View Document Here - Hanford Site

Quanterra Incorporated
13715 Rider Trail North
Earth Citv, Missouri 63045
314 298-8566 Telephone
314 298-8757 Fax
Bechtel Hanford Incorporated
3350 George Washington Way
Richland, Washington 99352
April 21, 1998
Attention: Joan Kessner
Project Number
Date Received by Lab
Number of Samples
Sample Type
SDG Number
Data Deliverable
I. Introduction
CASE NARRATIVE
^$9501112 >b
do,
ti
Environmental
Services
0(14.`332
^' R ^ ^^ ^ p
PR 1993 ^
RECEIVED i
550.260"—^
March 09, 10, 11, 12, 13 and 16, 1998
Fifteen (15)
Other Solid
W02275
Summary
le Ab
" OL 6 19 L95^
Between March 9 and 16, 1998, a total of fifteen (15) other solid samples were received by
Quanterra, Richland and was transferred to Quanterra, St. Louis for chemical analyses. Upon
receipt, the samples were given the following laborato ry ID numbers to correspond with the
specific client IDs:
The samples were filtered to separate the liquid phase from the solid phase. The solid phase
sample IDs are listed below:
St. Louis ID BHI ID Richland ID Matrix Date Receipt of
17199-001
BON680 80316001 Solid 09-MAR-98
17199-002 BON681 80316002 Solid 09-MAR-98
17200-001 BON685 80320501 Solid 11-MAR-98
17200-002 BON686 80320502 Solid 11-MAR-98
17200-003 BON687 80320503 Solid 11-MAR-98
17202-001 BON682 80318301 Solid 10-MAR-98
17202-002 BON683 80318302 Solid 10-MAR-98
17202-003 BON684 80318303 Solid 10-MAR-98
17203-001 BON688 80322101 Solid 12-MAR-98
17203-002 BON689 80322102 Solid 12-MAR-98
17221-001 BON690 80324301 Solid 13-MAR-98
17221-002 BON691 80324302 Solid 13-MAR-98
17224-001 BON692 80327101 Solid 16-MAR-98
17224-002 BON693 80327102 Solid 16-MAR-98
17224-003 BON694 80327103 Solid 16-MAR-98
o0006'L

Bechtel Hanford Incorporated
April 21, 1998
Project Number: 550.260
SDG: W02275
Page 2
imbanterra
Emironmental
Services
The liquid phase of the samples were placed in containers and put on hold for the following
sample IDs:
St. LouisID BHI ID Richland ID Matrix Date of Receipt
17199-003 BON681 FILTRATE 80316002 Liquid 09-MAR-98
17221-003 BON690 FILTRATE 80324301 Liquid 13-MAR-98
17221-004 BON691 FILTRATE 80324302 Liquid 13-MAR-98
17224-005 BON693 FILTRATE 80327102 Liquid 16-MAR-98
17224-006 BON694 FILTRATE 80327103 Liquid 16-MAR-98
1I. Analytical Results/ Methodology
The analytical results for this report are presented by analytical test. Each set of data includes
sample identification information, analytical results and the appropriate detection limits.
Analyses requested
PCBs (Aroelor-1254) by EPA 8080. ICP-Trace Metals (Lead) by EPA Method 6010. Mercury
by EPA Method 7471.
III. Quality Control
A Laboratory Control Sample and Method Blank were analyzed with each preparation batch
MatrixSpike and Matrix Spike Duplicate analyses were performed per the protocol for each
analyte in this SDG.
IV. Definitions
The following codes were used to denote laboratory quality control samples and can he found in
the data summary secti-)n of this report:
QCBLK- Quality Control Blank, Method Blank
QCLCS- Quality Control Laborator y Control Sample. Blank Spike
V. Comments
0 000 63

Bechtel Hanford Incorporated
April 21. 1998
Project Number: 550.260
SDG: W02275
Page 3
f,mbanterra
Environmental
Som, e,
Shipping and Receiving
There are no comments or nonconformances associated with the shipping and receivin g of these
samples.
Wet Chemistry
Percent Moisture analyses for the solid phase samples were requested after the priority results
were reported. A Percent Moisture report was transmitted by facsimile on April 13, 1998.
PCBs
There are no comments or nonconformances associated with this analysis.
Metals
Percent solids was not determined for the samples in SDG W02275. Due to software
configuration, the CLP forms list solid sample result units as " dry weight" and `7 solids as "
100 ". The results on the forms are actually mg/Kg as is and are not corrected for percent
solids. The figure of 100 was used as percent solids for calculation purposes only and does not
represent measured solids content of the samples.
The percent difference for the Lead serial dilution (12.9) was greater than 10. therefore all
associated data was flagged with a "E".
I certify that this data package is in compliance %vith the SOW. hoth technically and for
completeness, for other than the conditions detailed above. Release of the data contained in this
hard copy data package has been authorized by the Laboratory Manager or a designee. as
verified by the following signature.
Reviewed and approved:
Robert E. White
Project Manager
000-00y

Control #: B98-043
Sample Disposition Record Revisionu: O
Section 1 - BACKGROUND
SAF#: B98-061
OU: N/A
Project ID: 105-C Reactor
Task ID: 9
Sampling Event: 105-C Phase I & Phase If
Laboratory: Quanterra Incorporated
Project Coordinator: WEISS, RL
Task Manager: ARMATROUT. JF
Section 2 - SAMPLE INFORMATION
Number of Samples: 15
Date Initiated: 3/17/98
ID Numbers: BON680, BON681, BON683, BON684, BON686, BON687, BON688. BON691, BON692, BON693. BON694,
BON682, BON685, BON689, BON690
MATRIX:
Collection Date:
Section 3 - ISSUE
N/A
Class: Lab Direction
NCR Number: N/A
Type: Multiple Phase Sample
Description: Concrete samples were wet ground in the field. The procedure resulted in too much liquid for analysis of the
samples as a single phase
NCR Validation (Print/Sign) Date
Section 4 - DISPOSITION
Type: Use As Is
Description: For all samples, separate liquid from solid phase and analvze liquid for CrVI. For the following, assign new
sample numbers as shown to liquids and analvze liquid for all other consitituents identified for solid.
BON680(solid) to BON894 (liquid), BON683(solid) to BON895(liquid ). BON686(solid) to BON896(liquid),
BON68 (solid)
to BON897(liquid), BON692(solid) to BON898(liquid)
ol L '
Project Coordinator (^^PnL""Sign) Date
ARMATROUT, JF
Task Manager (Print/Sign Date
N/A
QA (Print/Sign) Date
Section 5 - INSPECTION (Issue Class: Nonconformance Onlvl
N/A
Inspection Number: N/A
Inspection Results: N/A
Inspector (Print/Sign) Date

Ouanterra April 13, 1998 10:47 am
Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev.
Master Sample Login: 17199
Project Manager: N. Price
Draft: final: Entered and Reviewed by:
{,M^
L^J ^{-^ PM Review:
Sample Header Template:
WO 22 75IAJC 2P,6
y
2 ,^^fy
Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Rad Category Red Semple ND.
Comments
# Container Type Analysis Class Preservative AnaL. Due Date Hold Date Site (Container Numbers:% Filled)
Data:
17199-001 BON680 Solid 09- 14AR-98 10:30 09-MAR-98 13:42 27-MAR-98 AIRBORNE 3
RICHLAND I.D. 80316001///ICAPT = PS ONLY.
1 PH - Plastic-250m1 HG/7471/04 S COLD 23-MAR-98 06-APR-98 R58
1 ICAPT/6010/04 S COLD 23-MAR-98 05-SEP-98 R5 11
1 PCB/8080/04 S COLD 23-MAR-98 23-MAR-98 R58
1 PM/17/04 S COLD 23-MAR-98 05-SEP-98 R58
17199-002 DON681 Solid 09-MAR-98 13:45 09-MAR-98 15:15 27-MAR-98 AIRBORNE 1
RICHLAND I.D. 80316002///ICAPT = PB ONLY.
1 PN - Ptastic-250mL HG/7471/04 S COLD 23-MAR-9B 06-APR-98 R5B
1 ICAPT/6010/04 S COLD 23-MAR-98 05-SEP-98 R5B
2 PCB/8080/04 S COLD 23-MAR-98 23-MAR-98 R5 1;
1 PM 1 IT/04 S COLD 23-MAR-98 05-SEP-98 R56
17199-003 SON681 FILTRATE Liquid 09-MAR-98 13:45 09-MAR-98 15:15 27-MAR-98 AIRBORNE 1
RICHLAND I.D. 80316002///ICAPT = PB ONLY.
1 PM - PlastiC-1 1- HOLD//04 S COLD 23-MAR-98 19-MAR-98 R5B
17199-004 SON894 Liquid 09-MAR-98 10:30 09-MAR-98 12:15 27-MAR-98 AIRBORNE 1
RICHLAND I.D. 80321501///ICAPT = PB ONLYWUSE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17199-001.
1 PH - Plastic-1 1- HG/7470/04 S COLD 23-MAR-98 06-APR-98 EMPTY
1 ICAPT/6010/04 S COLD 23-MAR-98 05-SEP-98 EMPTY
1 PCB/8080/04 S COLD 23-MAR-98 16-MAR-98 EMPTY
O C
3- =Sample has not been rad screened.
R7045-001 tv 8 -2 2 -7`
(364122:20) J
Page 1
(364122:20)
(364123:21)
(364122:20)
Screening not Required
(364312:2D)
(364312:20)
(364313:21 364323:22)
(364312:20)
(364316:99)
Screening not Required
Screening not Required-
(364317;99) (J
(364317:99)
(364317:99)
'fJ

Chain of
Custody Record
QUA 4124 0797
Client
gS^ 7 e p^ °^ ^C ^t K
IYU^S!
Project Manager
Dale
C#^l,^Q
1 ^^'C^
,^ SIG ^ R
Address Telephone Number (Area Code) ax Number Lab Number
City Slate Zip Code S ite Contact Lab Contact Analysis
s p (A ttach list if
ace ce is needed
Project Name( /^ ^ 0G
Con(rac t/PUrchasJrderlQu u 00lee No.
S
(4//,(^(I
Sample I.D. No. and Description
(Containers for each sample may be combined on one line)
GO
CarnerANaybdi Number
Matrix
Containers &
Preservatives
Date Time = a ° o o
Posslele na2ara ltlenbhCatlenJ npre ursposar
U
^.
-
Q'banterra
Chain of Custody Numbe
Page of
Special ions ru ec
Conditions of Receipt
(A lee may be assessed i/samples are retained
El Non -Hazard q Flammable El Skin le-dan( El Poison B Unknown Relurn To Chen l q Disposal By Lab q Archive For Months longer than 3 months)
Turn Around Time Required OC Requirements (Speci fy)
l /^ ) ^"J
q 24 Hours J [1 48 Hours q 7 Days q 14 Days V21 Days q Other
^ReMrqu a y' I 1 I^ r - lane 1. ecerved D e Time
—
If
Relinquished By Date Time . Received By Date Time
G elrnquished By Dale Time 3. Received By Date Time
DISTRIBUTION. WHITE - Slays with the Sample, CANARY - Returned to Cleat with Report, PINK - Field Copy
I
I`
I

I
Chain of
Custody Record
S I CDJa'D
QUA 4124 0797
Client Project Manager 1
1 Q^^^
of
Address Telephone Number (Area Code)/F Number Lab Number
C it
y State Zrp Code Site Contact Lab Contact
Project Name J ]\ ! Carner/Waybill Number
Contract/Purchase Order/Quote No.
Sample 1. 0. No. and Description
(Containers for each sample maybe combined on one line)
Matrix
Containers &
Preservatives
Date Time o _ "e n el `^ o = 0 a s 0
N i
Analysis
more space
^3 -1ZS1
(Att
ach list if
is needed
^iivanterra
Chain of Custody Numbe
Page o1
Special Instructions/
Conditions of Receipt
9L 8 g ---
ra v 3 v q C^ ^/ v l^ 8
L1 Non -Hazard q Flammable El Inifant El Poison B
I p
Unknown
rpie lapVSa1
7 Realm Io Client q Disposal By Lab q Archive For Months
(A lee maybe assessed it samples are retained
longer than 3 months)
Turn Around Time Required\^ /
-/
--D o! hlours El Hours El 7Days El 14 Days ^J 21 Days
'Alh fy
l
q I Ulher f I ^ I IJ Kn
J
QC Requirements (Speci fy)
I 5 n( /.k:r 1
LO
..- .. .............. ..r 3are
1. l (/Ll^'V
elinquisheOBy Date Time 2 Received By Data Time
Relinquished By Date Time 3. Receiver) By I Date I Time
DISTRIBUTION: WHITE - Stays with the Sample; CANARY - Returned to Client with Repo"; PINK - Field Copy

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-01 page I of
Collector Company Contact 'Telephone No. Project Coordinator Data Turnaround
R. Fahlberg Steve Marske 373-4316 WEISS, RI.
Project Designation
105C Phase I k Phase If -Conc
Sampling Location AF No.
21 Days
re te Samples 100 A re a B98-061
fee Chest No. Field Logbook No. Melbod of Shipment
_ 3 [land deliver
Shipped To
Quanteria Incorporated
POSSIBLE SAMPLE HAZARDSIREMARKS
0.adiasetive
Special Handling exciter Storage
31 LD
SAMPLE ANALYSIS
T . to I
U^V
Bslte Property No.
N /.^
Preservation
Type of Container
No. of( onlainer(s) 2
^
21
Volume
l^
IL
See item(I)in
Sp«ial
Waiom
SOI[^
^I
Bill of fading/Air illll No.
Ali /!,J
Sample No. Metric • Sample Dale Samplc'1lme *,5^ e
ON680 D I Other Solid -^ y-^ e 10 3 J LCC44 0N k 4 0 1
rI b
x^So r, l- /+ Ce, Fws^ 7wbo
SPECIAL INSTRUCTIONS / _- / Malris-
CHAIN OF POSSESSION Sign/Print Names s
s.,,i
(1)ICP Metals- 6010A(Sigxi 1race) l l-eadl, Mvauy-7471- ( CV) , Chmmiom 11, 7196. '1 t..i.^,ra
ehnquisbedB DalNrime ei By 1^ I Time PCB, X080 JArocl°r-1254 J, Gamma SpecnoscopY ((^"noo 117,C, ,hA60,Furapiuo M, 5p - c°hd
3^ 'a l Aril ^'-7 ( Europium-154, Europium-1551: Amencium- 2 41, Iso topic Plutonium, Isotopic Uranium: Sele sl. - o"J"
9 ^P.^CRIw I-.-t -l9
e q Mime R edBY 1 f Datc/T^me
NI alff -^03 Sf^ 1,9 - j7j/za 5 o wl•
teJ — a I'9( T^t^
y9 mot, ^o I l¢ Av; S^ IJ, 111 opt lnlida
in wished By Daleffime Recei ed By Dalc/linen ] n1 u . 1 .pinr
Nl Wipe
inquished By Dale/rime Received By Date/rim, I I " z
-J
^.eeiau„
nme,
LABORATORY Received By
SECTION
—'lisle
-__ _.. Uatu lime
FINAI.SMIPLE
DISPOSITION
IXsptnal Method - U sposed Bs --------
_
Uatclllme
__
--
1
1

Y
Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES T 1198-061-02
Collector Company Contact 'I elephant No. Project Coordinator DATA "I urnaround
R. Fahlbcrg Steve Manske 3734316 WEISS, RL
21 Days
Project Design ation Sampling Location AF No.
105-C Ph as e 1 R Phase II - Concrete Samples 100 Area B99-061
Ice Ch est No. Field Logbook No. Method or Shipment
Iland deliver
Shipped To Mile Property 1. Bill of Ladin A BIII No.
Quanterra In co rporated
POSSIBLE SAMPLE IIAZARDS/REMARKS
Radioactive
Special Handling And/or Storage
SAMPLE ANALYSIS
903W -burin 6031(^I - ILLcr-
Prae vAlinn
Type of Container
No. of Container(s)
Volume
Sample No. Matrix • Sample Dale Sample Time
ONSB1 N Other Soliq
P
2
IL
6m imm,l, in
Specid
^o/^ D3/,
3 /x/ Z- ^\Ir/ ^^ /d A ^ I
SPECIAL[ TRUC'IIONS Q tau is
CHAIN OF POSSESSION Sign/Print Names Vd ^.,. i
(I)ICI'Meais- 6010A ISupenrace) 1[rid), 7471 (CV) Cluumimn Ile.-7196.
e[i
e'
uished
y
Dale/Time
^ ^ p/
G
DAINI'ime
Reuiv
ive
B
Y On
Date/Time
151
- s
PCBs-80801Atoclor 12541, Gamma Spectnosc. py(Cesium-U7. Cohxll-60, Europium-152,
r-opium; 154, Eumpimm-1551; Amencium-241. Isotopic Plutonium; Isotopic IIranium, Sele
SdPnl sn -^9
r Ni[J^N (03 i Sr- $9 9a-- 7G I S^ "
T h 9 q^, b0fl
1 c-C7
gl
a
tc
"hat
'^t3^.
j
'nquished By Date/Time Received By DaterTime !'^ 1
ZD
'ntonshed By Dalelfime Received By Dalerlime
BORATORY 0.euived By
SECTION
Tine naie'I une
FINAL SAMPLE
DISPOSITION_
Diallo»I Mahod
--
Uisrysscd -- By -- -
- W(" (une
1
s•
-
_.
r
I
^ra.,t,>
I
Iv i
I
^ ;;'-?
l

Client Sample Screening Results
!0-Mar-98
CLIE14TCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCPMB
B M4CI /9/15981:42:00 PM 21A 7/10/199811:27:38 BOM4C1 30 16 A9^3777 e41 27.23 313
IQUID Bk . 3/10/1998 :51 AM BKO 100 4 0.04 0 0.8
AN Do /Ia1998 Alq: 3.00E-01 LDOEMI (DpM 3 .49E-01 (uCl/ 1.24E-05 CU 2.47E+01 ±2.3E+01 QA 0E+00 1.a0^
t mLt 2.1 UdU: L Bet; 3.42E+01 So):fl. 2E-03 LIL): +03 ±8.7E+OI I 2.0
Ue 'ylaq^
BHI BOM4 422
LIQUID
3/9/1998 1:42:00 PM QUAD I 3/10/199811:23'38 AM
7-. 3/10/19988:43:5 998 9:43
BOM4C2
IIK
30
100
6
3
.17
0.03
202 3 937333 -
/
95/ 0.95
AdD 3/1 Tol S., Alq: 3.00E-0 ^O^
E401 Alp; (Dp 0 (uCU 807E-06 (p 1.6 01 ± 2. 4E4 01 AT E+00 Lob
pt mR 2.6
BHI BON680S
NV: L
3 /9/1998 1:42:00 PM QUAD24D
Bel/Alq): /I.IIE I.1+OI
c
3 1 101 1998 11:23:51 AM BON690S
Ljll):
30
3.01E+02 3 +01
1130 37.6066667
I
124390
Alq
1.0E-0
e
4145, 4 333
SOLID Bkg: 3/10/1998 8:43:35 AM BKO 100 6 0.06 90 0.9
Ad Dol es 3/10/1998 To1Ee,Alq: 1.63E+02 9.81E401 Alp; (Dpm/.1.71E401 (uCU . 1.27E-02 (pCU -7.83E+01 ±9AE400 CAT 1.6E402
Lab
Pp/mp 88,1 / UNb: L me Bolt Alq), 9.19E+03 eo): 6. 116E+00 t4e)t 4.22E404 f 1.2E+02
111 /
2.48-03 Alt
1•IL
BHI BON681F 3 /9/19983:13:00 PM QUAD2 1 A 3/10/199811:54:54AM DON681F 30 3 0.12666667 96 2.4
LIQUID like: 3/101 1998 8:43:51 AM BKO 100 4 0.04 8o 01
Ad Delet 3/10/1998 Tot S., Alq: 1.80E+00 1.00E+01 Alp; (Dpm/ 3.23E-0 1 (uCU 2.62E-03 (pCU 1.45E+01 ± 2.4E+01 CAT 1.7E+00 Lab
PptmL: 6.9 U nite: L / ml Bel; Alq): 4.79E+00 So): 3.88E-04 LIL): 2.16E+02 ±3.IE+01 I I 2.3E-ul Alq
LIt
BHI BON6919 3/9/I9983:I 3 :00 PM QUAD2 1 B 3/10/199811:54:54 AM BON691S 30 13 0.40333333 234 6.55
SOLID BkL: 3/10/1998 8:43:31 AM BKO 100 3 0.03 95 0.95
Ad Dole: 3/10/1998 Tot Se, Alq: 1.90E+02 1.15E+02 Alp; (Dpm/ 2.38E+00 (uCU 1.93E-03 (pCU 1.02E+01 +5.3E+00 CAT 49E400 L.b
Pp/ me: 114.3 / Units: g i mg Bet; Alq): 1.35E+01 Sa): 1.16E-02 Lit): 6.08E+01 ± 4.6E+00 1 1.6E+00 Alq
ide
BHI BON69OF 3 /9/19981:42:00 PM QUAD24C 3/10/199911123:51 AM BON68OF 30 43 1.39333333 3426 113.39
LIQUID Blig: 3/10/19989:43:55 AM BKG 100 4 0.04 81 0.81
A nt Dole: 3/10/1998 Tot Se, Alq: 1.80E+00 1.00E+01 Alp; (Dpn3 4.48E-0 1 (uCU 3.64E-0 5 (pCl/ 2.02E401 + 2.2E+01 CAT L2E400 I..b
N P t m 3.4
P P Units; 1, ml Bet; AI 2.14E402
9):
n
So :
) 1.74E-02 L C): 9.66E+03 ± 1.7E+02 1 / 5.2E-03 Alq
Ide
10-Mar-98 Quan(erra Environment Se rvices, SCP V2.03 1

OateRme Received:
FIVISM t
SAMPLE CHECK-IN UST
y J^/3 S start (^(/0^1^
o
Work Order Number 0 ^0 ^^ SAF i J 11S - " t
Shipping Cantainv I-l
1f
b fain of Custody rt
fi ^1
RMSOW-43 -0003 -
1. Custody Seals oosttpp- g mr I iietibf ? Yes [pw[ I
Z
Custody Seals dated and signed?
Yes.H', [ I
3. Chain-d-Custodf rer 9 d preswe Yes [ I
1 t GC
4. Cooler temperature
5. VermicufiWpaddm materials is Wet [ j 'rl
6. Number of samples in shipping =muter.
Revision 5
YT'^ ^'
7. Sample holding 5nes exceeded? Yes [ ; uo [ }^
8. Sampws have:
pe hazard labels
dy seats maple labels
9. Sam s are_
__,Lim good mrdifiaon kalong
broken _gave air bubbles
10. Where any anomalies identified in sanpte receipt? Yes (j No
11. Description of anoma lies (utc'.ude sample numbers):
Sample Custcdia n/Laboatnrf.* —X. LL LIu.^ Date:
Telephoned To: Dn^_By
0000 11

Five* 1
SAMPLE CWCK4N UST
DatePrme Received:^ J 1 `J7S SGS W(),U7J
RFSHSOW 93-4003
Revision 5
ak
Work Order Number 86310 + 164 1 SAF * e9
g
A -
y
Shipping Container 10:W635 a%& of Custody * Imo( (1 - U.9 1 - 0a
1. Custody Seals an sltippi 9 container irfart? Yes Hl c ( ]
2 Custody Seals dated and signed? Yes ( No ( ]
3. Chain-of-Curb* n=rd present? Yes ]
4. Cooler temperak re
5. Vermiculite/pacidng materials is Wet [ Dry [ Y, /-A
6. Number of swoes in shipping ccldai er
7. Sample holding Imes exceeded? Yes [ ] No [ 9^
8.
3 '
have:
tape
custody seats
9. Sam are
in good con diti
on
broken
hazard lab els
?ppo¢iate sample Labels
kaking
Rave air bubbles
10. Where any anoma lies identified in sample receipt? Yes [ ] No [-]------
11. Description of anomalies (in clude sample manbers):
l eiepnui i^ 1 u. w by
0
Y
600012

Environmental
Contractor
Contractor ERC Team
Interoffice Memorandum
M. A. St. John x.0-19
40mm` Scc Below
°"7e l;ebruary 27.1999
0-o' S. L. Wi^ow
RadCun Eaginceriag
X3411531-070,
wuEcr. CVHlF FSTTMATE FOR S111PP1NC CONCRFTF. CORE SAMPLES
CCN: 055088
Job So. n1 92
W", O.P. Xft.I w
w
Oil a 1«c
MA w
$
C. !LO
The 1•olluwing calculations show that cvn: satnplawith a direct reading of equal to or less than
400.000 dpm/100cm' will be below the de fi nitionafradimttive mate rial as defined in 49 CFR 173.40 3
of 70 Bq/g (2F.3 pCi/g). L'ach sample will consistofcoacrcte mate rial from Ibur, two inch co re
samples and enough wat er to make r slum consiotocy. The distrihution of radionuc lides is bussed tin
previous concrete samples taker from the below grade Fad Storage Basin that would also he
representative of these cuncrcte samples.
iven:
Cylinder Vulurrtc = ttr'h Radius ofcaocrcte core (r) = I inch
Concrete Density = 2.35 g/cm' Height of care sample taken (h) - 0.25 inches
27 pCi = Dq Maximum & Lt Wading on core = 40,000 dpm/ 1 UUcm'
2?2 dpm = pCi
Calculations:
V - (3.14) (1 in.)'(U 25in) =0.78 in' (16.4 cm'/irrl(4 mix samples) = 51.2 cm,
(400,000 dpm/51.2 cm') (cm'1235 g) = 3.32E3 dpdg
3.32ED dpm/g (pCi/2.2 dpm) = 1.SE3 pCi/g or 9.4 8419
SI.W:did
Percent Distribution(7) Concemratina (oC: i/c)
ACo 0.17 2.55 pCi/g
'rrCs 82 1.2F3 pCi/g
131 E 0.33 4.95 pCi/g
134 E 0.05 7.5E-1 pCi/g
'Sr 17 2.55E: pC ilg
741 Am 0. W5 7.5F Z pCi/g
n9 210p u 0.1 1.5
TOTAL: 1.460 PCi/g
C(2 j! 5E
S. 6. Marske X5 -53
P. A. Newman X3-41
RadCun Enginee ring File/LB X0-23
Document and into Se rvices 1 10-09 00001)

eo-Z/-7b 11=ZBA RAOCC" 373 an7o n - C.
Environmental
Restoration =RC Team
Contractor
Interoffice Memorandum
To` D. A. St. John 1.0-19 da:
`o^''`` Sec Below nmr:
Concentration (vCi/e)
2.55 pCi/g
1.2F3 pCi/g
4.95 pCi/g
7.5E-1 pCi/g
2.55E2 pCi/g
7.5F.-2 pCilg
1.5 '/
I.46L3 pCi/g
February 27. 1999
S. L. Winslow
RadCon Engineering
X3-41/531-0706
suwzcr: CU141F FSTIMATE FOR SHIPPING CONCRETE CORE SAMPLES
Job N9.22192
DrOr,. ww
^Y^r ww
a^. ieec
AA
S w,
ww
ibwl CeA. 41W
CCN: 055088
The following calculations show that cu re samples with a direct reading or equal to or less than
400,000 dpm/100cm = will be below the de finition ol'radivactive mate rial as de fined in 49 CFR 173.40 1
of 70 Bq/g (2F.3 pCi/g). Each slugrle will consist of comrctc material from tiour. two inch core
samples and enough water to make a slur ry consistency. The distri bution of radionuc lides is based tun
previous concrete samples taken f ro m the below grade Fuel Storage B asin that would also be
representative of these concrete samples.
"ven:
Cylinder Volurnc = nr'h Radius of concrete core (r) = I inch
Concrete Density = 2.35 g/cm' l leight of core sample taken (h) = 0.25 inches
27 pCi = Bq Maximum direct reading on core = 400.000 dpm/lOUcm1
2.22 dpnn = pCi
Calculations:
V = (3.14) (1 in.)'(0.25in) = 0.79 in' (16.4 em'/in) (4 mn; samples) = 51.2 cm'
(400.000 dpm/51.2 cm) (cm'12.35 g) = 3.32E3 dpm/g
3.3213 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 BWg
S1. W AId
"'Ca
Percent Distribulion( 7o )
0.17
[IT
CS 82
12Eu 0.33
"°Eu 0.05
°0Sr 17
7°'Am
ZJ
"PU
0.005
0.1
TOTAL:
C(! ics:
S. G. Mtuske X5-53
P. A. Newman X3 -4 1
RadCun Enginee ring File/LB XO-23
Document and Info Se rv ices HO-09
GOOOi4

Quanterra 6W V S 014488
Effiroameattl
Son=
Condi ti on Upon Receipt Variance Report
St. Louis Laboratory
3
Client. _ Daze:_
Project No: -Sz) 2- Initiated by: oz,
f
Shipper/No: A i r b• rrt C RFA/COC Numbers: l Q y L4
Condition/Variance (Check all that apply):
1. q Sample received b roken leaking.
2. q Sample received without proper prese rv ative.
q Cooler temperature not within 4C ± 2C
q pH
q other:
Record temperature:
3. q Sample received in improper con ta iner.
4. q Sample received without proper paperwork. Explain:
5. q Paperwork received without sample.
6. q No sample ID on sample con tainer.
7. q Custody tape disturbed broken/missing.
q No variances were noted during sample receipt. Cooler
/
Login No.: / ^7/9'
8. q Sample ID on con tainer does not match sample ID
on paperwork. Explain:
9. q III coolers on airbill not received with shipment.
10. q Other (explain below!:
Temperature Upon Receipt:
Notes: C^ ' /, 5 ^— CJrt ^G(/t-e..s, So /cJl-I
Corrective Action:
A F C 0 1
CL I/,
/ L( 0 Lc t >fX
v=
q Client's Name: Informed verbally on: By:
q Client's Name: Informed in writing on: By:
q Sample(s) processed "as is".
q Sample(s) on hold unt il : If released. notify
Sample Control Supe rvisor Review: (or desienat Date
Project Management Review: (A— 71 G.,i^,— Date: 3 — If — ^.3
SL-ADMIN-0004. Rev¢ed 1121;95
SIGNED ORIGINAL xIL:ST BE RETAI N-ED IN THE PROJECT FILE
(p
^rC—
^i,Ji5

O
C
L=,
C
r4
Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-qb't'-0I
Collector Company (outnel I elrphone No. Project f nnrdinalor Wim I or11Nr n11111I
R. rahlberg Sieve Mnrske 171-411 1, WrISS, lll.
Project Designation
105-0 Ph ase 1 k Phase 11 -Concrete Samples
Sampling Lo ca tion
100 Area `
'AF No.
1198-0(I3
Ice Ch iral No. Field Logbook No. Method of Shipment
_ Iland deliver
3
fL
Shipped To )Belie Property No. 11111 of LadInR/Al, IIIII No.
Quenterra Incorporated N
POSSIBLE SAMPLE IIALARDS/RE AIARKS
Radioactive
Special Handling and/or Storage
8032150) G,
g o3aic^oi
I j^
(S
Preservation
Type of Container
No. of Conlabrer)s)
Volume
N°^r I -I
P
2
IL
5

1
Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST
Collec tor
R. 1'ahlhera
Project Design ation
105-C Ph ase I R Phase 11 - Concrete Samples
Ice Chesl No.
Shipped To
Quanleres Incorporaled
POSSIBLE SAMPLE IIAZARDS/REIIIARKS
Radioactive
Con+pany /'u ntact '1 e""'eNo.
Alcvc 1,10,4C:171-4716
Sampling Location
100 Aren
Field Lagbooh No.
L: -- L — l r ,. `
I
Project (bnrdin ldw
wFlxs. Ill.
SA F No.
I19 9 -01" 1
Nlethad of Shipment
(land deliver
Offislic Properly No.. BIII of lading/Alr Bill Nn.
il.i
Prtacnalion
I ype of fbnlRiner
No. of Conlalner(s)
Special llandlag end/or Storage
go3a^ ^ &YPU oa
SAMPLE ANALYSIS
Volume
Q^
L
BOA) 89
%^I LL I r 1 UIL41--1 ID 11 1\-LUll
p
2
IL
a«^ Ii5 in
063
u9x-Iwt o4 i ' ' ye !n' !
DAN 'l urnnnnmd
'n'l^o'•a' +
Sample No. Ma (rla• Semple Date Sample IIme N .. } vTe!.^. CVas , jl+^:n,tl ;]'-;a1 tf+ l! p^ ' sn-^
Othar6eRd-
1)
^- /Q " 9 cT
IAIN OF POSSESSION SIgNPrint Names
R npuhhed ^
/ '
S O
aldflm^ R ived By Daleyl irne
el uished8 By DnNllme
ReceNed0By Dat ime -G /
Impoished By Wicnime Received By Wlerlime
npuished By Dalerlime Received By Dale/lime
BORATORY
SECTION
FINAL SA pIP1.E
DISPOSITION
21 Days
Oft ^l y y^ x.,^%.- "7 _ +
SPECIAL INSI RUCTIONS
O ICP McWk 60104 S.. ( Pubacel lLeaJ), Mvcuq-7471-(CVI. Chromium tic.-7196,
PCI]s; 1100.0 254 1. Omnma Speetrnscq, ICesimn-117, COWL-60. r:uropium 157,
L.,.pmm . 134, Ellropium-1511, Amtpcitim-24 I', Isowrie Phllnili mn, knlnplc Upnnim, 5ele
Q n+hc/ -^ 9 /l/r-l.Kel (o3 Sf -&'9 50-- yp,^ /jr•
fi2o1299 ' Ci rbo t ^¢ ' 4c -iVr SCaot
/
Retsived By title Dam/lout
Disposal Mtlhod UispuuJ Uy
(^
_—_—___
Ualc/Iona
hSAllli
s s...l
to o,6,1
11 bade[
u - ol
4
Ill
WI
u,
q',re
\, \f4' r
^
..

Bechtel Hanford Inc. CHAIN Ole CUSTODY/SAMPLE ANALYSIS REQUEST u^xyet^Dt ! "' -'
olleclnr Company /'onlacl 'I elephone Nn.
Project ('oordinalor
R. rahlhcrg ./] Steve Mw4c 171 -4116
N119 1" S. It 1.
Project Designation Sampling Loca tion
'AF No.
105-C Phase 1 k Phase If - Concrete Samples 100 Arcn 1398-061
Ice Cheat No.^l /I^/^^^
JM 15
_
Field Logbook No. v
Method of Shipment
1lnnd deliver
Shipped To Offdle I'ropnly Nu 11111 of Lading/Air 11111 Nu.
Quanlena Incorporated AJ
OSSIBLE SAMPLE IIAYAR/RERIARkS
OS
RWIosed.8
pedalItandlingand/orStorage
^
1 l^lf{
SAMPLE ANALYSIS
1'yuerral an
Type of Container P
No. of Contriner(s) _
Volume
SD3^JS0e3 ^,,... gD^JC^3^
See 11em 1)' n
SMW
Sample No. Matrix • Sample Date Sample I une ) l^I - l} y}grrGr y, +1iA l. 4j j ^,f{P S!,.. T 5 5,1 : 4 t "` r
$ 0,(18 9 b G V('f1
Other Becht- ^^^- ff ^^^ CD
AIN OF PO ION Sign/Print Names
li ish By /] ime 1 Ree y Uaro/f lne
e 1 YI 0 1
/
ellnqu ithed By J DMNrime Received By % D.Wl,.c
eiinquished By DatdTime Received By Date/1imc
elinquished By DodeoM a Received By WWI u,
t"oNr"""
G
6
Ditta I nrnaround
21 Days
-- --
SPECIAL INSTRUCTIONS Liavis
(1) ICP Metals- 6010A ISupMmcel l Lead l'. Mncury -7471-(CV), Chrmnimn lln -7196,
PCBs - R080 lAroclor-11541; Gamrna Spectroscopy (Cesium-137, Cuhah-60, Europium-157,
N ropio n-154, EuropiumAinericimnPiuwnin,n;
-1551, -141; Isumpic Isrnnpic thorn mn; .Sete
/
^/Gl^l ( u-k'I -^9j /Ul (,^^ - r03 SV'- 8 Cf ^jQ
l
—tzek 99 . Carbon 4; 11C ¢,v1hJ'
/
LABORATORY Received By
_--_—_
role umdGmc ._
SECTION
FINAL SAMPLE
DISPOSITION
Dispovl Method Ustwsed By - llaic lime
5 1.
9p S„i,4
°,
n, u., I,^,m
t ..
Nl nTr
1

C^
C-3
C)
1"J
Cz
Client Sample Screening Results
12-Mar-98
12-Afar-98
Quanterra Environment Se rvices, SCP V2.03
/ ^
`N
3I^ZI11^
CLIENTCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCPMB
Bill BON697 3/12/1998 QUAD2 1 A 3/12/1998 11:01:02 AM BON687 30 7 0.18 74 1.54
LIQUID Bkg: 3/12/199812:01:04 AM BKO 600 32 0.05333333 556 0.9266667
Ad Dole: 7/12/1998 Tot So, Atq: 1.00E+00 I.00E+00 ^ Alp; 3
p; (Upm/ p - 8.19E-01 (uCU 3.78E-04 (pCU 3.78E+02 ±3.9E+02 CAT 6.6Ei..b
-02
Ppl mp 49 .6 / Units; 1 1 ml Bel; Alq): 3.27 E4 00 So): 1.48E-03 Leg): 1.48E+03 ± 2.8E+02 I 3.4E-0 2 X116

C
U
Client Sample Screening Results
12-Mar-98
v") ') 1 ^1 0
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM R
POW BON0 119 3/12 1 1998 QUAD2 1 B 3/12/199811:01:02AM BON0 1-19 30 5 0.105 155 4 1733333
LIQUID BkC: 3 1 12/1998 12:01:04 AM BKO 600 37 0.06166667 536 0.8933333
And Date: 3 1 121 1998 Tot Sa, Alq: 1.60E+01 I.00E+OI Alp; (Dpm/ 2.08E-0 1 (uCi/ 1.50E-04 (pC'V 9.36E+00 ± 2.3E+01 CAT 2.7E+00 Lab
Ppt mg: 7.4 i U nits: L ml Bet; Alq): 8.31E+00 Sa): 5.99E-03 LlC): 3.74E+02 ±3.7E+01 I 1.3E-01
POW B0 1 , 1010 3/12/1998 QUAD2 1 C 3/12/199511:01:02 AM B0 1,10J0 30 7 0.18833333 148 4.0233333
LIQUID RkC: 3/12/1998 12:01:04 A61 BKG 600 27 0.045 546 0.91
An] Dale: 3/12/1998 Tot Sa,Adq: 1.60E+01 1.00E+01 Alp; (Dpm/ 4.81E-0 1 (uCV 3.47E-04 (pCt/ 2.17E+01 ±2.3E+01 CAT 1, 2E+00 Lab
Ppt nil: 7.5 Units: L ! ml Bet; Alq): 7.89 E+ 00 Sa): 5.69E-03 LIC): 3.55E+02 + 3.6E+01 I 1.4E-01
Iq
Lit
POW BONOJI 3/12/1998 QUAD2 1 D 3/12/199811:01:02AM BONO31 30 12 0.31166667 132 3 3 75
LIQUID BkC: 3/ 12/199812:01:04 AAI BKO 600 53 0.08833333 615 1.025
Ad Date: 3/12/1998 Tot Sa, Alq: 1.60E+01 / LOGE+01 Alp; (Dpm/ 9.54E-0 1 (uCV 6.88E-04 (pCi/ 4.30E+01 ± 2.7E+01 CAT 5.8E-0 1 lab
P P1 m L 8.7 /
Units: L ml Bet; AI9) 6.56E+00 Sal: ) 4.73E-03 L IL): 2.96E+02 + 3.4E+01 I 1.7E-01 Alq
LIC
POW B0 1,14 119 3/12/1998 QUAD22A 3/12 1 1998 10:40:55 Abt BON4119 10 2 0.14666667 10 0.135
LIQUID BkC: 3/12.! 1998 12:01:14 MI BKG 600 32 0.05333333 519 0.865
Ad Date: 3/12/1995 Tot Sa, Alq: 2.00E+00 I.00E+01 Alp; (Dpnd 4.31E-01 (uCV 3.88E-05 (pCi/ 1.94E+01 ± 3.4E+01 CAT 1.3E+00 Lab
li ps ring: 2.7 / Units: L ml Bet; Alq): 1.65E-0 1 Sa): 1.48E-OS LAC): 7.41E+00 + 2.7E+01 I 6.7E+00
POW BON541 3/12/1998 QUAD22B 3/12/1998 10:40:55 AM BON541 t0 2 0.15166667 22 1.2516667
LIQUID BkC: 3. 12/199812:01:14 AM BKG 600 29 004833333 569 0.9483333
,W Date: 3/12/1998 Tot Sa, Alq: 1.00E+00 / 1 OOF- 01 Alp; (Dpn t/ 4.34E-0 1 (uCV 1.95E-05 (pC'V 1, 95E+01 +3.6EWI UA2 13E+00 Lab
Ppt ring: 2 / Unlls: L ml Bet; Alit): 2.30E+00 S.): 1 03E-04 LIC): 103C+02 + 4 .0E+01
Alq
N
Lig
1 Alq
4 SE-01
II I
POW BON595 3/12/1998 QUAD22C 3/12/199810: 40: 55 ANI BON595 10 1 0-04333333 14 0.4783333
LIQUID BkC: 3/12/1998 12:01:14 AM BKG 600 34 0.05666667 553 0.9216667
0 Ant Date: 3/12/1998 Tot S&Alq: 2.00E+00 / I.00E+01 Alp; (DpnJ 1.14E-01 (uCV 1.03E-05 (p(-V 5.13E+00 +3.3E+01 CAT /4.9E+00 lab
i
C
P Pt m G 2 / Units: L nil Bet, AI9h 8.68E-01 Sal: ) 7.82E-05 L IL ): 3 91E+01 + 3.2E+01 1 1.3E+00
AIq
1-IL
12-Mar-98 Quanterra Environment Se rvices, SCP V2.03

