pack your own capillaries for hplc and mass spec - Western Analytical

PACK YOUR OWN CAPILLARIES FOR HPLC AND MASS SPEC

Pack micro-columns of various length and diameterCompact design will not tip on the work surfaceSeals safely at pressures up to 6000 psiAssembles simply, without toolsPriced economicallyS a v e t i m e , m o n e y , andgain control by packingyour own capillary columns.Des i g n e d t o a c c o m modateempty fused silicaor PEEKsil columns of lessthan 1/32” in outer diameter,the Nanobaume isa compact 316 stainless steelunit built to pack tubing with asilica bed at high pressure. TheNanobaume may be usedfor packing at up to 6000 psigwith liquid media (not recommendedfor gas pressure) occupiesa small footprint on thebenchtop (at 2.5” in diameter,2.5” tall), and assembles easilyin a few simple steps. TheTefzel ® O-ring seals at highpressure by hand-tighteningonly. No wrenches are required.A magnetic Teflon ®stir bar keeps the silica slurrysuspended over a stir-plateduring column packing.1

P A R T S A N D A S S E M B L YSSI 02-01243-Way Valve withbottom ventCap LockPGS254SLM PressureGauge with U-433Gauge TeePressureSourceFingertight NutPressure VentFerruleDireciton of Pressure FlowEnd Fittingretains silica bedwhile packingCap SealStir BarGlass VialVial InsertCompleteColumn withEnd FittingsO-RingPacker BodySP-300Packing Unit3

C O M P O N E N T SC O L U M N E N D F I T T I N G SProvide system connections while retaining the silica bedReusable - simply replace the screen after multiple usesFor direct-connection of 360um or 1/32” OD columnsColumn End Fittings retain a silica bed while packing and connect the finishedcolumn to your system. They are reusable, and the filter screen whichretains the silica is easily replaced after multiple uses. The fittings below aremade for direct-connection of either 360µm or 1/32” OD columns. Note thatone endfitting may be modified into the other by exchanging both screenand microferrule, or use the F-385X to adapt 360µm tubing to 1/32” OD.Part Number Description Price360µmM-538M-126F-152360µm OD column End Fitting, with (5) 1µm Titanium screens, 10nLReplacement screens for M-538, 1µm, Titanium, 2-packReplacement microferrule for 360µm OD columns, PEEK$ 178.60$ 53.50$ 6.001/32”M-548M-134F-1121/32” OD column End Fitting, with (5) 1µm Titanium screens, 22nLReplacement screens for M-548, 1µm, Titanium, 2-packReplacement microferrule for 1/32” OD columns, PEEK$ 178.60$ 53.50$ 6.00MiscP-416F-385XReplacement female nut for M-538 and M-548, PEEKTubing Sleeve Adapter, 360um ID x 1/32” OD, PEEK, 10-pack$ 5.35$ 18.00P R E S S U R E S O U R C E A C C E S S O R I E SHigh-pressure tubing and connectionsGauges, valves, and flow control accessoriesConnection of the Nanobaume TM to a pressure supply source requires onlyan adapter and a length of high-pressure tubing. Inserting a gauge intothe fluid stream (using the Gauge Tee) will allow you to monitor the packingpressure. A 3-Way Valve is an easy way to connect or remove the unit fromthe pressure source. Please note that the SP-300 packing unit is recommendedfor use with liquid media only.Part Number Description PriceSS1030-5FTSS1030-20CMPK1030-GSSP-ISSD1ME2SSP-ISSD1MC2U 416U 401U 433PGS254SLMSSI 02-0124Tubing, 316 stainless steel, 1/16” OD x 0.030” ID x 5’ longTubing, 316 stainless steel, 1/16” OD x 0.030” ID x 20 cm longTubing, PEEK (green), 1/16” OD x 0.030” IDPort Adapter, SS316, 1/16” OD tube x 1/8” NPT, 90° anglePort Adapter, SS316, 1/16” OD tube x 1/8” NPT, straightReplacement Female Nut, for port adapter, SS316Replacement Ferrule, 1/16”, for port adapter, SS316Pressure Gauge Tee, with two 10-32 fittings for 1/16” tubingPressure Gauge, 0-10,000 psig, liquid filled, stainless steelThree-way valve with bottom vent, SS316$ 15.75$ 4.32$ 2.40 /ft$ 17.00$ 16.00$ 3.45$ 2.35$ 51.00$ 75.00$ 130.004

