Proton Nuclear Magnetic Resonance Spectroscopy

P a g e | 8ProcedureYour laboratory instructor will demonstrate how to:prepare a sample for NMR analysis.take an NMR spectrum.Special Deuterated solvents are available with which solutions of your compounds can beprepared. The deuterated solvent with then interfere with the proton NMR spectrum minimally.These solvents typically come with the TMS reference already added.You will be expected to master the use of the Department's spectrometer such that you canindependently take spectra without assistance.Each person in the laboratory class should take the spectrum of one of the following compounds:Ethyl Aminet-Butyl ChlorideEthyl Benzoatep-Bromo Toluene2-Bromo Butane1,2-Dichloro EthaneThen, as a class, you should collectively assign all the peaks in each spectrum to the Hydrogenatoms of the molecules comprising the compounds.