K) 'ApItN
CLIENT CODE ID MATRIXRECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
POW BON5 133 3 1 12/1998 QUAD22D 3/12/1998 10:40:55 AM BON5 133 10 1 0.055 22 1.2633333
LIQUID Bkg: 3/12 1 1998 12:01:14 AM BKG 600 27 0.045 562 0.9366667
AN Date: 3/12/1998 Tot Say Alq: 2.00E+00 1.00E+01 Alp; (DpM 1.27E-01 (uCV 1.14E-0 5 (pCV 5.71E+00 ± 3.5E+01 GAT 4.4E+00 Lab
Ppt mg: 3.7 / units: ts: 1, ml Bet; Alq): 2.36E+00 So): 2.12E-04 Llg): 1.06E+02 ±4.OE1
1
4.7E-01
AIy
I-I[
POW B01, 1589 3/12/1998 QUAD23A 3/12/1998 11:01:05 AM DON5 119 30 1 1 0.33166667 51 0.81
LIQUID Bkg: 3/ 12/199812:0 1.20 AAI BKG 600 21 0.035 534 0.89
AN Date: 3/12/1998 Tot Sa, Alq: 2.00E+00 1.00E+01 Alp; (DpM 937E-0 1 (uCV 8.80E-05 (pCV 4.40E+01 ± 2. 2E+01 CAT 5.7E-01 Lab
Ppt P P mL 3.3
Units: L ml Bet; AI9): 1.34E+00 Sa ) : 1.21E-04 L I[) 6.05E+01 + 2.0E+01
1
8.3E-01
AN
POW B0 1 , 1 50 3/12/1998 QUAD23B 3/12/1998 11:01:05 AM BONK5 30 5 0.09333333 40 0.3516667
LIQUID Bkg: 3/12/1998 12:01:20 AA1 BKG 600 44 0.07333333 589 0.9816667
Ant Date: 3/12/1998 Tot So, Alq: 2.00E+00 / 1.00E+01 Alp; (DpM 2.79E-0I (uCV 2.51E-0 5 (pCV 1. 26E+01 ±2.1 E+01 CAT 2.0E+00 Lab
Ppt mg: 2 ,- U nits: L ml Bet; Alq): 6.12E-01 So): 5.51E-05 Llg): 2.76E+01 + 1.9E+01 I 1.8E+00 Alq
POW B0N5D1 3/12/1998 QUAD23C 3/12/1998 11:01:05 Abl BON5D1 30 13 0.38666667 49 0.725
LIQUID Bkg: 3/12/1998 12:01:20 AS1 BKG 600 28 0.04666667 545 0.9083333
AN Date: 3/12/1998 Tot Sa, Alq: 200E+00 LOOE+01 Alp; (D i n/ 1.12E+00 (net/ 1.01E-04 (pC'I/ 5.05E+01 +2.3E+01 CAT 5.0E-0 I Lab
Ppt mg: 2 / Units: L ml Bet; Alq): 1.17E+00 Sp: 1.06E-04 L [): 5.28E+01 ± 2.0E+01
1
9.5E-01
AlqIt
POW BON6 1`9 3/12/1998 QUAD23D 3/12/1998 11:01:05 AM BON6E9 30 8 0.21333333 32 0.1533333
LIQUID Bkg: 3/12/1998 12:01:20 AAI BKG 600 32 0.05333333 548 0.9133333
AN Date: 3/12/1998 Tot So, Alq: 1.00E+00 1.00E+01 Alp; (DpM 6.29E-0 1 (uCV 2.83E-05 (pCV 2.83E+01 ± 2.1E+0I CAT 8.8E-01 Lab
Ppl mg: 0 Units: L ml Bet; Alq): 1.54E-01 So): 6.94E-06 LIg): 6.94E+00 + 1.6E+01 1 7.2E+00 AIq
Id[
POW BON6H0 3/12/1998 QUAD24A 3/12/199811: 00: 58 AM BON6110 30 4 0.06833333 36 0.2416667
LIQUID Bkg: 3/12/199812:01:08 AAI BKG 600 39 0.065 575 0.9583333
C^ Ant Dole: 3/12/1998 Tot Sa,Alq: 1.00E+00 I.00E+OI Alp; (Dpm/ 2.04E-01 (uCV 9.20E-06 (pCL/ 9.20E+00 +2.IE+01 CAT 2.7E+00 Lab
(J
Ppt mg: 0 Units: L ml Bet; Alq): 4.29E-01 So): 1.93E-0 5 Llg): I.93E+01 + I.BE+01 I 2.6E+00
All "It
12-Afar-98 Quanterra Environment Se rvices, SCP V2.03 2
AIL
1.1[

0uanterra March 23, 1998 03:02 pm
Account: 10722 Project: 550.260 ouanterra-Richland OAS No. 550.26 Rev. 2
Project Manager: N. Price
Master Sample Login: 17200/1
pf
Draft: Final: Entered and Reviewed by PM Review: !/^/\—
7^^1
r 1 fw^
Sample Header Template:
.^ (`
pll f,
A j( 1'. F
^'^ 1 - TOU^ 7
+aT"rT'
M^
Of *007
Sample No.
Co
Client ID C-Matrix Date: Collected Received Due Shipper Red Category gad SalRp(e No.
mm ents
N
Data:
Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:% Filled) I ,^ LZ-,^f
L—
17200-001 BON685 Solid 11-MAR-98 08;30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80320501//ICAPT = PIT ONLY//PCB 1254 ONLY///THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17200-005).
1 PN - Plastic-1 1, HG/7471/Q4 S COLD 27-MAR-98 08-APR-98 R5B (364124:99)
1 ICAPT/6010/04 S COLD 27-MAR-98 07-SEP-98 R5B (364124:99)
1 PCB/8080/04 S COLD 27-MAR-98 25-MAR-98 R5B (364124:99)
17200-OOIMS BON685 Solid 11-MAR-98 08:30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80320501//ICAPT = P8 ONLY/(PCB 1254 ONLY.
1 PN - Plastic-1L HO/7471/Q4 $ COLD 27-MAR-98 08-APR-90 R58 (3641Z4:99)
1 ICAPT/6010/04 S COLD 27-MAR-98 07-SEP-98 R58 (364124:99)
1 PCB/8080/Q4 S COLD 27-MAR-98 25-MAR-98 R5B (364124:99)
17200-OOlMSD BON685 Solid 11-MAR-98 08:30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80320501//ICAPT = PB ONLY//PCB 1254 ONLY.
1 PH - Plastic-1 1. NG/7471/04 S COLD 27-MAR-98 08-APR-90 R56 (364124:99)
1 ICAPT/6010/04 S COLD 27-MAR-98 07-SEP-98 R58 (364124:99)
1 PCB/8080/04 S COLD 27-MAR-98 25-MAR-98 R5B (364124:99)
17200-002 BON686 Solid 11-MAR-98 10:00 11-MAR-98 11:57 31-MAR-98 AIRBORNE 3 87042-001
RICHLAND I.D. 80320502//THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17200-004).ICAPT = PIT ONLY.//PCB 1254 ONLY;
1 PH - Plastic-1L HG/7471/Q4 S COLD 27-MAR-98 08-APR-98 R5B ' (364125;:99)
1 ICAPT/6010/04 S COLD 27-KAR-98 07-SEP-98 R5B (364125:99)
1 PCB/8080/Q4 S COLD 27-MAR-98 25- 14AR-98 R5B (364125:99)
17200-003 BON687 Solid 11-MAR-98 13:05 11-MAR-98 14:20 31-MAR-98 AIRBORNE 1
RICHLAND I.D. 80320503//ICAPT = Pit ONLY//PCB 1254 ONLY///THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17200.006)
1 PN - Plastic-1 1.HG/7471/Q4 S COLD 27-MAR-98 08-APR-96 R5 0
1 ICAPT/6010/Q4 S COLD 27-MAR-98 07-SEP-98 R58
i PCB/8080/04 S COLD 27-MAR-98 25-MAR-98 R58
,1-200-004 BON896 Liquid 11- 140 -98 10:00 11-MAR-98 11:57 31-MAR-98 AIRBORNE
G RICHLAND I.D. 80321503//ICAPT = PS ONLY//AROCLOR 1254 ONLY///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17200.002.
1 PN - Plastic-1 1.HG/7470/04 S COLD 27-MAR-98 08-APR-98 R5B
d 1
J i
ICAPT/6010/04
PCB/8080/04
S
S
COLD
COLD
27-MAR-98
27-MAR-98
07-SEP-98 R5 11
18-MAR-98 R5B
3 - =Sample has not been rad screened.
Page 1
(364126:99).
(364126:99)
(364126:99)
Screening not Required
1 Screening not Required
(364324p99)
(364324:99)
(364324:99)
^^UO2LG^

Project Manager: N. Price
Ouanterra March [3, 199B US:UC pm
Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev. 2
Master Sample Login: 17200
Draft: Final: Entered and Reviewed by: PM Review:
Samp le Header Template:
Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Red Sample No,
Comments
p Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:% Filled)
Data:
17200-005 DON685 FILTRATE Liquid 11-MAR-98 08:30 11-MAR-98 11:57 31-MAR-98 AIRBORNE
RICHLAND I.D. 80321501///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17200-001.
1 PN - Plastic-1L HOLD//04 S COLD 27-MAR-98 21-MAR-98 R58
17200-006 BON687 FILTRATE Liquid 11-MAR-98 13:05 11-MAR-98 14:20 31-MAR-98 AIRBORNE
RICHLAND I.D. 80321503///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17200-003.
1 PN - Plastic-1 1.HOLD//04 S COLD 27-MAR-98 21-MAR-98 R58
r-,
U
C^
3 - = Sample has not been red screened.
Page 2
t screening not ..R" !red
(365372:99)
1 Screening not Required
(365373:99).

^
Chain of
Custody Record
UOA 1134 11 19 7
Cleat
f3f^ l,lf^
51
Project Manager
L 6 0^S^;C^
t
Dal
I-Izr1^
Address Telephone Number (Area Code)/F Number Lab Number
Qty State Zip Code Site Contact Lab Contact
Prolecl NameA ' -
1
Contract Purchase Order/Quo te No
Sample 1. 13. No. and Description
(C:onldumas for each sample may be combined on ono line)
Date Time
Carder/WaybIll Number
Ma trix
1 wh. - i a,ard munnncen m pyrnple rn 1-0 al
^.-y I Non Hazard
q Flam m able f] Skm hrifanf q Poison B Unknown I
L ^XI
f
-Iurn Around Time Requeed
^
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4 flours q 4 8 Hours q 7 Days q 14 Days 21 Days q ^ Iher ^^ ^^ ^_
„ q^ e N y
Date ,^e
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l
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I

Ilecldel Ilan ford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES T u9a-Obi-ul 1''b` !
Collec for Counpauy Cnulocl 'I vlrphone No. Project l'unnlblalur I).Ia I or'us roond
It I uhiber8 slave KSnu.ske 171-4116 VVV.1.SX, Ill.
foujoel Designation Sampling Location
105-4' Phase I & Phase II -Concrete samples
100 Area `
AFNo.
1.—d)73
lu Chest No. Fi eld Logbook No. Method of Shipment
_ Iland deliver
hipped To ORaI(e 1'rnperty Nu. IIIII of Ladil KIA it 11111 No.
Qumncrra Incorporated N ^f- N 3f
POSSIBLE SAMPLE HAZARDS/REMARKS
RWlaanva
pedal Handling and/or Sto rage
A03^1 Sol /1 WmI
^D 3^1^/I ^lGl
SAMPLE ANALYSIS
Preservation
Type of Container P
21 Days
No. of Conlaiucr(s) 7 _.
Volume
IL
Sn ium I , In
I^^"^`I^°^•
"'"o,
sample No Matrix • Sample Da te sample'l imc ^`, ^", ', {^. ' 3g{ payenn '^ k 9 d 1
LN-
x"689- Other 6elirY
S -^ C^^ /[^ ,^ L^ LCK,1!1
e)N8 N L1eJ" 1
l—L
CILUN OF POSSESSION Sign/Print Names
Reliogai.hed 05 r Dwe/yLne
J -4'-Y a
Iq c 1
I P 2^^_, ^5 —
Ic/time
I
eel d 0y
l., A
I /rim.
I -1
R edgy 1- ` / Ua1e/I'ime10'-
eiu niched By UaWI...m Recei ed By WWI im. //
ioquishcJ By Dwcil ne Received By D.ICIFimc
IAIIOIIATORV
SECIIt1N
FINAL. SAKIPLE
DISPOSII ION
SPECIAL. INS'fRIICI'IONS
I ICP Mail. - 6010A S,, nuce Leal ' Merco 7471 - CV Chromium Ilea 7196;
NCB. - 8080 1Aroclor-13341; Gamma Spearosoupy IC.s om-137. Coba1660, Earopiwm 153,
liuopiwm 154. Luopiow 1351. A... oral-741; 1.°mpic Plwmmun; bolapie Unnlmn: S ol e
SeleR,w&- -'t9^ MLtCI-63 Sr- 5 5^ •
3ri, o -- tDrn-1
}Ee^t7^ - G0. r{J Uvl l¢ Fl cliv, t^ s^«-.,
Received By Title Dmdfimc
e•
—
f Q
1,5 A..
DL u,
T 1.:
W I W."
I. Ilq.i J
V yew^°n
x 0Lh,
I
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l
1
Manix
1LIDI
so - Sa6d
SL - 5;-1,
w"`
Di.po..I Mahal —. .-_
- -- Urs 1,used o y Dale/1'imc --
l=11
4
y

Iicchlel IlBnford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST lil8•h(fioI .,
'ulleclor
R Pnld6c tp
Project D es ignation
105 C Phase I & Phase 11 - Concrete Samples
Coulpuly Con fact
.1
hour Nn.
Slew Mnrskc :171-4116
Sampling Location
IDO Arco 1
Ice Ch es t No. Field Logbook No.
Shipped To
Quanleua Incorpo rated
POSSIBLE SAMPLE IIAZARDS/REAIARKS
RaJioanirc
peclal llandiing and/or Storage
1: - L- — / I o ^ `
Offrlle Proper ly No
`Q
Preservalion
'Iypc of Container
^60301^^ -m x,27 Da y
SAMPLE ANALYSIS
N^^•
No. of Conlainer(s) 1
Volume
IL
P
,..3'nW a
Project Courdlnalur or
WI T S$, Ill.
•AF No.
1198- 061
Alelhod of Shipment
hand deliver
Bill of LadinWAir Bill Nn.
iV A
fl urnaruund
No....O^a 1
21 Days
Sample No Matrix • Sample Dare Sample ' I hoc 4y i -...
Ilf 1Sk+x yux6^/3 eJ;
gef^.I4I
/5,;1'.^lfq ^' 1.
60.1. -64 Other 6elicY ^- /o- 9v" t7 fl s'^ `^ ^
..
/
x.o/^. , -•" 7 Yl t
onl8 q S
^'^'"
IAIN OF POSSESSION Sign/Print Nunn
R inquirhned 'pn\1 alelfim
1L^5°, S^^ 3 I^ ' ^3
R ived Dy Dalell'iine
_ r,
du uishcd DY Uale/Time R

0 J
d
^I
C)6-3
Ilechlel Ilanforll Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B9XybrBI
Collector ,y-
R. ISddhcrg 13I- ./(.J
Project Designation
105-C Phase I & Phase 11 -Concrete Samples
Company Conlacl 'P

C^
G
LJ
C%
ry
00
Client Sample Screening Results
12-Afar-98
CLIEN'1' CODE 11) AIATIUX RECEIVED DETECIOB ACQ DATE SAMPLE
DIII I1ON687 3/12 1 1998 QUAD21A 3/12/199811:O 1:02AM BON687
LIQUID Bkg; 3/12/199012:01:04 AM BKO
MINUTES CNTS A NET CPAI A CNTS 8 NET CPA1 B
n
30 7 0.18 74 1.54
600 32 0.05333333 556 0.9266667
Aid Ilde: 3/12/1998 To1 So, Alq: 1.00E +00 3 IAOE400 Alp; (Dyad 8 .39E-0 1 (uCll 3 . 78E-04 (pCU 3 .78E+02 ± 3 .9E+02 CAT / 6 .6E-02 Enk
Ppl uq: 49.6Units; 1. nil Bel; M q): 3.27E+00 Su ) : IABE-03 uv: 1.48E+03 f 2.8E+02 1 3.4E-02 M
q
18
12-Afar-98 Quamerra Environment Se rvices, SCP V2.03 1

Client Sample Screening Results
12-A far-98
CLIENT CODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
PGW BON0119 3112/1998 QUAD21B 3/12/199811:01:02AM BON0119 30 5 0.105 155 4.2733373
I.IQIIIU BUZ: 3/12/1998 12.01:04 AM DKG 600 37 0.06166667 536 0.8933333
Ad Dole: 3/12/1998 Tul Sy, AIq: 1.60E+01 1.00E+01 Alp; (Dpi./ 2.08E-0l (uCU 1.50E-04 (pC1/ 9.36E+00 ± 2.3E+01 CAT 2.7E+00 Lob
1'07 me: 7.4 ! U.N.. L / ,.,1 U... el..+• v atc+nn co+. c ooc na .1-1. a an c.na - a I.,., I / , ac n
. ALI
l`G\V BONOJO 3/12/1998 QUAD21C 3/12/199811:01:02 AM UONOJO 30 7 0.18833333 148 4.0233333
LIQUID 868; 3/12/1998 12:01:04 AM BKG 600 27 0.045 546 0.91
AW hole: 3/12/1998 Tut So, Alq: 1.60E+01 1.00E+01 Alp; (Dpnd 4.81E-01 (uCV 3.47E-04 (pCY/ 2.17E+01 ±2.3E+01 CAT / 1.2E+00 Lob
Ppl me: 7.5 Ud13: 1, / ml Bet; Alq): 7.89E+00 So): 5.69E-03 LIC): 3.55E+02 ± 3.6E+01 I 1.4E-0 I
Alq
LIJJ
POW BONOJI 3/12/1998 QUAD2ID 3/12/199811:01:02 A t BONOJI 30 12 0.31166667 132 3.373
I-lQU1U DUB: 3/12/1998 12:01:04 AM BK(J 600 53 0.08833333 615 1.025
Ad Dote. 3/121998 Tut So, Alq: 1.60E+01 / LOGE 101 Alp; (Dpnd 9.54E-01 (uC'U 6.88E-04 (p(-'U 4.30Et0l ±2.7E+01 CAT S.SE-01 Lob
Pptmt: 8.7 / Udta; L ml Bel; Alq): 6.56E+00 So); 4.73E-03 LIZ): 2.96E+02 f3.4E+01 I ! 1.7E-0 1 AN
Ids
POW BON4119 3/12/1998 QUAD22A 3/12/199810x40: 55 AM 13ON4119 10 2 0.14666667 10 0.135
I.IQOID IIUZ: 3/12/1998 12:01.14 AEl IJKG 600 32 0.05333333 519 0.565
AM Dole: 3/12/1998 Tut So, Alq. 200E+00 I.00E,01 Alp; (Dpnd 4.31E-01 (uC1/ 3. SSE-05 (pCU 1.94E+01 ±3.4E+01 CAT 1.3E+00 Lab
Ppl mZ: 2.7 / IIn11o: L / ml Bel; Alq): 1.65E .01 So): 1.48E-05 LIZ): 7,41 E+00 f 2.7E+01
I
/ 6.7E+00 Alq
148
POW BON541 3/12/1998 QUAD22B 3/12/199810:40:55 AM BON541 10 2 1E 15166667 22 1.2516667
LIQUID BUZ: 3/12/1998 12:01:14 AEI BKG 600 29 0.04833333 569 0.9483333
Aul hole: 3/12/1998 - -- 'I'ul So, Alq. 100E+00 IO0Ei01 Alp; (Dpnd 4.34E-01 (ICY/ 1.951:05 (pCU I95E101 ±3.6Ef01 CAT 1.3E+00 I.ab
Ppl n,Z: 2 ,/ UWte: L ml [let; Alq): 2.30E+00 So): 1.03E-04 J.IZ): 1.03E+02 ± 4.OE+01 1 4.8E-0 1
KAV IJON585 3/12/1998 QLJAI322C 3/12/1998 10:40:55 AEI BON595 10 1 0.04333333 14 0.4783333
(-_' LIQUID B4Z: 3/12/199812:01:14 AM BKG 600 34 0.05666667 583 0.9216667
l
AWnote: 3112/1998 '1'o1SO,Alq: 2.00E+00 IOOLM Alp; (Dpnd 1.14E-01 (ICU 1.03E-05 (pCY/ 513E+00 +3.3E+01 CAT 4.9E+00 Irb
Ppl mZ: 2 / Units: I. ml Bel; Alq): 8.68E-01 So): 7.82E-05 Ilit): 3.91E+0I ± 3.2E+01
I
1.3E100 Mq
Ile
%2-Afar-98 Quanterra Environment Services, SCP V2.03
y
/
LIL

C LIEN 'f('ODE 11) MATRIX RECEIVED
PGW BONSBS 3/12/1998
LIQUID
Aul Dule: 3/12/1998 Tut Sa, Alq: 2.00E100
C ='
U
Ppl me: 3.7 - Unllr, 1 1
12-.A far-9H
DETECTOR ACQ DATE SAMPLE MINUTES CN 'I'S A NET CPM A CNTS B NET CPbt B
QUAD22D 3/12/199810:40:55 AM BON5B3 10 1 0055 22 1.2633333
BkB; 3/12/199812:01:14 AM BKG 600 27 0.045 562 0.9366667
LOOEt01 Alp; (B lind 1.27E-01 (uCV 1.14E-05 (p(-'V 5.71E100 ± 3.5E-1 01 CAT 4.4E+00 IAIJ
ml Bel; Al 2-36E-100 So :
9Y• ) 2.12E-04 1. 1.06Ei02
ID:
QDanlerra Environment Se rvices, SCP V2. 0 3
t 4.0E+01
I / AN
4.7E-01
1.18
PGW 13ON5B9 3/12/1998 QUAD23A 3/12/199811:01:05Aki BON5B9 30 11 0.33166667 51 0.81
LIQUID BkB: 3/12/1998 12:01:20 AM BKO 600 21 0.035 534 0.89
Ail Dole: 3/12/1998 Tut So, Alq: 200E-100 LOOEi01
1- pt 1n8: 3.3 ! 11 11113: 11
Alp; (Dpnd 9.77E-01 (uCV 8.80E-0 5 (pCV 4AOE101 ± 2.2E+01 CAT 5.7E-0 1 l.ab
Bel; Al it); 1.34E-100 So): 1.21E-04 1.18): 6.05Ei01 +2.OEi01 I 8.3E-01 Alq
PGW BON5C5 3/12/1998 QUAD23B 3/12/199811:01:05AA1 BON5 42 5 30 5 0.09333333 40 0.3516667
LIQUID BkB: 3/12/199812:01:20 AM BKG 600 44 0.07333333 589 0.9816667
Aul Dune: 3/12 1 1998 '1'ol Sa,Alq: 2.00Ei OO / LOOE401
Ppt m8: 2 / Un113: 1- ml
PGW BON5U1 31 12/1998 QUAD23C 3/12/199811:01:05 AM BON5D1 30 13 0.38666667 49 0.725
LIQUID BkB: 3/12/199812:01:20 AM BKG 600 28 0.04666667 345 0.9083333
And Dole: 3 1 12/1996 Tut Sr,Alq: 2.00E+00 LOOEi01 Alp; (Dpm/ 1.12E+00 (uCV 1.01E-04 (pCV 5.05E+01 ±2.3E+01 CAT 5.0E-0 1 Lob
Ppl nq,: 2 / Units; I- -/ ml Bet; Alq): 1.17E+00 So): 1.06E-04 1.^8): 5.26E+01 ± 2.0E+01
1-18
1 Alq
/ 9.5E-01
118
POW BON6F9 3/12/1998 QUAD23D 3/12/199811:01:05AM BON6F9 30 8 0.21333333 32 0.1533333
LIQUID BkB: 3/12/199812:01:20 AM BKO 600 32 0.05333333 548 0.9133333
And Dote: 3/12/1998 'Iu1Su,Alq: 100E-100 1OOL101
Ppi nq: 0 , Anita: L nit
Alp; (Dpn3 2.79E-01 (uCB 2.51E-05 (pCV 1.26E+01 +2AE+01 CAT 2.0E+00 Lab
Bet; Alq): 6.12E-01 So): 5.51E-05 1.18): 2.76E+01 ± 1.9E01 I 1.8E+00 Alq
1-18
Alp; (Dpn3 6.2913.01 (u( 'V 2.831:05 (pCV 2.83E101 ± 2.IEf01 CAT 8.8E-01 IAIJ
Bet; Al it): 1.54 E-01 So): 6.94E-06 L1B): 6.94E+0U + 1.6E+01 I 7.2E+00 Alq
1-18
PGW BON6110 3/12/1998 QUAD24A 3/12/199811:0058AAI BON6110 30 4 0.06833333 36 0.2416667
LIQUID BkB: 3/12/1998 12:01:08 Ali] BKO 600 39 0.065 575 0.9583333
Aid D.w 3/12 1 1998 3'u1 So, Alq- LOOS+00 1.00E+01 Alp; ( Dpnd 2 .04E-01 (uCV 9 . 20E-06 (pCV 9 . 20E+00 + 2 . IE+01 CAT 2.7E+00 Lab
Ppt ut8: 0 Un113: I. , ml Bel; Alit): 419E -01 So); 1.93E-05 LAB): 1.93E-1 01 ± L8E+01 I 2.6E-100 All
1-18

uuanterra March e3, Tenn ua:ul pm
Project Manager: N. Price
Account: 10722 Project: 550.260 Ouanterra-Richland QAS No. 550.26 Rev. 2
Master Sample Login: 1720
1(^
Draft: Final: Entered and Reviewed by: c
///{//n)/

(l7
Chain of ^,; . Qivanterra
Custody Record
OHA 41-A msr
L c C'
CbeN _ .^
Project Manager
C 6 a 1- ^C^
Dat
7-1 Z- e-1 ^
AAdress Telephone Number (Area Code)/F Number Lab Number
Ciry Stale Z1p Code See Contact Lab Contact
Project Name . 0 / -- `
C...Wact Purchase Ordedouote No
r
^) (^ '^'^^^ 1
Sample 1, D. No. and Description
(Gonlainers for each sample maybe combined on one line)
Date Time
Carne rlWayblll Number
Matrix
$ m y
tL I _ _ I t ^l .^,?
3
^
d
`^
Containers s
Preservatives
o
i i
o
2
o
ti i
L, _
Analysis (A ttach list it
mores ace is needed
-
`
Chain of Custody Numbe
Page o!
0131
Special Instructions/
Conditions of Receipt
rossm;a rruam mennncaoon a1 7ple Disposal
_ (A lea maybe assessed it samples a re retained
Nun-f fazanl q Flarmnabla q SkWn I...1, - q Poison B Llnknuwn H turn 10 Clent q Disposal By l ab q Arcbrvu Tor _. _ Months longer than 3 months)
_-
n AO,
u round limo Regwred `pC Regmren^enls / (SpeutyJ r
aft q aeROUm q 0ays [71a Days z1Days 11 her ^^ ^^ ^ (-^^'> of
i ;had 3y^ -- -f -^
-
Date 1 _ Receued By Date Time
- - -- - - -
linq^ ^ncd Hy j -- ^ Date ^ Lrno 1. Received By -- --- - I Date I Time
--
9 ...... l¢'d B V
-- - - ^ Dal -j e 7inm - 3. nor ceivod By OBIa Time
Conmienis
DISTRIBUTION: WFIITE SIeVS wnh the Sample. CANARY - Retumetl to Client with Report; PINK -Field Copy

Bechtel Hanford Inc. I
'olleclor
Il.I ,Iilbcfg
Yo)ttl Iletgnallon
105-C Phase 1 A Phase II - Concrete Samples
cc Chest No.
CHAIN OF POSSESSION
^&.goohcd By
J
T.AIIOI1.51(1111' SVC- I ION
FINAI. SARIPI E
DISPOS1114 ON
Incorporated
POSSIBLE SAMPLE IIAZAHUS/a EMAn6S
Ndloacdva r
fly
CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES'1
Company ('nnlxrl ,'I el, phon y No. P rolerl Conr.11nxlnr
slevc Mnrske 111 4116 wpISS. 111 ^J
wrpling L oration -- AF NsS_
fT^
100 Arco 1195-1113
Field Logbook No. McOlod of Shipment
_- _ (-' Iland deliver
Offdle Properly No. 1101 of Lading/Air 111
N/ 1T ti /31
Name
`^
I ,
Preservation
Type of Container P
No. of ConlahrerlQ 2
Special Handling and/or Slonge ^ _ ^
Volume
I'^-•
/^ i M
srr iom 111 in
CSN
^
Il/IhLe• -, / i ^
sryctid
^0^2
f^ SANIPL E ANALYSIS ^.,.--, cam lyn `li^^
sample NO mairlx Sample [)are Sample 1111 I
Other Sehd- S ^ C^ .^/
I1 ^^ ^,'5)I
I
f- l4
ime
(1
i 1)alc/lime
DaINI c //
Dmerime
SPECIAL INSTRUCA IONS Matrix
(
s s.,d
l) ICPMdAI - 60101 IS upcnrecel lLcadl; Aicrany-7471-ICV1;Chromiom Ilex-7196;
S[ - s^^^^^.i
PCnr- 110801Arociur 12541. Gamma Spcmmf

Uechlel Hanford Inc. CHAIN Ole CUSTODY/SAMPLE ANALYSIS Itl:QUES'1'
Collector Company /'oulxcl 'I c1cphune Nu.
R I :nhlherp
Slcve Mprskc 371-1316
Prnlrxt Ilaignallun
105 C Phase I & Phase 11 - Concrete Samples
smulpling Localion
100 Area I
Ice Chest No. Field Logbook No.
(,-L _ I
Shipped I
1)uenlun Incnrpnu (ed
Poss l"LL SAMPLE IIAZanusntEMARKS
RaJiwclive
Special llandling and/or Storage
&^kooa e
SAMPLE ANALYSIS
Ondte 1'rup,rty No..
A i/`J
1'reservaliun
ra, `
e7
'i ype of Container 1'
No. of Containers)
Volume
IL
,..,P.
Sample No Matrix • Sample Date Sample 'I'6nc ° ^'
7111
3^'r als x,{S ee
. -7
'S P,? F x 5 ±•'SA
^r 3-,
: r
Project Coordinator
wFiss. RI.
SAF No.
1198-061
Method of Shipment
Iland deliver
(sill of Lading/Alr 11 111 Nn.
w
8m6" -Q7 Other 6eRd- ^- /Q- iJ (!t'r7 K.a
130AJ?q
ILUN OF POSSESSION Sign/Print Nunn
R inquished ll}
\,,r
"^ S •'
c S oi,eJRy
L',
am/fim q1
R ived Ry
^^ ^^ 305 4
Damn'imc
Received By
Dalen i1ne
Dal nine,
Rckslnls islmJ try
Dalc/l unc
ReccivcJ By Ila1c/I hnc
U
R ish

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST ^
1198y
!
"olleclnr ,/- Company Contact 'Iclephnnt Nu.
Project Coordinator
Data Turnaround
H. Iahlhcrg G . ^jl'j /(ter
.s(eve hlnlske 171-4116
wl;I%N. It
1•rolal Iltsignal un Sampling Location i 'AF Nu.
105 .0 Phasc I & Phase II - Concrete Samples 100 Area 1198-061
Ice Chest No.l yJ p /^ G/ Field Logbaok No. hiclhnd of Shipment
J M ^
^1J{O _ hand deliver
Shipped To Offsltt
Quanlxn• Incorporated
POSSIIILI: SAMPLE IIA7.AIInS/ItEhIAR6S
NaJluadbe
Special handling and/or Storage
j
-
I
pSAMPLE
ANALYSIS
Properly Nu
I,^d
1'rraerval nra
'i'ype of Coulnbmr
N11e
No. of Canlalner( . ) )
Vulwne
P LI
II,
See Oem (I I in
Special
I."'."i°"^
Sangdc No Matrix • Sample Dale Sample T rate l^ 5r , I '(rl,w
}'I}) ^, ^r ll lr i ,;1'li ^
I I ,111.
Other Selhf- ^ -/^_ ^ ^(^O (D
11 ^I i!: p1 1 ) 1 1
E^ ^ _I +':13 :.!>

V
CG
C7
Client Sample Screening; Results
l3-,Igor-98
QDanlerra Envi ronment Se rv ices, SCP V2.03
(F-ji ,^I1^I1^'
LIEN F( ME, 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPAIA CNTSU NETCP111B
Bill 130N687 3/12/1998 QUAD2IA 3/12/199811:01:02 AM BON687 30 7 0.18 74 1.54
uQIOD Bke: 3/12/199812x01:04 AM BKG 600 32 0.05333333 556 0.9266667
Aid Dale: 3/12/1998 'ru(Sa,Aly; IOOE100 I.00Ei00 Alp; (Dpad 8. 39E-01 (uCV 3.78E-04 (pCl/ 3.78E)02 ±3.9Et02 CAT6.6E-02 Lab
Ppl me: 49.6 Ihdb: L nd Bet; Alq); 3.27E400 Sa); 1.48):03 Lie): I48EiO3 ±2.SE402 I 3.4E-02
Alq
IAg
1

Client Sample Screening Results
12-A1ar-98
(3d EN "I'CODE 11) MATRIX RECEIVED BET ECI'Olt ACQ BATE SAMPLE MINUTES CNTSA NETCPNIA CNTSB NETCPMB
PGW BON01 1 9 3 1 12/1998 QUAD2 1 B 3/12/199811:01:02 AA1 BON0119 ---- _ 30 5 0.105 155 42733333
LIQUID Bbe: 3/12/1998 12:01:04 AM BKO 600 37 0.06166667 536 01933333
Aul Date: 3/12/1998 Tut Sa, Alq: 1.60E+0I I . 00Ei OI Alp; (Dpad 2.08E -0 1 (uCV 1 . 50E -04 (pCV 9 .36E+00 ± 2. 3Ei01 CAT 2 .7Ei00 Lab
1-p1mt: 7. 4 ml Bel; Alq): 8.31E+00 Sal: 5.99E-03 1.18): 3.74 E+02 f 3.7Ef01 I ^ 1.3E -0 I
P(iW BONOJO 3/12/1998 QUAD2IC 3/12/19981LO1.02AM BONOJO 30 7 0.18833333 148 4.0233333
LIQUID Bbt: 3/12/1998 12:01:04 AM BKG 600 27 0.045 546 0.91
AM Dule; 3 1 12/1998 T.1 Su, Alq: 1.60E-t01 1.00E+01 Alp; (DpnV 4.81E-0 1 (uCV 3.47E-0a (p(-'I/ 2.17E101 ±23E+01 CAT 1.2Ei00 Lab
Ppt me: 7.5 Unk.; I- ! nO Bet;Alq): 7.89E + 00 Sa); 5.69&03 I.Ie): 3.55E +02 ± 3.6E +01 I IAE-01 AIq
PGW BONOJI 3/12/1998 QUAD2ID 3/12/199811.01:02 AM BONOJI 30 12 0.31166667 132 3.375
1.1Quil) B4t: 3/12/1998 12:01 04 AM 11KO 600 53 0.08833333 615 1.025
Aul Dule: 3/12/1998 To1 Sa, Alq: 160E +0I / IOOEt01 Alp; (Dpud 9 . 54E-01 (uCV 6 . 88E-04 (pCV 4 . 30E101 ± 2.7E+O1 CAT 5 . 8E -0 1 Lab
Ppt 1nt: 8.7 - Unit.: 1 1 111 1 11,1; Alq): 6.56E+00 SO 4.731: 03 I. le): 2.96Er02 ± 3.4E+01 I 1.7E-0I AN
PGW BONAU
AM DUle: 3/12/1998
Ppl mt: 2.7
I.IQIIID
T.1 Sa, Alq:
hull.:
3/12/1998
200E+ 00
I.
QUAD22A
Ilbt:
IDOf1 OI
al l
3/12/199810:40:55 A61 BON-0 1 9
3 1 12/1998 12:01:14 AM BKG
Alp; (OpnV 431E-01 (uCV 3.SHE-05
BeQ AI 1.65E-01 Sa : 1.48E 05
4)1 )
10
600
( pCV
llel:
2 0.14666667
32 0.05333333
1.94Et01 ± 3AE+01
741E+00 S 2.7E 101
10
519
CAT
1
0.135
0.865
IIC
1•le
1 .3E100 Lab
Alq
6.7E 100
1dt
POW BON5 4 1 3/12/1998 QUAB22 11 3/12/199810: 41055 AM BON541 10 2 0.15166667 22 1.2516667
I.IQ(IIO Bbt: 3/12/1998 12:01:14 AM BKO boo 29 004833333 569 0.9483333
Aull).W 3 1 12/1998 1'u 1 Sa, Alq: IO01i+00 / I.00h WI Alp; (Dpud 4.34 E-01 (u('I/ 1.95E-05 (pCV 195Ef01 ±3.6E+01 CAT 1.3Ei00 Lab
1'pt u1t; 2 Unll.: I. all Bet; Alq): 2.30E+00 Sa): 1.03E-04 1.18): 1.03E+0] ± 4.0Et01 I 4.8E-0I
Aiq
Idt
POW BON585 3/12/1998 Ql1AB22C 3/12/19981OAU:55 AM BON585 10 1 004333333 14 0.4783333
O I.IQIIID Itbt: 3/12/199912:01:14 AM BKO 600 34 005666667 553 0.9216667
W AalD.Ie; 3/12/1998 '1.1 Sa, Alq: 2.001:100 100E-01 Alp; (Dpn) L14E-01 (u('U 1.03E-05 (pCV 5.13EfOO ±3.3Ei01 CAT / 49E+00 Lab
PPI mg: 2 / lJnlla: I. al l llel; AI4) :) 8.68E-OI Sa : 7.82E-(15 LIt): 391E+101 ± 7.2Er01
I
1.3E 100 ` Iq
4t
1 2-Afhr-971 Quanterra Environment Se rvices, SCI' V2.03 1

CLIEN"1' CODE IB MATRIX RECEIVED
POW BON5153 3/12/1998
LIQUID
And UWe: 3/12/1998 To( So, Alq: 2.00E+00
Ppl n, g: 3.7 (Inlly: I.
(') •Al212N
DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
QUAD22D 3/12/1998 10:40:55 AM BON5113 10 1 0.055 22 1.2633333
Bkg: 3/12/199812:01:14 AM BKO 600 27 0.045 562 0.9366667
1.00E+01 Alp; (DpnV 1.27E-01 (uCV 1.14E-05 (pC•V 5.71E+00 ±3.5E101 CAT 4AE+00 Lob
nd Bel; AI43: 2.36E+00 Sr ) : 212E-04 1. Ig): 1.06E+02 t 4.0E+01
I • i
4.7E-01
Alq
1.11
PGW 11ON589 3/121998 QUAD23A 3/12/199811:01.05 AM BON589 30 11 0.33166667 51 0.81
LIQUID Bkg: 3/121199812:01:20 AM BKO 600 21 0,035 534 0.89
And Dute: 3/12/1998 Tot Se, Alq: 2.00E+00 1.00E+0I Alp; (DpnJ 9.77E-01 (UCU 8.80E-05 (pCV 4440E+01 +2,2E+01 CAT 5.7E-01 Lob
Pp1 ntg: 3.3 Ihdis: 1- nd Bel; Alq): 1.34E+00 So): 1.21E-04 Ljg): 6.05E+01 ± 2.0E+0I 1 8.3E-01
POW BON5C5 3/12/1998 QIJAD238 3/12/199811:01:05 AM DON50 30 5 0.09333333 40 03516667
LIQUID Bkg: 3/12/199512.01:20 AM BKG 600 44 0.07333333 589 0.9816667
And Dule: 3112/1998 3'u1 Se, Alq: 200E+00 / I.00Et01 Alp; (DpnV 279E-01 (uCV 2.51E-05 (pCV 126E+01 ±2AE+01 CAT 2.OEi00 Lob
PpI mg: 2 / Uld1r: L m1 Bel; Alq): 6.12E-01 So): 5.51E-05 LIg): 2.76E101 ± I.9Et0(
1
1.8E+00 Alq
Is
POW BON5D1 3/12/1998 QUAD23C 3/12/199811:01:03 AM BON5D1 30 13 0.38666667 49 0.725
LIQUID Bkg: 3/1211998 12:01.20 AM BKG 600 28 0.04666667 345 0.9083333
AW nwe: 3/12/1998 '1'u1 S., Alq: 200E+00 1.00E+01 Alp; (DpL/ 1.12E400 (uCV 1OIE-04 (pCV 5.05E+01 ±2.3E+01 CAT 5.0E-01 Lob
1-pt mg; 2 / troll.: L / ml Bel; Alq): 1.17E+00 Se): 1.06E-04 LIg): 5.28E +01 12.0E+01
1
9.5E-01
Alq
1-Ig
PGW BON6i9 3/12/1998 QUAD23D 3/12/199811:01:05 AM BON61;9 30 8 0.21333333 32 0.1533333
LIQUID Bkg: 3/12/1998 12:01:20 AM BKG 600 32 0.05333333 548 0.9133333
Ant Dole; 3/12/1998 'IWS.,Alq: IOOE+00 LOOE101 Alp; (I)pm/ 6.29E-01 (uCV 2.83E-05 (pCV 2.83E+01 ±2.IEt01 CAT 8.8E-01 Lob
Pp1 m g; 0 1 Una; ll
1- ml Bel; Alq): 1.54E-01 So): 6.94E-06 LIg): 6.94E+00 ± 1.6E+01 I 7.2E+00
PGW BON6110 3/12/1998
LIQUID
Aid D.1,; 3/12/1998 1n1 S., Alq: I.VV1.100
CJ PlIt mg: 0 Unit.; L
G
QUAD24A 3/12/199811:00:58 AM BON6110 30 4 0.06833333 36 03416667
Bkg: 3/12/199812:01:08 AM BKG 600 39 0.065 575 0.9583333
1.000+01 Alp; (Dp / 2.046:-0I (tICV 9.20E-06 (pCV 9.20EWO ±21Et01 CAT 2.7E+00 Lob
nd Bel; Alq): 4.29E-01 So): 1.93E-05 I.Ig): 1.93E+01 ± I_SEW)
1
2.6E/00 Alq
LIg
12-A/nr-98 Quanterra Environment Services, SCP V2.03 ?
mq
Ids
A19
LIg

uuanterra march ca, ivvo uo:ur pm
n
Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev. 2
11 11
Master Sample Login: 17203 ^Q.n is r1q
".1,
Pr ject Manager: U. Price ^^
Fp4 o t
Draft: Fine L- Entered and Reviewed by: PM Review:
Sample Header Template:
Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Red Sample MD...
Cements:.
# Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Nudaers:% Filled) 1 1^ ?-I ^S
Data: W
17203-001 BON688 Sot id 12-MAR-98 09:15 12-MAR-98 13:53 01-APR-98 AIRBORNE Screening note. Required
RICHLAND I.D. 80322101//ICAPT = PH ONLY///PCB r S = AROCLOR - 1254///THIS SAMPLE MUST BE FILTERED TO CREATE FILTRATE SAMPLE 17203-004.
1 PH - Plastic-1 1 - HG/7471/g4 S COLD 26-MAR-98 09-APR-98 R108 (364154¢99) .
1 ICAPT/6010/04 S COLD 26-MAR-98 08-SEP-98 R108 (364154:99)
1 PCB/8080/04 S COLD 26-MAR-98 26-MAR-98 R10B (364154:99)
17203-002 BON689 Solid 12-MAR-98 13:15 12-MAR-98 14:30 01-APR-98 AIRBORNE. 3 R7043.001
RICHLAND I.D. 80322102//THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17203-003).ICAPT =.PB ONLY///PCB r S = AROCLOR - 1254.
1 PH - Plastic-1 1 - H 61 7471/g4 S COLD 26-MAR-98 09-APR-96 R108. (364155:99)
1 ICAPT/6010/04 S COLD 26-MAR-98 08-SEP-98 R10B (364155:99)
1 PCB/8080/04 S COLD 26-MAR-98 26-MAR-98 R10B (364155:99)
17203-003 BON897 Liquid 12-MAR-98 13:15 12-MAR-98 14:30 01-APR-98 AIRBORNE 1. Screening not Required
RICHLAND I.D. 80324101//ICAPT = P8 ONLY//AROCLOR 1254 ONLY///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17203-002.
1 PN - Plastic-IL HG/7470/04 S COLD 26-MAR-98 09-APR-98 RIOS (364325;99)
1 ICAPT/6010/04 S COLD 26-MAR-98 08-SEP-98 R10B (364325:99) ^.VO L L
_a
b11
1 PCB/8080/04 S COLD 26-MAR-98 19-MAR-98 R10B (364325:99)
17203-004 BON688 FILTRATE Liquid -. 12-MAR-98 09:15 12-MAR-98 14:30 01-APR-98 AIRBORNE 1 Screening not'; Required.
RICHLAND I.D. 80322101///USETHIS EMPTY BOTTLE FOR ` FILTRATE FROM SAMPLE 17203.00 1.
1 PN - Plastic- 1 1. HOLD//04 S COLD 26-MAR-98 22-MAR-98 R108: (365376:99)
r-.
._ l
CG
3 . 4$amipte has not been rad screened.
Page 1

Chain of
Custody Record
QUA 4124 0797
S1 ^ N_^` 1)
Client ^ ^ Project Manager ^ ^ Date _ ^ ^7
Address Telephone Number (Area Code)/ ax Number Lab Number
City State Zip Cotle Site Contact Lab Contact
Pooled Name /"^ r/ /' f- ^-^ ^ ^
I('
/fi
Contract Purchase Order/Quote No
` Sample 1. D. No. and Description
(Confamen for each sample maybe combined on one line)
C/^/^//A
Date Time
^ I C^ ^° '7 C'^^l In ^
CarrienWaybill Number
Matrix
gg
g
a m y j
y
=
Containers &
Preservatives
"o
i =
o
2
^o
^'
u Q L (/tl (1JC
Analysis (A ttach list if
mores ace is needed
Qi^uanterra
Chain of Custody Numb
I I
Page 1 of 1^
Special Instructions/
Conditions of Receipt
t`oss,ole Hazard lde identification I Saprple Disposal
—t^ DC1J
1t^l ^ Non
lee may be assessed it samples are retamed
q Non Hazard q Flamma ble [ImSk Initanf q Poison B Unknown 1 Be(,, Return , To Client q Disposal By Lab q Archive For Months longer than 3 months)
Tum Around Time Required OC Requirements (Specify)
q 4 Hnprs q 45 Hours q T Days q 14 Days W,
..._....^ _.. _r
C`)
I Days q
Olhor I
L^
1. Received By
.... ..,, .. r
eLnquuhed By IDate
Time 3. Received By
DISTRIBUTION WHITE Stays with the Sample. CANARY - Returned to Client with Report; PINK - Field Copy
0 too
Date I Time
^..

