Heat of <strong>Co</strong>mbustion of Liquid Hydrocarbon Fuelsby Bomb Calorimeter<strong>Test</strong> MethodHeat of combustion is determined in this test method by burning a weighedsample in an oxygen bomb calorimeter under controlled conditions.The heat of combustion is computed from temperature observations before,during and after combustion with proper allowances for thermochemicaland heat transfer corrections. Either isothermal or adiabatic calorimeterjackets can be used.Automatic CalorimeterThe automatic calorimeter is the latest system for determining gross calorificvalues of liquids and solid fuels. A higher level of automation with extremelysimple handling characterizes this device.In addition to the Isoperibolic measurement procedure, a Dynamic(reduced-time) mode is also available for the user. Different workingtemperatures can be selected for both procedures based on the temperatureof the connected water.To provide a supply of cooling water, the calorimeter can be connected to astandard thermostat or an appropriate permanently installed water connection,with a connection valve. The unit is equipped with a very convenient operatingpanel through which operation of the device takes place. The graphical displaywith active back lighting displays the appropriate status messages. Thetemporal course of a measurement that has been started and all currentparameters of the weighed in sample can be constantly monitored and arearranged to be clearly visible.<strong>Co</strong>nnections for analysis scale, printer, sample rack for identifying andmanaging samples are already integrated into the basic device. Thenetwork connection and the special configuration for data exchange can beimplemented at any time with LIMS.In combination with special halogen-resistant decomposition vesselsquantitative decompositions can be performed to determine halogen andsulfur content.Dimensions lxwxh,in.(cm)17 1 ⁄2x17 3 ⁄4x19 3 ⁄4 (440x450x500) Net Weight: 66 lbs (30 kg)<strong>Test</strong> MethodDetermines the Filter Plugging Tendency (FPT) of distillate fuel oils wherethe end use demands an exceptional degree of cleanliness. This test isapplicable to fuels within the viscosity range of 1.50 to 6.00 mm2/s (cSt) at40°C. The test is not applicable to fuels that are not clear and brightbecause water interferes with the measurement of filter plugging. Causesof poor filterability might include fuel degradation products, contaminantspicked up during storage or transfer, or interaction of the fuel with the filtermedia. Any of these could correlate with orifice or filter system plugging,or both.Automatic Filter Plugging Tendency Analyzer• Integrated <strong>Co</strong>oling System equipped with a single stage gas motorcompressor CFC free• Measuring device complete with support for filter, Beakers, PT100sensor Class A, level sensor, pressure gauge, tubes and joints.• Pump 20 mL/min• 6.4” TFT/LCD built-in touch screen panel PC for the managing of theanalyzer by means of Lab-Link Software• USB connection to an external printer or external PC• Storage capacity for more than 60,000 analysisSpecifications<strong>Co</strong>nforms to the specifications of:ASTM D2068; IP 387Electrical Requirements:115V 60Hz220-240V 50/60Hz76Specifications<strong>Co</strong>nforms to the specifications of:ASTM D240; D4809; D5865; D1989; D5468; E711; ISO 1928;DIN 51900; BS1016Measurement range: 40,000 JMeasuring mode: Isoperibolic 25°C; Isoperibolic 30°C;Dynamic 25°C; Dynamic 30°CIsoperibolic Measuring Time: Approximately 22 minDynamic Measuring Time: Approximately 7 minOxygen Operating Pressure: 30 bar<strong>Co</strong>oling Medium: Water via line, flow through quantity 60 + 10 liters / hourWater Operating Pressure: 1 – 1.5 bar max.Water <strong>Test</strong> Pressure: 10 barInterfaces: Serial (RS232); Parallel; Keyboard; Sample rack; External monitorCatalog No.K88800K88890Ordering InformationAutomatic Calorimeter, 115V 60HzAutomatic Calorimeter, 220V 50HzAccessoriesK88800-1 <strong>Co</strong>oling