Control of Continuous Flow Chemical Reactors: - CPAC - University ...

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Flow Rate vs. Reaction Progressn Slower flow rate(longer residencetime) correlated withhigher yieldn Too slow results inunsteady yield frominefficient mixing(outside reactorspecifications)Scores on PC 1 (64.43%)Samples/Scores Plot of Raman Data320.2 mL/min8 mL/min4 mL/min 2 mL/min 1 mL/min 0.5 mL/min10-1-2-350 100 150 200 250 300 3504 x 104 Samplen Boundaries defined:8 mL/min & 1 mL/min18
Catalyst Conc. Vs. Reaction Progressn Correlation betweenconcentration andyield of productn Little variation in yieldbelow 0.275Mn 2.2M solution resultedin significant increasein yield, but wasabove reactorspecifications19
Page 1 and 2: Control of ContinuousFlow Chemical
Page 3 and 4: Analytical Control System DesignOpt
Page 5 and 6: Sampling Systems• NeSSI Component
Page 7 and 8: NeSSI Sampling System for ReactorRa
Page 9 and 10: NeSSI Reagent Sampling SystemNeSSI
Page 11 and 12: Corning ® Advanced-Flow TM LFLow-F
Page 13 and 14: Full Reactor System w/Control2.5 ft
Page 15 and 16: Chemical Reactionn Esterification o
Page 17: Temperature vs. Reaction Progress
Page 21 and 22: PLS Raman Validation ModelYield Pre
Page 23 and 24: Real-Time Quantitative Yieldn Able
Page 25 and 26: Real-Time Quantitative Analysisn Ra
Page 27 and 28: Moffat Swern Oxidation of Alcoholn
Page 29 and 30: Experimental Batch - Developmentn R
Page 31 and 32: IR Reaction Progressn Reaction prog
Page 33 and 34: Infrared Conclusionsn Spectral chan
Page 35 and 36: Pre-processed Raman Data7000Reactio
Page 37 and 38: Raman Reaction PlotRAMAN SCORE PLOT
Page 39 and 40: Concluding Remarks onSpectroscopic
Page 41 and 42: Swern Reactor w/sampling + Analytic
Page 43 and 44: Data Fusionn There is no one perfec
Page 45 and 46: ResultsComparison of Individual Mod

Control of Continuous Flow Chemical Reactors: - CPAC - University ...

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