Bechtel HanforJ Inc. CHAIN OF CUSTODY/SAMI'Lle ANALYSIS REQUEST' 119A ^ 111 • 1•"e I d I
Collector longsanp ('onlaC( 'Velephone Nu, Project Coordlnalor Ilala 'Fonurnund
R. Foblbcrg
Project D esignation
105 .0 Phase 1 k Phase 11 - Concrete Samples
Steve Marskc
SamplingLocation
100 Area
1373-4316
-
WEISS, RI.
SAF Nn.
IIUR-11(/-g
21 Days
let Chest No. Field Logbou l, No. Method of Shipment
.133 _Z (land deliver
Mpped'i a
Quanlerra Incorporated
Ilfraile 1•roprrly Nu. But of L..il It1A Ir 11111 Nu.
•OSSIIII.E SAMPLE IIA%ARDS110:141ARKS
RWltsacllve
1're.ervalnn
7)penf Conbiner
N"ne
P
Special Ilandling and/or Storage
1/
7(03^^' ► L/1`-

^^^ tr al
Restoration Reatoratlon
Team
CCN: 055088
Jo ^ IItn
Contractor %.0W "^^"'r
Interoffice Memorandum aI{y W
TP D.A. St, Jahn 1.0-19 sac February 27.19%
Cnrua!
Scr Below pp1t S. L^i^ow
Ra dCun Eagim coat
)C,-41/531 -0700
suaaacr: CURIF. FSTIMATE FOR 51i1PPLN000lWRETE CORE SAMPLES
W r
II^Orr
The rullowing calculations show that cue somplawiih a direct reading of equal to ur lesis lhaa
400.Uou dpm/1 o0em r will be below the definitiaoafrar liu=tivc material as defined in 49 CFR 173.40
of 70 Bq/g (2>; pCi/g). Lath sample will cunsistof cm=ctc material from ruur. two inch ton
samples and enough water to ma4 a shiny constancy. *Me distribution of radionuclides is bar d tin
previous concrete samples Ld= fmm the belowgrr)e Ferl Storage Basin that would also Ix:
Nprescntative of these cuncrae samples
iver,
Cylinder Vulunie nth Radius of cwa= core (r) = I inch
Concrete Density = 2.35 g/cm 116ght of mwswoc taken (h ) - U15 inches
27 pCi = Dq
2?2 dprn = pCi
Mxdmtun di nt among on tort = 400.000 dpr. 3 :UUcm
Calculations:
V - (.-,. 1 4) (1 in.) '(U 25 in) = 0.78 m' (16.4 cm%'iu1 (4 am: samples) = 511 cm'
(400.000 dpm/51.2 cm) (cm'2.35 g) = 3-32E3 dp dg
3.320 dp rn/g (pCi2 2 dpm) = 1SE3 pCi/g or 514 kg
51.W:dld
Percent D'tstribution(V Cotmeration (VO/F.1
,.I Cc
0.17 255 pCV9
137 Cs
82 1 m pCi/g
132 E 0.33 4.95 PU3
"'Eu 0.05 7.5E-1 PCi/g
"'Sr 17 2.55E2 pCi/g
741 Ain
'
0.005 7.5F.-2 pCi/g
3 91tie'Pa 0.1 1.5 .J
(te n its:
S. (J. Marske X5-53
P. A. Newman X3-41
RadCun Engineering File!LB XO 23
floeumcnt and Into Services 110-09
TOTAL: 1.460 PCi/g

t e,
CIO
RFSH-SOW-93-0003 -
rJRevision 5
Figu re 1
SAMPLE CHECKA LIST
Dat&Mme Received ! `1 r) Mt .. ()Oa).29'
Work Order Number. bU3., I v^4a SAF #- _((^
Shipping Cbntainer ID: w Chain atCustody I wIk-Q(^ / - /G
1. Custody Seals on shipping contanrr intact? Yes I l
2. Custody Seals dated and signed? Yes [ No (1
3. Chain-d-Cuddy rec ord present? Yes No I 1
• e ^
4. Cooler terrmperatore
5. Vermicufdelpadcrg materials is Wet [ j C ry 13
6. Number of samples in shipping cmtainer. 1
7. Sample holding fines exceeded? Yes [ J No ( j
F Sa leshave
custody seals
hazard labels
,appropriate sample labels
9. -e6mples are:
in good otindi5on
leaking
broken have air bubbles
10. Where any anomalies identified in sample receipt? Yes (J No
11. Description of anoma lies (include sample numbers):

Client Sample Screening Results
13-Mar-98
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPAIA CNTSB NETCPIIIB
Bill BON688 3/13/1998 QUAD2IA 3/131199810:21:17 AM BON689 30 9 0.241428 $7 57 0.96
LIQUID Bkp 3 1 13/1998 1:30:18 AM 13KG 7110 41 0.05857143 638 094
An[ Dole: 3/13/1998 Tot Sa, Atilt 1.00E+00 , 1.00E+00 Alp; (Dpnd 1.21E+00 (uCV 3.43E-04 (pCl/ 5.43E402 ±4.1 E+02 CAT 4.6E-02 Lab
Pplmp 31.3 Unitas L n11 Bell Alq): 1.98E+00 Sap 8.94E-04 Leg): 8.94E+02 12.5E+02 I / 3.6E-02 Al"
/ Bill DON689 3/13/1998 QUAD2 1 B 3/13/199810:21:17 AM BON689 30 661 21.9790476 47333 1576.8733
(?On I gq '7 LIQUID Bkgt 3/13/19981:30: 18 AM BKO 700 38 0.03428371 672 0.96
Anl Datat 3/13/1998 T04 list, Algd 1.00E+00 , 1.00E+00 Alp; (Dpnt/ 2.196401 (uCV 9.84E-03 (pCl/ 9,84E+03 18.3E402 CAT 2.5E-03 Lab
Ppt mg: 30 / Unlbt L /, ml Bet; Alg )j 3.30E403 Sap 1.49E+00 Leg): 1.49E406 ±6.8E103
III /
3.4E-09,
Alq
Ids
BIII BON733 3/13/1998 QUAD2 1 C 3/13/199810:21:17 AM DON753 30 0 -0.0371429 84 1.9037143
SOLID Bkg: 3 1 13/1998 1:30:18 AM BKO 700 40 0.03714286 626 0.8942837
Asst Dates 3/13/1998 Tot So. Algt 2.50E +02 , 9.77E+01 Alp; (Dpm/ -5.47E-0 1 (uCV -6.30E-04 (pCi/ -2.52E400 ± 4.8E+00 CAT 2.3E+02 Lab
P itt mg: 97.7 / Units: g / mg Bet; Alq): 4.30E+00 So): 4.96E-03 Leg): 1.98E+01 ± 3.2 E+00
I
/ 3.0E+00 Alq
ug
BII( DON754 3/13/1998 QUAD2 1 D 3/13/199810:21:17 AM 13ON754 30 8 0.20666667 77 1.4709524
SOLID Bkg: 3/13/19981:30:18 AM BKO 700 42 0.06 767 1.0937143
And Dole: 3/13/1998 Tot Sa, Alq: 2.50E+02 Alp; (Dpm/ 1.31E+00 (uCV 1.34E-03 (pCl/ 6.16E+00 ±5.6E+00 CAT SJE400 Lab
Fist Mgt 96 Un11at g , mg Bet; Alq): 3.19E+00 So): 3.74E-03 Llg)t 1.49E+01 ±3.1 E+00
I /
6.7E+00
a`
Bill 13ON753 3/13/1998 QUAD22A 3/13/1998 10:21:21 AM BON753 30 3 0.05571429 70 1.4004762
SOLID Bkes 3/13/1998100:26 AM BKO 700 31 0.04428371 633 0.9328571
Aid Dates 3/13/1 Tot So, Alq: 2.50E+02 / 9.61E+01 Alp; (Blind 2.80E-0 1 (uCV 3.2SE44 (pCl/ 1.31E+00 14.3E+00 CAT^ 3.8E+01
Ppt mgt 96.1 holds g
mg Bet; Alq)s 2.98E+00 So): 3.50E-03 Leg): 1.40E+01 3 2.8E+00
7.2E+00
La Alit
I Ig
BIII BON736 3/13/1998 QUA1322B 3/13/1998 10:21:21 AM BON756 30 S 0.20952381 66 1.2314286
C AN Dates 3/13/1998
SOLID
Tot Sa, Alq: 2.30E+02
Bkg:
9.73E+0(
3/13/1998 1:30:26 AM BKO
Alp; (Dpnd 1.32 E+00 (uCV 1.53E-0 3
700
(pCl/
40 0.05714286
6.12E+00 ±5.OE+00
678
CAT
0.9685714
8.2E400 Lab
G
Nip
P itt mg: 97.3 / Units: g / , mg Bel; Alq): 2.57E+00 So): 2.97E-0 3 144): 1.19E+01 ± 2.8E+00
I /
8.4E+00
Adg
Lle
M
I3-Mar-98 Quanlerra Environment Se rvices, SCP V2.03 I

Project Manager: U. Price
wuanterra March 18, 1YYB 1(i am
Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev. 3
Master Sample Login: 17221
^/'^J ((^^
Draft: ina L Entered and Reviewed by: C5 PM Review: (y Qom_ ^ L^
Sample Header Template:
Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Red Sample No.
Comments
p Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:% Filled)
Data:
17221-001 BON690 Solid 13-MAR-98 08:15 13-MAR-98 10:35 OZ-APR -96 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80324301//ICAPT = P8 ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17223 .003.
1 PN - Plastic-1L HG/7471/Q4 S COLD 27-MAR-98 10-APR-98 R10A (364654:99)
1 ICAPT/6010/04 S COLD 27-MAR-98 09-SEP-98 R10A (364654:99)
1 PCB/8080/04 S COLD 27-MAR-98 27-MAR-98 R10A (364654:99)
17221-002 BON691 Solid 13-MAR-98 09:00 13-MAR-98 10:35 02-APR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80324302//ICAPT = P8 ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17221.004.
1 PH - Plastic-1 1- HG/7471/Q4 S COLD 27-MAR-98 10-APR-98 R10A (364655:99)
1 ICAPT/6010/Q4 S COLD 27-MAR-98 09-SEP-98 R10A (364655:99)
1 PCB/8080/04 S COLD 27-MAR-98 27-MAR-98 R10A (364655:99)
17221-003 BON690 FILTRATE Liquid 13-MAR-98 08:15 13-MAR-98 10:35 02-APR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80324301.
1 PN - Plastic-1 1- HOLD//04 5 COLD 27-MAR-98 23-MAR-98 R10A (364656:99)
17221-004 BON691 FILTRATE Liquid 13-MAR-98 09:00 13-MAR-98 10:35 02-APR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80324302, -
C.
1 PN - Plastic-1 1E HOLD//04 B COLD 27-MAR-98 23-MAR-98 R10A (364657:99)
^ l
G
G7
3 •= Sample has not been Pad screened.
Page 1
O
^d
Z ^.^

Chain of
Custody Record
QUA 4124 0]9]
/^ o —r e-r" r Y
C^
iiivanterra
Clienl Project Manager Date Chain of Custody Numb
101143
Address Telephone Number (Area Code)/F Number Lab Number
City
Project Name^^
C
Slate Zip Code
/^ (399 -(X p
Site Contact
Carrie rrWaybill Number
Lab Contact
Conlrac0'Purchase Order/Quote No
Matrix
Containers &
preservatives
Sample I. D. No and Description
(Conlaviers for each sample may be combined oil line)
Date Time
e vi 9i
v 8
2 i 2
°° a?
to Analysis ace
(Attach list if
is needed
Page of
Special Instructions/
Conditions of Receipt
Possible Hazard Identilication
q Nom Haza rd q Flam mable q Skin Irmant q Poison B Unknown
a ple Disposal
Return To Chem El Disposal By Lab El Arch,,, For Months
(A lee may be assessed if samples are retained
longer than 3 months)
L-Jyrm Around Time Required -- OC Requirements (Specify) - c
VR
urs q 48 Hours q 7 Days q 14 Days 21 Days q Other
uisDale
5
ished By Date
Time
Time
I- Received
eceived B
l // i` ^
D to
9-17-99
Date
Time
Time
i -lb 1b OD O g 2-0
3. Relmgmshed By Dale Time 3. Rererved By Date Time
Commonly
DISTRIBUTION: WHITE Slays with the Sa 1pir. CANARY - Relurned to Client with Repo rt ; PINK - Field Copy

Bechtel Hanford Inc. CHAIN Or CUSTODY/SAMPLE ANALYSIS, REQUEST B98-061-11 fare or
Collector "^
.o _c,.. 6jh"'
pjV Ikn+ {^gsrAl
Project Designation
105-C Phase I & Phase 11 - Concrete Samples
Campion) Contact 'Telephone No.
Steve Merskc 077-4316
n m pling Luution
100 Area l OS -C 1\P 4('^d 3
Project Courdinalnr
WIBSS, III.
AF No.
B98-061
Ice Chest No. Field Logbook No. Niched of Shipment
" L- I3U( — U7/
Iland deliver
hipped'To
Quen lcna Incorporated
POSSIBLE SAMPLE I IAZARDS/REIIIARKS
Radioactive
Special I landling and/or Storage
SAMPLE ANALYSIS
1Rdte Property Na.
w 1l
Preservatlon
None
Type of Container P
NB. of Coniainer(s) (
Volume
S!X G()/ s^
/,-)h^l7
d D3,;24^'2r- -C"w, 96
Sample No. - 'mo nts etrix • Sample Date Sample Time
I L
Seelmmlll in
i.e.(l
In,smcli.n,
hill of La li /Air Bill No.
^ ^.
Data 'I urnarouod
21 Days
BON690 01 Other Solid MA2g6 IS c 1XI /
CIIAIN OF POSSESSION SIg ntPrint Names
Rellnquidr D.N?hna Red Dala i
p
iaNgT+B /O J S ^/T A
inquhhcJ BY Dete/rim. Received By OD emlfln^c
lingwshcd BY UalJrime Received BY DatefTimc
elinquith

CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-12 r•ae ! ar !
R ct 4
Company Conracl
Sieve 6lurske
'I'cieplunm No.
3734316
project Coordinator
wlgsS, Rl.
Dols Turnaround
'amplhlg Location
AF No.
Phase II - Concrete Samples
100 Arca — I OS C. R e a e iuv 1199-061
ke a. Field Logbook No.
F—L-13U
Method of Shipment
p I oL
1 land deliver
'hipped '1' t,
Quanterr9 in corporated
Offalle Property No.
MA
(fill of Lading/Air hill Nu.
I,vA
POSSIBLE SAMPLE IIAZARDSlREMARKS
Rdiwaim
'perial Handling and/or Storage
SON691
SAMPLE ANALYSIS 4_
So3a4 CkM 9o3^4 -r-«
Semple No.
01OR
f10^
Preservation
'type of Container
a^^•
Nu. or Containers) 2
Volume
P
II-
.See imm I q in
Sp

cc*
Environmental
Job Vo.22172
Restoration
Contractor ERC Team u. c.. rw
Interoffice Memwandum a' 1 91C
TO D. A. St. John x.0-19 MTL Febmary 27,1999
nru:tc
See Below mc"' S. L. Winslow
RadCun Engineering
X.1-41/531-0700
suarecr: CVIAIF FSTIMATEFOR SWPING CONCRF•TF. CORE SAMPLES
.0 w
Sw.^Cnr !fib
The fulluwing calculations shoe that cure samples with a direct reading of equal to or less than
400,000 dpm/l00cm' will be bdow the definition ofralivactive mate rial as defined in 49 CFR 173.403
of 70 Bq/g (2F.3 pCi/g). Lachmmple will consistofcoacrete material from four, two inch co re
samples and enough water to mAe a slurry consi s:cary. The distribution of radionuclides is bused an
previous concrete samples wkm from the below grade Fuel Storage Basiu that would also be
representative of these concrete samples.
••von:
Cylinder Volume - nrh Radius of cam= core (r) = 1 inch
Concrete Density = 2.35 g/cm `Ileight of cure swrtple taken (h) — U.25 inches
27 pCi = Dq Maximum d irect reading on core = 400,000 dpm/IUUcat'
2.22 dpm = pCi
Calculations:
V — (3.14) (1 in.)'(0 25in) = 0-79 in' (16.4 cm `/irr) (4 cure samples) = 512 cm'
(400.000 dpm/5 L2 cm`) (cm'235 g) = 3.32E3 dpm/g
3.32L3 dpm/g (pCi/2.2 dpm) = 1.5 113 pCi/g or 55.4 E4'g
SLW:dld
Percent Distrtbation(%) Cong=ration (vCi/e )
"Co 0.17 235 pCi/g
17Cs 82 13F3 pCilg
WEu 0.33 4.95 pCi/g
"°Eu 0.05 7.5E-1 pCi/g
"ST 17 2.55E2 pCi/g
241
Ain
Z3912
'pu
0.005
0.1
7.5F.-2 pCi/g
1.5 -
Co ies:
S. 0.lvdarske X5-53
P. A. Newman X 3-41
RadCun Engineering File/LB X0-23
Document and into Serv ices 130.09
TUrAI-: 1.460, pCi/g
(-U00049

9.
Samp are:
'Ries
in good condition
broken
Figure t
SAMPLE CHECK-IN LIST
Date/rme Received: nn221 ^Y D 3 ^l srrr.
FF
Work Order Nurnber. & 42Z SaF # ^O -GYP
Shipping Container 10: ru -0 ^ C^ Chain dQatody #
leaking
lave air bubbles
RFSH-SOW-93-0003
Revision 5
1. Custody Seals on 9**g cont*w intact? Yes (q' o [ ]
z Custody Seals dated and signed? Yes [^}'^io ( ]
3. Chain-of-Custody record preset Yes . o [ J
4. Cooler temperature
5. Vermiculite/packing materials is Wet [ ] Cry 4/(yL
6. Number of samples in shipping container.
7. Sample holding times exceeded? Yes [ ] No
S.
Samp have:
tape _hazardbabeis
wstody seals _apprgsafe sample labels
10. Where any anomalies identified in sample receipt? Yes [ ] No [^
11. Descrip ti
on of anomalies ( include sample n abers):
Sample
Telephoned To:
r_=

C^
C-J
CG
L7
Client Sample Screening Results 1,
13-Mar-98
1,
0, 3, 10
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
Blll BON690 3 1 13/1998 QUAD24B 3/13/19981; 15:37 PM BON690 30 7 0.17619048 71 1.3838093
LIQUID Rks: 3/13/1998 1:30:14 AM DKO 700 40 0.03714286 688 0.9829571
And Date: 3/1311998 Tot Se, AIq; 1.00E+00 , 1.00E+00 Alp; (Dpm/ 3.84E-0 1 (uCV 2.63E-04 (pCl/ 2.63E+02 ± 2.6E+02 CAT 9.3E-02 Lab
Ppl mp 13.5 Units: L ml Bet; AIq): 2.64E+00 So): 1.19E-03 I 48): 1.19E+03 ± 2.5E+02 I / 4.2E-02 AIq
BHI 13ON691 3/13/1988 QUAD24C 3 1 1311998 1:15:37 PM SON691 30 2 0.00666667 30 -0.002857
LIQUID BkSs 3 1 13/1998 1:30:14 AM BKO 700 42 0.06 702 1.0028571
AM Dale: 3/13/1998 Tot So. Alq: I.00E+00 1.00E+00 Alp; (Dpm/ 2.02E-02 (uCV 9.12E-06 (pCV 9.12E+00 ± 2.0E+02 CAT 2.7E+00 Lab
Pptm8: 1.5 / Uatta: L / , ml Bel; Alq); -9.36E-03 Saj: -4.21 E-06 L f8): 4.21E+00 ± 1.6E+02 I / 1.0E+00 AIq
Lis
13-Afar-98 Quanterra Environment Se rvices, SCP V2.O3 /
1.18

(Ruanterra G w ^- 5L 014514
EoAroommtar
sermw
Condition Upon Re ce
ipt Variance Repo rt
St. Louis Laboratory
Client. r`i ^}6 Date:
Login No.:
7
? — 1 / " U Time:
Project No: Initiated by:
Shipper/No: 9 3 5 2 2- 1 1 RFA/COC Numbers: ^^^/[/ 7
ConditionNari ce (Check all that apply):
L q Sample received broken/leaking. S. q Sample 0) on container does not match sample ID
3. q Sample received without proper prese rv ative. on paperwork. Explain:
q Cooler tempera ture not within 4°C --- ?•C
Record tempera ture:
q pH 9. q All coolers on airbill not received with shipment.
q other. 10. q Other (explain below)
3. q Sample received in improper container.
4. q Sample received without proper paperwork. Explain:
5. q Paperwork received without sample.
6. q No sample ID on sample container.
7. q Custody tape dis turbed/broken/missing.
—@'- No variances were noted during sample receipt. Cooler Temperature Upon Receipt: yr^-
Notes:
Corrective .action:
q Client's Name: Informed verbally on: By:
q Client's Name: Informed in writin g on: BV:
q Sample(s) processed 'as is".
q Sample(s) on hold until: f released. noufv:
\
-7 g I,
Sample Control Supe rv isor Review: or desi gnate) I cc : 37 — [ / _
Project Mana gement Review: 7\ t—L—
SL-ADMIN-0003. Revised :1!'_4/95
q
Date: 3 — ^ I --v
SIGNED ORIGINAL MUST BE RETAINED IN THE PROJECT FILE

Q'Auanterra 014501
Condition Upon Receipt Variance Report
St. Louis Laboratory
Client: t/GC'^ Date: 3 — 7 , `!
Project No: 5250 -2(G 6 Initiated by: o-. A-Pi
Shipper/No: RF VCOC Numbers: /7 0 C sL
Condition/Variance (Check all that apply):
'1
Login No.: / 72-2-/
I. q Sample received broken/leaking. 8. q $am pie ID on container does not match sample ID
2. q Sample received without proper preservative. onn paperwork. Explain:
q Cooler temperature not within 4-C t 2°C
Record temperature:
q pH 9. q All coolers on an-bill not received with shipment.
q other: 10. q Other (explain below)
3. q Sample received in improper container.
4. g/ Sample received without proper paperwork. Explain:
5. q Paperwork received without sample.
6. q No sample 1D on sample container.
7. q Custody tape disturbed/broken/missing.
^d No variances were noted during sample receipt Cooler Temperature Upon Receipt:
Noes:
Corrective Act on: t
Q^I., (" ?3) t II !
q Client's [me: Informed verbally on: By:
q Client's Name: Informed in writine on: By
q Sample(s) processed "as is".
q Sample(s) on hold until If released. notify
Sample Control Supervisor Review: (or desi gnate) Date:
Project Management Review: L— " I tN^ Date: J _ (^/ 79
SL-AD?dIN:)004. Revised I1;--1/95
SIGNED ORIGINAL ^',IL'ST BE RETAINED IN THE PROJECT FILE
_-7
tme:
(1 00 053
lozr

— - - --- --- - -- -- WO 2?^ s Q-- - -
' L Qanterra Q April O8, 1998 02:33 pm
Ac count: 10722 Project: 550.260 QunterrRichland
a a- OAS No. 550.26 Be,, 3
Master Sample Login: 172
Project Manager: W. Price
222J4
Draft: Final: Entered and Reviewed by: S^^`^Q^, n'/^'. ^ PM Review: I/C07`^//^
Sample Header Template:
Sample No Client ID C-Matrix Date: Collected Received Due Shipper Bad Category Rad Sample No,
Comments
N Container Type Analysis Class Preservative Anal. Due Data Hold Date Site (Container Numbers:& Filled)
Data
17224-001 BON692 Solid 16-MAR-98 08:30 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80327101//ICAPT = PB ONLY//AROCLOR 1254 ONLY"
' FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECO ME S SAMPLE 17224-004.
LJ v L 2")
PN - Plast ,ll, HG/7471/Q4 S COLD 30-MAR-96 13-APR-98 R10A (364686:99)
1 ICAPT/6010,'24 S COLD 30-MAR-98 12-SEP-98 R10A (364686:99)
1 PCB/8080/Q4 c COLD 30-MAR-98 30-MAR-98 R10A ( 364686:99)
17224-002 BONG93 Solid 16-MAR-98 09:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required
RICHLAND i - D. 80327102 !; ICAPT = PB ONLY//AROCLOR 1254 ONLY/ !iFlLiER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOME S SAMPLE 17224-005.
- IN Plastic-1L HG/1471 1I Q4 S COLD 30-MAR-98 11-APR-98 R10A (364687:99)
1 ICAPT/6010/Q4 S COLD 30-MAR-98 12-SEP-98 RIGA (364667:99)
1 PCB/8080/Q4 S COLD 30-MAR-98 30-MAR-98 R10A (364687:99)
17224-003 BONG94 Solid 16-MAR-98 10:25 16-MAR-98 12:15 03-APR 4d AIRBORNE 1 Screening not Required
RICHLAND I.D. 803271031/ SOAP: = PB ONLY,'/AROCLOR 1254 ONLY///F'ILtER AND ANALYZE SOLID PORTION ONLY, ;SQUID PORTION BECOME S SAMPLE 17224-006.
1 IN Plastic 11, NO, 7471/Q4 COLD 30 MAR-96 13 APR 98 R10A 1364688:99)
1 ICAPT'/a010iQ4 .. COLD 30-MAR-98 b'LP 98 R10A (364688:99)
PCB/8 '",80;Q4 5 COLD 30-MAR-98 30 MAR-98 R101. 68
11224-004 BJPB9b Liquid 16 MAR-9 8 08:30 16-MAR-98 12:15 03 APR 0 AIRBORNE 1 Screening noL Requilad
RICHLAND I.D. 80327801;'1/ICAPT = PB ONLY'/AROCLOR 1254 ONL Y iTH: SAMPLE IS THE FILTRATE FROM SAMPLE 17224-001-
. FN - 2)est 1 c- :L r 147. 04
ICAPT 6010; Q4 _
COLD
(101D
,- APR-9n
_)i-APR 98 1Z
.Pp,8 R10A
- EP -98 R10A
1364689,99)
1364689:99)
1 PCB/8C80/Q4 _ COLD p1-APR-98 MAF 98 R10A !364689:991
X 229-OJS B ON,,, FILTRATL' Liquid -6 -MA.-, , 9 25 16 Mild ,8 12 :15 ciI( ':E Ai3 BORNE 1 Screen il4 1r.. krq..0 ed
'v 1(t `.AN: 1 327102:'/lI^AnT - . -_._!:AR 1254 ONL ..^ ^Ah CLe i= THE FILTRATE FROM SAM; E . 7 229 u02.
i YL 1L 1 .- ,.ti CGLD _ -AFR-9' .,r.., od RI'A ',364690:99, W O
:
17224 CL6 F(N 6 94 FILTRATE L q,i7 MAR 36 10 c :6 MAN 5 F _ RBOR1; _
RICHLrU F 2 1 1'3"-ICAPT rP.. i ARJ( LO R 2. 4 ONL^ _..__ FP^PLE 1 5 THE FILTRATE FROM SAMPLE 2 _t3.
O
G
CG
cl(
.R.
1 t a, JLS .. , .., ,. „ .. RIOA i364,4, 991
/
1^
( V
-2
t
t^^^
Sc eeci^y n t kequll^d
L e ) S
)
V '/
7 1^ Y-0

Dr a f tM
W. Price
Quanterra April 13, 1998 10:36 am
Account: 10722 Project: 550.260 Ouanterre-Richland OAS No. 550.26 Rev. 3^^^
Master Sample Login:
Our"
'^ifr^
D ref t: Final Entered and Reviewed by:
PM Review: ^s^fA
Samp le Header Template:
1722224777
^^y^—in
1.
Q'"A lye r^0i^"
Semple No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Rad Sample No.
Comments
N Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:% Filled)
Data:
17224-001 SON692 Solid 16-MAR-98 08:30 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80327101//ICAPT = PB ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17224-004.
1 PN - Plastic-1 1. HG/7471/Q4 S COLD 30-MAR-98 13-APR-98 R10A (364686:99)
1 ICAPT/6010/04 S COLD 30-MAR-98 12-SEP-98 R10A (364686:99)
1 PCB/8080/04 S COLD 30-MAR-98 30-MAR-98 R10A (364686:99)
1 PM/IT/Q4 S COLD 30-MAR-98 12-SEP-98 R10A (364686:99)
17224-002 BON693 soLid 16-MAR-98 09:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80327102//ICAPT = PS ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17224.005.
1 PN - Plastic- 11 HG/7471/Q4 S COLD 30-MAR-98 13-APR-98 R10A (364687:99)
1 ICAPT/6010/04 S COLD 30-MAR-98 12-SEP-98 R10A (364687:99)
1 PCBi8080/Q4 S COLD 30-MAR-98 30-MAR-98 R10A (364687:99)
1 PM/IT/04 S COLD 30-MAR-98 12-SEP-98 R10A (364687:99)
17224-003 DON694 Solid 16-MAR-98 10:25 16-MAR-9812:15 03-APR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80327103//ICAPT = PB ONLY//AROLLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17224.006.
1 PN - Plastic-1L HG/7471/04 S COLD 30-MAR-98 13-APR-98 RIUA (364688:99)
1 ICAPT/6010/04 S COLD 30-MAR-98 12-SEP-98 R10A (364688:99)
1 PCB/8080/04 S COLD 30-MAR-98 30-MAR-98 RiOA (364688:99)
1 PM/IT/Q4 S COLD 30-MAR-98 12-SEP-98 R10A (364688:99)
17224-004 BOB898 Liquid 16-MAR-98 DB:30 16- 14AR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required
RICHLAND I.D. 80327801///ICAPT = P8 ONLY//AROCLOR 1254 ONLY///THIS SAMPLE I $ THE FILTRATE FROM SAMPLE 17224-001. W02281
1 PN - Plastic-IL HG/747D/Q4 S COLD 01-APR-98 13-APR-98 R10A (364689:99)
1 ICAPT/6010/04 S COLD 01-APR-98 12-SEP-98 R10A (364689:99)
1 PCB/8080/04 S COLD 01-APR-98 23-MAR-98 R10A (364689:99)
17224-005 0ON693 FILTRATE Liquid 16-MAR-98 09:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required
RICHLAND J.D. 803271021//ICAPT = PB ONLY//AROCLOR 1254 ONLY///THIS SAMPLE IS THE FILTRATE FROM SAMPLE 17224-002.
1 PN - Plastic-11. HOLD//04 S COLD 01-APR-98 26-MAR-98 R10A (364690:99)
( .-17224-006 BON694 FILTRATE Liquid 16-MAR-98 10:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required
C-., RICHLAND I.D. 80327103///ICAPT = PB ONLY//AROCLOR 1254 ONLY///THIS SAMPLE IS THE FILTRATE FROM SAMPLE 17224-003.
J 1 PN - Plestic-1 1. HOLD//04 S COLD 01-APR-98 26-MAR-98 R10A (364691:99)
Ci
LI
UI
3-=Sample has not been cad acreened.
Page 1

Chain of
Custody Record
QUA 4124 07 97
S i Io
L't LO 10"banterra
Client
d , _.
'lfXn^'l n Project Manager Oaf I ^—
C
Address Telephone Number (Area Code) Fax Number Lab Number
City State Zip Code Site Contact Lab Contact
Project Name
Contract'Purchase Order/Quote Noo -
Sample I.D. No and Description
(Containers for each sample may be combined i on one line)
7 V l 1^
^2 3
VI
-
— / n / CarrierlWaybill Number
Date Time
Matrix
gg
3 E - 3 a
Containers 8
Preservatives
°
i o 6 ^o
N i
Analysis
more s ce
(Attach list if
is needed
Chain of Custody Numb P,t
1 o -
Page of
Special Instructions/
Conditions of Receipt
P >a,
(A lee may beetl if samples are retained
El No,, Hazard q Flammable q Sbn Irnlan( L1 Poison B Vonknowi, Return To Client El Disposal By Lab q Archive For Months longer than 3 months)
Turn Around Time Required OC Requirements (Specilyr
q 24 tVrirs q 48 Hours q / Days q 14 Days y21 Days q Other
in uished Date Tema 1. Re ed By s Date Time
`-- 2. Relinquished By Dale Time 2 Received By Date Time
- J
R ^.^n uished q BY ^ Dale f Time — 3. Received BY
I Dale I Time
GominenR
DISTRIBUTION: WHITE - Slays with the Switch,, CANARY - Returned 10 Client with Report PINK - Field Copy
1
4 6

Chain of
Custody Record
OIIA- Al 24 n>G]
loo [D
Client Prolecl Manager
c^
Dat
3111- 9
Address Telephone Number (Area Code) Number Lab Number
City Zip Code Site Contact Lab Contact
Project Name
^^,y ^' (/
L^r I I
C
^"
ContrectPurchase OrderlQuote No
Sample 1. D. No. and Description
Coma, ners for each sample maybe combined on one line)
^
CarriegWaybill Number
Matrix
Date Time °m - o =
Containers 8
Preservatives
ei
OX,
=
0 30 m
Analysis
more spa
r
(A ttach list A
is needed
CO"'banterrla
Chain or Custody NumbC(
11 0450
Page ^ of
Special Instructions/
Conditions of Receipt
rossore nezam Idenuncanon
q NonHaeard q Flammable El Skin Initant El Poison B nknuwn
a' nPie "bposai
Return To Client El Disposal By Lab El Archive For Months
(A lee me
longer fh n 3
ssessed if samples are retained
onths)
Turn Around Time Regmree OC Requirements (Specify) ///
q 4 Hours
in quishe
P.^
q 4 8 Hours El Days El 14 Days 21 Days q Other
D e
1 3
T
l 66
Received By
w ^^D /
Date
1
1190quished By Date Hme 2 Hecervad fly
C
^Aelingwshed By Date Time 3. Received By
Commerns
DISTRIBUTION: WHITE Slays mIh Ibo Sarnple. CANARY -Returned to
1
Time
— —_ — I Date I Time

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUE'S1' B98- 061 -16 rase ! "' !
ollector^5/ Q4r.4 ., ,/ /
KAIU f
Company C'nnlecl 'I'tlrydmnr No.
Steve Mnrskc ,171-4114
Project Coordlnalur
WP]SS, R1,
Project D esignallon unpling Location 'AP Nn.
105C Pha se I & Phase 11 - Concrete Samples 100 Area 1598-001
Ire Cheat No. Field Logbook No. Method of Shipment
I land deliver
Shipped To
Quanlcr ts Incorpo rated
Offailc Property No. 15111 ur Ladin g/Air 0111 No.
POSSIBLE SAMPLE IIA7ARDS/REMARKS
Radlosclive
Preservation
"""•
Special Handling and/or Storage
SAMPLE ANALYSIS
I y'pe of Con tamer
Nu. o(l'0nleiner ( s)
volume
S06- tooa^7S
IL
S. in
sr«id
momuiom
Data 'Turnaround
21 D21yS
^03a I CIS m gD3^ r1 (Zc^c<
Sample No. Matrix • Sample Dale Sample Time 1
I' os•...'•' j '^V
^•^..
1. O 2 Other Solid 3 -/6-^8 (^ 3 -^ e, o -
SPECIAL INS"TRIK-1 IONS
CIIAIN OF POSSESSION Sign/Print Names
(II ICI• MeW,-6010A (S.patmce) 11.< ad), hlercwy-7471 (CV), C1. ....mm Ilse 7196,
di
Q.e ,
Relinquished By
Dats?ims
^6 f{A ?9>3 /2 / S
Ualdfime
R e By
Recei) ve Y ^I
imc
`
Uale imc
I'CBs,1080(Aivd,)rr 12541, Gainu Spccouv

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST 1198- 11 61 - Id
ollector
Q C.hlh.r
Project Designalian
3 ^N
ompany Contact
' Steve Marske
Sampling Location
'Telephone No.
373-41IG
Project Coordinator
wl;lSS, fit-
'AF No.
Dalo Turnaround
2I
105 -C Phase 1 & Phase II - Concrete Samples 100 Area 1198-061
fee Chest No. Field Logbook No. Method of Shipment
I land deliver
'hipped To Offsinr Properly No. Rill of Lading/Air Dill No.
Qulnterra Incorporated
POSSIBLE SAMPLE IIAZARDS/RERIARKS
Radloacdn
Special Ilandling and/or Storage
SAMPLE ANALYSIS
1'reservalloo
7 ype of Container
Nn. of Container(s)
g o3 ^1 I G^-t r -, g o3a^a P-6,d
Sample No Matrix • Sample Date Sample Timc
"""•
Volume IL
P
2
See item (1) In
Speaid
Inanu,"on. -
ON693 Q 2 Other Solid _ 6 _ O Ja — ( /^
Clit OFP SSfS ON Sign/Print Names - ( 1) ICP McUk - 6010A (Supunace) 11 cadl. Mercury - 7471 -(CV), Chrommm Ilex - 7196,
el 'uis By DaIHTime
iengte 98 S
R B' Uale i c
Relinquished BY Date/filne Received BY (N,L 7ale/iinle
(CLY 1
Rflinquidled By Daldllnm Received By Damn nm
^rilrf^JVi-79' /V rC(Cel-(a3 •Y= S ^1, 90- TdfLiSr' echnei,'uwt 99 C^ubo l c /`
J h ^ ^/ / 3-,-”
l
Days
.
SPECIAL INS I'BUCI IONS Man, ,
PCBs - 8080 (Aunt., -1254 ) , Gamma 5penmscopy ICevum-137, Coha 11-60, Europium-152,
Europium-154, Lnopwm-1551, Anmunu nr 241. Isotopic Plulounnn; Isotopic Uranium; Sete
5
SL
so
51
-
-
-
-
Sem,„mt
S„ im
Sn.Jye
'uished By DaldGne Received By 1lale 7 lint
1. - qwa
Bdumn
U, X - OiAu
L ORATORY Received By ]ide DaldTime
SECTION
FINALSAMPLE Mspwd Me1hm1 Disposed By -- -- Date'lbur
DISPOSITION
o A
Ps
D1.
- oJ1el
11,,,,ns„nJ,
u,,,m I,ywm

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS KEQUIsS'f B98- 061-15 " vc ! "r i
olleclorpp p
('nm pp ny (^nslacl 'I clephmle No.
Mp "^^
A4,,4
Steve Manske 3.73 4116
Project Designation Sampling Location
105-C Phase 1 k Phase II - Concrete Samples
100 Area
Projerl ( -uordinator
WII ISS. Hi
'AF No.
1198-061
I ce Chest No. Fi eld Logbook No. Method of Shipment
Iland deliver
- hipped To
Qllmnella lncurpormcd
POSSIBLE SAMPLE IIAZARIIS /RF-hIARKS
Radipanive
Special Dandling and/or Storage
SAMPLE ANALYSIS
ORaile Properly No. Hill of Lading/Air (till No.
I'rcservpllnn
'T ) pe of ( nnialner 1
No. of ('onldner( s)
\'ulunm
^o3an 1 U^ L.enti go3 a ^
2
IL
Scc non I I l m
Strcatl
I^'r'11e"""a
flala I ornaruund
Sample No Matrix a Sample Dale Sample Time ,}^INe s^„ u s ^, - r es 'j" r ; It r:, ., 1 ~,r f "
BON694 03 Other Solid
CI IN OF 'OSSFS'ION
F
0.el ' BIY'o Dalelfime
/6 AtA R9B ^Z ^^
Relin fished B Date/ 1anc
yrr y
Sign/Prim Nunes
Ra U rT r
T214 ^-
Received B '\ Dam/tim e
Relui4uisheJ - By UauRirne Receircd By hale/I nne
Inthatitoshed Ua¢fflme Recdred By Ua1ell in¢
LABORATORY
SF.(TI ON
TINA S
-SAhIPLE
IIISP(ISIII(1N
Y
SPECIAL INS I' RUC" I' IONS
11)Is- a08 01roclor 12 5upallncc111cadlAkmup-7J]I-(CVI. Clllomiwu 111%-)196.
Ls CB -. 154, oclnr-23J1, Gn11nnn Spenrosc'+Py IC esvum 117. Cnbah-60. burnpiva+-132,
I:mupiuurl3J. llumpuumlSS;,An¢uamm241. lsnl upic l'Lilunmin. 11 0111,1 11 ILaniunr. Selc
^/ ^
5_/e111 jU"1^ -79 / / ,
/vfC / Qy ^^a / ^r
^ ^^-f[A O /, / — /O"'rtt^
^
ec / 9 ,/(h
y^
^ (/&r o/
- l¢' ^^ ^3 S41)
Received By lisle Daelunc
Dn sd Mnbod -"-- ---__-'-
1 S UIdl uu<
21 Days
I
St_
So
Matrix
s,,
5'^.
%Id"d
%t.
w
'v
s
- II I.nly
scud
tr,l
^
Il,
UL
- I4wn 5.IW.
leiiio l ..p,w,
Ripe
1. t ignW
v - rcra+11,.,,
% +nnr+

