of ichthyosaurbones after partial preparation in acid(field of view shown on A).without being noticed. These inletscontinuously have to be temporarily closedoff with cement. When doing this it isdifficult to keep a continuous and permanentclosure without unwanted impregnation of theadjacent bone and softened sediment. Thebone's calcite infilling is also eaten away;this considerably weakens the bone, which isalready suffering from deformations,haircracks, and fractures.Large artists' paint brushes can be used toclean away the residue of dried and powdery,caked sediment sludge; they should be heldsome two-thirds of the way down the length ofthe hairs so that a relatively firm yetyielding brush results. This brushwork mustbe done without applying too much pressure.Another general rule is to take care whereyou do not expect bone, and to avoidexcessive lateral cutting, graduallydeepening a level area instead. Progressslowly and methodically.The application of careful and, if possible.repeated coats of consolidant is importantfor the strengthening of skeletal parts.Each portion of bone should be consolidatedas it is revealed, so preparation should onlyprogress by millimetre layers. Only the bonemust be soaked, and this is not easy incomplicated structures. Restoration,
.fractures, and cracks can be made good with acement made of cellulose lacquer, 'Lithophon'(no longer used; a powdered meal of organicand~~ ~ ~inorganic comoonents) and oowderedm~ -~ ~colouring matter, and if necessary syntheticresin.A practical exampleIchthyosaur fragments in a slab from theUnteren Stein of Holzmaden were prepared withacid (Fig.7). This specimen was made easierto deal with by levelling the surface, and bycarefully watching the progress of treatmentand the behaviour of the bones duringtreatment and consolidation. Treatmentrequired 91.5 hours in acid and 250 hours inwater (frequently changed) to remove theacid. The result. was an average dissolutionof 7-8mm of matrix, corresponding to acontinuous rate of 0.07mm per hour (the rate,however, falls away' sharply when the acidgrows weaker and is not really measurable).Verv thin lavers of shale or of harder rockenciosed in the limestone delayed theprocess, but frequent renewal of the acidconsiderably encouraged the treatment. Itwas necessary to interrupt preparation seventimes for a cycle of washing, drying, andconsolidation to remove the undissolved rock.Further examplesAn ichthyosaur mandible from the Arietenkalk(Lower Lias, Gryphaea limestone, Wiirttemherg)was extracted by acid. The limestone wasefficiently removed by the strongestconcentration (17%) of acetic acid. Therewas little insoluble residue, which requiredless frequent removal than in the previousexample from the Upper Lias. However, thin-irregular layers in the rock form toughcrusts which had to be regularly removed toensure uniform solution.ACKNOWLEDGEMENTTra~slated hy Mr A.C. Benton from theoriginal German article, Larcher, F. andKeller, T., 1976. Praparationstechniken desLias-epsilon-Schiefers. Praparator, 22,213-220. Some of the tradenames of resins,etc., mentioned in the original German havebeen omitted as they are unavailable in thiscountry. I am grateful to Fritz Lorcher,Thomas Keller, and the publishers ofPraparator for permission to use theirarticle and photographs, to Thomas Keller forchecking the translation, and to the AreaMuseum Council for the South West for payingtranslation charges. - M.A. Taylor.Herr R. Uttenweiler (Dotternhausen) providedFigs.2, 3A, 4-6.McGowan, C. 1973. The cranial morphology ofthe Lower Liassic latipinnateichthyosaurs of England. Bull. Brit.- Mus. nat. Hist. (-.l, 24, 1-109. [A'Carbowax' method for reconstructionwork on original bony elements etchedout by acid is described on p.106 etseq.1.Rixon, A.E. 1968. The development of theremains of a small Scelidosaurus from aLias nodule. Museums Jl, 67, 315-320.Toombs, H.A. and Rixon, A.E. 1959. The useof acids in the preparation ofvertebrate fossils. Curator, 11,304-312.Fritz LorcherandThomas KellerPalaanthrop. Abt.Forschungsinstitut SenckenbergSenckenberganlage 256000 Frankfurt 1West GermanyTranslation received from M.A. Taylor 29 August 1984.
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