E M P T Y C O L U M N SF U S E D S I L I C A E M P T Y C O L U M N SMethyl-Deactivated and Undeactivated optionsPolyimide coated for strengthUsing fused silica tubing is an economical way to make your own customcolumns. It may be cut to length by the user and will sustain Nanobaume TMpacking pressure. Although referred to as “360 micron” by the industry, typicaltolerances are ±10µm on the OD, ±3-4µm on the ID. Priced per meter.Part Number Description PriceFS-315 Precision fused silica tubing cutter $ 215.00DE-050363DE-100365DE-25035050µm ID x 363µm OD, Deactivated fused silica100µm ID x 365µm OD, Deactivated fused silica250µm ID x 350µm OD, Deactivated fused silica$ 25.00 / M$ 16.00 / M$ 15.00 / MUNDE-005363UNDE-010363UNDE-020363UNDE-050363UNDE-075363UNDE-100363UNDE-200363UNDE-2503635µm ID x 363µm OD, Un-Deactivated fused silica10µm ID x 363µm OD, Un-Deactivated fused silica20µm ID x 363µm OD, Un-Deactivated fused silica50µm ID x 363µm OD, Un-Deactivated fused silica75µm ID x 363µm OD, Un-Deactivated fused silica100µm ID x 363µm OD, Un-Deactivated fused silica200µm ID x 363µm OD, Un-Deactivated fused silica250µm ID x 363µm OD, Un-Deactivated fused silica$ 13.00 / M$ 13.00 / M$ 13.00 / M$ 13.00 / M$ 13.00 / M$ 13.00 / M$ 13.00 / M$ 13.00 / MP E E K s i l T ME M P T Y C O L U M N SFused silica lined PEEK tubing, UndeactivatedAvailable in pre-cut lengths onlyPEEKsil TM is fused silica tubing covered by a PEEK polymer sheath, suppliedhere in 1/32” OD. Mechanically stronger than fused silica tubing alone, it isreadily adaptable to typical stainless or polymer connections and fittings.Part Number Description Color Price/2-pkSGE0624241SGE0624242SGE0624243SGE0624261SGE0624262SGE0624263SGE0624271SGE0624272SGE062427325µm ID x 1/32” OD, 50 mm long, 2 pack Orange25µm ID x 1/32” OD, 100 mm long, 2 pack Orange25µm ID x 1/32” OD, 150 mm long, 2 pack Orange50µm ID x 1/32” OD, 50 mm long, 2 pack Beige50µm ID x 1/32” OD, 100 mm long, 2 pack Beige50µm ID x 1/32” OD, 150 mm long, 2 pack Beige75µm ID x 1/32” OD, 50 mm long, 2 pack Black75µm ID x 1/32” OD, 100 mm long, 2 pack Black75µm ID x 1/32” OD, 150 mm long, 2 pack Black$ 13.30$ 14.50$ 17.95$ 13.30$ 14.50$ 17.95$ 13.30$ 14.50$ 17.955

A C C E S S O R I E SPart Number Description Color PriceSGE0624311SGE0624312SGE0624313SGE0624341SGE0624342SGE0624343100µm ID x 1/32” OD, 50 mm long, 2 pack Red100µm ID x 1/32” OD, 100 mm long, 2 pack Red100µm ID x 1/32” OD, 150 mm long, 2 pack Red150µm ID x 1/32” OD, 50 mm long, 2 pack Purple150µm ID x 1/32” OD, 100 mm long, 2 pack Purple150µm ID x 1/32” OD, 150 mm long, 2 pack Purple$ 13.30$ 15.00$ 17.95$ 13.30$ 14.50$ 17.95N A N O B A U M E T MR E P L A C E M E N T P A R T SOrder parts to replace lost or broken itemsPurchase spares for products frequently usedSome Nanobame items may need to be replaced due to normal wear. Nicks and scratches onthe face of the Cap Seal or O-ring, for example, may hamper sealing at higher pressures. Youmay also want to purchase spares for some higher-use items, such as glass vials or ferrules.Part Number Description PriceSP-300-02SP-300-03SP-300-04SP-300-06VL-001XF-151F-113F-200-01P-550Nanobaume Cap SealNanobaume Static O-ring, ETFE with Inconel springNanobaume Vial Insert for 6x32mm glass vial, PolypropyleneNanobaume Teflon Stir Bar, 2x2 mmGlass Vial, 300µL, 6mm x 32mm, pack of 10Ferrule for 360µm OD columns (use with F-200-01 nut), Kel-FFerrule for 1/32” OD columns (use with F-200-01 nut), PEEKFingertight Nut, 10-32 threads, without ferrule, red DelrinPlug, 10-32 (for pressure testing of the Nanobaume unit), PEEK$ 115.00$ 125.00$ 105.00$ 8.00$ 5.00$ 10.95$ 7.15$ 1.05$ 2.15S I L I C A B U L K M A T E R I A LPack columns with the phase of your choiceOther packings available - please inquireA number of small particle silicas are available below. Select a phase to suit your needs andorder by the gram. Other packings are available; please contact your distributor for a broaderselection or allow our technical staff to suggest a material tailored to your requirements.Part Number Description Price /gmBMSE0503BMCT0510BMHY0501BMPR0503BMODS0503BMC180501HBMC80501BMC180501Strong Cation Exchange, PolySULFOETHYL A, 5µm, 300ÅWeak Cation Exchange, PolyCAT A, 5µm, 1000ÅHydrophilic Interaction, PolyHYDROXYETHYL A, 5µm, 100ÅHydrophobic Interaction, PolyPROPYL A, 5µm, 300ÅC-18, 5µm, 300ÅC-18, 5µm, 100Å Hydrophilic EndcapC-8, 5µm, 100ÅC-18, 5µm, 100Å$ 60.00$ 60.00$ 60.00$ 60.00$ 60.00$ 30.00$ 30.00$ 30.006Nanobaume TM is a Trademark of Western Fluids Engineering & Mfg, LLCTeflon ® and Tefzel ® are Registered Trademarks of E.I. du Pont deNemours and CompanyKel-F ® is a Registered Trademark of the 3M CompanyPolySULFOETHYL A, PolyCAT A, PolyHYDROXYETHYL A, andPolyPROPYL A are trademarks of PolyLC Inc.PEEKsil TM is a Trademark of SGE International Pty. Ltd.PEEK TM polymer is a Trademark of Victrex PLC

PRODUCTS FOR HPLC AND FLUID TRANSFER800.5 41 . 8 4 2 1 w w w. Wes t e r n A n a l y t ical.com