CCN: 055088
Environmental
Job No. 22192
Restoration
Contractor ER^ Team o. ' MO
Interoffice Memorandum
7O I). A. St. John LO-19 DAM I;ebruary 27.1998
I nPI"-5!
*
Scc Bclow "o"r` S. L. Winslow
RadCun Engineering
X3-41/531 40706
suuEcT. CURT F: FSTTMATE FOR S111PP1NG (-VNCRFTF. CORE SAMPLES
r.... w^
OIL"IW
IAA ww
Liloc . !1O
The Following calculation show that curt: samples with a direct rending of equal to ur less than
400.000 dpm/I0(kan = wllbcbclow the definition ofratlivactive matcrialas defined in 49 CFR 173.403
of 70 By/g (2F3 pCi/g). L•ach sample will consist of concrete mate rial from four - two inch core
samples and enough waterto make a slurry consisxmy. The dist ri hution of radionuclides is based tin
previous concrete samples tak«t from the below grade Fuel Slortge Basin that would also lx;
representative of these concede samples.
'iven:
Cylinder Volume - nr'h Radius ofcowxte core (r) = 1 inch
Concrete Density = 2.35 glom' Height of cmL^s_ample taken (h) - U25 inches
27 pC:i = Dq Maximum ilkeet reading on core = 400,000 dpm/1 UUcm'
2.22 dpm = pCi
Calculations:
V - (3. 14) (1 in.)'(0 25in) = 0.78 in' (16.4 cm J/irrj (4 cure samples) = 511 cm'
(400.000 dpm/51 2 cm) (='2.35 g) = 3. 3 2E3 d;m/g
3.32L I dpm/g (pCi2.2 dpm) = 1.5E3 pCi/g or 55.4 By/g
SI.W:dld
'OCo
Percent Disr ributionMo
0.17
IJ7cS 82
'uEu
033 0
I"Eu 0.05
o'Sr 17
'°'Ain 0.005
'J91'"pu 0.1
TOTAI-:
Cn ics:
S. (J. Nlarskc X5-53
P. A, Newman X3-4 1
RadCun Engineering File LB XO-23
Doeumen: and Info Services 110-09
Coetrntration (oC:i/e)
2.55 pCi/g
1.2F3 pCi/g
4.95 pCi/g
7.5E-1 pCi/g
2.55E2 pCi/g
7.5F.-2 pCi/g
1.5 nCi/e
1.4603 pCi/g

Figure 1
SAMPLE CCK-IN LIST
DateMme Received: l^ ^0^^^ SG#: &ZQQ7,-^
RFSH-SOW-93 -0003
Revision 5
Work Order Number. 0 ^3c^^ 0^ SAF #: -
ShippingContainerID: -0 ChainofCustody# ' gW^J^^v
1. Custody Seals on shipping container intact? -
Yes [ 1
2. Custody Seats dated and signed? Yes No [ )
f t^^
3. Chain-of-Custody record present? Yes Cij /No [ )
4. Cooler temperature
^O
5. Vermiculitefpaci ing mate ri
als is Wet [ ] Dr/—{ ^^^^
6. Number of samples in shipping container.
(
r'
7. Sample ho&q times exceeded? Yes [ ] No (^
8. Samples have:
--^Zape
custody seals
9. Same are:
in good condition
brdm
hazard labels
appropriate sample labels
leaking
have air bubbles
10. Where any anoma lies identified in sample receipt? Yes [ I No Cl/
11. Descrip tion of anomalies (include sample numbers):
Sample CustodiargUbo
Telephoned To:
7
o^
/
Date: ^O/C)

Client Sample Screening Results
17-Mar-98
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
B ill BOIU10 3/17/1998 QUAD2IB 3/17/19989:38:04AM 0011110 30 11 0.32 107 16266667
SOLID Bbg: 3/17/199812:19:30 AM BKO 600 28 0.04666667 364 0.94
AN Dale: 3/17/1998 Tot Sa, All: 3.00E+02 , 1.02E+02 Alp; (DpM 2.10E+00 (uCV 4.66E-03 (pCU 9.33E+00 f 5. 311+00 CAT 3.4E+00 I.b
Ppl mgs 101.6 Unita: O / , mg Bel; All): 3.73E+00 So): 1.27E-0 2 LIE): 2.34E+01 ± 3.4 11 +00
1 ",
3.9E+00
All
Bill BOHJII 3/17/1998 QUADZIC 3/17/19989:38:04AM B011111 30 13 0. 37333333 308 9.2816667
SOLID Bbg: 3/17/199812:19:30 AM BKO 600 36 0.06 391 0.983
Ad Dote: 3/17/1998 Tot So, Alls 3.00E+02 , 9.93E+01 Alp; (DpM 1.90E+00 (uCV 4.31E-03 (pCU 8.62E+00 f 3.4E+00 CAT 3.8E400 Lab
PPlmgt 99.8 Unite: 8 mg Dell Alq)i 2.068+01 5.): 4.668-02 1,11)1 9.338+01 S f.98+00 1 " 1.18i U0 All
• 1.18
Bill B0H112 3/17/1998 QUAD2 1 D 3/17/19989:38:04AM B011112 30 12 0.34666667 212 6.1383333
SOLID mist 3/17/1998 12:19:30 AM BKO 600 32 0.03333333 557 0.9283333
Ad Dalai 3/17/1998 Tot Ba, Atli 3.00E+02 , 9.91E+01 Alp; (DpnJ 1.98E+00 (uCV 4.30E-03 (pCU 8.99E+00 13.4E+00 CAT 3.6E+00 Lab
Ppl mp 99.1 i - Udb: g ^'- mg Bet; All): 1.36E+01 Sa): 3.10E-02 LIE): 6.20E+01 f 4.9E+00 1 / 1.6E+00 All
4E
Bill BOIU13 3/17/1998 QUAD22A 3/17/19989:38:08 AM BOIIJI3 30 1 -0.0183333 346 10.638333
SOLID Bbg: 3/17/1998 12:19:41 A61 BKO 600 31 0.05166667 337 0493
AM Dalai 3/17/1998 Tot So, Atilt 3.00E+02 9.87E+01 Alp; (DpM 4.95E-01 (uCV -1.81E-03 (pCU -3.63E+00 ± 4.6E+00 CAT 3.0E+02 Lab
Ppt mg: 98.7 - U nitas g , mg Bel; Alq): 2.30E+01 So): 5.25E-02 LIE): I.03E+02 ± 6.1E+00 I 9.3E-01
Bill 80}1114 3/17/1998 QUAD22B 3/17/19989:38:OSAb/ 0011114 30 20 0.39666667 670 21.383
SOLID Bbg: 3/17/1998 12:19:41 AM BKO 600 42 0.07 569 0.9483333
Ad Dotes 3/17/1998 Tod Sa, All: 3.00E+02 , 1.08E+02 Alp; (Blind 2.83E+00 (uCV 3.91E-0 3 (pCU 118E+01 f5.1E+00 CAT 4.2 E+00 Lab
Ppt mgt 107.8 i Unites g / , mg Bell Alq): 4.74E+01 50), 9.90E-02 1-10 1.9 11 E+02 S t.0E+00 1 /
Bill BON692 3/17/1998 QUAD22C 3/17/19989:38:08 AJ.1 BON692 30 7 0.19166667 310 9.375
LIQUID Bbg: 3/17/1998 12:19:41 AM BKO 600 23 0.04166667 373 0.9383333
i Ani Dote; 3/17/1998 Tot Sa, All: 1.00E+00 , 1.00E+00 Alp; (Dpnd 2.40&01 (uCV 1.08E-04 (p(V 1.08E+ 02± 1.9E+0I CAT 2.7E-0I Lob
Ppt mg: OA Ulnas L ml Bet; All): 1.73E+01 So): 7.8,E-03 LIE); 7.81E+03 ±4.9E+02
1
/6AE-03
All
17-Mar-98 Quanlerra Environment Se rvices, SCP V2.03 /
^3
3.1E-0I
All
All
tat

C ^'
U :7)
.A
CLIENT CODE ID MATRIX RECEIVED DETECTOR % ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
Bill BON693 3/17/1998 QUAD22D 3/ 17/19989:38:08AM BON693 30 7 0.16166667 117 296
LIQUID BLS: 3/17/199812:19:41 AM UKO 600 43 0.07166667 564 0.94
AM Date: 3 1 17/1998 Tot Se, Alq: 1.00E+00 , 1.00E+00 Alp; (Dpm/ 6.55E-0I (uCV 2.95E-04 (pCl/ 2.95E+02 ±3.7E+02 CAT 8.5E-02 lab
Ppt m8: 53.2 / Units: L ! ml Bet; Alq): 6.09E+00 Sa): 2.74E-03 40): 2.74E+0l ± 3.4E+02 I LBE-03 Alq
LI S
Bill BON694 3/17/1998 QUAD23A 3/17/19989:38:12 AM DON694 30 6 0.11166667 57 0.6816667
LI
QUID Bkg: 3/17/1998 12:19:48 AM BKO 600 53 0.08833333 611 1.0183333
AM Date: 3/17/1998 Tot Sa, Adq: 1.00E+00 , 1.00E+00 Alp; (Dpm/ 5.45E-0 1 (uCV 2.45E-04 (pCV 2.45E+02 ± 3.8E+02 CAT LOE-0 1 Lab
Pplmp 55.1 ./ Units: L ml Bel; Alq): 1.78E+0O Sa):
I
/ q
8,02E-04 48): 9.02E402 4 2.4E+02
6.2E-0 2
Ill[
BBf BONSM6 3 1 17/1996 QUAD23B 3/17/1998 93 8:12 AM BONSM6 30 119 3.92 5799 192.32333
LIQUID Blq: 3/171 1998 12:19:48 AM BKO 600 28 0.04666667 586 0.9766667
Aal Dal es 3/17/1998 Tel Se, Allis 6.00E+00 , 1.006101 Alp: (Upm/ 7.45E+00 O,CV 7.01 H4A (pCV 1.376+07 14 09 401 CAT 7.3E-07 14,16
Pplmp 3.5 ,/ UNta, L ml Bell Alq), 3.66E+02 Sa); 9.88E-0 2 14 8): 1.65E+04 3: 2,2E+02 I 3 .0E-0 3 Alq
,^
L18
Bill BONSM7 3/17/1998 QUAD23C 3/17/19989:38: 12 AM 130NIN17 30 23 0.71833333 107 2.6683333
LIQUID 848: 3/17/1998 12:19:48 AAI BKO 600 29 0.04833333 539 0.8983333
And Dale, 3/17/1998 Tot Sa, Alq: 6.00E+00 / 1.00E+01 Alp; (Dpm/ 2.18E+00 (u (-V 5.89E-0 4 (pCV 9.81E+01 ±2.7 E+01 CAT 2.5E-0 1 Lab
Ppl mp 5.9 i Unlla, L , ml Bel; Alq): 4.79E+00 Sa); 1.29E-03 40 2,16E+02 ± 3.0E+01 I - ^- 2.3E-01
Bill B0N8M8 3/17/1995 QUAD23D 3/17/19959:38:12AM BONSMS 30 36 1.13666667 114 2.89
LIQUID 848: 3/17/1998 12:19:48 AA1 BKO 600 38 0.06333333 346 0.91
Anl Dale: 3/17/1998 Tot Sa, Mq: 6.00E+00 1.00E+01 Alp; (Dpnd 3.46E+00 (uCV 9.36E-04 (p(-'V 1.56E+02 + 3.0E+01 CAT 1.6E-0 1 Lab
Piss mg: 3.5 / Units: L ml Bel; Mq): 4.83E+00 Sa): 1.31E-03 LIZ) : .18E+02 ± 2.9E+01
I
2.3E-01 Alq
1.15
17-Mar-98 Quanlerra Environment Se rvices, SCP V2.03 2
Lis LIB

A,, -i/I fIY6
—1 ` c,ir3
Beclael llRnforfl Inc. CHAIN Ol e CUS'I'ODWSAMPLE ANALYSIS ItEQOES'I' I 1j9NjIM-L6
'a1lrslnf f Cuwpni y CoMmirl lrlrphnue Nu. 1'rulrrl f'enrdln^lur Ibb - 1 car n[. uand
R Rr.4 1 2Aidt
SlcvcMarske 171-4716 WIIY1.Irl.
2I I)i
Project Designation Sasnph"It Lo ca tion tiAF No. ,(j^^J11 Ins
105C Phase I R Phase II • Concrete Samples 100 A,ca ' Will. 3 1 fl.J(I(/r''^I
Ice Cheal No. Held Logbook No, Method of Shipment
Ilend deliver
Shipped To Uffrllr 1'rmpaly Nu. 11111 of Lullnµ/Air 11111 Nu.
Quanlerrs Incorporated
POSSIBLE SARIPLE IIAZARnS/REMARKS — "M•
1 1rnrrrallon i r i
Rrdioaclive
Special llandling and/or Storage
S03a 79 - ►^ g o3a^ - /
SAMPLE ANALYSIS
I y'pe of Coulainer
No. of Contalnerls)
Volume
P
-_...
7
—
—^ ^.. _.. I
IL - ^-
Srrihrmll,ha
sp«i.1
ImWmom .
/
3 `6 y` 5F-)6— to oa3^i
sample 140 Matti. Sample [talc Songdc lime ♦.bl fr^ 5 '.:I^I j alYhi, "'.k: .i'^ ,1 (I'j j)lp rl',YF4':)ia': hr •f 1 ,h rll, o'I I,m,Ct 1 j •i s;C+ n •II' _.
N 898
.01ha, So
w TL
CIIAIN OF POSSESSION S ign/Prin t Nunes
Rdr ) 1)aterfime Be [ a Bj I /lime/
R f' /e Hq?9B /I i $ G

Client Sample Screening Results
l7-Mar-98
CLIENT CODE ID MATRIX RECEIVED DETECTOR AC'Q DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
BIII B0H110 3/17/1996 QUAD2 1 B 3117/19999:38:04AM 8011110 30 II 0.32 107 2.6266667
SOLID Bkg1 3/17/1991112A9:30 AM BKO 600 28 0.04666667 564 0.94
Ad Dole, 3/17/1998 Tot Se, AIq, 3.00E+02 , 1.02E+02 Alp; (Dpm/ 2.10E+00 (uCU 4.66E-03 (pCU 9.33E+00 ± 5.3E+00 CAT 5AE+00 Lob
Ppt mip 101.6 Udb, 0 j mg Bel; Alq): 5.73E+00 Sep 1.27E-02 LIg): 2.54E+01 3 3.4E+00
i '
3.9E+00 Alq
1•le
BIII 8011111 3/171 1998 QUAD2 1 C 3/17/19989:38:04AM 8011111 30 13 0.37333333 308 9.2816667
SOLID Bkp 3/17/1998 12:19:30 AM BKO 600 36 0.06 391 0.983
Ad Dates 3/17/1998 Tot Sa,Algl 5.00E+02 , 9.95E+01 Alp; (Dpn,/ 1.90E+00 (uCl/ 4.31E-03
Pplmg: 99.5 Udla: g mg Bel; Alq): 2.06E+01 So): 4.66E-0 2
Bill 6011112 3/171 1998 QUAD2 1 D 3/17/19989:38:04AM B011J 1 2
SOLID Bkgt 3/171 1998 12:19:30 AM BKG
Ad D ole: 3 1 17/1998 Tot Se, Mq: 5 .00E+02 9.91E,01 Alp; (1)p,N 1.981:+00 (.Cl/ 4.301:03
Ppe mg: 99.1 i - Units: g / mg Bel; Alq): 1.36E+01 So): 3.10E-02
(pCU 8.62 E+00 ± 5.4E+00 CAT 5.8E400 Lob
I.Ig): 9.32E+01 ± 5.9E400 1 1.1 E+00 Alq
: IdL
30 12 0.34666667 212 6.1383333
600 32 0.05333333 557 0.9283333
(pCU 8.99E+00 ± 5.4E+100 CAT 5.6E:00 Lob
I,Ig): 6.20E+01± 4.9E+00 I j - 1.6E+00 Alq
IAZ
BIII 8011113 3/17/1998 QUAD22A 3/17/19989:38:OBAM B01IJ13 30 1 -0.0183333 346 10.638333
SOLID Bkg, 3/17/1998 12:19:41 AM BKO 600 31 0.05166667 537 0.895
Ad Dates 3/171 1998 Tot So, Alq, 5.00E+02 , 9. 117E+01 Alp; (Dpm/ •7.93E-0 1 (uCU . 1.81E-03 (pCV -3.63E+00 +4.6E+00 CAT 5.0E+02 Less
Ppt mg: 98.7 Units: g mg Bel; Alq): 2.30E+01 So): 5.25E-02 Leg): 1.03E+02 j6.1 E+00
1
j" 9.5E-01 Alq
1•le
Bill BOIIJ 1 4
3/17/1998 QUAD22B 3/17/19989:38:08AK1 B011114
30 20 0.59666667 670 21 3 85
SOLID
Bkg; 3/171 1998 12:19:41 AKf BKO
600 42 0.07 369 0.9483333
Ad Dol e,3/17/1998 Tot Se, Alq: 3.00E+02 1.011E+02 Alp; (Dpm/ 2.83E+00 (UCU 3.91E-0 3 (pCU I.I&E101 ± 3.1E400 CAT 4.2E+00 Lob
P iss mg: 107.8 . Udb: g^ , mg Bel; Alq): 4. 74E+01 Se): 9.90E-0 2 Ljg): 1.98E+02 ±B.OE too 1 / S.IE-01 AIq
1•IL
Bill BON692 3/17/1998 QUAD22C 3/17/1998 9:38:08 AK1 BON692 30 7 0.19166667 310 9.375
LIQUID Bkg: 3/17/1998 12:19:41 AKI 13KO 600 25 0.04166667 375 0.9383333
Ad Date: 3 1 17/1998 Tot Se, Alq: 1.00 V,+00 1.00E+00 Alp; (Dpn3 2.40E-01 - (uC'U 1.08E-04 -- (pCU -- 1.08E+02 -- -_
± 1.9E+02 CAT 2.3E-0 1 Lab
Piss mg: 0.4 Udb: L , ml Bel; Alq): 1.73E 101 So): 7.81E-03
i
LIg): 7.8IE403 ±4.9E)02
i
Alq
6.4E-03
IdL
17-Afar-98 Ouanterra Environment Se rvices, SCP V2.03 J

Qyrhianterra
;ter
Sty
orrecti Action
(o
Client's Name: G
C Client ' s Name:
Condition Upon Receipt Variance Report
St. Louis Laboratory
,tva Atot7lr.^.a.F.c,
Informed verbally on: Bv:
Informed in writin g on: By:
014501
Login No.: / 721-¢
Client. Due: _ 7- `T,f Ime: 0 Y o
Project No: S-50. 2G D Initiated by: o -A J—kh
Shipper/No : -7
ConditionNariance (Check all that apply): y):
RFA/COC Numbers: /7 D C
.. q Sample received b roken/leaking. 8. q Sample ID on container does not match sample ID
2. q Sample received without proper preserva tive. on paperwork. Explain:
•
q Cooler tempera ture not within 4"C _ 2C
Record temperature:
q pH 9. q All coolers on airbiil not received with shipment.
q other: 10. q Other (expla in below):
.. q Sample received in improper container.
j Sample received without proper paperwork. Explain:
5. q Paperwork received without sample.
6. q No sample ID on sample con tainer.
-. q Custody tape dis turbed/brokervmissing.
C No variances were noted
Notes: ,3 -r- ^,l b ^ Z
I^^^ 610
Sample(s) processed "as is".
\
sample receipt Cooler Tempera ture upon Receipt.
7 ?o3i^Pdi
,P.ch/.2.0• t
ll
/-A CT e^ —/ ^^Q 4 / [Y rl Ss^^^i 3t ^^,
C Sample(s) on hold unt il : If released. no tify
Sample Control Supe rvisor Review: (or designate) Date: ?" ^ 7 —
Project Management Review: ^ Date: 7 —/P -1Y
SL.ADMIN-0004. Reviseo :! '24/95
SIGNED ORIGINAL NR;ST BE RETALNED IN THE PROJECT FILE
L

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON680
OUanterra-Richlanci
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/09/98
Receipt Date 03/09/98
Report Date 04/08/98
cuanterra ID 17199-001
Blank Sample Prep. Analyses Detection
Analyte CAS Number Name Date Date Result Unit Oual. Limit Dilution
Aroclor-12 4 11097-69-1 QCRLK167668-1 03/18/98 0 / 0/98 63 UG/KG 33 .2
DCS 2051-24-3 QCBLK167668-1 03/18/98 03/30/98 88 %REC .2
TCM% 877-09-8 OCBLK167668-1 03/18/98 03/30/98 80 7.REC .2
"11^^5

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON681
Analyte
Duanterra- Ri chI and
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/09/98
Receipt Date 03109/98
Report Date 04/08/98
Duanterra ID : 17199-002
Blank Sample Prep. Analyses Detection
CAS Number Name Date Date Result Unit Dual. Limit Dilution
Aroclor-1 54 11097-69-1 DCBLK167668-1 03/18/98 03/30/98 UG/KG U 33 .2
DC8 2051-24-3 QCBLK167668-1 03/18/98 03/30/98 101 %REC .2
TCMX 877-09-8 QCBLK167668-1 03/18/98 03/30/98 105 %REC .2
"1 0

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: SON685
Anal yte
DCB
TCMX
Blank Sample
CAS Number Name
11097-69-1 OCBLK1681 3-1
2051-24-3 QCBLK168133-1
877-09-8 QCBLK168133-1
Ouanterra-Richland
3350 George Washington way
Richland, WA 99352-1613
Project: 550.260
Semple Date 03/11/98
Receipt Date 03/11/98
Report Date 04/08/98
Duanterra ID 17200-001
Prep. Analyses Detection
Date Date Result Unit Dual- Limit Dilution
03/24/98 0 /2 /98 33 UG/KG U
03/24/98 03/25/98 90 %REC 1
03/24/98 03/25/98 103 %REC 1
, 7.s

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON685
Guanterra-Richland
3350 George Washington Nay
Richland, NA 99352-1613
Project: 550.260
Sample Date 03/11/98
Receipt Date 03/11/98
Report Date 04/20/98
Guanterra ID 17200-001MS
Blank Sample Prep. Analyses Detection
Analyte CAS Number Name Date Date Result Unit Qua(. Limit Dilution
Aroclor-1016 12674-11-2 QCSLK16813 -1 03/24/98 0 /25/98 a6 %REC
Aroclor-1260 11096-82-5 QCBLK168133-1 03/24/98 03/25/98 77 %REC 5
DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 90 %REC 5
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 106 %REC 5
V _i"074

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client 10: 80X685
Analyte
Aroclor-1016
Aroclor-1260
DCB
TCM%
Blank Sample
CAS Number Name
12674-11-2 OCBLK168133-1
11096-82-5 QCBLK168133-1
2051-24-3 QCBLK168133-1
877-09-8 QCBLK168133-1
Duanterra-Richland
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Prep. Analyses
Date Date
03/24/98 03/25/98
03/24/98 03/25/98
03/24/98 03/25/98
03/24/98 03/25/98
Sample Date 03/11/98
Receipt Date 03/11/98
Report Date 04/08/98
Duanterra ID 17200-OOIMS
Detection
Result Unit dual. Limit Dilution
%REC 5
%REC - - 5
90 %REC 5
106 %REC .5
J 7'

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON685
Duanterra-Richland
3350 George Washington way
Richland, WA 99352-1613
Project: 550.260
sample Date 03/11/98
Receipt Date 03/11/98
Report Date 04/08/98
Duanterra ID : 17200-GOIMSD
Blank Sample Prep. Analyses Detection
Analyte CAS Nunber Name Date Date Result Unit DuaL. Limit Dilution
Aroclor-1016 12674-11-2 QCSLK168133-1 03/24/98 03/25/98 84 %REC .5
Aroclor-1260 11096-82-5 QCBLK168133-1 03/24/98 03/25/98 81 %REC .5
DC8 2051-24-3 QCSLK168133-1 03/24/98 03/25/98 91 %REC .5
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 104 %REC .5
.,0076

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: SON686
AnaLyte
DC8
rCMx
Blank SampLe
CAS NLEber Name
11097-69-1 QCBLK168133-1
2051-24-3 QCBLK168133-1
877-09-8 QC8LK168133-1
Quanterra-Rich Land
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/11/98
Receipt Date 03/11/98
Report Date 04/08/98
Quanterra ID 17200-002
Prep. Analyses Detection
Date Date Result Unit Qua L. Limit Dilution
03/25/98 84 %REC
03/25/98 89 %REC 9
A077

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON687
Analyte
ouanterra-Richlana
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/11198
Receipt Date 03/11/98
Report Date 04/08/98
0uanterra ID : 17200-003
Blank Sample Prep. Analyses Detection
CAS Number Name Date Date Result Unit Dual. Limit Dilute on
Aroclor-1254 11097-69-1 OC8LK168133-1 03/24/98 03/25/98 33 UG/KG U 33
Oc8 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 90 %REC
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 105 %REC

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: SON682
Ouanterra-Richland
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/10/98
Receipt Date 03/10/98
Report Date 04/08/98
Duanterra ID 17202-001
Blank Sample Prep. Analyses Detection
Analyte CAS Number Name Date Date Result Unit Oual. Limit Dilution
Aroclor-12 4 11097-69-1 QCBLK168133-1 03/24/98 03/25/98 33 UG/KG U 33 1
DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 91 %REC 1
TCMK 877-09-8 QCBLK168133-1 03/24/98 03/25/98 100 %REC t
x,00079

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON683
Analyte
Duanterra-Richland
3350 George Washington Nay
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/10/98
Receipt Date 03/10/98
Report Date 04/08/98
Duanterra ID : 17202-002
Blank Sample Prep. Analyses Detection
CAS Number Name Date Date Result Unit Dual. Limit Dilution
Aroclor-12 4 11097-69-1 DCBLK16 133-1 03/24/98 03/25/9 33 UG/KG U 33 1
DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 91 %REC 1
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 86 %REC 1

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON684
Duanterra-Richland
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/10/98
Receipt Date 03/10/98
Report Date 04/08/98
Ouanterra ID : 17202-003
Blank Sample Prep. Analyses Detection
Analyte CAS Number Name Date Date Result Unit Dual. Limit Dilution
Aroclor-12 4 1 "
07-69-1 QCBLK168133-1 03/24/98 03/ /98 33 UG/KG U 33 1
DCB 2051-24-3 QCSLK168133-1 03/24/98 03/25/98 88 %REC 1
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 94 %REC 1

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Duanterra-Richland
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/12/98
Receipt Date 03/12/98
Report Date 04108/98
Client ID: BON688 Duanterra ID : 17203-001
Blank Sample Prep. Analyses Detection
Analyte CAS Number Name Date Date Result Unit Dual. Limit Dilution
Aroclor-12 4 11097-69-1 QCBLK168133-1 03/24/98 03/25/98 33 UG/KG U 33 1
OCS 2051-24-3 QCSLK168133-1 03/24198 03/25/98 92 %REC 1
TCMK 877-09-8 QCBLK168133-1 03/24/98 03/25/98 105 %REC 1
(J00S^:

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON689
Analyte
Blank Sample
LAS Number Nam
Ouanterra-Richland
3350 George Washington Nay
Richland, WA 99352-1613
Project: 550.260
Prep. Analyses
Date Date
Sample Date 03/12/98
Receipt Date 03112/98
Report Date 04/08/98
Ouanterra ID : 17203-002
Detection
Result Unit OuaL. Limit Dilution
p roctor-1254 11097-69-1 QCBLK168133-1 03/24/98 03/25/98 UG/KG U 33 1
DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 90 %REC 1
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 65 %REC 1
^J

Duanterra-Richland
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Category: PCB's Sample Date 03/13/98
Method: EPA 8080 Receipt Date 03/13/98
Matrix: SOLID Report Date 04/08/98
Client ID: BON690 Duanterra ID 17221-001
Blank Sample Prep. Analyses Detection
Analyte CAS Number Name Date Date Result Unit DuaL. Limit Dilution
Aroclor-1254 11097-69-1 QCBLK16825 -1 03/25/98 03/29/98 33 UG/KG U 1
DC8 2051-24-3 QCBLK168253-1 03/25198 03/29/98 94 XREC 1
TCMX 877-09-8 QCBLK168253-1 03/25/98 03/29/98 73 XREC
OS 6

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON691
Duanterra-Richland
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/13/98
Receipt Date 03/13/98
Report Date 04/08/98
Ouanterra ID 17221-002
Blank Sample Prep. Analyses Detection
Analyte CAS Number Name Date Date Result Unit DuaL. Limit Dilution
Aroclor-1254 11097-69-1 QCBLK168253-1 03/25/98 03/29/98 33 UG/KG U 33 1
DCB 2051-24-3 QCBLK168253-1 03/25/98 03/29/98 108 %REC 1
TCMX 877-09-8 QCBLK168253-1 03/25/98 03/29/98 82 %REC 1
, 6087

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: SON692
Analyte
Duanterra-Richland
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/16/98
Receipt Date 03/16/98
Report Date 04/08/98
Duanterra ID : 17224-001
Blank Sample Prep. Analyses Detection
CAS Number Name Date Date Result Unit Dual. Limit Dilution
Aroclor-1254 11097-69-1 QCBLK168253-1 03/25/98 03/29/98 33 UG/KG U 33 1
DCB 2051-24-3 QCBLK168253-1 03/25/98 03/29/98 92 %REC 1
TCMK 877-09-8 QCBLK168253-1 03/25/98 03/29/98 74 %REC 1
tj

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client ID: BON693
duanterra-Richland
3350 George Washington Nay
Richland, WA 99352-1613
Project: 550.260
Sample Date 03/16/98
Receipt Date 03/16/98
Report Date 04/08/98
duanterra ID 17224-002
Blank Sample Prep. Analyses Detection
Analyte CAS Number Name Date Date Result Unit dual. Limit Dilution
ArocLor-1254 11097-69-1 QCBLK168253-1 03/25/98 03/29/98 33 UG/KG U 3 1
DCB 2051-24-3 QCBLK168253-1 03/25/98 03/29/98 95 %REC 1
TCMX 877-09-8 QCBLK168253-1 03/25/98 03/29/98 87 %REC 1
J08 9

Category: PCB's
Method: EPA 8080
Matrix: SOLID
Client 10: SON694
Anatyte
Aroclor-
DCB
TCMX
Quanterra-Richland
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Stank Sample Prep. Analyses Detection
CAS Number Name Date Date Result Unit Qua L. Limit Dilution
2051-24-3 QCSLK168253-1
877-09-8 QCBLK168253-1
03/29/98 98 %REC
03/29/98 93 %REC
Saapie Date 03/16/98
Receipt Date 03/16/98
Report Date 04/08/98
Quanterra ID 17224-003
^i.,^J0

Lab Name: OUANTERRA.MO Contract:
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 6.0 (g/ml) G
Level: (low/med) LOW
Moisture: not dec. dec.
Extraction: (SepF/Cont/Sonc) Sonc
GPC Cleanup: (YIN) N pH:
CAS NO. Compound
1D EPA SAMPLE NO.
PCB ORGANICS ANALYSIS DATA SHEET
SAS No.: SDG No.: W02275
EONG80
Lab Sample ID: 17199-001
Lab File ID:
Date Sampled: 03-09-98
Date Extracted: 03-18-98
Date Analvzed: 03-30-98
Dilution Factor: 0.2
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 63
U Concentration of analyte is less than the value given.
FORM I PEST
"j0J X93

1D EPA SAMPLE NO.
PCB ORGANICS ANALYSIS DATA SHEET
I
BONG81
Lab Name: OUANTERRA.MO Contract 550.260
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 6.0 ('g/ml) G
Level: (low/med) LOW
% Moisture: not dec.
Extraction: (SepF/font/Sonc)
GPC Cleanup: (Y/N) N
CAS NO. Compound
dec
pH:
Sonc
SAS No.: SDG No.: W02275
Lab Sample =D: 17199-002
Lab File ID:
Date Sampled: 03-09-98
Date Extracted: 03-18-96
Date Analyzed: 03-30-98
Dilution Factor: 0.2
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 33 U_
U: Concentration of analyte is less than the value given.
FORM I PEST
j0O94

Lab Name: OUANTERRA MO Contract:
Lab Code: ITMO Case No.:
Matr_%: (soil/water) SOIL
Sample wt/vol: 30.0 (g/ml) G
eve_: flow /med) LOW
% Moisture: not des. dec.
Extraction: (SepF/font/Sonc) Sonc
GPC Cleanup: (YIN) N pH:
CAS NO. Compound
11097-69-1 ------ Aroclor-
1D EPA SAMPLE NO.
PCB ORGANICS ANALYSIS DATA SHEET
SAS No.: SDG No.: W02275
BON685
Lab Sample 1D: 17200-001
Lab File ID:
U Concentration of analyte is less than the value given.
FORM I PEST
Date Sampled: 03-11-96
Date Extracted: 03-24-98
Date Analyzed: 03-25-98
Dilution Factor: 1
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
33 1 U
1, -J0095

Lab Name: OUANTERRA MO Contract:
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/ml) G
Level: (low/med) LOW
Moisture: not dec. dec.
Extraction: (SepF/Cont/Sonc) Sonc
GPC Cleanup: (YIN) N pH:
CAS NO. Compound
1D EPA SAMPLE NO.
PCB ORGANICS ANALYSIS DATA SHEET
SAS No.: SDG No.: W02275
BONG86
Lab Sample ID: 17200-002
Lab File ID:
Date Sampled: 03-11-98
Date Extracted: 03-24-98
Date Analyzed: 03-25-98
Dilution Factor: 1
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 33 U
U Concentration of analyte is less than the value given.
FORM I PEST
"j
I

Lab Name: OUANTERRA,M0 Contract:
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/ml) G
Level: (low/med) LOW
W Moisture: not dec. dec.
Extraction: (SepF/Cont/Sonc) Sonc
GPC Cleanup: (Y/N) N PH:
CAS NO. Compound
1D EPA SAMPLE NO
PCB ORGANICS ANALYSIS DATA SHEET
550.260
SAS No. SDG No. W02275
BONG97
Lab Sample ID: 17200-003
Lab File !D:
Date Sampled: —03----1-98
Date Extracted: 03-24-98
Date Analyzed: 03-25-98
Dilution Factor: 1
CONCENTRATION UNITS:
(ug/L or ug/Kq) UG/KG
11097-69-1 ------ Aroclor-1254 33 -U--
U: Concentration of analyte is less than the value given,
FORM I PEST
1- U009 "1

Lab Name: QUANTERRA,MO Contract:
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.1 jg/ml) G
Level: (low/med) LOW
°s Moisture: not dec. dec.
Extraction: (SepF/font/Sonc) Sonc
GPC Cleanup: ,Y/N) N pH:
CAS NO. Compound
ID EPA SAMPLE NC.
PCB ORGANICS ANALYSIS DATA SHEET
iBON682
SAS No.: SDG No.: W02275
Lab Sample ID: 17202-001
Lab File ID:
Date Sampled: 03-10-98
Date Extracted: 03-24-98
Date Analvzed: 03-25-98
Dilution Factor: 1
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 33 ^—U_i
U: Concentration of analvte is less than the value given.
FORM I PEST
00098

Lab Name: QUANTERRA,MO Contract:
Lab Code: ITMO Case No.:
Matrix: (scii/water) SOIL
Sample wt/vol: 30.0 (g/ml) G
Level: (low/med) LOW
% Moisture: not dec. dec.
Extraction: (SepF/font/SOnc) Sonc
GPC Cleanup: (Y/N) N pH:
in EPA SAMPLE NO.
PCB ORGANICS ANALYSIS DATA SHEET
550.260
SAS No.: SDG No.: W02275
Lab Sample ID: 17202-002
Lab File ID:
Date Sampled: 03-10-98
Date Extracted: 03-24-98
Date Analvzed: 03-25-98
Dilution Factor: 1
BONG83 -^
CONCENTRATION UNITS:
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 33 1 U
U: Concentration of analyte is less than the value given.
FORM I PEST
(:00099

Lab Name: OUANTERRA,MO Contract
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.1 (g/ml) G
Level: (low/med) LOW
% Moisture: not dec.
Extraction: (Sep F/font/SOnc)
GPC Cleanup: (YIN) N
CAS NO. Compound
1D EPA SAMPLE NO.
PCB ORGANICS ANALYSIS DATA SHEET
dec.
pH:
Sonc
550.260
SAS No.: SDG No.: W02275
SON684
Lab Sample iD: 17202-003
Lab File ID:
Date Sampled: 03-10-98
Date Extracted: 03-24-98
Date Analyzed: 03-25-98
Dilution Factor: 1
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG 4
11097-69-1 ------ Aroclor-1254 33 U
U: Concentration of analyte is less than the value given.
FORM I PEST
"00100

Lab Name: OUANTERRA MO Contract:
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/ml) G
Level: (low/med) LOW
% Moisture: not dec. dec.
Extraction: (SepF/font/SOnc) Sonc
GPC Cleanup: (Y/N) N pH:
ID EPA SAMPLE NO.
PCP ORGANICS ANALYSIS DATA --HEST
550.260
SAS No.: SDG No.: W02275
SONG88
Lab Sample ID: 17203-001
Lab File ID:
Date Sampled: 03-12-98
Date Extracted: 03-24-98
Date -nalvzed: 03-25-98
Dilution Factor:
CONCENTRATION UNITS:
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 33 U
i
U: Concentration of analyte is less than the value given.
FORM I PEST
:. V V i V l

Lab Name: OUANTERRA,MO Contract:
Lab Code: ITMO Case No.:
Matrix: !Soil /water) SOIL
Sample wt/vol: 30.2 (g/ml) G
Level: (low/med) LOW
% Moisture: not dec. dec.
Extraction: (SepF/font/Sonc) Sonc
GPC Cleanu p : (YIN) N pH:
1D EPA SAMPLE NO.
PCB ORGANICS ANALYSIS DATA SHEET.
550.260
SAS No.: SDG No.: W02275
BONG89
Lab Sample =D: 17203-002
Lab File ID:
Date Sampled: 03-12-98
Date Extracted: 03-24-98
Date Analyzed: 03-25-98
Dilution Factor: 1
CONCENTRATION UNITS:
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 33 U
U: Concentration of analyte is less than the value given.
FORM I PEST
100102
—

Lab Name: QUANTERRA,MO Contract:
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/ml) G
Level: (low/med) LOW
% Moisture: not dec. dec.
Extraction: (SepF/font/Sonc) Sonc
GPC Cleanup: (Y/N) N pH:
1D EPA SAMPLE NO.
PCB ORGANICS ANALYSIS DATA SHEET
550.260
SAS No.:
SDG No.: W02275
3ON690
Lab Sample ID: 17221-301
Lab File ID:
Date Sampled: 03-13-98
Date Extracted: 03-25-98
Date Analvzed: 03-29-98
Dilution Factor: 1
CONCENTRATION UNITS:
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 1 33 1 U
U: Concentration of analvte is less than the value given.
FORM I PEST
00103

Lab Name: QUANTERRA,MO Contract: 550.260
1D EPA SAMPLE :70.
PCB ORGANICS ANALYSIS DATA SHEET
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275
Matrix: (soil/water) SOIL Lab Sample ID: 17221-002
Sample wt/vol: 30.1 (g/ml) G Lab File ID:
Level: (low/med) LOW Date Sampled: 03-13-98
o Moisture: not dec. dec. Date Extracted: 03-25-98
Extraction: (SepF/font/SOnc) Sonc Date Analyzed: 03-29-98
CPC Cleanup: ;Y/N) N pH: Dilution Factor: _
BON691
CONCENTRATION UNITS:
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 33 U
U: Concentration of anal; ,te is less than the value given.
FORM I PEST
r u0iO4

Lab Name: QUANTERRA.MO Contract: 550.260
1D EPA SAMPLE NO.
POE ORGANICS ANALYSIS DATA SHEET
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275
Matr'_x: (soil/water) SOIL Lab Sample ID: 17224-001
Sample wt/vol: 30.0 (g/ml) G Lab File ID:
Level: (low/med) LOW Date Sampled: 03-16-98
o Moisture: not dec. dec. Date Extracted: 03-25-98
Extraction: (SepF/font/Sonc) Sonc Date Analyzed: 03-29-99
GPC Cleanup : (YIN) N pH: Dilution Factor:
EON692
CONCENTRATION UNITS:
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 33 U
U: Concentration of analyte is less than the value given.
FORM I PEST
1 00105

Lab Name: QUANTERRA MO Contract:
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/ml) G
Level: (low/med) LOW
Moisture: not dec. dec.
Extraction: (SepF/Cont/Sonc) Son
GPC Cleanup: (Y/N) N pH:
CAS NO. Compound
11097-69-1 ------ Aroclor-1254
ID
PCB ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
BON693
550.260 _!
SAS No.:
SDG No.: W02275
Lab Sample ID: 17224-002
Lab File ID:
U: Concentration of analyte is less than the value given.
FORM I PEST
Date Sampled: 03-16-98
Date Extracted: 03-25-98
Date Anal y zed: 03-29-98
Dilution. Factor: 1
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
33 I-'J

Lab Name: OUANTERRA,MO Contract:
Lab Code: ITMO Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/ml) G
Level: (low/med) LOW
% Moisture: not dec.
Extraction: (SepF/font/SOnc)
GPC Cleanup: (YIN) N
CAS NO. Compound
ID EPA SAMPLE NO.
PCB ORGANICS ANALYSIS DATA SHEET
dec.
pH:
Sonc
550.260
SAS No.: SDG No.: W02275
SON694
Lab Sample ID: 17224-003
Lab File ID:
Date Sampled: 03-16-98
Date Extracted: 03-25-98
Date Analvzed: 03-29-98 ._
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
11097-69-1 ------ Aroclor-1254 33 U
U: Concentration of analyte is less than the value given.
FORM I PEST

Category: Mercury
Method: EPA 7471
Matrix: SOLID
ouanterra-Richland
3350 George Washington Way
Richland, WA 99352-1613
Project: 550.260
Semple Date 03/09/98
Receipt Date 03/09/98
Report Date 04/20/98
Client Ouanterra Blank Saapte Prep. Anityses Detection
ID ID Analyte CAS Number Name Date Date Result Unit Ouai. Limit Dit.
BON680 17199-001 Mercury 7439-97-6 OCBLK168655-1 03/30/98 03/30/98 0.10 MG/KG 0.033 1
BON681 17199-002 Mercury 7439-97-6 OCBLK168655-1 03/30/98 03/30/98 0.03 MG/KG B 0.033 1
BON685 17200-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
BON685 17200-001M5 Mercury 7439-97-6 OCSLK168333-1 03/25/98 03/25/98 116 XREC 1
BON685 17200-001MSD Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 111 %REC 1
BON636 17200-002 Mercury 7439-97-6 OCBLK168333-1 03/25198 03/25/98 0.13 MG/KG 0.033 1
BON687 17200-003 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
BON682 17202-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
BON683 17202-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.10 MG/KG 0.033
BON684 17202-003 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
BON688 17203-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
BON689 17203-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.04 MG/KG 0.033 1
BON690 17221-001 Mercury 7439-97-6 OCSLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
BON691 17221-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
SON692 17224-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.16 MG/KG 0.033 1
SON693 17224-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
BON694 17224-003 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
NA OCLCS168655-1 Mercury 7439-97-6 OCBLK166655-1 03/30/98 03/30/98 116 %REC 10
NA OCBLK168655-1 Mercury 7439-97-6 OCBLK166655-1 03/30/98 03/30/98 0.017 MG/KG U 0.033 1
25

category: Mercury
Method: EPA 7471
Matrix: SOLID
QUanterra-Richland
3350 George Washington Nay
Richland, WA 99352-1613
Project: 550.260
Sample Date NA
Receipt Date NA
Report Date 04/08/98
Client Quanterra Blank Sample Prep. Analyses Detection
ID ID Analyte CAS Number Name Date Date Result Unit Qua L. Limit Dil
NA QCLCS168333-1 Mercury 7439-97-6 QCBLKI 33-1 03/25/98 03/25/98 107 KREC 10
NA QCBLK168333-1 Mercury 7439-97-6 QCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1
^^ 6