water supply unit, 115V 60HzK88890-1 <strong>Co</strong>oling water supply unit, 220V 50HzK88800-2 Pressure Gauge, OxygenTo reduce the pressure of the oxygen cylinder to 30 barK88800-3 Standard Decomposition VesselK88800-4 Decomposition Vessel, Halogen ResistantFor quantitative decomposition determine halogen andsulfur contentK88800-5 <strong>Co</strong>nnection valveRequired for permanently installed water connectionAutomatic Filter Plugging Tendency Analyzer (FPT)Catalog No.KLA-6KLA-6 (220)Ordering InformationKLA-6 Automatic FilterPlugging TendencyAnalyzer (FPT)Automatic Filter Plugging Tendency Analyzer (FPT),115V 60HzAutomatic Filter Plugging Tendency Analyzer (FPT),220-240V 50/60HzAccessoriesKLA-1820-8013 Glass Fibre Filters, pk of 100KLA-PT100-CAL Calibration Box and CablesKLA-DB-KIT Kit of <strong>Co</strong>nnectors and Cables for <strong>Co</strong>ld range
Oxidation Stability of Foods, Oils, Fats and Biodiesel Fuels<strong>Test</strong> MethodFor the determination of the oxidation stability of samples (solid, semisolid,or liquid), in order to determine product quality and obtain valueadded information related to the fat oxidation processed in samples of foods,oils, fats and Biodiesel Fuels.Oxidation <strong>Test</strong> ReactorThe Oxidation <strong>Test</strong> Reactor is a versatile instrument suitable for a wide rangeof oxidation stability and shelf-life applications including:• Prediction of the oxidation stability during shelf-life studies, by analyzingthe product at defined time intervals and building an experimental curve• Evaluation of the adequacy of storage conditions• Evaluation of an optimal packaging solution• <strong>Co</strong>mparison of the oxidation stability of different formulas for foodpreparations• Evaluation of the oxidative stability of vegetable oils of differentbotanical origin• Evaluation of the effectiveness of antioxidants• Information on product oxidation when the oxidation flex is not visible,especially for products with a low fat content (4-5%). In this case, productoxidation can be achieved by combining the Oxidation <strong>Test</strong> Reactor withthe gas chromatographic technique.The Oxidation <strong>Test</strong> Reactor is a complete solution, controlled entirely by theWindows ® -based oxidation software capable of providing high added valueinformation concerning fat oxidation processes in foods, oils, fats andbiodiesel fuels.The Oxidation <strong>Test</strong> Reactor works directly on the whole sample without theneed for preliminary fat separation, and is suitable for the determination of thequality and the state of preservation of the sample.An extremely simple and intuitive instrument equipped with two separatetitanium chambers in order to analyze the same sample in duplicate ordifferent samples at the same time, under the same conditions.The stability of the sample is determined by accelerating the oxidation processusing high temperatures (from Ambient to 110°C) and a pre-determinedoxygen pressure. Oxygen is consumed during fat oxidation and it is thisdecrease in oxygen pressure that enables us to obtain useful informationconcerning the sample.The intuitive software controls the entire process in a user friendly way and theoperator can record data in a database, compare tests, export the data to anExcel file, filter and order the data quickly and easily.K83100 Oxidation <strong>Test</strong> ReactorSpecificationsBased on the Specifications of:ASTM D942; IP 142Temperature Range: Ambient to 110°CNumber of Oxidation Chambers: 2Chamber Capacity: 100mLPressure Range: 0 – 8 barInterface: USBOverpressure: Safety ValveOut of Range Temperature: Visual AlarmDamaged Probe: Visual AlarmElectrical Requirements:220-240VAC, 50/60Hz<strong>Inc</strong>luded AccessoriesOxidation SoftwareUSB CableSample Holder (6)Spacer (4)Dimensions wxdxh,in.(cm)14.6 x 19.4 x 7.6 (36.5x48.5x19)Net Weight: 36.3 lb (16.5 kg)Catalog No.K83100Ordering InformationOxidation <strong>Test</strong> Reactor, 220-240V 50/60Hz77