Category: ICAP Metals
Method: EPA 6010
Matrix: SOLID
Duanterra-RichLano
3350 George Washington way
RichLand, WA 99352-1613
Project: 550.260
Sample Date NA
Receipt Date NA
Report Date 04/08/98
CLient Duanterra Blank Sample Prep. Analyses Detection
ID ID Analyte CAS Number Name Date Date Result unit Oual. Limit Dil
NA OCLCS168299-1 Lead 7439-92-1 OCOLK168299-1 03/25/98 03/25/98 100 %REC 1
NA QCBLK168009-1 Lead 7439-92-1 QCBLK168C09-1 03/23/98 03/23/98 0.21 MG/KG B 0.30 1
NA QCBLK168299-1 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 0.16 MG/KG B 0.30 1
BON680 17199-001 Lead 7439-92-1 QCSLK168009-1 03/23/98 03/23/98 10.9 MG/KG E 0.30 1
BON681 17199-002 Lead 7439-92-1 QCHLK168009-1 03/23/98 03/23/98 3.7 MG/KG E 0.30 1
BON685 17200-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.2 MG/KG E 0.30 1
BON685 17200-OOlMS Lead 7439-92-1 QCSLK168299-1 03/25/98 03/25/98 90 XREC 1
SON685 17200-OOlMSO Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 88 %REC 1
BON686 17200-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 11.8 MG/KG E C.30 1
SON687 17200-003 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.7 MG/KG E 0.30 1
8ON682 17202-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.7 MG/KG E 0.30 1
SON683 17202-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 7.6 MG/KG E 0.30 1
BON684 17202-003 Lead 7439-92-1 GCBLK168299-1 03/25/98 03/25/98 3.3 MG/KG E 0.30 1
BON688 17203-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.0 MG/KG E 0.30 1
9ON689 17203-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 9.0 MG/KG E 0.30 1
SON690 17221-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.4 MG/KG E 0.30 1
SON691 17221-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 2.9 MG/KG E 030 1
BON692 17224-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 10.6 MG/KG E 0,30 1
BON693 17224-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 4.2 MG/KG E 0.30 1
BON694 17224-003 Lead 7439-92-1 OCBLK168299-1 03/25/98 03/25/98 3.6 MG/KG E 0.30 1
NA QCLCS168009-1 Lead 7439-92-1 OCOLK168009-1 03/23/98 03/23198 102 %REC 1

U.S. EPA - CLP
COVER PAGE INORGANIC ANALYSES DATA PACKAGE
Lab Name: QUANTERRA MO Contract: 550.260
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275
SOW No.: SW846
EPA Sample No.
_BON692
_2 0 11 680
_BON681
BON682
_B0N683
_BON684
_BON685
_BON685SD
_BON685S
_BON686
_BON687
_B0N688
_BON689
_BON690
_BON691
_BON693
BON694
Were ICP interelement corrections applied ?
Were ICP background corrections applied ?
If yes - were raw data generated before
application of background corrections ?
Comments:
Lab Sample ID
17224-001_
17199-001
17199-002
17202-001
_17202-002
17202-003
17200-001
_17200-OO1SD_
17200-OO1S
17200-002
_17200-003^
17203-001_
17203-002
17221-001
17221-002J
17224-002
17224-003
Yes/No YES
Yes/No YES
Yes/No 7C
I certify that this data package is in compliance with the terms and
conditions of the contract, both technically and for completeness, for
other than the conditions detailed above. Release of the data contained
in this hardcopy data package and in the computer-readable data submitsed
on floppy diskette has been authorized by the Laboratory Mana ger r -he
Manag er's designee, as verified by the following signature.
Signature: Name:
Date Title:
COVER PAGE - IN SW-^46
7 A
, - J 1

U.S. EPA - --LP
INORGANIC ANALYSES DA '.-=ET
^
BON692
Lab Name: QUANTERRA MO
Lab Code: - TMO Case No.:
Matrix (soil/water): SOIL
Level (low/med): LOW
Solids: 100.0
Contract:
SAS No.: SDG No.. W02275
Sample ID: 17224-001
-,--e Received: 03/15/98
Concentration Units (ug/L or mg/kg dr.; :oeight)
CAS No. Analyte Concentrat Q
7439-92-1 LeaT 1C._^^ E
7439-97-6 Mercury-0.15– — -
Color Before: Clarity Before:
Color After: Clarity After:
^7omments:
-
^I
I
P
CV
MG/KG
=1
-
-I
SW-84h

Color Before:
Color After:
Comments:
I- . .EPA - =
1 --PA :SAMPLE No.
INORGAN_ - ANALYSES -ATA. -HEET I
BON630
Lab Name: QUANTERRA MO
Lab Code: ITMO Case No.:
Matrix (soil/water): SOIL
Level (low/med): LOW
Contract:
SAS No.:
5 .26G
SDG No.:
Lab Sample ID:
Date Received:
W02275
17199-001
03,`(J9/9 c
% Solids: 100.0
Concentration Units "ug/L or mg/kg dry weight): MG/KG
CAS No.
7439-92-1
7439-97-6
Analyte Concentration C Q IM
LeadI 10.9
Mercury_ O.lO CV
I-
i
—
I-
. ,
.
Clarity Before : TP_xr^:^e.
Clarity After: Art-facts:
_ ten,•, _ - _^^
i
SW-n46

U.S. EPA CLP
1 EPA SAMPLE NO -
INORGANIC ANALYSES DATA SHEET
BGN631
Lab Name: QUANTERRA MO Contract: 550.260
Lab Code: ITMO Case `To.: SAS No.: —I SDG o.: ;102275
Matrix (soil/water): SOIL
Sample ID: _7199-00:
Level (low/med) LOW Date Received: 3;09/98
s Solids: 100.0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7439-92-1
7439-97-6
Analyte
Lem
Mercury
Concentration Q
i– i
3.7 E
0.03 B
Color Before: Clarity Before: Text re:
Color After: Clarity After:
Comments:
i
–i
N
5
_V
i
SW-146
131
i

U.S. EPA --LP
1 EPA SAMPLE NO.
INORGANIC ANALYSES DATA SHEET
20N682
Lab Name: QUANTERRA MO Contract: -750.260
Lab Code: ITMOCase No.: SAS No.: SDG No.: W02275
Matrix (soil/water): SOIL Lab Sample ID: 17202-001
Level ;low/med): LOW Date Received: 03/10/98
Solids: 100.0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No. Analyte Concentration C Q M
7439-92-1 Lead 3.7 E P
7439-97-6 Mercury_ 0.02 U ^CV
Color Before: Clarity Before:
-
exture:
Color After: Clarity After: = -facts: -
Comments:
I_
-
SW-846
r. 2

U.S. EPA --LP
1 EPA SAMPLE NO
INORGANIC ANALYSES DATA SHEET
3ON683
Lab Name: QUANTERRA MO
Lab Code: ITMO Case No.:
Matrix (soil/water): SOIL
Level (low/med): LOW
% Solids: 100.0
Contract:
SAS No.:
550.2 6 0
SDG `:o.:
Lan Sample ID:
Date Received:
W02275
17202-002
03!10/98
Concentration Units (ug/L or mg/kg dry weight)
CAS No. Analyte ( Concentration C
7439-92-1 Le —a—(l Le 7.6
7439-97-6 Mercury_ 0.10
Color Before: Clarity Before:
Color After: Clarity After:
Comments:
Q
'— I
M
CV
—
MG/KG
^'extnre
rt -acts.
SW-846
^33

U.S. EPA - CLP
1 EPA SAMPLE 70
INORGANIC ANALYSES DATA SHEET
30N634
Lab Name: QUANTERRA MO Contract: 550.260
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275
Matrix (soil/water): SOIL Lab Sample 1D: !7202-20
Level !low/med): LOW Date Received: 03/10;98
Solids: 100.0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No. Analyte Concentration . 0 Q M
I
7439-92-1 Lem—3.3 E P
7439-97-6 Mercury_ 0.02 U A
Color Before: Clarity Before: 7extsre:
Color After: Clarity After: Artifacts:
Comments:
-34
SW-&4F

U.S. EPA _LP
i EPA SAMPLE NO.
INORGANIC ANALYSES DATA SHEET
BONG85
Lab Name:QUANTERRA MO Contract: 550.250
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275
Matrix (soil/water): SOIL
Lan Sample ID: 17200-001
Level (low/med): LOW Date Received: 03/11/98
°a Solids: 100.0
Color Before:
Color After:
Ccmments:
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7439-92-1
7439-97-6
Analyte Concentration
Lead 3.2
Mercury_ 0.02
Clarity Before:
Clarity After:
C Q M
E P
U ACV
—
–i —
i
– —
I
Texture:
art «acts
" ^.i -J5
SW-646

U.S. EPA - CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSES DATA SHEET
BON685
Lab Name: QUANTERRA MO Contract: 550.260
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275
Matrix !soil/waterj: SOIL Lan Sample ID: 17200-002
Level (low/med): LOW Date Received: 03/11/99
Solids: 100.0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No. Analyte Concentration C Q M
7439-92-1 Lear 11.8 _E_ P
7439-97-6 Mercury—0.13 Cv
Color Before: Clarity Before: Texzure:
Color After: Clarity After: Art __`acc3:
Comments:
I
SW-846
136

U.S. EPA CLP
1 EPA SAMPLE NO
INORGANIC ANALYSES DATA SHEET
BON687
Lab Name: QUANTERRA MO Contract: 550.260
Lab erode: ITMO Case No.: SAS No.: S D G No.: W02275
Matrix (soil/water): SOIL — Lab Samp le ID: 17200-00:'
Level (low/med): LOW Date Received: 03/11/98
Solids: 100.0
Color Sefore:
Colcr After:
Comments:
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7439-92-1
7439-97-6
Analyte
Lea^—
Mercury_
Concentration C Q
Clarity Before:
Clarity After:
3.7 - E -
0.02 U
–I
M
P
CV
I — I
I
i
ext. _:
Artifacts:
" 13 '7
SW-946

U.S. EPA - CLP
1 EPA SAMPLE NO.
INORGANIC ANALYSES DATA SHEET
BON688
Lab Name: QUANTERRA MO
Lab Code: iTMO Case No.:
Matrix (soil/water): SOIL
Level (low/med): LOW
Solids: 100.0
Contract: -^_ .260
SAS No.: SDG No.:
Lan Sample ID:
Cate Received:
W02275
17203-001
03/12/98
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7439-92-1
7439-97-6
Analyte
Leaa-
Mercury_
Concentraticn.0 Q
3.0^ E
0.02 U
Color Before: Clarity Before: Texture:
Color After: Clarity After: Artifacts:
Comments:
FORM I - IN
i
—I
M
P
CV
ff.
l) ^J i J
SW-846

Color Before:
Color After:
Comments:
CAS No.
7439-92-1
7439-97-6
J.S. EPA CLP
'
1
INORGANIC ANALYSES DATA SHEET
EPA SAMPLE NO.
BON6c9
i
Lab Name: QUANTERRA MO
Lab Code: ITMO Case No.:
Matrix (soil/waer): t SOIL
Level (low/med): LOW
Solids: 100.0
Contract: 550.260
SAS No.: SDG No.:
n Sample La ID:
Date Received:
W02275 _
17203-002
03/12/98
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Analyte Concentration Q
Lead -9.0 _ I _E
Mercury_ 0.04
Clarity Before:
Clarity After:
i
—
—I
M
P
CV
Texture:
Art--`acts:
SW-=46
139

U.S. EPA CLP
1 SPA SAMPLE '7j 0
INORGANIC ANALYSES DATA SHEET
BON690
Lab Name: QUANTERPA MO Contract: 550.250
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275
Matrix (soil/water): SOIL Lab Sample ID: 17221-007
Level (low/med): LOW Date Received: 03/13;'98
°s Solids: 100.0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No. Analyte Concentration , (- Q ^M
7439-92-1 Lem— 3.4 E P
7439-97-6 Mercury 0.02 U CV
I_
I
I I
— I
– i -
-I —
Color Before: Clarity Before: Texti:re:
Color After: Clarity After: Art_-acts:
:7 omments:
sw---;6

U. E. EPA - CT
1 EPP_ SAMPLE NO.
INORGANIC ^,NALYSES DATA -HEET
Lab Name: QUANTERRA MO
Lab Code: _TMO Case No.:
Matrix (soil/water): SOIL
Level (low/med): LOW
o Solids: 100.0
Contract:
SAS No.:
X20 260
SDG No.:
Lan Sample ID:
Date Rece_ved:
BON691
W02275
17221-,702
03/13/58
Color Before:
Color After:
Comments:
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7439-92-1
7439-97-6
i
Analyte I Concentration!CI Q M I
Lear—2 . 9 E P
Mercury_ 0.02 U CV
Clarity Before: exture
Clarit y After: Artifacts:
vO141
SW-c}6

CAS No. Analyte
7439-92-1 Lem
7439-97-6 (Mercury_
U.S. EPA - CLF
1 EPA SAMPLE NO
INORGANIC ANALYSES DATA SHEET
-N69_
Lab Name: QUANTERRA MO Contract: 000.260 _1
1
Lab Code: ITMO Case ^;o.: SAS No.: SDG No.: ::02275
Matrix (soil/water): SOIL _L__aE Sample ID: 17224-00
Level (low/med): LOW Date Received: 03/16/98
% Solids: 100.0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Concentration C
'3 c
0.02 U
_i
–
Q M
Color Betcre: Clarity Before: Text r
Color Af*_er. Clarity After: Art S: —
Comments:
E
i
P CVI
SW- Hfir,

Color Before:
Color After:
Comments:
U.S. EPA CLP
1 -xPA ',AM P LE 0.
INORGANIC ANALYSES DAT I SHEET
SONG 741
Lab Name: QUANTERRA MO Contract: 550.260
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275
Matrix soil/water): SOIL Lab Sampie ID: 17224-003
Level ;low/med): LOW Date Received: 03!16/98
% Solids: 100.0
Concentration Units (ug/L or mg/kg dry weight): MG//KG
CAS No. Analyte
7439-92-1 LeacT-
7439-97-6 Mercury_
Concentration C Q M
_ I
3.6 E P
0.02 U jCV
Clarity Before:
Clarit y After:
I_
i
i
"excure:
Art '_facts:
J i i
SW-^4F

Bechtel Hanford, Inc.
3350 George Washington Way
Richland, WA 99352
April 21, 1998
Attention: Joan Kessner
SAF Number
Date First Sample Received
Date SDG Closed
Number of Samples
Sample Type
SDG Number
Data Deliverable
CERTIFICATE OF ANALYSIS
B98-061
March 9, 1998
March 16, 1998
15
Other-Cement
W02275
21 Day Summary
°ivanterra
Emironmrnra7
sen'u es
lc^ In ti
I. Introduction
Between March 9, and March 16, 1998, 15 21-day TAT other-cement samples were received
by the Quanterra Environmental Se rvices Richland Laboratory (QESRL) for radiochemical and
chemical analysis. Upon receipt, the samples were assigned the following laborato r y ID
numbers to correspond with the Bechtel Hanford, Inc. (BHI) specific IDs:
QESRL ID Ji BHI iD# YIATRI% DATE OF RECEIPT
80316101 BON680 Soil 3/9/98
80316102 BON681 Soil 3/9/98
80318401 BON682 Soil 3/10/98
80318402 BON683 Soil 3/10'98
80318403 BON684 Soil 3/10/98
80320601 BON685 Soil 3111198
803 2 0602 BON686 Soil 3i 11.'98
80320603 BON687 Soil 3x 11 "98
80322201 BON688 Soil 3/12x98
80312 1_02 BON689 Soil 3.12.'98
80324401 BON690 Soil 3J13^98
80324402 BON691 Soil 3; 1?x98
80327201 BON692 Soil 3.16,98
80327202 BON693 Soil 3, 16,98
80327203 BON694 Soil 3116,98
r1
G0I)..

Bechtel Hanford, Inc.
April 21, 1998
Page 2
II. Analytical Results/Methodology
iivanterra
EnOronmenral
Souk ,
The analytical results for this report are presented by laboratory sample ID. Each set of data
includes sample identification information, analytical results and the appropriate associated
statistical errors.
The requested analyses were: Alpha Spectroscopy
Americium-241 by method RICH-RC-5062
Plutonium-238, -239/40 by method RICH-RC-5062
Uranium-234, -235, -238 b_y method RICH-RC-5062
Gamma Spectroscopy
Gamma Scan by method RICH-RC-5017
Gas Proportional Counting
Total Strontium b y method RICH-RC-5006
Liquid Scintillation Counting
Carbon-14 by method RICH-RC-5022
Nickel-63 by method RICH-RC-5069
Selenium-79 by method RD-3253
Technetium-99 by method RICH-RC-5029
Chemical Analyses
Chromium Hex by EPA method RICH-RC-5005
III. Quality Control
The analytical results for each analysis performed under SDG WO-2 -2 75 include a minimum of
two Laboratory Control Samples (LCS) and one method (reagent) blank. Any exceptions have
been noted in the "Comments" section_
Quality control sample results are reported in the same units as sample results.
(JO U.;

Bechtel Hanford, Inc.
April 21, 1998
Page 3
IV. Comments
Alpha Spectroscopy
Q,P'uanterra
Environmental
Services
Americium-241 by method RICH-RC-5062
The LCS, batch blank, sample duplicate (BON680 and BON687) and sample results are within
contractual requirements.
Plutonium-238 -239/40 by method RICH-RC-5062
The LCS, batch blank, sample duplicate (BON680 and BON687) and sample results are within
contractual requirements.
Uranium 234, -235 -238 by method RICH-RC-5062
The LCS, batch blank, sample duplicate (BON680) and sample results are within contractual
requirements. The RPD values for sample duplicate BON693 were slightly greater than the first
level of evaluation criteria but the values met the second level evaluation criteria. Rich Weiss
gave approval to report the data on 4/6/98.
Gamma Spectroscopy
Gamma Scan by method RICH-RC-5017
The LCS, batch blank. sample duplicate (BON680 and BON685) and sample results are within
contractual requirements_
Gas Proportional Counting
Total Strontium by method RICH-RC-5006
The LCS, batch blank, sample duplicate (BON680 and BON690) and sample results are within
contractual requirements.
Liquid Scintillation Counting
Carbon-14 by method RICH-RC-5022
The LCS, batch blank, sample duplicate (BON680 and BON684) and sample results are within
contractual requirements.
Nickel-63 by method RICH-RC-5069
The LCS. batch blank, sample duplicate (BON680 and BON688) and sample results are within
contractual requirements.
G0Oit

Bechtel Hanford, Inc.
April 1-1, 1998
Page 4
^%%uanterra
F.mironm

O
FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/9/1998 10:30:00 AM
LAB SAMPLE ID: 80316101 REPORT NBR: 4835 RECEIVED DATE: 3/9/1998 1:42:00 PM
CLIENT ID: BON680 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
COUNTING
ERROR(2s)
TOTAL ERROR
(2s) MDA
REPORT
UNIT YIELD RST/MDA RST/CNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALQ
UNIT
DETECTOR
ID
METHOD
NUMBER
TC-99 -5.03E+02 1.5E+03 4.8E+03 3.63E+03 pCi/sam 95.10% -0.14 -0.33 4/2/98 0.000414 SA LSC RICHRC5078
AM-241 6.72E+03 1.2E+03 1.7E+03 1.57E+02 pCi/sam 74-90% (429) (5.4) 4/3/98 0.000368 SA ALPHA-SPEC RICHRC5057
HEXCHROME 4.00E-03 00E+00 0.0E+00 200E-03 mg/L N/A (2.) N/A 3/10/98 100.0 ML SPECPHOTO EPA7196
U-234 8.61E+01 1.0E+02 1.0E+02 1.19E+02 pCi/sam 80.30% 0.73 0.84 4/3/98 0000376 SA ALPHA-SPEC RICHRC5030
U-235 0.00E+00 0.0E+00 8.8E+01 7.98E+01 pCdsam 80.30% 0 N/A 4/3/98 0.000376 SA ALPHA-SPEC RICHRC5030
U-238 8.37E+01 1.0E+02 1.0E+02 1.35E+02 pCi/sam 80.30% 0.62 0.82 4/3/98 0.000376 SA ALPHA-SPEC RICHRC5030
PU-238 5.26E+02 2.4E+02 2.SE+02 7.49E+01 pCi/sam 62.20% (7) (2.2) 3/31/98 0000368 SA ALPHA-SPEC RICHRC5010
PU239/40 1.82E+04 1.4E+03 2.8E+03 1.26E+02 pCi/sam 62.20% (143.6) (12.8) 3131/98 0.000368 SA ALPHA-SPEC RICHRCS010
AM-241 6.78E+03 1.0E+03 1.2E+03 N/A pCi/sam N/A N/A (6.6) 3/26/98 0.2355 SA GAMMA RICHRC5017
CO-60 4.21E+04 7.SE+02 4.3E+03 N/A pCi/sam N/A N/A (56.3) 3/26/98 0.2355 SA GAMMA RICHRC5017
CS-137DA 1.49E+06 4.9E+03 1.5E+05 N/A pCi/sam N/A N/A (305.4) 3/26/98 0.2355 SA GAMMA RICHRC5017
EU-152 4.14E+04 2.0E+03 4.6E+03 N/A pCi/sam N/A N/A (21.) 3/26/98 0.2355 SA GAMMA RICHRC5017
EU-154 5.81E+03 8.0E+02 9.9E+02 N/A pCi/sam N/A N/A (7.2) 3/26/98 0.2355 SA GAMMA RICHRC5017
EU-155 -1.37E+02 6.9E+02 6.9E+02 1.06E+03 pCi/sam N/A -0.13 -0.2 3/26/98 0.2355 SA GAMMA RICHRC5017
STRONTIUM 4.67E+05 1.0E+04 1.7E+05 1.79E+03 pCi/sam 97.00% (260.4) (46.8) 4/1/98 0000367 SA AS RICHRC5006
C-14 1.90E+02 1.0E+03 1.6E+03 2.40E+03 pCi/sam 100.00% 0.08 0.19 4/9/98 0.00064 SA LSC RICHRC5022
NI-63 4.16E+06 2.1E+04 5.0E+05 4.48E+03 pCi/sam 76.70% (928.9) (1969) . 4/3/98 0.000367 SA LSC RICHRC5069
O SE-79 2.01E+03 2.0E+03 7.3E+03 4.60E+03 pCi/sam 71.50% 0.44 (1.) 4/1/98 0.000372 SA LSC RICHRC5043
C.
Number of Results: '18
Comments:

FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/9/1998 1.45:00 PM
LAB SAMPLE ID: 80316102 REPORT NBR: 4835 RECEIVED DATE: 3/9/1998 1:42:00 PM
CLIENT ID: BON681 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
COUNTING
ERROR(2s)
TOTAL ERROR
(2 s) MDA
REPORT
UNIT YIELD RST/MDA RSTICNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALQ
UNIT
DETECTOR
ID
METHOD
NUMBER
TC-99 352E+00 1.4E+01 42E+01 323E+01 pCi/sam 95.10% -0.11 -0.26 3/31/98 0.0458 SA LSC RtCHRCS078
AM-241 319E+00 2-3E+00 2.3E+00 1.08E+00 pCi/sam 87.10% (3) (14) 4/4/98 0.046 SA ALPHA-SPEC RICHRC5057
HEXCHROME 2.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3/10/98 100.0 ML SPECPHOTO EPA7196
U-234 159E+02 2.5E+01 5.4E+01 4.10E+00 pCi/sam 19.80% (38.8) (6.2) 4/5/98 0.044 SA ALPHA-SPEC RICHRC5030
U-235 8.15E+00 5.8E+00 6.3E+00 2.76E+00 pCi/sam 19.80% (3.) (1.4) 4/5/98 0.044 SA ALPHA-SPEC RICHRCS030
U-238 1.83E+02 2.7E+01 6.2E+01 4.66E+00 pCi/sam 19.80% (39.4) (6.7) 4/5/98 0.044 SA ALPHA-SPEC RICHRC5030
PU-238 0.00E+00 00E+00 5.2E-01 4.65E-01 pCi/sam 77.40% 0. N/A 4/3/98 0.046 SA ALPHA-SPEC RICHRC5010
PU239/40 3.92E+00 1.6E+00 1.7E+00 7.84E-01 pCi/sam 77.40% (5.) (2.4) 4/3/98 0.046 SA ALPHA-SPEC RICHRC5010
CO-60 4.22E+01 2.7E+01 2.8E+01 5.77E+01 pCi/sam N/A 0.73 (1.5) 3/27/98 0.0541 SA GAMMA RICHRCS017
CS-137DA 4.95E+02 7.2E+01 8.7E+01 N/A pCi/sam N/A N/A (6.9) 3/27/98 0.0541 SA GAMMA RICHRCS017
EU-152 1.87E+01 89E+01 8.9E+01 148E+02 pCi/sam N/A 0.13 0.21 3/27/98 0.0541 SA GAMMA RICHRC5017
EU-154 1.14E+02 9.0E+01 91E+01 1.75E+02 pCi/sam N/A 0.65 (13) 3/27/98 0.0541 SA GAMMA RICHRCS017
EU-155 -3.69E+01 65E+01 6.5E+01 101E+02 pCi/sam N/A -0.37 -0.57 3/27/98 0.0541 SA GAMMA RICHRCS017
STRONTIUM 6.20E+02 3.2E+01 2.2E+02 1.34E+01 pCi/sam 9880% (46.3) (19.5) 4/2198 0.0476 SA AB RICHRC5006
C-14 8.68E+00 1 4E+01 2.2E+01 3.30E+01 pCi/sam 10000% 0.26 061 4/2/98 0.0467 SA LSC RICHRC5022
NI-63 4.47E+02 2.1E+01 8.1E+01 2.74E+01 pCi/sam 9930% (16.3) (21.6) 4/5/98 0.0458 SA LSC RICHRC5069
SE-79 -5.63E+00 1.5E+01 5.6E+01 3.72E+01 pCi/sam 70.40% -0.15 -0.36 4/13/98 00464 SA LSC RICHRC5043
C
[Number of Results: 17
C^
Comments:

FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/10/1998 8:35:00 AM
LAB SAMPLE ID: 80318401 REPORT NBR: 4835 RECEIVED DATE: 3/10/1998 1:05:00 PM
CLIENT ID: BON682 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
TC-99 -2.99E+01
AM-241 4.68E+00
HEXCHROME 2.00E-03
U-234 2.85E+01
U-235 4.09E-01
U-238 3.68E+01
PU-238 0.00E+00
PU239/40 2.37E+00
CO-60 -2.12E+01
CS-137DA 3.28E+02
EU-152 -1.29E+01
EU-154 -4.98E+01
EU-155 1.26E+01
STRONTIUM 7.92E+01
C-14 3.73E+01
NI-63 2.42E+02
SE-79 -1.33E+01
dumber of Results: '17
G
Cl)
Comments:
COUNTING TOTAL ERROR
ERROR(2s) (2 s)
3.0E+01 9.3E+01
4.3E+00 4.3E+00
0.0E+00 0.0E+00
8.3E+00 9.9E+00
1.2E+00 1.2E+00
9.5E+00 1.2E+01
0 0E+00 1 2E+00
2.0E+00 2.0E+00
3.9E+01 3.9E+01
6.5E+01 7.3E+01
9 0E+01 9.0E+01
1.2E+02 1 2E+02
8.4E+01 8.4E+01
2.1E+01 3.6E+01
3 3E+01 5.1E+01
3.2E+01 1.0E+02
3.7E+01 1.3E+02
REPORT
MDA UNIT YIELD
6.98E+01 pCi/sam 95.10%
3.83E+00 pCi/sam 81.70%
2.00E-03 mg/L N/A
4.01 E+00 pCi/sam 56.60%
3.21E+00 pCi/sam 56.60%
4.14E+00 pCi/sam 56.60%
1.10E+00 pCi/sam 74.40%
1.85E+00 pCi/sam 74.40%
6.47E+01 pCi/sam N/A
N/A pCi/sam N/A
1 .51E+02 pCi/sam N/A
1.96E+02 pCi/sam N/A
1.39E+02 pCi/sam N/A
3.35E+01 pCi/sam 94.50%
7.60E+01 pCi/sam 100.00%
6.16E+01 pCi/sam 95.20%
8.78E+01 pCi/sam 75.40%
RSTIMDA RST/CNTERR
-043 -(1-)
(1.2) (1 1)
1 N/A
(7.1) (3.4)
0.13 0.34
(8.9) (3.9)
0 N/A
(1-3)
(1.2)
-033 -0.54
N/A (5.)
-009 -014
-025 -0.42
009 0.15
(2A) (38)
049 (L1)
(39) (Z5)
-0.15 -0.37
ANALYSIS ALIQUOT ALQ DETECTOR METHOD
DATE SIZE UNIT ID NUMBER
3/31/98 0.0206 SA LSC RICHRC5078
4/4/98 0.021 SA ALPHA-SPEC RICHRCS057
3/11/98 1000 ML SPECPHOTO EPA7196
4/4/98 0.0243 SA ALPHA-SPEC RICHRC5030
4/4/98 0.0243 SA ALPHA-SPEC RICHRCS030
4/4/98 0.0243 SA ALPHA-SPEC RICHRC5030
4/3/98 0021 SA ALPHA-SPEC RICH RC5010
4/3/98 0.021 SA ALPHA-SPEC RICHRC5010
3/27/98 0.0537 SA GAMMA RICHRC5017
3/27/98 0.0537 SA GAMMA RICHRC5017
3/27/98 0.0537 SA GAMMA RICHRC5017
3/27/98 0.0537 SA GAMMA RICHRC5017
3/27/98 0.0537 SA GAMMA RICHRC5017
4/2/98 0.0208 SA AB RICHRC5006
4/2198 0.0204 SA LSC RICHRC5022
4/5/98 0.0212 SA LSC RICHRC5069
4/13/98 0.0183 SA LSC RICHRC5043

ISOTOPE
TC-99
AM 241
U-234
U-235
U-238
PU-238
PU239/40
AM-241
CO-60
CS-137DA
EU-152
EU-154
EU-155
STRONTIUM
C-14
NI-63
SE-79
Qlumber of Results
G
Comments
RESULT
-1.14E+03
2 94E+03
9 18E+01
0 00E+00
4 30E+01
8 36E+01
5.23E+03
2 84E+03
8.29E+03
1 28E+06
1 57E+04
2 42E+03
4 15E+02
6 71 E+05
7 01 E+02
4.05E+05
1.16E+03
117
FORM Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/10/1998 9:45:00 AM
LAB SAMPLE ID: 80318402 REPORT NBR: 4835 RECEIVED DATE: 3/10/1998 1:05:00 PM
CLIENT ID: BON683 ORDER NBR: B98-061 MATRIX OTHER
COUNTING TOTAL ERROR
ERROR(2s) (2s)
1.8E+03 5.8E+03
7.3E+02 8.5E+02
9.8E+01 9.9E+01
0.0E+00 7.3E+01
6.9E+01 7.0E+01
9.7E+01 9.7E+01
7 6E+02 1.0E+03
5.4E+02 6.1 E+02
3.7E+02 9.1 E+02
2.3E+03 1.3E+05
2.1E+03 2.6E+03
4.6E+02 5.2E+02
7.1 E+02 7.1 E+02
1.2E+04 2.5E+05
1 1E+03 1 7E+03
6.7E+03 5.2E+04
1.9E+03 6.9E+03
REPORT
MDA UNIT YIELD
4.39E+03 pCi/sam 95.10%
1.23E+02 pCi/sam 98.10%
1 22E+02 pCi/sam 92.90%
6.61 E+01 pCi/sam 92.90%
1.22E+02 pCi/sam 92.90%
7 54E+01 pCi/sam 61.80%
1.27E+02 pCi/sam 61.80%
N/A pCi/sam N/A
N/A pCi/sam N/A
N/A pCi/sam N/A
N/A pCi/sam N/A
9.24E+02 pCi/sam N/A
1.18E+03 pCi/sam N/A
2.12E+03 pCi/sam 97.20%
2 49E+03 pCi/sam 10000%
4.29E+03 pCi/sam 8200%
4.35E+03 pCi/sam 78.60%
RST/MDA RST/CNTERR
-0.26 -0.62
(24-) (4)
075 094
0. N/A
0.35 0.62
(1.1) 087
(41.1) (6.8)
N/A (5.2)
N/A (22.4)
N/A (564.8)
N/A (7S)
(2.6) (5.3)
0.35 0.58
(3159) (54.2)
0.28 065
(94.6) (60.7)
0.27 0.62
ANALYSIS
DATE
4/2/98
4/3/98
4/3/98
4/3/98
4/3/98
3/31/98
3/31/98
3/26/98
3/26/98
3/26/98
3/26/98
3/26/98
3/26/98
4/1/98
4/9/98
4/3/98
4/1/98
ALIQUOT ALQ
SIZE UNIT
0.000342 SA
0.000355 SA
0.00037 SA
0.00037 SA
0.00037 SA
0.000355 SA
0.000355 SA
0.229 SA
0.229 SA
0.229 SA
0.229 SA
0.229 SA
0 229 SA
0.000349 SA
0.000617 SA
0.000359 SA
0.000357 SA
DETECTOR
ID
LSC
ALPHA-SPEC
ALPHA-SPEC
ALPHA-SPEC
ALPHA-SPEC
ALPHA-SPEC
ALPHA-SPEC
GAMMA
GAMMA
GAMMA
GAMMA
GAMMA
GAMMA
AB
LSC
LSC
LSC
METHOD
NUMBER
RICHRCS078
RICHRC5057
RICHRC5030
RICHRC5030
RICHRC5030
R ICHRCS010
RICHRC5010
RICHRC5017
RICHRC5017
RICHRC5017
RICHRC5017
RICHRC5017
RICHRC5017
RICHRC5006
RICHRC5022
RICHRC5069
RICHRC5043

FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/10/1998 1:20:00 PM
LAB SAMPLE ID: 80318403 REPORT NBR: 4835 RECEIVED DATE: 3/10/1998 1:05:00 PM
CLIENT ID: BON684 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
COUNTING
ERROR (2 s)
TOTAL ERROR
(2 s) MDA
REPORT
UNIT YIELD RSTIMDA RST/CNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALQ
UNIT
DETECTOR
ID
METHOD
NUMBER
TC-99 -1.93E+01 2.9E+01 90E+01 6.91E+01 pCi/sam 95.10% -0.28 -0.67 3/31/98 0.0214 SA LSC RICHRC5078
AM-241 301E+00 31E+00 3.1E+00 3.09E+00 pCi/sam 92.60% 0.97 098 4/4/98 0.0219 SA ALPHA-SPEC RICHRC5057
HEXCHROME 2.00E-03 00E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3/11/98 100.0 ML SPECPHOTO EPA7196
U-234 4.07E+01 98E+00 1 2E+01 2.37E+00 pCi/sam 63.30% (17.1) (4.1) 4/4/98 0.0226 SA ALPHA-SPEC RICHRC5030
U-235 3.45E+00 2.9E+00 3.0E+00 2.70E+00 pCi/sam 63.30% (1.3) (1.2) 4/4/98 0.0226 SA ALPHA-SPEC RICHRCS030
U-238 3.57E+01 9.2E+00 1.1E+01 3.50E+00 pCi/sam 63 30% (10.2) (3.9) 4/4/98 0.0226 SA ALPHA-SPEC RICHRCS030
PU-238 0.00E+00 0.0E+00 1.1E+00 9.66E-01 pCi/sam 76.10% 0. N/A 4/3/98 0.0219 SA ALPHA-SPEC RICHRC5010
PU239/40 1.28E+01 4.3E+00 4.6E+00 1.44E+00 pCi/sam 76 1 0% (8.9) (3.) 4/3/98 0.0219 SA ALPHA-SPEC RICHRC5010
CO-60 -1.94E+01 4.5E+01 4.5E+01 7.58E+01 pCi/sam N/A -0.26 -0.43 3/27/98 0.05 SA GAMMA RICHRC5017
CS-137DA 1.37E+03 1.2E+02 1.8E+02 N/A pCi/sam N/A N/A (11.6) 3/27/98 005 SA GAMMA RICHRC5017
EU-152 -3.76E+01 9.4E+01 9.4E+01 155E+02 pCi/sam N/A -0.24 -0.4 3/27/98 0.05 SA GAMMA RICHRC5017
EU-154 1.52E+01 11E+02 1.1E+02 197E+02 pCi/sam N/A 0.08 0.13 3/27/98 0.05 SA GAMMA RICHRC5017
EU-155 6.76E+01 80E+01 8.0E+01 1.31E+02 pCi/sam N/A 0.52 0.85 3/27/98 0.05 SA GAMMA RICHRC5017
STRONTIUM 1.30E+03 7.1E+01 4.3E+02 3.26E+01 pCi/sam 87.40% (40) (18.4) 4/2/98 0.0218 SA AB RICHRC5006
C-14 -2.42E+00 2.9E+01 4.6E+01 7.00E+01 pCi/sam 100.00% -0.03 -008 4/2/98 0.0223 SA LSC RICHRC5022
NI-63 2.47E+02 3.1E+01 9.8E+01 593E+01 pCi/sam 94.30% (4.2) (7.9) 415/98 0.0223 SA LSC RICHRCS069
SE-79 3.29E-01 3.1E+01 1.1E+02 7.38E+01 pCi/sam 73.70% 0. 0.01 4/13198 0.0223 SA LSC RICHRC5043
C-)
(_Number of Resu lts: 117
^t
C-e
Comments:

FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/11/1998 8:30:00 AM
LAB SAMPLE ID: 80320601 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11:57:00 AM
CLIENT ID: BON685 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
COUNTING
ERROR(2s)
TOTAL ERROR
(2 s) MDA
REPORT
UNIT YIELD RST/MDA RST/CNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALQ
UNIT
DETECTOR
ID
METHOD
NUMBER
TC-99 -801E+00 2.9E+01 9.1E+01 6.98E+01 pCi/sam 95.10% -0.11 -0.27 3/31/98 0.0213 SA LSC RICHRC5078
AM-241 3.65E+00 3.6E+00 3.7E+00 2.47E+00 pCi/sam 83.00% (1.5) 0 ) 4/4/98 00207 SA ALPHA-SPEC RICHRCS057
HEXCHROME 2.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3/12/98 100.0 ML SPECPHOTO EPA7196
U-234 3.50E+01 8.7E+00 1.1E+01 1.46E+00 pCi/sam 58.10% (24.) (4) 4/5/98 0.0257 SA ALPHA-SPEC RICHRC5030
U-235 4.27E+00 3.1E+00 3.1E+00 2.17E+00 pCi/sam 58.10% (2.) (1.4) 4/5/98 0.0257 SA ALPHA-SPEC RICHRCS030
U-238 5.12E+01 1.1E+01 1.4E+01 2.17E+00 pCi/sam 58.10% (23.6) (49) 4/5/98 0.0257 SA ALPHA-SPEC RICHRC5030
PU-238 3.65E-01 8.0E-01 8.0E-01 1.59E+00 pCi/sam 80.20% 0.23 0.46 413/98 0.0207 SA ALPHA-SPEC RICHRC5010
PU239/40 4.36E+00 2.6E+00 2.7E+00 1.07E+00 pCi/sam 80.20% (4.1) (1.7) 4/3/98 0.0207 SA ALPHA-SPEC RICHRCS010
CO-60 5.67E+01 3.4E+01 3.4E+01 6.81E+01 pCi/sam N/A 0.83 (1.7) 3/27/98 0.0504 SA GAMMA RICHRC5017
CS-137DA 2.82E+02 66E+01 7.2E+01 NIA PCs/Sam N/A N/A (43) 3127/98 00504 SA GAMMA RICHRC5017
EU-152 6.01E+00 87E+01 87E+01 1.46E+02 pCi/sam N/A 0.04 0.07 3/27/98 0.0504 SA GAMMA RICHRC5017
EU-154 689E+01 1.0E+02 1.0E+02 1.98E+02 pCi/sam N/A 0.35 0.66 3/27/98 00504 SA GAMMA RICHRC5017
EU-155 3.04E+01 7.6E+01 7.6E+01 1.20E+02 pCi/sam N/A 0.25 0.4 3/27/98 0.0504 SA GAMMA RICHRC5017
K-40 1.49E+03 12E+03 1.2E+03 NIA pCi/sam N/A N/A (1.2) 3/27/98 0.0504 SA GAMMA RICHRC5017
STRONTIUM 4.78E+01 1.7E+01 2.3E+01 2.99E+01 pCi/sam 88.20% (1.6) (2.8) 4/2/98 0.0211 SA AB RICHRCS006
C
C-14 2.95E+01 3.3E+01 5.1E+01 7.60E+01 pCi/sam 100.00% 0.39 0.89 412198 0.0203 SA LSC RICHRC5022
O NI-63 -303E-01 29E+01 89E+01 7.01E+01 pCi/sam 85.70% 0 -0.01 415/98 0.0208 SA LSC RICHRC5069
F-^
5E-79 -117E01 3.3E*01 1.2E+02 7.94E+ 01 pCi/sam 73.50% -0.15 -0.35 4/13/98 0.0207 SA LSC RICHRC5043
Number of Results: 18
Comments:

ISOTOPE RESULT
TC-99 1 13E+02
AM-241 3 74E+03
U-234 7 12E+01
U-235 5 94E+00
U-238 2 27E+01
PU-238 4 97E+02
PU239/40 1 34E+04
AM-241 3 72E+03
CO-60 8.22E+03
CS-137DA 1.36E+06
EU-152 9 35E+03
E U-154 1 85E+03
E U-155 -1 56E+01
STRONTIUM 4 33E+05
C-14 6.59E+02
NI-63 2.76E+05
c1
^ SE-79 7.68E+02
~lumber of Results: '17
Comments:
COUNTING TOTAL ERROR
ERROR(2s) (2 s)
10E+03 3.2E+03
5.3E+02 7.7E+02
6.6E+01 6.8E+01
2.8E+01 2.8E+01
3 8E+01 3.9E+01
1.6E+02 1.7E+02
8.2E+02 1.9E+03
2.5E+03 2.5E+03
2.7E+02 8.6E+02
1.4E+05 1.4E+05
1 SE+03 1.7E+03
3.8E+02 4.2E+02
7.7E+02 7.7E+02
6.3E+03 1.6E+0S
5 9E+02 9.1 E+02
3.7E+03 3.5E+04
7.8E+02 2.9E+03
FORM Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/11/1998 10:00:00 AM
LAB SAMPLE ID: 80320602 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11:57:00 AM
CLIENT ID: BON686 ORDER NBR: B98-061 MATRIX: OTHER
MDA
REPORT
UNIT YIELD RST/MDA RST/CNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALQ
UNIT
DETECTOR
ID
2.40E+03 pCi/sam 95.10% 005 0.11 4/2/98 0.000626 SA LSC
5.14E+01 pCi/sam 105.50% (72.8) (7.) 4/3/98 0.000836 SA ALPHA-SPEC
898E+01 pCi/sam 73.10% 0.79 (1.1) 4/4/98 0.000839 SA ALPHA-SPEC
8.35E+01 pCi/sam 73.10% 007 0.22 4/4/98 0.000839 SA ALPHA-SPEC
7 20E+01 pCi/sam 73.10% 0.31 0.59 4/4/98 0.000839 SA ALPHA-SPEC
5.00E+01 pCi/sam 6330% (9.9) (3.2) 3/31/98 0.000836 SA ALPHA-SPEC
3.36E+01 pCi/sam 63.30% (398.7) (16.4) 3/31/98 0.000836 SA ALPHA-SPEC
N/A pCilsam N/A N/A (1.5) 3/26/98 0.4107 SA GAMMA
N/A pCi/sam N/A N/A (30.9) 3/26/98 0.4107 SA GAMMA
N/A pCi/sam N/A N/A (10.) 3/26/98 0.4107 SA GAMMA
N/A pCi/sam N/A N/A (6.4) 3/26/98 04107 SA GAMMA
N/A pCi/sam N/A N/A (4.9) 3/26/98 0.4107 SA GAMMA
1.25E+03 pCi/sam N/A -0.01 -0.02 3/26/98 0.4107 SA GAMMA
8.16E+02 pCi/sam 99.90% (530.) (68.5) 4/1/98 0-000837 SA AB
1.34E+03 pCi/sam 100.00% 0.49 (1 1) 4/9/98 0.001142 SA LSC
2.00E+03 pCi/sam 76.00% (138.3) (74.3) 4/3/98 0.000831 SA LSC
1.80E+03 pCi/sam 79.50% 043 0.99 4/1/98 0.00085 SA LSC
METHOD
NUMBER
RICHRC5078
RICHRC5057
RICHRC5030
RICHRCS030
RICHRC5030
RICHRCS010
RICHRC5010
RICHRC5017
RICHRCS017
RICHRCS017
RICHRC5017
RICHRC5017
RICHRC5017
RICHRCSW6
RICHRC5022
RICHRC5069
RICHRC5043

FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/11/1998 1:05:00 PM
LAB SAMPLE ID: 80320603 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11'.57.00 AM
CLIENT ID: BON687 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
COUNTING
ERROR(2s)
TOTAL ERROR
(2s) MDA
REPORT
UNIT YIELD RSTIMDA RST/CNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALO
UNIT
DETECTOR
ID
METHOD
NUMBER
TC-99 -9.47E+00 2.5E+01 7.9E+01 6.04E+01 pCi/sam 95.10% -0.16 -0.37 3/31/98 0.0245 SA LSC RICHRCS078
AM-241 3.43E+00 3.1E+00 3.1E+00 186E+00 pCi/sam 93.80% (1.8) (1.1) 4/4/98 0.0245 SA ALPHA-SPEC RICHRCS057
HEXCHROME 3.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A (1.5) N/A 3/12/98 1000 ML SPECPHOTO EPA7196
U-234 4.23E+01 1.1E+01 1.4E+01 282E+00 pCilsam 47.30% (16.1) (4.) 4/4/98 0.0272 SA ALPHA-SPEC RICHRCS030
U-235 6.00E-01 1.3E+00 1.3E+00 2.62E+00 pCi/sam 47.30% 0.23 0.46 4/4/98 00272 SA ALPHA-SPEC RICHRC5030
U-238 4.88E+01 1.1E+01 1.5E+01 2.98E+00 pCi/sam 47.30% (16.4) (4.3) 4/4/98 0.0272 SA ALPHA-SPEC RICHRC5030
PU-238 8.22E-01 1.3E+00 1.3E+00 2.04E+00 pCi/sam 58.70% 0.4 0.65 4/3198 0.0255 SA ALPHA-SPEC RICHRCS010
PU239/40 7.04E+00 3.6E+00 3.7E+00 2.23E+00 pCi/sam 58.70% (3.2) (2.) 4/3/98 0.0255 SA ALPHA-SPEC RICHRC5010
CO-60 6.12E+00 3.9E+01 3.9E+01 6.99E+01 pCilsam N/A 0.09 0.16 3/27/98 0.0517 SA GAMMA RICHRC5017
CS-137DA 1.48E+03 9.8E+01 1.8E+02 N/A pCilsam N/A N/A (151) 3/27/98 0.0517 SA GAMMA RICHRCS017
EU-152 403E+01 9.2E+01 9.2E+01 1.59E+02 pCi/sam N/A 0.25 0.44 3/27/98 0.0517 SA GAMMA RICHRC5017
EU-154 -4 46E+01 1.1E+02 1.1E+02 179E+02 pCi/sam N/A -0.25 -0.41 3/27/98 0.0517 SA GAMMA RICHRC5017
EU-155 -1.89E+01 7.4E+01 7.4E+01 1 15E+02 pCi/sam N/A -0.16 -0.26 3/27/98 0.0517 SA GAMMA RICHRC5017
K-40 1.91E+03 1.1E+03 1.1E+03 N/A pCi/sam N/A N/A (1.8) 3/27/98 0.0517 SA GAMMA RICHRC5017
STRONTIUM 6.79E+02 5.1E+01 2.5E+02 3.46E+01 pCi/sam 86.30% (19.6) (13.3) 4/2/98 0.0241 SA AB RICHRC5006
C-14 9.21E+01 3.0E+01 4.5E+01 6.40E+01 pCi/sam 100.00% (1.4) (3.1) 4098 00243 SA LSC RICHRC5022
NI-63 1.60E+02 2.6E+01 8.0E+01 5.20E+01 pCi/sam 93.70% (3.1) (6.1) 4/5/98 0.0255 SA LSC RICHRCS069
Fes+
SE-79 8.50E-01 2.7E+01 97E+01 6.33E+01 pCi/sam 74.30% 0.01 0.03 4/13/98 0.0257 SA LSC RICHRC5043
C.) Number of Results: 18
Comments:

FORM Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/12/1998 9:15:00 AM
LAB SAMPLE ID: 80322201 REPORT NBR: 4835 RECEIVED DATE: 3/12/1998 1:53:00 PM
CLIENT ID: BON688 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
TC-99 -3.92E+00
AM-241 1 42E+00
HEXCHROME 2.00E-03
U-234 3.81E+01
U-235 1.44E+00
U-238 4.34E+01
PU-238 -5.63E-02
PU239/40 1.06E+00
CO-60 5.23E+01
CS-137UA 6.18E+02
EU-152 1 68E+01
EU-154 -1.14E+01
EU-155 2.57E+01
K-40 5.80E+03
STRONTIUM 2.08E+02
C-14 2.28E+01
c-) NI-63 7.60E+01
C SE-79 -1.37E+00
h-^
"Number of Resu lts: 118
Comments:
COUNTING TOTAL ERROR
ERROR(2s) (2 s)
2.5E+01 7.7E+01
2.1E+00 2.1 E+00
0.0E+00 0.0E+00
9.4E+00 1.2E+01
2.0E+00 2.0E+00
1 0E+01 1.3E+01
8.0E-02 8.0E-02
1.2E+00 1.2E+00
3.6E+01 3.6E+01
8.0E+01 1.0E+02
86E+01 86E+01
1.1E+02 1.1E+02
7.5E+01 7.5E+01
7.6E+02 9.6E+02
3.1 E+01 7 5E+01
2.6E+01 4.1E+01
2.3E+01 7.1 E+01
2 6E+01 9.4E+01
REPORT
MDA UNIT YIELD
5.82E+01 pCi/sam 95.10%
2.97E+00 pCi/sam 86.60%
2.00E-03 mg/L N/A
3.39E+00 pCi/sam 5480%
3.39E+00 pCi/sam 54.80%
2.61E+00 pCi/sam 54.80%
1.61 E+00 pCi/sam 72.60%
9.52E-01 pCi/sam 72.60%
7.23E+01 pCi/sam N/A
N/A pCi/sam N/A
1.43E+02 pCi/sam N/A
1.87E+02 pCi/sam N/A
1.20E+02 pCi/sam N/A
172E+03 pCi/sam N/A
3.47E+01 pCi/sam 73.80%
6.00E+01 pCi/sam 100.00%
5.05E+01 pCUsam 95.10%
6.14E+01 pCi/sam 76.70%
RST/MDA RST/CNTERR
-007 -016
048 0.68
1- N/A
(11 2) (41)
0.42 0.72
(168) (4.3)
-0.04 -0.71
(i.t) 087
072 (1 5)
N/A (77)
0.12 02
-006 -01
0.21 034
(3.4) (7.6)
(6.) (6-8)
0.38 087
(1.5) (33)
-0.02 -005
ANALYSIS
DATE
3131/98
4/4/98
3/13/98
4/4/98
4/4/98
4/4/98
4/3/98
4/3/98
3/27/98
3/27/98
3/27/98
3/27/98
3/27/98
3/27/98
4/2/98
4/2/98
4/5/98
4/13/98
ALIQUOT ALQ
SIZE UNIT
00254 SA
00255 SA
100.0 ML
0.0264 SA
0.0264 SA
0.0264 SA
0.0255 SA
0.0255 SA
0.0507 SA
00507 SA
0.0507 SA
00507 SA
0.0507 SA
0.0507 SA
0.0254 SA
0.0257 SA
0.0259 SA
00257 SA
DETECTOR
ID
LSC
ALPHA-SPEC
SPECPHOTO
ALPHA-SPEC
ALPHA-SPEC
ALPHA-SPEC
ALPHA-SPEC
ALPHA-SPEC
GAMMA
GAMMA
eIDLllr_1
CeL1S11ra
GAMMA
GAMMA
AB
LSC
LSC
LSC
METHOD
NUMBER
RICHRCS078
RICHRCS057
EPA7196
RICHRCS030
RICHRCS030
RICHRC5030
RICHRCS010
RICHRCS010
RICHRCS017
RICHRCS017
RICHRC5017
RICHRC S017
RICHRC5017
RICHRCS017
RICHRC5006
RICHRC5022
RICHRC5069
RICHRCSO43

FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/12/1998 1:15:00 PM
LAB SAMPLE ID: 80322202 REPORT NBR: 4835 RECEIVED DATE: 3/12/1998 1:53:00 PM
CLIENT ID: BON689 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
COUNTING
ERROR(2s)
TOTAL ERROR
(2 s) MDA
REPORT
UNIT YIELD RST/MDA RSTICNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALQ
UNIT
DETECTOR
ID
METHOD
NUMBER
TC-99 2.45E+02 9.7E+02 3.0E+03 2.22E+03 pCi/sam 95.10% 0.11 0.25 4/2/98 0.000677 SA LSC RICHRC5078
AM-241 313E-03 6.6E+02 8.4E+02 140E+02 pCi/sam 86.50% (22.4) (4.7) 4/4/98 0.000655 SA ALPHA-SPEC RICHRCS057
U-234 266E+01 43E+01 4.3E+01 755E+01 pCdsam 8150% 035 0.62 4/4198 0.000662 SA ALPHA-SPEC RICHRC5030
U-235 0.00E+00 0.0E+00 4.5E+01 4.10E+01 pCi/sam 81.50% 0. N/A 4/4/98 0.000662 SA ALPHA-SPEC RICHRC5030
U-238 5.81 E+01 6.1 E+01 6.1 E+01 6.92E+01 pCi/sam 81,50% 0.84 0.96 4/4/98 0.000662 SA ALPHA-SPEC RICHRCS030
PU-238 214E+02 1.1E+02 1.2E+02 6.59E+01 pCi/sam 70.80% (3.2) (1.9) 3/31/98 0.000655 SA ALPHA-SPEC RICHRC5010
PU239/40 6.89E+03 6.3E+02 1.1E+03 7.19E+01 pCi/sam 70.80% (95.8) (10.9) 3/31/98 0.000655 SA ALPHA-SPEC RICHRC5010
AM-241 2.75E+03 4.7E+02 5.4E+02 N/A pCi/sam N/A N/A (5.9) 3/26198 0.42 SA GAMMA RICHRC5017
CO-60 3.83E+03 1.8E+02 4.2E+02 N/A pCi/sam N/A N/A (21.7) 3/26/98 0.42 SA GAMMA RICHRC5017
CS-137DA 6.16E+05 1.9E+03 6.2E+04 N/A pCi/sam N/A N/A (320.5) 3/26198 0.42 SA GAMMA RICHRC5017
EU-152 6.96E+03 8.6E-02 1.1E+03 WA pCi/sam N/A N/A (8.1) 3/26198 042 SA GAMMA RICHRC5017
EU-154 1 74E+03 2.0E+02 2.7E+02 4.53E+02 pCUsam N/A (3.8) (8.7) 3/26/98 0.42 SA GAMMA RICHRC5017
EU-155 1.34E+02 3.3E+02 3.3E+02 5.05E+02 pCi/sam N/A 0.27 0.41 3/26/98 0.42 SA GAMMA RICHRC5017
STRONTIUM 4.06E+05 70E+03 1.5E+05 1.02E+03 pCi/sam 94.20% (3991) (58.2) 4/1/98 0.000661 SA AB RICHRC5006
0-14 3.75E+01 6.0E+02 9.3E+02 1 42E+03 pCi/sam 100.00% 0.03 0.06 4/9/98 0.001081 SA LSC RICHRC5022
c:
NI-63 2.23E+05 3.7E+03 2.9E+04 2.42E+03 pCi/sam 77.30% (923) (60.) 413/98 0000675 SA LSC RICHRC5069
O
I,_
SE-79 -6.38E+02 10E+03 38E+03 244E+03 pCi/sam 76.00% -026 -0.63 4/1/98 0000657 SA LSC RICHRC5043
G Number of Results: 17
Cov ents:

TC-99
AM-241
HEXCHROME
U-234
U-235
U-238
PU-238
PU239/40
CO-60
CS-137DA
E U-152
EU-154
EU-155
-8 74E+00
3 67E+00
9 OOE-03
3 48E+01
6.02E-01
3.72E+01
3.57E-01
1.28E+01
3.99E+01
9.23E+02
1 09E+00
-1 13E+02
-1 46E+01
K-40 1.18E+03
STRONTIUM 6.13E+02
C 14 5.30E+01
C) NI-63 1.99E+02
O
1-+ SE-79 1.80E+01
CT)
Number of Results: 18
FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/13/1998 8:15:00 AM
LAB SAMPLE ID: 80324401 REPORT NBR: 4835 RECEIVED DATE: 3/13/1998 10:35:00 AM
CLIENT ID: BON690 ORDER NBR: B98-061 MATRIX: OTHER
COUNTING TOTAL ERROR REPORT ANALYSIS ALIQUOT ALQ DETECTOR METHOD
ISOTOPE RESULT ERROR(2s) (2 s) MDA UNIT YIELD RST/MDA RST/CNTERR DATE SIZE UNIT ID NUMBER
Comments:
2.7E+01 8.3E+01 635E+01 pCi/sam 95.10% -014 -0.33 3/31/98 0.0233 SA LSC RICHRC5078
3.3E+00 3.4E+00 300E+00 pCi/sam 89.30% (1.2) (11) 4/4/98 0.0234 SA ALPHA-SPEC RICHRC5057
0.0E+00 0.0E+00 2.00E-03 mg/L N/A (4.5) N/A 3/13/98 100.0 ML SPECPHOTO EPA7196
9.2E+00 1.1E+01 2.75E+00 pCosam 54.00% (12.7) (3.8) 4/4/98 0.0251 SA ALPHA-SPEC RICHRC5030
1.2E+00 1.2E+00 1.63E+00 pCi/sam 54.00% 0.37 0.5 4/4/98 0.0251 SA ALPHA-SPEC RICHRC5030
9.5E+00 1.2E+01 2.75E+00 pCi/sam 54.00% (13.5) (3.9) 4/4/98 0.0251 SA ALPHA-SPEC RICHRC5030
7.1E-01 7.2E-01 9.67E-01 pCi/sam 72.60% 0.37 0.5 4/198 0.0234 SA ALPHA-SPEC RICHRC5010
4.3E+00 4.6E+00 1.44E+00 pCi/sam 72.60% (8.9) (3.) 4/3/98 0.0234 SA ALPHA-SPEC RICHRC5010
4.2E+01 4.2E+01 7.63E+01 pCi/sam N/A 052 0.96 3127/98 0.0532 SA GAMMA RICHRC5017
9.0E+01 1.3E+02 N/A pCi/sam N/A N/A (10.3) 3/27/98 0.0532 SA GAMMA RICHRC5017
9.5E+01 9.5E+01 1.62E+02 pCi/sam N/A 0.01 001 3/27/98 0.0532 SA GAMMA RICHRC5017
11E+02 1.1E+02 167E+02 pCi/sam N/A -0.68 -(1.1) 3/27/98 0.0532 SA GAMMA RICHRC5017
8.7E+01 8.7E+01 1.42E+02 pCi/sam N/A -0.1 -0.17 3/27198 0.0532 SA GAMMA RICHRC5017
8.4E+02 8.5E+02 N/A pCi/sam N/A N/A (14) 3/27198 0.0532 SA GAMMA RICHRC5017
4.7E+01 2.3E+02 2.97E+01 pCi/sam 95.80% (20.6) (13.1) 4098 0.0234 SA AB RICHRC5006
3.0E+01 4.6E+01 670E+01 pCi/sam 100.00% 0.79 (1.8) 4/2/98 0.0233 SA LSC RICHRC5022
3.2E+01 9.8E+01 6.31E+01 pCi/sam 80.10% (3.2) (6.3) 46198 00246 SA LSC RICHRC5069
3.2E+01 1.2E+02 7.52E+01 pCi/sam 69.20% 0.24 0.57 4113/98 0.0234 SA LSC RICHRCSO43

FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/13/1998 9:00:00 AM
LAB SAMPLE ID: 80324402 REPORT NBR: 4835 RECEIVED DATE: 3/13/1998 10:35:00 AM
CLIENT ID: BON691 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
COUNTING
ERROR(2s)
TOTAL ERROR
(2 s) MDA
REPORT
UNIT YIELD RSTIMDA RST/CNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALQ
UNIT
DETECTOR
ID
METHOD
NUMBER
TC-99 282E+01 28E+01 86E+01 6.38E+01 pCi/sam 95.10% 0.44 0 ) 3131/98 00232 SA LSC RICHRCS078
AM-241 2.31E+00 2.7E+00 2.7E+00 2.08E+00 pCi/sam 86.20% (1.1) 0.87 4/4/98 0.0241 SA ALPHA-SPEC RICHRC5057
HEXCHROME 200E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3113/98 100.0 ML SPECPHOTO EPA7196
U-234 2.94E+01 7.9E+00 9.SE+00 2.12E+00 pCi/sam 65.10% (13.9) (3.7) 4/4/98 0.0249 SA ALPHA-SPEC RICHRC5030
U-235 1.01E+00 1.5E+00 1.5E+00 2.12E+00 pCi/sam 65.10% 0.48 068 4/4/98 0.0249 SA ALPHA-SPEC RICHRC5030
U-238 3.25E+01 8.3E+00 1.0E+01 2.81E+00 pCi/sam 65.10% (11.6) (3.9) 4/4/98 0.0249 SA ALPHA-SPEC RICHRC5030
PU-238 0.00E+00 0.0E+00 1.2E+00 1.10E+00 pCi/sam 64.10% 0, N/A 4/3/98 0.0241 SA ALPHA-SPEC RICHRC5010
PU239/40 6.11E+00 3.2E+00 3.3E+00 1.10E+00 pCi/sam 64.10% (5.5) (1_9) 4/3/98 0.0241 SA ALPHA-SPEC RICHRC5010
CO-60 -276E+01 3.9E+01 3.9E+01 6.25E+01 pCi/sam N/A -0.44 -0.71 3/27/98 0.0504 SA GAMMA RICHRCS017
CS-137DA 3.77E+02 8.5E+01 9.3E+01 N/A pCi/sam N/A N/A (4.4) 3/27198 0.0504 SA GAMMA RICHRC5017
EU-152 1.70E+01 8.6E+01 8.6E+01 1.45E+02 pCi/sam N/A 0.12 0.2 3/27/98 0.0504 SA GAMMA RICHRC5017
EU-154 344E+01 94E+01 9.4E+01 1 70E+02 pCi/sam N/A 0.2 0.37 3/27/98 00504 SA GAMMA RICHRCS017
EU-155 2.20E-01 7.6E+01 7.6E+01 1.20E+02 pCi/sam N/A 0 0. 3/27/98 0.0504 SA GAMMA RICHRC5017
STRONTIUM 1.36E+02 2.3E+01 5.1E+01 2.85E+01 pCi/sam 91.90% (4.8) (5.9) 4098 0.0241 SA AB RICHRC5006
C-14 509E+01 30E+01 46E+01 670E+01 pCi/sam 100.00% 0.76 (L7) 412/98 00232 SA LSC RICHRC5022
NI-63 8.95E+01 2.4E+01 7.3E+01 5.16E+01 pCilsam 102.30% (1.7) (3.7) 4/5198 0.0241 SA LSC RICHRCS069
SE-79 -1.32E+01 3.3E+01 1.2E+02 7.98E+01 pCi/sam 68.00% -0.17 -0.4 4113/98 0.0223 SA LSC RICHRCSO43
Qlumber of Results: 17
O
Comments:

C
H
FORM I Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: OUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/16/1998 8:30:00 AM
LAB SAMPLE ID: 80327201 REPORT NBR: 4835 RECEIVED DATE: 3/16/1998 12:15:00 PM
CLIENT ID: BON692 ORDER NBR: B98-061 MATRIX: OTHER
ISOTOPE RESULT
COUNTING
ERROR (2 s)
TOTAL ERROR
(2 s) MDA
REPORT
UNIT YIELD RST/MDA RST/CNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALO
UNIT
DETECTOR
ID
METHOD
NUMBER
TC-99 -1.27E+03 92E+02 29E+03 224E+03 pCi/sam 95.10% -0.56 -(1.4) 4/2/98 0.00067 SA LSC RICHRC5078
AM-241 7.76E+03 1.0E+03 1.7E+03 138E+02 pCi/sam 96.40% (56.4) (7.5) 4/4/98 0.000667 SA ALPHA-SPEC RICHRCS057
U-234 2.97E+01 4.4E+01 4.4E+01 6.23E+01 pCi/sam 83.00% 0.48 0.68 4/4/98 0.000664 SA ALPHA-SPEC RICHRCS030
U-235 -1.24E+00 2.5E+00 2.5E+00 6.23E+01 pCi/sam 8100% -0.02 -0.5 414/98 0.000664 SA ALPHA-SPEC RICHRCS030
U-238 2.60E+01 4.4E+01 4.4E+01 8.27E+01 pCi/sam 83.00% 0.31 0.59 4/4/98 0.000664 SA ALPHA-SPEC RICHRC5030
PU-238 4.46E+02 2.0E+02 2.1E+02 9.00E+01 pCi/sam 54.10% (5) (2.2) 3/31/98 0.000667 SA ALPHA-SPEC RICHRC5010
PU239/40 1.53E+04 1.2E+03 2.5E+03 102E+02 pCi/sam 54.10% (150.2) (13.1) 3131198 0.000667 SA ALPHA-SPEC RICHRC5010
AM-241 7.27E+03 4.1E+02 8.4E+02 WA pCi/sam N/A N/A (17.7) 3/26/98 0.4048 SA GAMMA RICHRC5017
CO-60 6-13E+03 2.5E+02 6.6E*02 N pCi/sam N/A N/A (25.) 3/26/98 0.4048 SA GAMMA RICHRC5017
CS-137DA 766E+05 1.2E+03 77E+04 N/A pCi/sam N/A N/A (618.9) 3/26/98 0.4048 SA GAMMA RICHRC5017
EU-152 3.30E+04 1.4E+03 3.6E+03 NA pCi;sam N/A N/A (22.9) 3/26/98 0.4048 SA GAMMA RICHRC5017
EU-154 601E+03 5.5E+02 8.2E+02 N/A pCi/sam N/A N/A (10.9) 3/26/98 0.4048 SA GAMMA RICHRC5017
EU-155 3.25E+02 4.4E+02 4.4E+02 723E+02 pCi/sam N/A 0.45 0.74 3/26/98 0.4048 SA GAMMA RICHRC5017
STRONTIUM 4.56E+05 7.2E+03 1.7E+05 1.06E+03 pCi/sam 93.90% (430.5) (63.) 4/1/98 0.000683 SA AB RICHRC5006
C-14 467E+02 6.5E+02 1.0E+03 1.50E+03 pCi/sam 100.00% 0.31 0.72 4/9/98 0.001022 SA LSC RICHRC5022
NI-63 3.44E+05 4.4E+03 4.3E+04 227E+03 pCi/sam 81.30% (151.7) (78.) 4/3/98 0.000684 SA LSC RICHRC5069
SE-79 -2.43E+02 9.6E+02 3.5E+03 2.29E+03 pCi/sam 82.80% -0.11 -0.25 4/1/98 0.000646 SA LSC RICHRC5043
Number of Results: 17
Comments:

ISOTOPE
TC-99
AM-241
HEXCHROME
U-234
U-235
U-238
PU-238
PU239/40
CO-60
CS-137DA
EU-152
EU-154
EU-155
STRONTIUM
C-14
NI-63
SE 79
RESULT
5 17E+00
5 54E+00
1 40E-02
3 33E+01
3 54E-01
1 95E+01
0 00E+00
1 03E+01
2.65E+01
1 32E+03
1 62E+01
1 56E+02
4 84E+01
1 34E+03
1.22E+02
8 09E+00
1.97E+00
COUNTING TOTAL ERROR
ERROR(2s) ( 2 s)
2.6E+01 8.3E+01
3.9E+00 4.0E+00
0.0E+00 0.0E+00
7.9E+00 9.8E+00
9.4E-01 9.4E-01
6.0E+00 6.9E+00
0.0E+00 1.0E+00
3.7E+00 3.9E+00
3.7E+01 3.8E+01
1 .3E+02 1 9E+02
1.0E+02 1 0E+02
9.1 E+01 9.3E+01
7.1 E+01 7.1 E+01
6.9E+01 4.5E+02
3.2E+01 4.7E+01
2.6E+01 8.0E+01
3.1 E+01 1.1E+02
FORM Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/16/1998 9:25:00 AM
LAB SAMPLE ID: 80327202 REPORT NBR: 4835 RECEIVED DATE: 3116/1998 12:15.00 PM
CLIENT ID: BON693 ORDER NBR: B98-061 MATRIX: OTHER
Number of Results: 17
0
0
Comments:
MDA
REPORT
UNIT YIELD RSTIMDA RST/CNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALQ
UNIT
DETECTOR
ID
6.21E+01 pCi/sam 95.10% 0.08 0.2 3/31/98 0.0238 SA LSC
1.87E+00 pCi/sam 91.60% (3.) (1 4) 4/4/98 0.0247 SA ALPHA-SPEC
2.00E-03 mg/L N/A (7.) N/A 3/16/98 100.0 ML SPECPHOTO
2.63E+00 pCi/sam 6820% (12.7) (42) 4/4/98 0.0256 SA ALPHA-SPEC
2.32E+00 pCi/sam 68.20% 015 0.38 4/4/98 0.0256 SA ALPHA-SPEC
1.87E+00 pCi/sam 68.20% (10.4) (3.2) 4/4/98 0.0256 SA ALPHA-SPEC
9.04E-01 pCi/sam 77.40% 0. N/A 4/3/98 0.0247 SA ALPHA-SPEC
9.03E-01 pCi/sam 77.40% (11.5) (2.8) 4/3/98 0.0247 SA ALPHA-SPEC
7.00E+01 pCi/sam N/A 0.38 0.71 3/27/98 0.0512 SA GAMMA
NA pCi/sam N/A N/A (10.1) 3/27/98 00512 SA GAMMA
1.69E+02 pCi/sam NIA 0.1 0.16 3/27/98 0.0512 SA GAMMA
1.87E+02 pCi/sam N/A 0.84 (1.7) 3/27/98 0.0512 SA GAMMA
1.17E+02 pCi/sam N/A 0.41 0.68 3/27/98 0.0512 SA GAMMA
296E+01 pCi/sam 83.20% (45.3) (19.4) 4/2/98 0.0247 SA AB
6.50E+01 pCi/sam 100.00% (1.9) (3.8) 4/2198 0.0238 SA LSC
6.22E+01 pCi/sam 81.50% 0.13 0.31 4/5/98 0.0246 SA LSC
7.32E+01 pCi/sam 72.40% 0.03 006 4/13/98 0.0228 SA LSC
METHOD
NUMBER
RICHRC5078
RICHRCS057
EPA7196
RICHRC5030
RICHRC5030
RICHRC5030
RICHRC5010
RICHRC5010
RICHRCS017
RICHRCS017
RICHRC5017
RICHRCS017
RICHRC5017
RICHRC5006
RICHRC5022
RICHRC5069
RICHRCSO43

ISOTOPE RESULT
TC-99 1.04E+01
AM-241 3.42E+00
HEXCHROME 2.00E-03
U-234 4.54E+01
U-235 9.73E-01
U-238 4.12E+01
PU-238 0.00E+00
PU239/40 1.39E+00
CO-60 4.71E+00
CS-137DA 283E+02
EU-152 -4.07E+01
EU-154 1.48E+02
EU-155 3.95E+01
K-40 1.80E+03
STRONTIUM 1.41E+02
C-14 3.99E+01
NI-63 7.75E+01
C) SE-79 122E+01
O
)Yujnber of Results: 18
C.1
Comments:
FORM Date: 4/16/1998
SAMPLE RESULTS
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/16/1998 10:25:00 AM
LAB SAMPLE ID: 80327203 REPORT NBR: 4835 RECEIVED DATE: 3/16/1998 12:15:00 PM
CLIENT ID: BON694 ORDER NBR: B98-061 MATRIX: OTHER
COUNTING TOTAL ERROR
ERROR(2s) (2 s)
2.7E+01 8.4E+01
3 4E+00 3.5E+00
0.0E+00 0.0E+00
1.0E+01 1.3E+01
1.6E+00 1.7E+00
9.8E+00 1.2E+01
0.0E+00 1.4E+00
1.6E+00 1 6E+00
3.7E+01 3.7E+01
7.8E+01 8.3E+01
9 0E+01 9.0E+01
1.0E+02 1.0E+02
9.0E+01 90E+01
8.5E+02 8.7E+02
2.4E+01 5.2E+01
3.0E+01 4.6E+01
2.8E+01 8.6E+01
3.0E+01 1.1E+02
MDA
REPORT
UNIT YIELD RST/MDA RST/CNTERR
ANALYSIS
DATE
ALIQUOT
SIZE
ALQ
UNIT
DETECTOR
ID
6.27E+01 pCi/sam 95.10% 0.17 0.39 3/31/98 00236 SA LSC
231E+00 pCi/sam 8250% (15) (1 ) 4/4/98 0.0224 SA ALPHA-SPEC
2.00E-03 mg/L N/A 1. N/A 3/16/98 100.0 ML SPECPHOTO
3.58E+00 pCi/sam 63.20% (12.7) (4.4) 4/4/98 00226 SA ALPHA-SPEC
3.09E+00 pCi/sam 63.20% 0.31 0.59 4/4/98 00226 SA ALPHA-SPEC
398E+00 pCi/sam 63.20% (10.4) (4.2) 414/98 0.0226 SA ALPHA-SPEC
1.26E+00 pCi/sam 60.00% 0. N/A 4/3/98 0.0224 SA ALPHA-SPEC
1.26E+00 pCi/sam 60.00% (1.1) 0.87 4/3/98 0.0224 SA ALPHA-SPEC
6.49E+01 pCi/sam N/A 0.07 0.13 3/28/98 0.0524 SA GAMMA
N/A pCi/sam N/A N/A (3.6) 3/28/98 00524 SA GAMMA
1.49E+02 pCi/sam N/A -0.27 -0.45 3/28/98 0.0524 SA GAMMA
197E+02 pCi/sam N/A 0.75 (1.5) 3/28198 0.0524 SA GAMMA
1.53E+02 pCi/sam N/A 0.26 0.44 3/28/98 0.0524 SA GAMMA
N/A pCi/sam N/A N/A (2.1) 3/28198 0.0524 SA GAMMA
2.77E+01 pCi/sam 85.90% (51) (5.8) 4/2/98 0.0233 SA AB
6.80E+01 pCi/sam 100.00% 0.59 (1.3) 412/98 0.0228 SA LSC
6.22E+01 pCi/sam 89.90% (1.2) (2.7) 415/98 0.0222 SA LSC
6.97E+01 pCi/sam 75.40% 0.17 041 4/13/98 0.023 SA LSC
METHOD
NUMBER
RICHRC5078
RICHRC5057
EPA7196
RICHRC5030
RICHRCS030
RICHRC5030
RICHRC5010
RICHRC5010
RICHRC5017
RICHRCS017
RICHRC5017
RICHRC5017
RICHRC5017
RICHRC5017
RICHRC5006
RICHRC5022
RICHRC5069
RICHRC5043

Quanterra Data Review C3eddist
RADIOCHE.^IIISTRY
^xorle G4ver -atnoer r:r. ^3 I L 1 ^' 3 ^ ^ 4 ^ 3 aC^ ^i322 L ^5 a^
Ciem :D'
No Datc —
tau Saremie ^'umbcor SI7G: l.^ 22 7
Method7m ?ammeters: YYl - 7• ti \
_
0
Nam= C)'.a, r D e C en.. z„+
Item I Ycs (.0 I aeN) I ?UA(J)
A. Callbnsfon I
1. Is the nh'bratim dmmtam[im alluded Wtete mp6obk? I I
& Sample Analrus
1. Am _he satt role yields iNut acstttaoc c mu? I J
2 Wes.ul sample holdins tiara ma? I / J
7. Is the sar..pic .Milumttm Detacib le .iennv < the C. Deeatm Limit? I I I
C- QC Sampiea
I. Is ute Siaric i.id wtb= ameounce airma I / I I
Li st^ .e `.Iinu:am - OtIaC ble A=WY CQ the olank rtsW S Ibe C urnnn Deuaion I I I / ! `
J. Is the aiank .quit < L: :he Cantraa Daman Imo?
a. Is the aia > I;- the C.xtQae D • iirdt bee < C^ Dc m m Cinut? I ^_
`. Isthe.iari'.3ult>the Camrt Dace:m i.:mis ba :be smile rtauit

Comments n any -No' response:
First L :ei 3e•.iett
Second Lecd Re•.ie•xv
Form d LS-078.2i%.
Qaaatcra Data Review Chedciist
RIDIOCHENUSTRY
Work Cyder number ( or. SL^31 ^_ y I(o! ,S^CI(o "`22Z 244 ^.3^^^--
Cietn ID: R N r—
Due oats: - G - 9
Lab Sammie Number or SDG,i tr.!
Method Test ?ammeter: f t a ut
Z27^
Munn- Q L L L. r'r
Rnnevl I Ye (•/) I `loft) I &A(1) I'Lard
Review lJl
A. CaUbmtIon
1. Is the nhbtwbb docwnevacm inchtded Wore app6ethle?
I
I /
a Simple AtWpis
I. Am the sample vielda wmitm atzsatatre anena7
I /^
Z W ere 311 sample holdms time nn^
I I
3. Is the s ie Mnimum Detectable A=nr y < the C^ Detattna Lent?
C. QC Samples
1. Is the blank •leld Wthm •=cs, siren.
:. Is the Minunum Detectable A=vnY for the Blanc rout S the Caaae Daaston
Litrut?
3. Is the blank . ^ it < L: the Caneacc Detemon L _.?
S, Is the alw3 > I,- the C.Yne9G Dawson L 1t tta < C.IICYS Dc,— Llmnl?
!. Is the olaruc It> the ComnG Desec'on :nut hotthe sa>Rle nstt

First Lc. ei
Second '_z% -I
Form d 1-64 i96. Ret 1
Quzu= a Data Review Checklist
RADIOCHE KISTRY
Work Oraerypnoer ,ak
^3^ 4 8031 ^1 ^3ao6 ^^zzz 8^3^'r X27
Cicm!D' .tJ N --j_
Due Due: 4—
Lab Sartmie ` umber or SOG:
1lethod -M .'mntmurs: P •^ ^
Muni.
Renew Item ( Yea (J) I !7o (J) I WA(J) 11'Sssei
;ess^ (.0
A. Cailbrauoit
1. Is the calrlumas doaunau ation included where applicable?
a Sempie .iadrsie
I /
1. Arc the sample yields within •^^mane citniat
Z Were all sample holding:imn me?
I ^^
7. Is :he zvrpie 11uumum De:stahle k=hN < the Cm Detection Limit^
C QC Samples
1, Is the biarA '•+eid wthin ae-eovncc ct.—t . a
f.
T?Ithe ^•t^.lf:3ml Der[Cadlt.i4'.IVIN:Cf :h the C,lntl
Detection a^:?
ctC4an . J l but the sampie rmlh

Qumzm a Data Review Cheddist
RADIOCHEMISTRY
war< over -umaer ^, t: i 31(o I 3 i v F^3 a•o 3 Z zZ 8C3 a 7
Clem fn . $1+Z
Due our. Lk- (O - k
Cab Sammie Number ar SDG: (P ZZ 7
Nethed 7= is tsnnes:
u,avc C: ^_CeM^.,-t
A. CGllbradon
1. Is the ralibn = doevmerpasim aebsdeb w e s¢eahl ?
se„ICV lt® I Ye(J) I No(J) I VA(J)
& Semple Arraign I
1. Ate the sample neids sec" tt= a^OUptx esteriat
I
II
17niew (J)
I /
II II
Z. W ere all ==It holdio3 time inn? I ^ I j ^ I i
3. Is Ne sample \Ivsirss,m, Dens-^bk .ieJnry < yeGmn Deserswn Ijmit^ I I j l— ^ I
C QC Sampies I
1. Is the blamer •.field within aetrar>re =t .a
Is :he `du= Detectable Aesn,v far l le Sara rink S the Cc Des ern I
Lirmt7
3. Is the dia r=un < l.= the Cra¢,a D^am tin?
4. IS [he JINN > I,- the C.M?]C: DacJan i -1t II, < O,,,, a DQeGr41 LIIIYIT
!. is the dark .a it > the Car, n L)d=on _:= hoebe samplensuh

Qaaatena Data Review Checklist
RADIOCE9MMY
Work Order„ambtlsk 8031 .3q T031G 03 0(0 8(3 D -a 3aNN o317^
C.iaa ID: U ^//
Due Datc.
Lab Satmk Number m SDO:
GG
'to ^I
w^ as -t S
Mepmd Tea Pu® U
^O
M. Mx
Rin wltm Ye(J) HON) VA(V) Tiled
A. Cailbradoa
1. Is the dbalmdoc mausum u tchwad- Im M*kz [a?
IL Sample Analysis
1. M the sa iple yidda with= ameouac= abeia? !/ 3 /
2 Were all sample bolding tesee an? I I I -
3. Is the saaWie Minnu m Deeaahle .Acm y < the Conta ct Deua an Unav
^v
Date y^^ %^J
Date:
` 3 `
I 3
C QC Sample
1. Is the blank yield wigs acceptance ancris 3
^tthe Mim nu n Dd=able Activity la the black ^ 5 the Ceetraa D etec tive (
I I I _ i
3. Is the blank teals < L_ the C.smaa Ddectta Lunt? I
3
3 I r
`,
S. Is the blank > It' the Contact Ddemm Lim but < Catract Detection Lao I ( 3 I -
5. Is the blank result > the Contract Deeom Lank but the savle renh

Qutm=Ta Data Rcview CLeddiu
RADIOCIM0 1LSMY
Wok O mer,mtsea r,t $ 316 1 8011V43 9° a()6 3:) ;t
Chen ID*
Dim Dare lily
Lab Sammie Nmobw er SDCr.
.Method Tea Psnsrm
41sms
I
>n. ^a a "7 5
RZME Item Yam (J) 140(01 ) I WA(J ) 1^Ised
Rs+isr•!Jl
A. Ca llbradam
1. Is the sal3num doemameam ioduded Mus a*kabia? ^.
S Sampee Asuiris
1. An the sarmle?itidt - anseuome avmia? !/
1 Were all samplc bold* —m?
3. Is the sur¢ie 4fakmem Daemhle Acuvdr < the Camas Datum t3mt? I I 3
C. QC Samples
1. Is the blank r cld wirhm scecomma m a 3 I I I
2 Is the 4lutunum Daeamble Amvm (rr the blank rack S the Caara a Detetim
[.unit?
I
3
I /_
3. V the blank trsua < I!- :he Caatna Docc uau Unlit? I
3
/
s. Is the blank > Ir the Caeeraa Daaaeo 1= ba < C.srmaa Damask omit? I I ( 3 '
3. Is the blank :mh> the Cauraaa Dettsesm Lino bm the sampie nmlt < the Cavaa
Detaitan Lirtut^. I f 3
6. Is the i.CS rook wuhm a¢sprafoe vuaa?
7. Is the LCS neldvdth in aaxponre cmrna
8. Is the LCS Mirm Detecahk Acttrn:/ 5 the Camaa Deenim Lam?
9. 415%4tSD rauln aM peld nm •^ r++^+ mtau7
10. Duplicate wnple tesuus and r dd am s¢epuoce av I
D. Other
1. Are all `iomm nfommsm vsmded and ased?
Are ail required forms Ned oLaC
3. Corm= acbodaioa used? I
4. Traractpuen ducked.'
S. Were all calculaiau ducked at a nar>nam fsogo ? ei
6. Unats Checked'
Comments on any -No' response:
First Lwe! 3etdav: L% Li- `E^^{^t` Date:
Second LL%--! Rrviewl Date:
Form #: LS -038 .2 196. Rev 4
3
I I I j
60 57

QUANTERRA LABORATORY NONCONFOR:N L-kNCE VIEmO (NCNI)
PAGE 1 OF 2
Project ID:
Sample Numbers:
r
M
NCM mriated by
0 32 -7,202 D 03^7^a
Tests: —f^o
Matrix: y ^l u / D^ 7
Analytical Area (cheek soorooriate area):
LOG =: RD-98,
• Sample control q GC Cl Wttchemistry l O-lData review
• Organic preparation q HPLC q heals P'Rkadiochemistry
• Inorganic p reparation q GC/MS q Reporting q Bioassay
Nonconformance (check appropriate area):
Holding Time rzolations (exceeded by days) QuAyAssurance/Quality Control
Category 1. Laboratory Independent q 17. QC data repo rted outside of controls
q I. Holding time expired in transit q 13. Incorrect procedure used
q 2. Sample received > 48 hrs. or I/2 holding time has
expired
q 19. SOP intentionally modified tivith QA and Tech. approval
q 3. Test added by client after expiration q 20. Imalid instrument calibration
Category Il: Laborator y Dependent
q 4. Instrument failure
Cl 21- Insu ffi
cient sample received for proper analysis
Incomyror Incomplete Client Deliverable
q 5. Analyst error q 2 Hardcopy deliverable error
q 6. Login error q -13. Electronic deliverable error
q 7. Miscommunication
Reported detection limits eleti-ated due to:
q 8. Other (complete description required) q 24. Sample matrix
Category III: Analysis Reruns (OA, QC) q 2i. Insufficient sample volume
q 9.
IQ
Surrogates
Inte
q 26- Other (complete description required)
27. Other (specify): _
ZL CGh- `C
rn al Standards
q 11. Spike Reco • eries
q 1 2. Blank Contamination
Category Il'. .anal.sis Rerms (Conf+nrtation)
q 13. Second column
q 1 4. Contamination check
q 15. Confirmation of matrix effects
q 16. Other (complete desc ription required)
Noti fi cation ( check appropriate area):
Com>¢nts/Espla^ination
Client noti fied by (name and date): Client "s name and respon s e
d
VtSu ` do ^, f _
GU! 71{7 ^E?L t /
q jtf «Hung q by facsimile q process "as is" q re-_ t mple
be telephone . Ap othe (explain) Z,2, I jo jli hold until q otSer (explain)
Project Manager (signature and date): l f z
0058

Corrective Action
QUANTERRa LABORATORY NONCONFORMANCE MEMO (NCNI)
PACE 2 OF 2
Root Cause 1 nitkLI and date:
LOGO: RD-93-
1, hlrCC^ ^iiu^ s- ( n6o u)GnewPDtU^- ^r^¢>i^C -
Corrective Action Initial and Date: (1q C
Responsibility for performing CA assigned to:
Actions to prevent recurrence Initial and Date:
First Level Supenisor
Responsible Manager: o /
__Ouality Assurance Review
Dy al/ omaly
O Further action required:
Assi gned to:
QA signature:
Corrective Action Ve rification
11 Verified
^' 4
0 Cannot Verif} (specify reason): 1 ^ (` I
Nonconformance demo Closure
QA signature/date:
Date:
Date:
Cl Deficienev O Rerun
Date:
/
n
CO5
_

Quanterra Data Review Cbeddist
RADIOCHEMISTRY
'Cork Che er nvmtser r a,: 1 I Sn31e FSO a S-03 2 2 Z SO 71
1
C:imt!D'
Due Date. -
Lab Samvie `:timber or SM.
method -,m?aametcs: C
Manx:
Z. Z7
Ramme Item
,L Calib ration
t. Is the calibration daautsemaomf urluded Weee anpiicaW
I
IL Sample ..A W7sis I
1. Are the sarfrole vichh vmmma aemtaoae attersa7
:. Were ill Saafple holding tines met'
3. Is the SN.:^ to Meruratem Dee imcle Acu"N< the Camae D eseeem Lann7 I
I
Yet (!) I `!o (!) I WA(!) I ^^IsW
( f
1l
^_
f
I I ^^/I
I C QC Sunpies
1. Is she burn '•teld w thin ^.c asma j
:. lathe .`,1__-urrz Detactable .ae_•nty for she Defe ction
Litfsif^.
3. Is the oianx Tuft < IG the Cancan Deecvan L:mei
4. Is the ours > I,: the C.xeaaa De' .n i:sesf ba < Cman Dese c,, Limit? I I f_
sr;e.11,
!. 13 1he'JIarC :'31+I1 > Ltx C^- Dc %rC.IOn l:mn bm the s=%* l estdl < :he Ccnf
Detection um.:'
6. Is the i ZS cult wthm m=a' I I I i .
7 . Is the :CS p,etd W then ]CL4N1C m1m.
9. Is the LCS llmunum DCIL is 1 J"N < Lhc C as yh D et,,m LSLt?
9, MS, MSD Buis and "sold ere: ac^[anc stem?
10. DuPii^e sur.Ple real(: and ^seid mee. ac-Hang amsa? ^ I I ^ i
D. Other
I. .Are all Scnnr-ncrtnanoa indudd and noted?
:. Are all ree_ud forma tiled out' I ^ I
3. Curry me •_-odolog, used'
a. Tat s ..p , cn cheekd'. I I I
I
7. Were ail n:alaneess aheeitd at a muumum fsequ , f 7
6. Cn.0 cnccawd' I I /
Commen: on on} "`o' resocnse: /U( A [ i-^, hk /u dr^S -/cr ^^L 1 _
First Ln.i R_•.-te•.v"
Date
Second Le.e!Rr.7e•.v-
Form d LS S. ; 96 Rcc
Date:
0000
I

First Lie! R.ne.v Date
Second Leve! 2etie•.r
Form O LS -013? /96, l
Quanterra Dan Review C3eekku
v
RADIOCHEEi LIMY
Work Ordermunberrsh ^i31g^ ^.}I(,I ,^}J^b Oj^j^ S^'^i X 44 53 ^.3.)
Client ID' f•f
Due Datr. y — `i
Lab Sumvie Vumbr or SDG:
Method Tm paamens:
Mama: I
pas Item Yes (.0 *V) I WA(^/) 2^Iasd
Rass!!1
A CallbmClom
1. Is the calibruim doounammm i tchded.Me appiimbler
IL Semple AimiTsis
1. Are the sample Melds wahm aaxpummorsona?
` f
I
I /
2. Were all sauvle holding tnm on? I I I
I Is the satstple Minimum Desemab ie Aaeite < the C•amsa Daeomm Limb? I I '
C QC Samples
I. Is the blank Meld within a¢epaa: alum
Z. Is the Misumum Daauble Aaivny for the Mani must S Ibe C.amact Detemon I
Limit? I
3. Is the blatu :sub < Ii= the Ceeffiaa Des>am L ou?
a. I: the blank > 1 12 the Coma Daemon Lvb bu < Comma Deuam li®t?
I ( /;
I I I _
I J I 1
S. Is the blank result > the Co runa Dana Lines but :be sample tub

QuanaTm Data Review Chedd ist
RADIOCHE1IISMY
W ork Ot numurtat 8o31,e 'F5-03DOC 3222 ,3.-)4 FC3a _7.x_
C' unt lD
K ^,—
Due Date: - la - Q Y
Lib Samo!e Namur oe SDCr
l.J q) 22 -7 S
Nethad TeR ?atYRtei T TrtiP Sri
Matnz 0
A. Cillbnason
'
1. [s the olibatim dnaatmtatim ivrudd w.hee a, pwank?
EL Sen
AA&' sia
Revmne It= I Yes (.0 I fb(J) I WA(^) I ~Ieved
RMtN it l
'°le the ' vi
I I I i
1. Are sample elds ndu, iteiat
^.Wed all sple am haldig tea =?
3. Is the San:pie Mitsomaa Deeraa!e Aa < the Camas Deeasv Sims^ I I
C QC Sampies
1. Is the b!anit '.ieid wIf= srntvtc =
the M llllt'LmDctE le.A . N fO :he Aum.,. S:Sc CJIDIY['JC'i on
". is
3. Is the olank suit < l.= :be C. a Deeevon Ua 7
I I I
a. IS lh. 013 > I :he C.Imlf. Dneeaen L:ILI bn < C^ DecaiYO Lzma7 I ' I ^.^
!. Is the o!arx X12 > the Ca .. Jeecott Z 1= bee ^hc sa npie resod

Qoanterra Dua R rinr Checklist
RADIOCFI DUSTRY
wnrk order-^,n^,.t ^'t^31 b I ^c3 i 8 4 FC3ao^C 5D3 a^ `6C3,P -7 )-
Cientll)*
Due Due--
\_k
- Cl 0
Lab Surtnic Numhtr ar SDG: (,L Z2 -7 ^5
Nahed —ea ?•^---T TO -r Q Sr
.tune O
Rene,. fleet I Yta(.0 I MoN) (
1. ton =ii
i
I. Is the nlihruim docamtcvatton inducted Wiere^c7
R Semple.arm17s6
I. Are the sueic sidle.Wun acGeptante mreriat
I
- Were 111 simple bolding tuna met? I /
3. Is the s . to Amarr+mt Dete=ble iGlnty < DeCaman Desecuao Limn?
C. QC Sempies
I. Is the Mara '.l cld Wtlml aLCplylCe ^1[er.1
Is:he IIr==M J

Quantem Data Review CSedtEu
RADIOCHMMISTRY
W«konuok ^'31^t ^^i v 53o3a^^ 8^3aaa 8^3a - 7 a
Cient ID-
Due Dac.
Lab Sammie *lumber or SDCr.
A, J a a 7 S
Method Tea parameters C - 1 Li
\4atrim
A. Callbrulos
1. Is the calibration doammaom ecbadtd share appli able?
S Semple Aasl7312
1. Ara the sample viddis - acnnece anaria7
times hem I Yea(.) No(1) I ;UA(.) 2-lavel
Rsaieaal.\
2. Were all sample hold ing mm meteI /
3. Is the satpie Mkum ma Detectable .iron) < the Caaa t Deemm Li aise?
C QC Sunple
1. Is the blank held within acmaas am eria
I /
2. Is the Vint mire Detectable Ac m iv the blank nsuh S ibe Cm
Limit?
a Detection I I
f
' I _
`
i
f
3. Is the blank ;cult < lQ Ibe C.aueact Deueflon Lin? I I I I / i
4. Is the blank > 1 R the Cacact Desom Lies bet < C vdria Detec oeu UnuL7 I I '
3. Is the blank vault > the Canna De sera s limn his the sample ratk < the Cacao
Detcuon Umtl?
I
I I ^-
6. Is the LCS result within a¢cpunc Ivan? I/ I I '
7. Is the LCS said within aonptm c ena
B. Is the LCS M inimum Detectible Ass'm S the Carona Deuoos Lion? I I I
9. MSi\fS r) .cults and y aid sheet acmuene cs ma? I I l
10. Duplicate sample saints aid yi eld tots acceptance ancria?
D. Other
I. Ara all Noncoafimnanca ncludd aid acted?
2. Are ail required Corms filed ate
3. Cortex methodolo gy used?
4. Transmpuan checked? I ^^
S. Were all calcttlatons ch ecked a a ev®a® frequency? I f '
6. Uni ts check ed?
Comments on any -No' rspcnse:
First L^:el Rabe% ^— Date:
Second Ltvcf Review Date:
Form ; LS-033,2!96.
V14 r S
006

Comm.it5 on am" No' resoc 0:
First Lrrei Rr.ie:v:
Second Letic! Actiie:r
Form = LS-0 1 8.2 i96.
Qunu=Ta Data Review Checklist
RADIOCHL USTRY
Wark Order-umta: Est O^'^^^7^ ^ 31 O ^^^lT-^O ^^Z2^ ^3a^L.
cian:n N.^ C
Due oast: L 1y -C !
Cab Saenoie Number a SM t,J 2 Z 'T
Method `a[ .'aaametom S 'e - -7
A. Calibradon
1. Is the elibmm dawmeaduian inchnded *wc ag6cahk?
M Sample AaW7 312
Rrne+lt® Yea (J) `*(J) WA LgVel
icriw (J:
I
Dauc A _
Dale
I //
1. Art the sample vields Imdun
aarmaom entnar I I/
2. Were all sample holding tim es mn?
I I I I
3. Is the satr•ie Minimeam Dc=:.xole A=v < ftC.ma s Desectsm Lmd?
C. QC Samples
1. Is the bunk •deld . dun .^-. :tsntcc a:tea
0. Is the.`.linurum Cor des: blank a®u Sdse Catm'aa Detection
L nit"
3. Is the mask ^asuit < L: :he Canna aet,=a n L ma? I/
4. Is the Manic > I,-- the Cantne D^on Lain bn< Ca mcn e Dcamomn Lamas? I
'., fs Use blar3c ^3nll > Use Cantrac: Jenee:oo Lma he the sale nssl[

First Lz:,i Rv.ietc
Second '_=^ e! R- iew-
Form = LS-)',8.2/96.
Qu=ern Data Review Check fist
RADIOCHEaM 4-(;^ cr^ ,
J. were all :al.-llsstaru :Pecked at a :wmr:S n rsc epumv?
6. Units checkd?
COmmen Ls on any'-`o' resccns:: i1,'• ,LDL
'es It" L^(,^ G"X— Q
Date -^fJ
D= Y 6 ^^
j
6060

Qaaaterra Data Review C3eddist
RADIOCHIJ. Y
waeit order -umbe (It `a'A3 i Fs ^{ 8C3 i ^! `6C'3 ^ c^SG;S ^ .^. a ^rG3 ^ ^f N ^t 3 3 7
cient :D: t k -7
Due Date:
L . Y
4 -
Lab Samote Vumbe or SDQ
Method Tea ?a=nswer: 7—C - 9
Natnrc G +h P
-22-7,.5
Renew ltea I Yes (.1 ) I No (,0 I VA(.t)
A. CAUbmtlon I
1. Is the alibtmm dootmemommon mc!uded -tax agfehlst
I /^
B. Sample Ameiyms
1 . Are the sample yyields-was
asreounm msaut
:, Were all Sample holding—me?
I
I I /
3. Is the sampic Minimum Dcw=ble iC.tnN n Detmsm Limis^. I ,'}
C QC Semple,
Y^
I ge LAvd l
-CT ^ I^ ^
L is the hi= 1eid wtthta as = atma I I I
L is t he Micur..um Da --r •. .iCtnty :or the blank arta
S th Ca Damson
I I -
3. is the Mark ^11 < L- :he Can== _-aecvon Irma? I /sue I _
a. Is the oiu > I,: Itta Camas ',?ct¢:ton L .Vt but < C. Doccum Lunt?
3. IS the D[wk : It > the Cams.-. C

Richland Laborato ry
Quanterra Data Review Check List
Work Order Number(sl: 9'U3
Lab Sample Numbers or SDG: ^Z / 7
Method/TestiParameter. e^f^
A. Initial Calibration
METALS
vyZ ^^
Review Item
1. Performed at required frequency wih required number of levels?
2. Correlation coefficient within QC limits?
3. Initial calibration ve rification (ICV) analyzed immediately after calibration
and results within QC limits? V
4. Initial calibration blank(ICB) analyzed immediately after ICV and
concentrations of all paramete rs < reporting limit?
B. Continuing Calibration
1. CC V analyzed at required frequency and all parameters within QC lirnits?
2. CCB analyzed at required frequen cy and all results < reporting limit?
C. Sample Analysis
1. Were any samples with concentrations above the linear range for any parameter
diluted and reanalyzed?
Yes
V)
No
(V)
N/A 2nd Level
Review ( 3 ^
2. Were all sample holding times met? i
D. QC Samples
1. All results for the preparation blank below limits?
2. MS or MS/NISI) recove ries within QC limits and n/aRPD (forMSD) acceptable ^C
3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable?
4. Analytical spikes within QC li
mits where applicable?
S. ICP only: One se rial dilution performed per SDG?
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy ?
7. ICP only: Interference check samples GCSA, ICSAB) and FECAL analyzed at the
re uired fre uencies and within 9C limits?
page 1 of 2
606

E. Other
1. Are all nonconformances included and noted?
2. Is the cormct date and time of analysis shown?
Review Item ( Yes
( ^)
3. Did the analyst sign and date the frmt page of the analytical tmm?
4. Correct methodology used?
5. Transcrip tions chocked?
No
(V)
N/A 20 Level
Review (^)
6. Calculations checked at minimum frequenc y? 3 ^/
7. Units checked?
Comments on any "No" response:
Analyst: Kw Lz e 7 ^ ^O n ^ Date:
Second-Level Review: 12 Ie Date: 3/4/"
Form No. CG-191. Rev. 2,1/97
page 2 of 2 Go b
i

Richland Laborato ry
Qanter a Data Review Check List
METALS
Work Order Numberts): 31ffzl S7 3)11
Lab Sample Num bers or SDG: u/ .^275 4J 0
Method/Test/Parameter. U+lo ur?L L Tl?-47f
A. Initial Calibration
1. Performed at required frequency wih required number of levels?
2. Correlation coefficient within QC li
mits?
Yes No N/A 2"d Level
Review Item Review (^)
3. Initial calibration ve rification (ICV) analyzed immediately after calibration
and results within QC limits? L/ j
4. Initial calibration blank(ICB) analyzed immediately a fter ICV and J
concentrations of all parameters < repor ti ng limit?
B. Continuing Calibration
L CC V analyzed at required frequency and all parameters within QC limits?
2. CCB analyzed at required frequency and all results < repot ting limit?
C. Sample Analysis
1. Were any samples with concentrations above the linear range for any p arameter
diluted and reanalyzed? v i'
2. Were all sample holding times met?
D. QC Samples i
1. All results for the prepara ti on blank below limits?
2. MS or MS/NiSD recove ries within QC limits and °/aRPD (for MSD) acceptable ^F
3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable?
4. Analy tical spikes within QC limits where applicable?
5. ICP only: One se rial dilu tion performed per SDG?
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy ?
7. ICP only: Interference check samples (ICSA, ICSAB) an d MCAL analyzed at the
required frequencies and within limits?
—I
page 1 of 2 GUI U

E. Other
1. Are all nonconformance included and noted?
2. Is the correct date and time of analysis shown)
3. Did the analyst sign and date the front page of the analytical run?
4. Correct methodology used?
5. Transcriptions checked?
6. Calculations checked at minimum frequency?
7. Units checked?
Comments on any "No" rssponsc:
Analyst: -^?C, Lg_ '7^) ^G
^ ^
^)
Second-Level Review: 1/7?^^34/j/^
Form No. CG-191. Rev. 7, 1/97
Review Item Yes No N/A 22° Level
Review (/)
Date: 3//l /9e
Date: 31191?^
page 2 of 2 [ ^! 1

Richland Laboratory
Quanterra Data Review Check List
METALS
Work Order Numher(s): Q a2 ] 9 7
Lab Sample Numbers or SDG: /V 2 2-7 S t &-)C2291
Method/Test/Parameter: Qk*t, L - rr
A. Ini tial Calibration
Yes No N/A 2°d Level
Review Item (1) Review (V)
1. Performed at required frequency wih requited number of levels? 3 /
2. Correlation coefficient within QC limits?
3. Initial calibration ve rification (ICV) analyzed immediately after calibration
and results within QC limits?
4. Initial calibration blank(ICB) analyzed immediately after ICV and
concentrations of all paramete rs < repor ti
ng limit? / _I
B. Continuing Ca lib
ration
1. CCV analyzed at required frequency and all parameters within QC limits?
2. CCB analyzed at required frequency and all results < reporting limit?
C. Sample Analysis
1. Were any samples with concentra tions above the linear range for any parameter
diluted and reanalyzed?
2. Were all sample holding times met?
D. QC Samples
1. All results for the prepara tion blank below limits? j
2. MS or MS/NiSD recove ries within QC limits and °/aRPD (for MSD) acceptable?^^^
3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable?
4. Analytical spikes within QC limits where applicable?
5. ICP only: One serial dilu tion performed per SDG?
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency?
7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the
required frequencies and vvithin C limits?
page 1 of 2
8 4
60"tZ

E. Other
1. Are a ll nonconformances included and noted?
2. Is the correct date and time of analysis shown?
3. Did the analyst sign and date the from page of the analy tical run?
4. Correct methodology used?
5. Transc riptions chocked?
Rem Item Yes No N/A 224 Level
Review (V)
6. Calculations checked at minimum 5squmcy?
7. Units checked? j
Comments on any "No" m6ponse:
Analyst: ^Q7^P ` 41
d 3
Second-Level Review: ^al^f p
Form No. CG-191. Rev. 2, 1/97
Date: 3 z/ fzpz
Date: 31145
page 2 of 2 6 0 7 3
I

Richland Laborato ry
Quarteim Data Review Check List
METALS
_^b!_31 i srLf ^_
Work Order Num ber(sl: ZbL gp
Lab Sample Numbers or SDG: ^^ W O
Method/Test/Parameter:
A. Initial Calibration
1. Performed at required frequency wih requited number of levels?
2. Correlation coefficient within QC limits?
Yes No N/A 2°a Level
Review Item (`) Review (v)
3. Initial calibration ve ri fication (ICV) analyzed immediately after calibration
and results within QC limits?
4. Initial calibration blank( ICB) analyzed immediately after ICV and
concentrations of all parameters < reporting limit?
B. Continuing Calibration
1. CCV analyzed at required frequen cy and all parameters within QC limits?
2. CCB analyzed at required frequency and all results < repor ting limit?
C. Sample Analysis
L Were any samples with con centrations above the linear range for any p arameter
diluted and reanalyzed? v
2. Were all sample holding ti
mes met?
D. QC Samples
L All results for the prepara tion blank below limits?
2. MS or MS/MSD recove ries within QC limits and °/d2PD (for MSD) acceptable? py
3. LCS percent recove ry within QC limits and %RPD (for LCSD) acceptable?
4. Analytical spikes within QC limits where applicable?
5. ICP only: One se rial dilu tion performed per SDG?
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency ?
7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the
re aired fre uencies and within C limits? `/
I
3
i ^^
page 1 of 2 60! 4
—i
_r
P,

E. Other
1. Are all nonconfonnances included and noted?
Review Item Yes
( ^)
2. Is the correct date and time of analysis shown? 3
3. Did the analyst sign and date the front page of the analytical rm?
4. Correa methodology used?
No
(^)
NIA
(^)
221 Level
Review ( 3 )
5. Transcriptions checked? 3 j
6. Calculations checked at minimum frequency? 4
7. Units checked? C7
Comments on any "No" response:
Analyst: y O'XC e- ^o^ 0 Date: 3/ ( 8/ p k
Second-Level Review: ^^1. ^

Richland Laboratory
Quanterra Data Review Check List
N =ALS
Work Order Numbedsl: 8C 3
Lab Sample Numbers or SDG: &. b :-^ a O
Method/Test/Parameter. y)
A. Initial Calibration
1. Performed at required frequency wih required number of Levels?
2. Correlation coefficient within QC limits?
Yes No N/A 2"d Level
Review Iten (V) Review (^)
3. Initial calibration veri fication (ICV) analyzed immediately after calibration
and results within QC limi ts?
4. Initial calibration blaak(ICB) analyzed immediately after ICV and i
concentrations of all paramete rs < reporting limit?
3
I
B. Continuing Calibration
L CCV analyzed at required frequency and all parameters within QC limits? / 3
2. CCB analyzed at required fn quen cy and all results < reporting limit? 3 —^
C. Sample Analysis
1. Were any samples with concentrations above the linear range for any parameter
diluted and reanalyzed?
2. Were all sample holding times met?
D. QC Samples —i
L All results for the preparation blank below limits? t/ v
2. MS or MS/MSD recove ries within QC limits and %RPD (for MSD) acceptable4 ov v
3. LCS percent recove ry within QC li
mits and %RPD (for LCSD) acceptable?
4. Analy tical spikes within QC limits where applicable?
5. ICP only: One serial dilution perfo rmed per SDG?
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy?
7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the j
required frequencies and within QC limits? 3
3
3
—
3 i
page 1 of 2 / U

E. Other
Review Item Yes
(3)
1. Are all nonconformances included and noted? 3 j
2. Is the correct date and time of analysis shown?
3. Did the analyst sign and date the front page of the analytical run?
4. Correct methodology used?
5. Transc riptions checked? i
6 Calculations checked at minimum frequency?
7. Units checked?
Comments on any "No" response:
Analyst: Date: ,311 p k
Second-Level Review: /),^ Date: 3 . 1-191y F
Form No. CG-191. Rev. 2. 1/97
No
(-01)
N/A
(3)
2=d Level
Review ( 3 )
page 2 of 2 li 0 i i

Richland Laborato ry
^w° ` alters Data Review Check List
METALS
Work Order Num ber{s): Yo y y
Lab Sample Numbers or SDG: 14,0 ,,?Q75
Method/Test/Parameter. C & ^j Q
A. Initial Calibra tion
Review Item
1. Performed at required frequency wih required num ber of levels?
2. Correlation coefficient within QC limits?
3. Initial calibration verification (ICV) analyzed immediately after calibration
and results within QC limits? j
4. Initial calibration blank(ICB) analyzed immediately after ICV and
concentrations of all parameters < reporting limit?
B. Continuing Calibration
L CCV analyzed at required frequency and all parameters within QC limits? t,-'
2. CCB analyzed at required frequency and all results < repor ting limit?
C. Sample Analysis
1. Were any samples with concen trations above the linear range for an y parameter
diluted and reanalyzed?
2. Were all sample holding times met?
D. QC Samples
L All results for the prepara tion blank below limits?
2. MS or MS/NISD recoveries within QC limits and %RPD (for MSD) acceptable?; p'k
3. LCS percent recove ry within QC limits and %RPD (for LCSD) acceptable?
4. Analytical spikes within QC limits where applicable?
Yes No N/A 2°a Level
Review (^)
5. ICP only: One serial dilu tion performed per SDG? ^1
3
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency?
7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the
required frequencies and within 2C limits?
page 1 of 2 Go! u
i

E. Other
1. Are all nonconformances included and noted?
2. Is the correct date and time of analysis shown?
Review Item Yes
( ^)
3. Did the analyst sign and date the fiont page of the analy tical tun?
4. Correct methodology used?
5. Transcrip tions checked? 3
No
(^)
N/A
(^)
2—d Level
Review (V)
6. Calculations checked at minimum frequency? 3 i"
7. Units checked?
Comments on any "No" response:
Analyst: `,(^ X Le j1/^12a1^
Second-Level Review:
Form No. CG-191. Rev. 2. 1/97
page 2 of 2
Date: 3 //L ^rfR
Date: 3//E
Go -, J

Richland Laboratory
Quante"a Data Review Check List
METALS
Work Order Number(sl: X '.
lab Sample Numbers or SDG: U) L2275
Method/Test/Parameter: '
A. Ini tial Calibration
1. Performed at required frequency wih required num ber of levels?
2. Correlation coefficient within QC limits?
Yes No N/A 2°d Level
Review Item Review ( 3 )
3. Initial calibration ve rification (ICV) analyzed immediately after calibration
and results within QC limits?
4. Initial calibration blank(ICB) analyzed immediately after ICV and
concentrations of all parameters < reporting limit? 3
B. Continuing Calibration
1. CCV analyzed at required frequency and all parameters within QC limits?
2. CCB analyzed at required frequency and all results < repor ting limit?
C. Sample Analysis
I. Were any samples with concen tra ti
ons above the linear range for any parameter
diluted and reanalyzed?
t/ 3
2. Were all sample holding ti mes met? j
D. QC Samples lj
1. All results for the prepara ti
on blank below limits?
2. MS or MSQvISD recove ries within QC li
mits and °/dtPD (for MSD) acceptable?!! 1 F
3. LCS percent recovery within QC limits and °/gRPD (for LCSD) acceptable? I I —^
4. Analytical spikes within QC limits where applicable? 3
5. ICP only: One serial dilu tion performed per SDG? 3 j _
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy?
7. ICP only: Interference check samples (ICSA, ICSAB) an d MCAL analyzed at the Lj
re uired fre uencies and within C limits?
page 1 of 2
^.
_I
G 0 j 0

E. Other
1. Are all nonconformances included and noted?
2. Is the correct date and time of analysis shown?
Review Item Yes
(^)
3. Did the analyst sign and date the front page of the analytical run?
4. Correct methodology used?
5. Transcriptions checked?
6. Calculations checked at minimum frequency?
7. Units checked?
Comments on any "No" response:
Analyst: 41 z i_e_ `7 ^0.^1
^
^^ ""
Second-Level Review: r pt A&d
Form No. CG-191. Rev. 2, 1/97
page 2 of 2
Date:
3
No
V)
Dater IZ P%
NIA 29° Level
Review V)
/
V0$t

CHAIN OF
CUSTODY FORMS

C_
C
or
v
Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -01 Page 1 of !
Collector Company Contact Telephone No. Project Coordinator Data Turnaround
R. Fahlberg Steve Ma rske 373 4 316 WEISS, RI.
21
Project Designation Slorpling Location SAF No. Days
105-C Phase I & Phase If -Concrete Samples 100 Area B98-061
Ice Chest No. Field Logbook No. Method of Shipment
_^ - - C, — Iland deliver
Shipped 'I (I
Quanterra Incorporated
Olfsite Perty rop No. Bill of Lading/Air Bill No.
POSSIBLE SAMPLE IIAZARDS/REMARKS
Radw.,m, c
Sproul llandling and/or Sloragc
SATIPLE ANALYSIS
^^ Preservation
rv^ae
Type of Container p
No. of Cnnlainer ( s) -
Volume \'
(^/^ Sa i¢m 111 In
^ J 'L
SPed.l
Imwnio^s
Ci ^^^^J
w
11-
Sample No Matrls• Sample Date Santple'fime s"'td v ^. qti` a5„tY [:'••^:, jg .r'n'3!^* , sl'^.rlt'°,:. 'f.^s '^a i aa q^%',`:-
C,
L
BON680 CI Other Solid
S
SPEI LAI. INS 11 4 IRONS Matrix
111 %IN III I'IOSSI..SSIOV Sign/Print Nawr.
III I( -I' hlc0a6- 60 ttA lSupal0accl l eudl, Mcauq - 9421 - (CV ) , C6rumnmin llt, " 7146,
s
sk
_
-
s,,d
sa.linan
I(LIlP1 .Lcdlly (I - Y•/- D1 Iuuc Rua dIII
-2 O
U I..... Pill, 8080,iAi 1
I 0 . I I54, I. 0 I
1 ill.tia 0a S,,,,ou..ulY (e 0137,
1551"A a .. 0 24I I 0 ryi. I Wlu 0wn
bait6(11
I mpie Il y a
Vi t 152
n . SO,
sU
si.
-
sWi4
61,dae
of na1 + 0 0lcluu^ 14c uJlq
^^
10e1f5111uu
- ^^(^ } C` `j 9
. Mi LrCI
r a ,j^0.1
L3 Sr- 90 EDIT l Sr
1, ¢^t s
A
" V , Can
141w 1 uuLed 11 1Ito, nue wl scd it, I>.em' Inn e v q
I(c
^^
.
a
i
m
UI
I
-
nil
a s " I m
ho-
III - 111pe
hall uyw.Lcl I10 U.uc l un. I(cco.cd II Ill.nc l llv. I I w ^
11111110A 111111 It nr.l Ito Iltic Uam^l lnm
St( IOUs
FIN'AI SVAII'Lf. 14 1.Iki'll 111.1 .0111, Ilalc/I inm
I IISI'IISI I IfIN

C
cc:
li.-
Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -02 Page I of
-'olleclor Company Contact Telephone No. Project Coordinator Data Turnaround
R. Fahlherg Steve Marske 373 -4316 WEISS, RL
21 Days
Project Designation Sampling Location SAF No.
103-C Phase 1 & Phase II -Concrete Samples 100 Area B98-061
Ice Chest No. Fie ld Logbook No. Method of Shipment
Hand deliver
'hipped To Mile Properly Bill of Ladin Air Bill No.
Quanterra Incorporated
POSSIBLE SAMPLE IIAZARDS/11EAIARKS
Radioaclim
S pecial Ilandling and/or Storage
SANIPLE ANALYSIS
Prese valion
None
Type of Container P
No. of Container(s) Z
Volume
IL
sw acm t 11 In
speci al
m,wnrnns
Sample No Mali:y • Sample Date Sample Time }-^ _, ` `.I z, =,gyp' = • s -:t(do. -
BON681 j, -^ Other Solid — 3 ' ^," Z
I SPF.CIA I. INSIRI C"II ONS Matrix
HAIN OF PO SSE SSION
ItcLw uuhcJ e" Dnm"Imo
Sign/Print Names
Re

Environmental
Contractor
Contractor
Visa
Team
Interoffice Memorandum
M.
'.nrna!
D. A. St. John r.0-19
See Below
°"M 1'ebruary 27.1999
rtiaa S. L. Winslow
RadCun Engineering
X3-41/531-0700
susurcr: CURIF ESTIMATE FOR S111PP1NGCON[:RETF. CORE SAMPLES
CotQatration (obi/e)
2.55 pCilg
1.2F3 pCi/g
4.95 pCi/g
7.5E-1 pCi/g
2.550 pCifg
7.5E-2 pCi/g
1.5 1
1.46L'3 pCi/g
CCN: 055088
Job No. 22192
Wnm•A.av Ap
Div w•
a, ion
nn v
c•n wn
Swwn Cob Im
The 1i111uwing calculations show that core sample: with a direct reading of equal to or Icss than
400.000 dpm/1Merin' will be below the definitionorrulivactive material as defined in 49 CFR 173.403
of 70 Bq/g (2F.3 pCi/g). Each sample will consist of contxete material from four, two inch core
samples and enough water to arike a slurry consismacy. 'the distribution of radionuclides is hued on
previous concrete samples rakcn from the below gtadie Fuel Storage Basin that would also he
representative of these concrcec samples.
(jiven:
Cyiinder Volumc = itA Radius of concrete core (r) = I inch
Concrete Density = 2.35 g/em' Height of cam sample taken (h) - 0.25 inches
27 pCi = Dq Maximum 5rn:1 reading on core = 400,000 dpna/ I OOcm'
2.'_2 dpm = pCi
Calculations:
V — (3.14) (1 in.)'(0 25in) = 0.78 in' (16.4 ciOin-' (4 con: samples) = 51.2 cm'
(400,000 dpm/51.2 cm) (cm'/2.35 g) = 3.32E3 dpVg
3.321:3 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g
SI.W:dld
°Co
Percent Distribution(`7)
0.17
"'cs
432
EU
82
0.33
1"Eu 0.05
90Sr 17
7Ai Ain 0.005
239'rx'Pu
0.1
TU rAr-:
('epics:
S. 0. Marske X5-53
P. A. Newman X3141
RadCun Engineering file/LB XO-23
Document and Into Services 010-09
'0
0085

Environmental
Restoration ERC Team
Contractor
Interoffice Memorandum
TO' D. A. St. John I.0-19 LATE: l-ebruary 27. 1998
"O''' F'` ' See 13clow
FROM:
* Av
S. L. Winslow
RadCon Enginuing
X3-41/531-0706
suwECT: CURIE ESTIMATE FOR SHIPPING CONCRETE CORE SAMPLES
Concentration_(^Ci/;>
2.55 pCi/g
I.2F.3 pCi/g
4.95 pCi/g
7.5E-1 pCi/g
2.55E2 pCi/g
7.5F.-2 pCi/g
1.5 2C.Ug
1.46E3 pCiig
Job No. 22172
wnan 0.epmrRpu.N .nU
P+Ow w^
I 1 V w/,
W n l0,
CCN: 055081;
s^+l..,cw. !Fw
The ibllowing calculations show that core samples with a direct reading of equal to or less than
400,000 dpm/100cm' will be below the definition of radioactive mate rial as defined in 49 CFR 173.40±
of 70 Bq/g (2F3 pCi/g). Lach sample will consist of concrete materi al from [our. two inch core
samples and enough water to make a slurry consistency. 'fhe dislrihution cdmdionuclides is based on
previous concrete samples taken front the below grade Fuel Stora ge Bas in that would also be
representative of these com:rctc samples.
'ven:
Cylinder Volume = nr'h Radius of concrete core (r) = I inch
Concrete Density = 2 3 5 ylem' Ileight of care sample taken (h) - 0.25 inches
27 pCi = Bq Maximum direct reading on :ore = 400.00 0 dpnl/lUUcn1`
2.22 dpm = pCi
Calculations:
V - (3.14) (1 in.) 2( 0.25in) = 0.78 in' (16.4 can `/in) (4 cure samples) = 51.2 cm'
(400.000 dpm/51.2 cm) (cm'2.35 g) = 3.32E3 dpm/g
3.3213 dpnn'g (pCi/2.2 dpm) = 1.5E3 pC'i/g or 55.4 Bq/g
SI VAld
Percent Distribution( 7o )
'"Co 0.17
"'Cs 82
1 1 Lu 0.33
"°Eu 0.05
"°Sr 17
'°' Arn 0.005
"°'="'Pu 0.1
TOTAL
Copies:
S. 6. Marske X5-53
P. A. Newman X3-41
RadCun Enginee ri ng File/LB XO-23
Document and Info Se rvices 110-09
V^^O

F%jwI 1
SAMPLE CNECX-IN LIST
CaterTime Received: . ^ 151 SG*
wcnc Order Number L' ? i ( ^' ^(GI Say 1R- C^^ ^I
Shipping Container IDk l SJ^ Chin dCustody;
RFSHSOw-93-0003 -
Revision
^1
(1 ^^' l
1. Custody Sealsaod*Ong , I i ktar Yes IC II
2 Custody Seals d*d and signed? Yes K,40 No I 1
3. Chain-of-Custody recatd presenO
GC
Yes I 1
4. Caalet temperaftae
5. Vennici telpad* materials is Wet ( ; 3rY ( l
6.
Number of samples in shipping corainer
7. Sample holding Imes exceeded? Yes [ ; No I 1
8. Sammhave
tape hazard Labels
seats appropriate sample labels
9. samples are_
_SLm good wnd ition lealdng
broken _ have air bubbles
10. Where any anomalies identified in sample receipt?
11. Cescsiption of mana lies (nude sample numbers)_
Sample Custcdianllabaatorl '^ Date_
Yes I 1 No I
Telephoned To: Ongy
IA
60S;

Frlrr 1
SAMPLE CHECK-IN UST
DateMme Received: SG#:
^^c ^ sc ar-^--aoo_ -
4" Sion
Work Crder Number. l'^ ^^ SAF #:-
Shipping Container ID: U d chair of Custody # I ^ (J - ^^ ^^
1. Custody Seals an shipping contain ritW. Yes I I
2 Custody Seals dated and signed? Yes ( No [
3. Chain-of-Custody record present? Yes

Client Sample Screening Results
I D-Mar-98
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
BII ON14CI 3/9/19981:42:00 P7)2 1A 3/10/199811:23:38 BOM4CI
(QUID 1HI+kg,
3/10/1998 ^ :51 ANI BKG
An]D t /10/1998 ' ,Alq: 5.00E-01 01 (Dpm/ 5.49E-01 (uCl/ 1.24E-0j
,-Ppt mg:2.1 Unita: L Bet; ): 5.42E+01 So);--J.hE-0 3
DI11 130 1,14C2 3/9/19981:42:00 PM QUAD2 1 B 3/101 19981123:38AN1 BON14C2
LIQUID Bkg: 3/10/1998 8:43:51 A BKG
A nI Dgt : 3/10 ToI Sr, AIy: 5.00E-0^ OE+01 Alp; (Dp V 738 -0 (uCU 8.07E-06
/Pptmg: 2.6 Inks: /L m Bet( ,-^q): I.IIE+01 2.51E-04.
30 16 9.49333333 841 27.233333
i
100 4 0.04 0 0.8
2.47E+01 ± 2.3E+01 CAT OE+00 1.
LIg )i 1'44+03 3 8.7E+01 I 2A ^^^L`^
w 6
0.03
(p 1.6 01 ± 2.4E
Llg): 5.01E+02 .3E
202 833333 -
95 "-^ 0.95
4T E+00 Lob
I Alq
11111 BON680S 3/9/1998 1:42:00 PM QU kD24D 3/1 0/'199811:23:51 AN1 BON680S
30 1130 37.6066667 124390 4145.4333
90G 100 6 0.06
0.9
I SOLID Bkg: 3/10/19988:43:55AN1 BKG
AN Dote: 3/10/1998 Tot Sa,Alq: 1.63E+02 9.81E+01 Alp; (Dpm/ -1.71E+01 (uCU 4.27E-02 (pCV .7.83E+01 ±9.4E+00 CAT 1.6E+02 Lab
Ppt mg: 98.1 / UNta:g mg Bel; Alq): 9.19E+03 So): 6.86E+00 Ljg): 4.22E+04 ± 1.2E+02
III
2.4E-03
14c I-IC
DIII BON681P 3/9/19983:15:OOPM QUAD2IA 3/10/199811:54:54AN1 DON68IP 30 5 0.12666667 96 2 4
G a LIQUID Bkg: 3/10/1998 8:43:51 AN1 BKG 100 4 0.04 80 0.8
An] Dote: 3/10/1998 Tot So, Alq: 1.80E+00 100E+01 Alp; ( )pm/ 3.23E-0 1 (uCU 2.62E-05 (pCU 1.45E+01 ± 2.4E+01 CAT 1.7E+00 lab
I-pt mg: 69 Units: 1. / ml Bel; Alq): 4.79E+00 So): 3.88E-04 Ljg): 2.16E+02 ± 3.1E+01 I 2.3E-0t
Alq
BIII BON681S 3/9/19983:15:00 PM QUAD21B 3/101199811:54:54 AM BON681S 30 13 0.40333333 234 6.85
GSOLID Bkg: 3/10/19988:43:51 ANt BKG 100 3 0.03 95 0.95
AN Date: 3/10/1998 3'ot Sa,A1q: 1.90E+02 1.1511+02 Alp; (Dpnt/ 2.58E+00 (uCU 1.93E-03 (pCU 1.02E+01 ±5.5E+00 CAT 4.9E+00 lab
Ppt mg: 114.5 Unite: g / mg Bet; Alq): 1.55E+01 So): 1.16E-02 Llg): 6.09E+01 + 4.6E+00 I , 1.6E+00
DIII 13ON6801 : 3P)/19981:42.001'M QUAD24C 3/10/199811:23:51 AN1 11ON680P 30 43 1.39333333 3426 11339
LIQUID llkg: 3/10119988:43:55 AM BKG 100 4 0.04 81 0.81
AnlDate: 3/10/1998 'Pot Sa,Alq: 1.80E+00 LOOLWI Alp; (Dpntl 4.48E-0 1 (uCU 3.64E- 0 5 (pCU 2.02E+01 +2.2E+01 CAT 1.2E+00 tab
Pp( mg; )A /^ Unite: I. nJ IRq Alq): 2.141:+02 So): 1.74E-02 Leg): 9.66E+03 + 1.7E+02 1 5.2E-03
r
^
'^I i^ 1) 9. Y , '17 1, I cA^4
O 0-.4/nr-9N QDanterra Environment Se rvices, SCP V2.03
CO )
Alq
Ids
I'll:

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-o61-03 vase ! '/ !
ullectur Company Contact Telephone No. Project Coordinator Data Turnaround
R. Iahlhcr,
Project Pro Designation
I Des i ,
Steve Niarske
Sampling Location
373 -4316 WEISS, RL
SAF No.
21 Days
105 C Vhax 18' Phase II -Conercre Samples 1(111 Area 898-061
Ice Chest Nu. Meld I. ,ghouh No. Method of Shipment
L- L J r _ Hand deliver
Shipprd IF, 011silr 1'roperty No. Bill of fading/Air Bill Nu.
I luanwira lncorpofFacd n IF
POSSIBLI. SAN11'LL IJAZAlt DS/REMARKS
RaJioaa i.c
Special Ilandlln8 and/or Sturaye
Presen'atiun
I)pe of Container
No. of ('ontalner ( s)
\'olmne
(^^^ 'y^ ^''^
111
S:ANIP1.F 0%
CIJLk>« -7,
031 g ^a C^ c h i X0-5
Sample No Nlalric Sample Dare Sample 'I 11 11 c
BON682 Other Solid
P
IL
sec uem (p m
saeoal
SPE('LU. INS IRE 'CI'IONS
N1mriy
I OI: POSNI.SSION ,'Ign/Prini Name,
( 111( I N1n.d.-bnI''%'s .niF") ll aaJ l, Ntocl- w 74 71- I C V). C hmm moi l l° -119e,
s
SI.
- soil
- seammu
1 cl Iqm ch

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -04 page 1 of !
Collector Company Conlact Telephone No. Project Coordinator Rata -turnaround
R. Fahlberg Steve Marske 373-0316 WEISS, RI,
Project Resignation Sampling Location SAF No. 21 Days
105-C Phase I & Phase II - Concrete Samples 100 Area B98-061
Ice Chest No. Field Logbook No. Melbod of Shipment
L.°L — l 3 C ) r — 2
Hand deliver
Shipped 1'.
Quanerre Incorporated
POSSIBLE SAMPLE IIAZARRS/REMARKS
OBske Property No., .
AL-11-4
r+aa.
Bill of Lading/Air Bill No.
A'
Radioacl,e
Preservation
'pecial handling and/or Storage
SA MPLF. ANALYSIS
'Iype of Container
No. of Container(s) -
Volume
P
IL.
5.^ m01in
SaCn1
10'^^.°1O°`
03193 Chi g0318^ Pao(-
Sample No Matrix Sample Date Sample Time ^ni 1111, ^`-E .-+p ;, ^. M ,+ '#„n c fr v ' ,. S+}
BON683 O^ Other Solid /lJ S D ^l r'j7 X '^ 9 _ t
11 UN
01 PO.SSI SSION
It i.... ..aJ l^i /^^ ^^Ii^9 un
^^^ o ^ 3
11eWignnh d ll/
SPF('L I. INS TI1VC110 11 S Mumix'
Sign/Print Nwura S
(I11(l'M

C
l
Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-05 Page 1 of i
Collector
R. Fahlberg
Company Contact
Steve Marske
Telephone No.
373 -0316
Project Coordinator
WEISS, RL
Data Turnaround
Project Designation Sampling Location SAF No.
21 Days
105-C Phase I & Phase 11 - Concrete Samples 100 Area B98-061
Ice Chest No. Field Logbook No. Method of Shipment
4- L — / 3 2 [land deliver
'hipped "I o Offske Property No. Bill of Lading/Air Bill No.
Quanterra Incorporated
POSSIBLE SAMPLE IIAZARDS/REMARKS
Radioactive
S pecial Handling and/or Storage
SAMPLE ANALYSIS
Preservation
Type of Container
No. of Container(s)
Volume
r+o^e
p
IL
See Item ( 1) in
Speaal
Io:nom"'^`
803183 ^^ gc^31^'4 ^^d
Sample No Mavis Sample Date Sample Iime n^ 1L .E--;t' ry aii v`; ;/!
BON684 3 Other Solid S/`/ `.r ^, `. '^ V
CHAIN OF POSSESSIO N
RJulgnuhnl n1 h,,, s^ U lc 5
./^0< P
RcLm mha fy IJeLL`I ic
Rcllnqul>heJ 11 1 Dale Tmm
Sign/
i
J Recce Ily
Lcl.edIt,
Remi.eJ Hp
int Names
/
1lalel1lnm
amfllme
v Dm,Tlnle
ti
SPECIAL INSTRUCTIONS Ma tr ix
s
I R 1 1 Nlo, is b010A (Super ace) ILead); Mercup - 7471 -(CV), Chromuun flea -7196, SG
IV II, 8080 ( All i 1211 1lice, t SI t sc P) (Ce'ium 1 V C ,bah-60, Europium I S'_. SO
L uy'w -U.L 1'.......n-139;. Ai w ......n-24 1 Isotopic P wo iiu . Isuwpic t)mnu m. Sell SI
-1 G N'
"lPn (f(Is'1 - 19 N^ ^/-6^ Sr-^^ -/o- - u^ / Sr, U
Teoh 17q (^ bon 14, , 46 71/( 'ly Sean 1)
or
I

Environmental
Restorati on
Contracto ERC Team
Interoffice Memorandum
zO D. A. St. John r.0-19 b"rz0 February
27. 1999
1"Y1• '` See Below
l
ncoa: S. L. Winslow
RadCun EngUla:ring
S1. W:dld
to Co
137 CS
Percent Distribution(r/o)
0.17
82
132EU
ueEu
0.33
0.05
"Sr 17
741 Ain
209/zwpu
0.005
0.1
TOTAL:
X.1 -41 1531-0700
suuecr: CURIE. ESTIMATE FOR SHIPPING CONCRETF. CORE SAMPLES
Job '49. 22192
wwvwll^Mwsrw '10
D,DW NA
il ♦ www
a' Vole
R11
caw vw
CCN: 055082t
The lirllowing calculations show that con; sampicswith a diner reading of equal to or less than
400.000 dpm/IOOcm z will be below the definition of radioactive material as defined in 49 CFR 173.40:
e
of 70 Bq/g (2F3 pCi/g). Lath sample will consist of concret inaterial from four. two inch core
samples and enough water to make a slung consistency. 'Ile distribution of radionuclides is haled on
previous concrete samples taken from the below grade Fuel Storage Basin that would also be
representative of these concrete samples.
(jivgn::
Cylinder Vulurm = nr'h Radius of camrlete corer) = I inch
Concrete Density = 2.35 g/cm' Height of c:cee samplc talcen (h) - U.25 inches
27 pCi = Bq Maximum dimt reading on core = 400,000 dpm/IUOcmz
222 dpm = pCi
Calculations:
V-(3.14)(1 in.)-(025in) = 0.78in'(16.4cm'/irrj(4 core samples)=512 cm'
(400.000 dpm/51.2 cm) (cm' 12.35 g) = 3.32E3 dp Wg
3.321:3 dpm'g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 841g
Conics:
S. 0. Marske X5-53
P. A. Newman X3 -4 1
RadCon Engineering File/LB XO-23
Document and Into Services 110-09
Cotltsatration (tom/0
2.55 pCifg
1.2F3 pCi/g
4.95 pCilg
7.513 -1 pCi/g
2.55E2 pCi/g
7.5F.-2 pCi/g
1.5 VQr
1.461'3 PCi/g
X090

Figure 1
SAMPLE CHECK-IN LIST
DateTme Received: 3C//11'0 ICES 14 t /^ SG#:_ ^ 2 ^^^^
Work Order Number. 0 t ^^`T SAF #-
Shipping Container 10: ^ C ^ h h6^ Chain of Custody # L - (L
1. Custody Seals on shipping container intact?
2. Custody Seals dated and signed?
3. Chain•of-Custody record present?
4. Cooler temperature
5.
Vermiculite/packing materials is
6. Number of samples in shipping container.
7. Sample holding times exceeded?
8. Samples have:
J tape hazard labels
_custody seals app ro priate sample labels
9. Samples are:
V .n good condition leaking
broken have air bubbles
10. Where any anomalies identified in sample receipt? Yes f 1 No [ -,/
11. Description of anomalies (include sample numbers):
Sample Date:
Telephoned To: On gy
N,
PFSH-SOW-93-0003
Revision 5
Yes [+40 11
Yes ( `el^4o (1
Yes ( No [ 1
Wet [ 1 C ry tTr G-( ,
Yes (I No (I
LU9`

Client Sample Screening Results 3 l0
10-Mar-98
CLIENTCODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCPMB
bhi BON682F 3/10/19981:05:00 PM QUAD2IA 3/10/19983:01:18PM BON682F 30 Is 0.56 69 1.5
1
/ I LIQUID Bkt: 3/10 1 1998 8:43:51 AM BKG 100 4 0.04 80 01
A nt Date: 3/10/1998 Tut Sa, Alq: 1.80E 4 00 , LOOE+01 Alp; (Dpm/ 1.89E+00 (uCV 1.53E-04 (pCV 8.51E+01 ± 3.1E+01 CAT 2.9E-0 1 Lab
_
Ppl mt: 1 L5 Unite: L 3' , ml Bet; Alq): 2.79E+00 So): 2.26E-04 Lit): 1.26E+02 + 2.6E+01
I I^
4.0E-0f
Alq
ut
Ant De / 0/1998 Tot a, Al 2.000
pt m!;: j Un 13;/L
1.00E+0 AI (DpM 0 L^+00 ( 'V O.00E (pCV .00E+00i* Num! CAT 3A)E+00 Lab
I
ml 1A; q): O.00Et00 )3^0.00E+00 LIlU :OOE00 ± qNu ! -^ 2.OE00
1.
Bill -BBN68'2S 3/10/19981:05:00 I'M QUAD2 1 B 31 10/19983:01:18PM DON682S 30 937 31.2033333 87485 2913.2167
^O(o$3 5
SOLID Bkp 3/10/19988:43:31 AM BKO 100 3 O.OI 93 0.95
AM Date: 3/10/1998 ToISa,Alq: 2.00E+02 9.15E+01 Alp; (Dpn3 2.39E+00 (uCl/ 2.35E-03 (pC9/ 1.18E+01 +6.3E+00 CAT 4.3Et00 Lab
Ppt nq: 91.5 1 1,11 13: g / m8 net; Alq): 6 49E43 Se); 6.39E100 LIt): 3.I9E 4 04 ± 1.1!102
111
'v_ 3.1 F.-03 Alq
LIt
Bill BON683F 3/10/19981:05:00PM QUAD2 1 C 3/10/19983: 01 :ISPM BON693F 30 127 4.13333333 9212 306.17667
M LIQUID Bkg: 3/10/1998 8:43:51 AM BKG 100 10 0.1 89 0.89
An] Date: 3/10/1998 Tot Sa, Alq; 1. 11 0E+00 1.00E+01 Alpi (Dpm/ 3.34E+00 (4C7/ 2.71E-04 (pCY/ 1.lIEw2 f3.4Ew 1 CAT 1.7E-0 1 4b
Pptmt: 7 3 Units: 1, 3 ml Bet; Alq): 6.06E+02 So): 4.91E-02 Lit); 2.73E+04 ±2.8E+02 I (/LBE-0 7
^C
Bill BON683S 3/10/19981:05:00 PA1 QUAD2 11) 3/10/19983:01.18 PM LION683S 30 5 0.02666667 75 1.68
g0^68as SOLID Bkt: 3/10/19988:43:51 AM BKG 100 14 0.14 82 0.82
' 1 1 D Anl Datc 3/10/1998 Tut Se, Alq: 2.00E+02 J/
8.53E+01 AI p; (DpM 6.13E-0 2 (uCY/ 6.30E-05 (pCY/ 3.23E-0 1 ± 3.3E+00 CAT 1.2E+02 Lob
'll
Pptmt: 85.3
Units: g mg Bet; Alq): 3. 72E+00 Se): 3.93E-03 LIt): 1.96E+01 ±3.6E+00 I L S.IE+00 AIq
I-It
LI
1 U-.1 far-98 Quanterra Environment Se rvices, SCP V2.83 I

(7--
C)
Client Sample Screening Results
11-Mar-98
®x)11 I^
CLIENT CODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
Bill BON684 3/11/1998 QUAD2 1 A 3/ 11 /19989:5104AM BON684 30 9 0.23333333 109 27716667
C -' LIQUID Bkg: 3/11/19992:34:24 AM BKO 600 40 0.06666667 517 0.8616667
Anl Date: 3/11/1998 Tot So, Alit : 2.00E+00 1.00E+00 Alp; (Dpm/ 1.04E+00 (uCB 9.38E-04 (pCl/ 4.69E+02 ± 3.9E+02 CAT 5.3E-02 Lab
Ppt sing: 49,7 Units: L ml Bet; Alq): 5.94E +00 Sa): 5 . 35E-03 LI8): 2.67E +03 ±3.4E+02 11.9E-02
BHI BON783 3/11/1998 QUAD21H 3/11/19989:51:34AM BON783 30 6 0.14333333 35 0.2383333
LIQUID Bkg: 3/11/19982:34:24 AM BKG 600 34 0.05666667 557 0.9283333
Ant Date: 3/11/1998 Tot Sa, Alq: 1.00E+01 1.00E+01 Alp; (Dpm/ 4.39E-0 1 (uCt/ 1.98E-04 (pCl/1.98E+01 ±2.IE+01 CAT 1 .3E 400 Lab
Pptme: 0 Units: L , ml Bet; Alq): 3.72E-01 Ss): 1.68E-04 LI8): 1.68E+01 ± 1.7E+01 I 3 .0E+00 LIC
C) 11-Mar-98 Quanterra Environment Se rvices, SCP V2.03 1
'Iq

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST 698-061-06
Collec Compan) Contact Telephone No. Project Coordinator Data Turnaround
It Pahlbcrg ^(,(
Steve N1a rske 373-4316 WEISS. RI_
Project Designation trampling Location 'AF No.
105-C Phase I k Phase II - Concrete Samplcs 100 Area B98-061
Ice If No. Field Logbook No. Method of Shipment
— Z
hand de li ver
Shippcd'IL ll,kc Property No. Bill of La t in /Air Bill Nu.
Quanlerru h 1 c0rpnmlad
POS9BLL SAMPLE IL\ZARDSBEM:A RKS
Itadluaclne
Jpecial Han dling and/or Storage
Presen'alion
Iypc of Container
rA
rv o,l=
No. of ('ontaincr(s) -
'plu m e
^^ /,
5.\MI'Lh: :V^.^ \\:\11515
Sample No Slamy ' Sample D at e Sample Mime
BON685 C)' Other Solid ^.- /_ 3
P
I1.
Sae uanlll nl
Inwua arm
SPI'.('L\1. INS I fit l (' IONS
21 Days
Pare 1 !
( \IN OI POS.SI'.SSION Sigel/1 1 1'1111 Names SS, II
III II1'M.lal,,-o 110%ISI I Il IL cl l l.. ,id i. Nkc -7471- 1( V) . C hromlun, l 1c\-7106. SI SuIJO 11.
a= I't It enXO ,AI a .tut 1 Sp 'I ascot ( ]. C (6,11-60 I_ p v m sal u
L. 1.111

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-07 Page ! or !
( 'effector
R. Fahlhcrg rLJ(
Company Contact Telephone Nu. Project Coordinator Data Turnaround
Steve hlarske 373-4316 WEISS, RL
Project Designat en 'ampling Location SAF No.
105-C Phase 13 Phase II - Concrete Samples 100 Area B98-061
Ice Chest \'o.^l y^ p ^/1 r— / Field Logbook No. 3
Method of Shipment
J M "9` 10 _ ^L (land deliver
Shipped to
Quante ira IncogwraleJ
POSSIBLE SAMPLE IIA%ARDS/REI11ARKS
RaJiaaaivc
)ffske Property No
Prne rvat on
N..
Bill of Lading/Air Bill No.
N
"type of Container
P
Special Handling and/or Storage
SA NIPIL .-ANA L}'SIS
No. of Cunlalner ( a) -
Volume
IL
S ec aan (I I ,n
Spc ,xl
loroou,nos
21 Days
X03, ^C^ m
SanlpleNo. Matrix • SampleDale Sample Tinic rn, - S s - m R:j^ k>i d 9'p Fik'^,4?+.+i„^';}i• r ,'lfl r^'{t I+tom,,,(.`-^„t
SON686 N Other Solid - )^_ f/
^d 0 (]
SPECIAL INSTRUCTIONS Matrix
AIN 0 F POSSESSION
1, y shcJ N^
//]^
^S l ^^ V „^a
Sign/Print Names __
(1) ICI'Maa6- 6010A (S upen,acu)if eadl, Mercup-7471-(CV), Clo.on flex-)196,
key a - Ihre^unc 1'Ui^ 5080 1 1 SJ " (Ian aSlx -211, 1 Ce' 137 C bah 60 L ru( um 15 1 -
^^h.......,*1 1 : - I"s; - A" iv c,nn?JIla l,nc lhu r S.Iv
^^ i (
S
SE
S1
,I
-
-
-
So,i
SNuncn,
SoI,J
ucLmgm.L.J B. Inec lw^^
.^
" I " nqI.11wu„n
I

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -08 Page I f
'olleetur Company Contact Telephone No. Project Coordinator Data Turnaround
R. Fahlberg I Steve Marske 373-4316 WEISS, RL
Project Designation Sampling Location SAF No.
105-C Phase I k Phase II - ('o 11 crete Samples 100
Area LL — 1 3 B98-061
Ice Chest No. Field Logbook No.
L L - _ Z
Shipped 10
Quantcrra Incorporated
POSSIBLE SAMPLE IIALARDS/RE\L\RKS
xodioaclive
Special Handling and/or Storagc
p
^/p
S\1111'1,L AN, 1,%SIS
Method of Shipment
Hand deliver
Offske Property No Bill of Lad in /Air Bill No.
Preservalion
rvon.
'I ype of Container P
Nn. of Container(s)
V'nlu me
I f.
Sec i te m 10 in
Specul
Innmaiuns
"/`loll / c-^^
Sample Na Matrix Sample Dale Sample'I'ime ?'>'^Y'S^D:"itP, ,hst°eft';a ,M. Li
BON687 Other Solid S - - ^Y .^ U S ^Z C a
21
DAYS
A^,^
'.9nuv{c,,+pT'f'.`
SPECIA1. INSTRI1CI IONS Matrix
11 %1'% 01 POSSESSION Sign Print Names
fl) I(I'Alna6-eu II^A ltiupul^accl ll.eaul, Meaup- "TJTI-(CVj. Chroinmm lle^-T196,
s
9i
- S'11
- S

Environmental
Restoration FJ^C Contractor Team
D- mow+ A
Interoffice Memorandum a'
911 V
TO ' 1:). A. St. John r.0-19 DA TE ' hebruary 27.1999
n,•n:s'
See Below raOW S. L. Winslow
R ulCun Engineering
X'+-4 1 /531 -0 706
WJUECT: CURIE. FSTiMATE FOR SUPP1NC CONCRETE CORE SAMPLES
CCN: 05508lt
W° A 2Z'n
awl e0^ orb
The following calculations show that cur sunplawith a direct reading of equal to ur icss than
400.000 dpm/10(km' will be below the definition of radioactive mate rial as de fi ned in 49 CFR 173.40;
of 70 Bq/g (2F.3 pCi/g). Lach sample will consist of concrete material form four, two inch con
samples and enough water to make a slutr • consissncy. The diianhution of radionuclides is biped un
previous concrete samples taken front the below grade Fuel Storage Basin that would also he
representative of these concrete samples.
Given
Cylinder Volume = arh Radius ofco=cte core (r) = I inch
Concrete Density = 2.35 g/cm' Height of core sample taken (h) — 0.25 inches
27 pCi = Bq Maximum tEmt reading on core = 400.000 dpm/100cat"
2. 22 dpin = pCi
Calculations:
V — ( 3.14) (1 in.) `( 0.25ia) = 0.79 in' (16.4 cm 'in') (4 Lure satuplcs) = 512 cm'
(400.000 dpni/5 L2 cm) (em'/2.35 g) = 3.32E3 d;mlg
3.3213 dpm/g (pCi/2.2 dpm) = 1.5E3 pC'ilg or 55.4 Bq/g
ti1.W:dld
Percent Distrihution(`l) Concentration ( L Cih)
°Co 0.17 2.55 pCi/g
"'Cs 82 1.2F3 pCi/g
"lieu 0.33 4.95 pCUg
"'Eu 0.05 7.5E-1 pCi/g
°0Sr 17 2.55 112 pCi/g
"Ann 0.005 7.5E-2 pCi/g
139124111
Pu 0.1 L5- C
Civics:
S. Ci. Nlarske X5-53
P. A. Newman X1-41
RadC'on Enginee ring File.!LB XO-23
Document and Intb Services 110-09
TOTAL: 1.4613 pCi/g
Gido

Environmintil
Contractor
Contractor ERC Team
Interoffice Memorandum
TO' I). A. St John LO-19 DATE:
Sec 13clow
Corr=ration (pCi/0
2.55 pCi/g
1.2E3 pCi/g
4.95 pCi/g
7.5E-1 pCi/g
2.55E2 pCi/g
7.5F-2 pCi/g
1 5 OCUM
1.4613 pCi/g
373 °"79 F"-02
1^ebruary 27. 1999
At
nto+t: S. L. Winslow
RadCun Engineering
X34 1/531-0706
SU BJECT. C'URIF ESTIMATE FOR SJUPP1NGCONCRF.TE CORE SAMPLES
Job No. 22171
.^wY..YY.... b
D\.0 . -A
Ol e for
n v
CCN: 055088
.Su^w\Cob !I!0
The hollowing calculations Show that con: 5amplawith a direct reading of equal to or less than
400.000 dpm/l0(km' will be below the definition of radivactive material as defined in 49 CFR 173.403
of 70 Ay/g (2F.3 pCi/g). Lach sample will cunsistof concrete material itu n four - two inch co re
samples and enough water to make a slurry consL*ncy. 'Fhe distribution of radionuc lides is based on
previous concrete samples uJten front below grade Fuel Storage Basin that would also he
representative of these concrete samples.
(jiver:
Cylinder Volume = n r'h Radius of concrete core (r) = I inch
Concrete Density = 2.35 g/em `Height of com sumple taken (h) - 0.25 inches
27 pCi = Dq Maximum Jima reading on core = 400.000 dprn/IUOcaY
2.22 dprn = pCi
('alUUldlions:
V - ( 3.14) (1 in.)'(U 25in) = 0.79 in' (16.4 car/i n -')(4 cure simplcs) = 512 cm'
(400.000 dpnr/51.2 cm') (cm' 12.35 g) = 3.32E3 dpn/g
332L3 dpm/g (pCi/2. 2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g
ti1.W:dld
°Co
"'Cs 82
02 E
Percent Distribution(%)
0.17
0.33
'"Eu 0.05
"'Sr
17
W ,.iun
taoawPu
0.U05
0.1
TU'fAL
('ones•
S. (i. Marske X5-53
P. A. Newman X3 -4 1
RadCun Enginee ring File/LB XO-23
Document and Into Services 110-09
6 16.4.

Oate/7me Received:
Figure 1
SAMPLE CHECK4N LIST
~ ! ^^ I S Ll SGS Li ln Z^7S
(j
Work Order Number. ^1 ^^^^^L'^^^ SAF
RFSH-SOW-93-0003 -
Revision 5
Shipping Container 1 0: 51)1 90 Chain ofCustody # ^ 7^^ ^ – ^L ^ ^^^o ^ L ^
1. Custody Seals on shipping container intact? Yes [ ] No ( ^
2. Custody Seals dated and signed? Yes [ ] No [ 11^
3. Chain-of-Custody record present? Yes W N or( ]
4. Cooler temperature l
L)
S. Vermiculite/packing mate rials is Wet [ ] t ry (I
6.
Number of samples in shipping container.
7. Sample holding times exceeded? Yes [I No (I
8. Samples have:
tape hazardlabe
astcdy seals _appropriate sample labels
9. Samples are:
o good condition ­le akn9
broken have air bubbles
10. Where any anomalies identified in sample receipt? Yes [J'No [ ]
11. Description of anomalies (include sample numbe#
Sample CustodianlLaboratc ry: — L^_ ( a te: ^,
Telephoned To: On gy
I 'l

RFSH-SO W-93 -0003
Revision 5
Figure 1 _
SAMPLE CHECK-IN LIST
OateMme Received: nn `^ SG#:
b /^; ^nns^^
Work Order Number. 5^ ^ w tk i.^ tJLE'
Shipping Container 10: Chain of Custody -616
1. Custody Seals on shipping container irdact? Yes t /No (1
2. Custody Seals dated and signed? Yes l7 No (1
3. Chain-of-Custody record present? C Yes "b ( I
4. Cooler temperature
5. Vermiculite/packing mate ri als is Wet I! D ry ( -r'
6. Number of samples in shipping container:
7. Sample holding times exceeded? Yes ( ] Vo [ }
6.
10.
Sam s have:
tae hazard labels
^tody
seals _appropriate sample labels
9. Samples are:
in good condi tion leaking
broken _have air bubbles
Where any anomalies iden tifi ed in sample receipt? Yes (] No [,
11. Desc ription of aromalies (include sample num bers):
Sample Custodian/Laborato ry: ^jL 3/y1 ^J(Jjr`Z,/,/e:
Telephoned
IA
pp
C-1 03

n
Q 0 3 X05 Cy r,-) D 3-)6& - Zed
Client Sample Screening Results
11-Afar-98
/0 — rye ^^ 1
CLIENTCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSR NETCPMB
Bill BON685 3/11/199812:00:00 PM QUAD23A 3/11/19981:02:54 PM BON685 30 3 0.025 44 0.525
V I
LIQUID Bkg: 3/11/1998234:41 AM BKO 600 45 0.075 565 0.9416667
An] Dale: 3/11/1998 Tot Sa,Alq: LOOE 4 00 LOOI;f OO Alp; (Dpm/ 6.25E-0 2 (uCU 2.81 E-05 (pCl/ 2.81E+01 + 1.9Ei02 CAI' 8.9E-01 Lots
Ppl mg: 2.9 / Units: L ml Bet; Alq): 9.83E-0 1 So): 4.43E-04 Ljg): 4.43E+02
+2.OE+02
Bill BON686 3/11/1998 12:00:00 PM QUAD23B 3/11/19981:02:54 PM BON696 30 1712 57 127510 4249.4083
V LIQUID Bkg t3/11/1998 2:34:41 AM BKO 600 40 0.06666667 555 0.925
Ant Dow 3/11 1 1998 To1Sa,Algi LOOEt00 1.00E+00 Alp; (Dpm/ 1.50E+02 (uCU 6.77E-02 (pC7/ 6.77E+04 t2.3E+03 CAT 3.7E-04 Lab
Ppt mg: 95.5 UNb: L ml Bel; AI 9.32E+03 So): 4.20E+00 L 4.20E+06 + 1.2E+04
111
1.2E-06 Alg
F—^ l-hinr- vN 011 BnlerrB Envlrunmcnl Se rvices, SCP V2.03
G
I
I.IE-01
Alit
LI[

Client Sample Screening Results
12-Afar-98
CLIENT CODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
BBI BON687 3/12/1998
V
LIQUID 3
And Date: 3/12/1998 Tot St, Alq: 1.00E+00 3
Ppt m8: 49.6Units: L
/
QUAD21A
Bke:
1.00E+00
nil
3/12/199811 :01:02AM BON687
3/12/1998 12:01:04 AM BKG
Alp; (Dp W 8.39E-0 1 (uCl/ 3.78E-04
Be(; AIql^ 3.27E+00 Sal: ) 1.48E-03
30 7 0.18 74 1.54
600 32 0.05333333 556 0.9266667
(pC7/ 3 .78E+02 + 3.9E+02 CAT 3 6.6E-02 Lab
L le)^ 1.48E+03 + 2.8E+02 I 3.4E-02
Ci
H
C ( 12-Afar-98 Quanterra Environment Se rvices, SCP V2.03 I
Alit
Ide

^J
J
J
-T
Bechtel Hanford Inc CHAIN OF CUSTODY/SAMPLE ANALI'SIS REQUEST B98- 661 -09 pare ! ^( !
Collector
R. I'allbere
^y^
DD (A
Company' Contact
Steve Nlarskc
"I"elephone No.
373-4316
Plotter( Coordinator
WIiISS, BI"
Project Designation Sampling Location SAF No.
10?-C Phase I k Phase II - Cuncrcle Sanlplce 100 Area B98-061
Ice Chest No. Field Loghonk No.
_ — I '^ C3
Nlethod of Shipment
Hard deliver
Shipped In Offshe Propero No. Bill of I.Ad inll/Air Dill No.
Quanmrru Incorpo rated ^/
POSSIBLE SA NIPLE 11.1LA RDS/RF,NIARGS
Nadioaclir.
Special Handling and/or Storage
1. NN IA SIS
L) I Cam ^C'3 -) r' ^
Preservation
I ype of ( retainer
No. of ( onlatner(s)
\'olumc
_ 'U^^1.^ 5«mm Ulm
Symi.l
Lou„^o„„
w(
Sample NU. Nfalm Sample Dale smilplc I III1C
11_
Daw Turnaround
BON68B Other Solid ti' _ _ = (.i / _,:C .^ t J^- ^•' la C
C11kIN OF POSSESSION
^I
^< "I .1.111 ”L.
Sign/frill Names
LA
14ur. ^,I IIJ __ ^(,^ ( "1 _^
21
Days
SPE( I I I I, INS VIIC 1IONS Nlulri,
11) ICI' Rlela6 - I , ,iv, i v, Uu mieeccl II eud Nlacul 1411 Chnnmu^I Ile. - 1196
KVI.
111i.1.m , rXel 6:3 SC S4 ! /o - IS/
JJJ
^eC^nef^uyv^ -9^l C^rLbv^ -(¢
NeI )1,.dIt. Ueielwr, Necrncdill U.ue lum / i ^Vl
R .... yim...A H 'U,Ilc I Ka.anid lli Uem luu`
L.\I1111

Bechtel Hanforfl Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -10 Page i nr
Collector Company Contact 7 elephone No. Project Coordinator Data Turnaround
R. Fahlberg Steve Marske 3734316 WEISS, RL
Project Designation Sampling Location 'AF No.
105-C Phase I & Phase II -Concrete Samples 100 Area B98-061
Ice Chest No. Field Logbook No. 7
Method of Shipment
/ 7 / —/3 (D _ Z Iland deliver
'hipped lo Offsite Property No.. Bill of Lading/Air Bill No.
Quanterra Incorporated
POSSIBLE SAMPLE IIALARDS/RENIARKS
Radioactive
Special Handling and/or Storage
Preservation
'type of Container
No, of Container(s)
Volume
SANII'LE AN.U.\'SIS I^
Sa ucm fIl n
Speual
Innmciinns
3
r
II.
a^
21 Days
0 L, ''- G2
Sample Nn. Matrix ' Sample Date Sample Time ° ;, i u a ,, d; • '.J: ,.:. t'd. ."f .'^rtA`. `Ht :.Sr yB lkl . , :`° C' ' . + y rr_ ' . :' '..
BON689 V Other Solid -12 - 131S
SPECIAL INSTRUCTIONS Ma trix'
CIIAIN OF POSSESSION Sign/1' it][ Names S - s,,,1
(1) CPMemis- 6010A ISupnoxcl lLcedlMcraoy-/4/1-(CV), Chraniwn lien-/196. S[ - 5

Environmental
Restoration ERC ream
Contractor
Interoffice Memorandum
TO'' D. A. St. John LO-19 arc
nrua'
5).W:dld
Set; Below Fa"`
Percent DistrihutionM
°Co 0.17
(IT C." 82
132 E 0.33
'"Eu 0.05
A7Sr 17
'"'Ain 0.005
'''"'"'Pu 0.1
TDTAL:
T_ -^7n
l-ebruary 27.1998
S. L. Winslow
RadCun Engiw:cring
X341/531-0706
sualacr: CVRIK FSTIMATE FOR Stl1PP1N000NCUTF. CORE SAMPLES
Job No. 22172
v..,. J. A....r w
P.D. wA
CCN- 055088
ov IO.0
nn v.
tae w.
L..a. CeM 'rV
The IbIlowing calculations show that con; sampltswith a direct reading of equal to or less than
400.000 dpm/100cm' will be below the definition of riftwctive material as defined in 49 CFR 173.40-,
of 70 By/g (2F3 901g). Lach sample will consist ofcoacrctc material from four. two inch co re
samples and enough water to make a slurry consisxncy. '11w distribution of radionuclides is based on
previous concrete samples taken front the below Vade Fuel Sloragc Basin that would also he
representative of these cuncretc samples.
(jiven:
Cylinder Volume = nrh Radius of concrete core (r) = I inch
Concrete Density = 2.35 gJcm' height of core sample taken (h) - 0.25 inches
27 pCi = Bq Maximum &vet reading on con = 400,000 dpm/lUucalt
2.22 dpm = pCi
Calculations:
V-(3.14)(1 in.) `(025in) = 0.78 in' (16.4cm `/inj(4 van: samples) = 512 Lm'
(400.000 dpm/5 L2 cm) (cm/2.35 g) = 3.32E3 dpm/g
3.321:3 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 kg
C(Mics:
S. (. Marskc X5-53
P. A. Newman X3-41
RadCun Engineering He!LB XO-23
Document and info Services 130-09
Cona mtration (uC:V0
2.55 pCiig
1.2F3 pCi/g
4.95 pCiig
7.5E-1 pCilg
2.55E2 pCi/g
7.5F.-Z pCi/g
1.5 OCUZ
1.460 pCi/g
nl
0103

Environmental
Job No. 22172
Restoration
Contractor a,.n,. w,
Interoffice Memorandum"` w•~ a' iolt
n w
S WA
S~ Cod. !m
Concentration (pCi/")
2.55 pCi/,v
1.2F.3 pCi/g
4.95 pCi/g
7.5E-1 pCi/g
2.55E2 pCi/g
7.5F.-2 pCi/g
1 5 nCi/g
1.46L'3 pCiig
CCN: 055081,
r ERC Team -^- A ^°
TO; I). A. St. John 1.0-19 °ATL` hebtuary 27. 1999
' OM1'" Scc Below FROM: S. L. Winslow
RadCua Engineering
?634 1/531-0706
suuecT. Cl:R1F: FSTfMATE FOR SHIPP1NCCONCRETE CORE SAMPLES
The following calculations shnw that core s arnplcs widi a direct reading of equal trl or less than
400,000 dpm/ 1 00em' will be below the de fi nitionofradioactive material as defined in 49 CFR 173.403
of 70 Bq/g (2F3 pCi/g). Gach sample will consist of concrete mate rial from four, two inch co re
samples and enough water to make a slurry coruiSrncy. 'I-he distribution of radionuclides is based on
previous concrete samples taken front the below grade Fuel Storage Basin that would also he
rcprescntative of these concrete sunples.
Given:
Cylinder Volutuc = nrh Radius of caucrcte core (r) = I inch
Concrete Density = 2.35 elem' height of con: sample taken (h) — 0.25 inches
27 pCi = Dq Maximn m liwt reading on core = 400.000 dpnt/1 Wcar
2.22 dpm = pCi
Calculations:
V — (3.14) (1 in.) `(0 25in) = 0.79 in' (16.4 cm'/iii) (4 core samples) = 512 cm'
(400.000 dpm/5 L2 cm) (cm'/2.35 g) = 3 3 2E3 dtm/g
3.32L3 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g
51.W:dld
mCu
117
C.
Percent DistributionO
0.17
82
"`flu 0.33
1"Eu 0.05
1'Sr 17
'°'Ain
11 91'4U
Pu
0-UU5
0.1
TO rAi
Cn ies:
S. (J. Marske X5-53
P. A. Newman X3111
RadCun Engineering file. !LB X0-23
Document and into Services 110-09
0109

Figure 1
^I
Date/Time Received: `l
^.Z-
Q
^%1 ^v SGS.,
RFSH-SOW-93 -0003
Revision 5
SAMPLE CHECX-W UST _ v
Work Order Number.
SAF S ^(j CzQ3 ^j ^j–(,^¢ 1 -
Shipping Container ID: "K-R .
//}}
chain o(Qstody S ^g 3 Dot ^1 -09
^1rAq?,
1. Custody Seals on shipping contairx intact? Yes [q/No ( I
2. Custody Seals dated and signed? Yes B-INo (1
3. Chain-of-Custody record present? Yes ( No (1
4. Cooler temperature l
o
5. VerrnicufdeJpacking mate ri
als is Wet [ Dry k/l )—
in
6. Number of samples shipping cadainer.
7. Sample holding times exceeded? 2« Yes No [
8. Samples have:
tape `hazard libels
_____custody seals _approprieie sample labels
9. Sam les are:
in good condition Ong
broken Inge air bubbles
10. Where any anomalies iden tified in sample receipt? Yes (j No
11. Descrip ti
on of anomalies (include sample numbers:
Telephoned To: On gy
C,li^

Figu re 1
RFSH-SOW-93-0003
Revision 5
SAMPLE CHECK-IN LIST
S
Date^me Received: , ^I ^ l^^l / SG# l l^ ^l ^— 7
1
Work Order Number. SAF #: f5 1 — -
Shipping Container ID: Chain of Custody if
1. Custody Seals on shipping contakw intact? Yes [ 1,140' [ 1
2. Custody Seals dated and signed? Yes [I No ( ]
3. Chain-of-C ustody record preserd? Yes _ ,] No ( ]
4. Cooler temperature
5.
/` e
"7
VermicuWpacicing mate ri
als is Wet [ [ C ry (^
6. Number of samples in shipping cmtainer. c
7. Sample holding ti
mes exceeded? Yes [ ] No [ ]
8. Sa les have:
Pe
/ custody seals
hazard labels
_appropriate sample labels
9. —8mptes are:
in good condition leaking
broken have air bubbles
10. Where any anomalies identified in sample receipt? Yes [ ] No
11. Desc ri ption of anomalies (include sample numbe rs):
Sample Custodian/Laborato ry:
Telephoned To: On.
14
C11i

(7)
^ 96 . D3 1 C'-.n, 3
Client Sample Screening Results
13-Mar-98
( J
CLIENTCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NET CPMB
Dill BON698 3/13/1998 QUAD2IA 3/13/199810:21:17 AM BON699 30 9 0.24142857 57 0.96
O I LIQUID Bkg: 3/13/1998 1 :30:18 AM BKG 700 41 0.05857143 658 0.94
An! Date: 3/13/1998 Tot Se, Algl 1.00E+00 , 1.00E+00 Alp; (DpM 1. 21E+00 (uCV 5.45E-04 (pCV 5.45E+02 t 4.1E+02 CAT 4.6E-0 2 Lab
Ppt mg: 51.3 1^ Units: 1 1 ml Bet; Alq): 1.98E+00 Sa): 8.94E-04 Llg): 8.94E+02 ± 2.5E+02 I / 5.6E-0 2 Ni
Bill 130N689 3/13/1998 QUAD2113 3/13/199810:21:17 AM I1ON689 30 661 21.9790476 47335 1576.8733
OLIQUID Bkg: 3/13/1998 1:30:18 AM BKG 700 38 0.05428571 672 0.96
And Date: 3/13/1998 Tot Sa, Alq: 1.00E+00 1.00E+00 Alp; (DpM 2.19E+01 (uCB 9.84E-03 (pCV 9.84E+03 + 8.5E+02 CAT 2.5E-03 Lab
Ppt mg: 50 / Units: L / , ml Bet; Alq): 3JOE+03 Sa): 1.49E+00 Ljg): 1.49E+06 + 6.8E+03
IIt
/ 7.4E-05
MLIL
13 111 IION753 3/13/1998 QUAD2 1 C 31]3/199810:21:17 AM BON753 30 0 -0.0571429 84 1.9057143
SOLID Bkg: 3/13/19981:30: 1 8 AAt BKO 700 40 0.05714286 626 0.8942857
An] Date: 3/13/1998 Tot Sa, Alq: 2.50E+02 9.77E+01 Alp; (DpM -5.47E-0 1 (uC i/ -6.30E-04 (pCU -2.52E+00 ± 4.8E+00 CAT 2.5E+02 Lab
Ppt mg: 97.7 Units: g
/
/ mg Bet; Al Alq); 4.30E+00 Sa ) : 4.96E-03 L c)^ 1.98E+01 ± 3.2E+00 I / 5.0E+00
Bill BON734 3/13/1998 QUAD2 113 3/ 13/199810:21:17AAI BON754 30 8 0.20666667 77 1.4709524
SOLID Bkg: 3/13/1998 1:30:18 AM BKG 700 42 0.06 767 1.0957143
And D ate: 3/13/1998 Tot Sa. Alq: 2.50E- +02/9.60E + 01 Alp; (DpM 1 .31E+00 (uCit 1.54E-03 (pCV 6.16E+00 ±5 .6E+00 CAT HAE+00 tab
Ppt mp 96 Units: g mg Bel; Alq): 3.19E+00 Sa): 3.74E -03 Leg): IA9E +0 1 ± 3 . 1E+00 I / 6 . 7E+00
BIII BON755 3/13/1998 QUAD22A 3/13/1998 10:21:21 AA1 BON755 30 3 0.05571429 70 1.4004762
SOLID Bkg: 3/13/19981:30:26 AN] BKG 700 31 0.04428571 653 0.9328571
Ant Dale: 3/13/1998 Tut Sa,Alq: 2.50E+02 9.61E+01 Alp; (DpM 2.80E-0 1 (uCl/ 3.28E-0 4 (pCi/ 1.31Et00 +4.5E+00 CAT 3.8E+0I Lab
Ppt mg: 96.1 Units: g mg Bel; Alq): 2.98E+00 Sa): 3.50E-03 Ljg): 1.40E+01 ± 2.8 E+ 00
/
I l
Alq
Ll g
Llg
7.2E+00 Alq
LI g
13111 11ON756 3/ 13 /1998 QUAD22B 3/13/1998 10:21:21 Mt 130N756 30 8 0.20952381 66 1.2314286
SOLID nkg: 3/13/1998 1:30:26 AM BKG 700 40 0.05714286 678 0.9685714
AN Hate: 3/13/1998 Tot Sa, Alq: 2.50E+02 9.73E+01 Alp; (DpM 1.32E+00 (uCI1 I.53E-03 (p(7/ 6.12E+00 ±S.OE+00 CAT 8.2Et00 Lab
Ppt mg: 97.3 / Unitr. g / , mg Bet; Alq): 2.57E+00 Sa): 2.97E-03 LIg): 1.19E 4 01 + 2.5E+00 I / SAE+00
Alq
Llg
1^-s
^e
ra
13-h/ar-98
Quanterra. Environment Se rvices, SCP V2.O3

G_
Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-o61-I I Parc ! of I
Collector
n
J !-.. "'aIF=> ^ y qh+ / RQ - A
Project Designation
105-C Phase 1 A Phase II - Concrete Samples
ornpany Contact Telephone Nu.
Steve Marske 373-4316
Sampling Location 1_
10O Area (os -c IMP twvc 3
Project Coordinator
WEISS, RI,
F No.
098-061
Ice Chest No. Field Logbook No.
I
r L_ '3 UC1
Alethod of Shipment
Iland deliver
Shipped 'I u
Quanterra Incorporated
Bill of Lach/Air Bill No.
POSSIBLE SAMPLE IIAZARIIS/REMARKS
Radioaco,,,
Special Handling and/or Storage
SAMPLE ANALYSIS
Olfsitc Property No.
NA
Preservation
'I ype of Container
Nn, of ('oriminer(s)
/Vll/l"/
Volume
/ J
Nose
I I.
See imm I I)ir
Special
Insimcram
N
Data Turnaround
2
^ Days
-Ckk ivA 9 6-^)a425-
Sample No - >j /
rH 0
mric • Sample Dole Sample Mime - ..... ! }'t gr ,. .2
,,^, ..:
BON690 G I Other Solid (3 MA (Z^l t'^ fJ Li I c
SPECIAL INSTRIC I IONS
t'ILMN OF POSSESSION Sign/Print Names
.
(1) KTMndls- 6010A(Sop,rlrace) I Lead), Mercwy-7471-(CV); C'hrumlum Ilea -7196,
1t6 00p uhe li' lot 12541; Damns Spectroscopy Dam.Tu, Re ei B' Ddie,' n ICBs 6080 lA¢n D
IC smm-U7 Cobal"O,Eur pion-152,
^p
oop, n 191. 1. , u n-1551, A e,c un-241 I I , ¢ Ismoprt 1r000000 s.1c
^i NqR rCJLI^.^ 5 C
p %//
P c mq^^^.hcd lb _._ li ci cl n, 1

c)
H
1Q
Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 - 12 Paee !
Cullectur
`1
pp
+tam -per & l i) -r / ^a IN I
Project Designation
10 -C Those I k Phase II - conciew Sulllples
Company Contact
Steen hla rs ke
Sampling Location
10O Arca — I OS f- p Ilea ( +0 3
Ice Chest Nu. Field Logbook No.
EL -I IUA -6 L
Shipped 7L
Offs to Property No.
Ouanicrra Incorpurmcd
POSSIBLE SAi\IPLE IUZ\RDS/BENIARFS
Badioaciice
Special Ilandthig and/or Smreac
BON691
^03^G CAM
Simple No I I I )
O.^
S:k1I 1 1.1;
AN%11SIS
h1A
Prnscrcaliun
Telephone No.
373 -4316
Project Coordinator
WEISS. RL
SAF No.
B98-061
Method of Shipment
Iland del I%er
Bill of Lading/Air Bill No.
w^
Data Turnaround
we -_--
2 nays
'1'1'pe of Container i 1
Nu. W 1loth... r'I'1^1 I _.
\'plume
IL
see ueni lu in
sn=.ml
^03r^ 4^ - i^^(n( Ll-
Iri% a .tialllple Pate Sample I II11C
Other Solid 13 M RR ^/ Q ^(J ^^ —?
--
_ -
L
- -1
l I
l f
SPLCUL INSIRI I - IONS Main
( HAIN OF POSSESSION Sign/Print Nit s s,,,i
1111CI'MUa6-onl uq lS,ipuvecq lead;. Al t..... 74al- IC VL C6mauum lien-7190_ g. Spa
Ita-1 ^,,,
,d i, n,
Nd nq ,I .J
n Jp le4 1 UaI, Imm Re Dmclm,. I('0 - 8080 Ioi I I4 l ,G.iiiiin,i Stearn,- pp 1- in-13 7, C pbah60_f I n-15?- do s..i
P 1 in-I,I P -hit A u_}i I. I. P . I I I ue I.ul, pl. li I i. Sale V r..
^CQ,eC/L
13H92
yg b3^ ^- .C- /3 )
- -- u.l- I ^„e p^ 'd - ,, .Ie 1,^^e I UC/cp-Y^., SelPn.If CM -7^1^ N^^jEe/-103; Sr-^FJ, ^I ,I ^
90 7 15
Te ^^lef L(^ ^q ' L'arbon -l¢
ff
III, I- 1 m, ken nl P7 Ualc I me "ic v
Hehn.pu,h ed ii, )a” lime Itacmled It, I)mo 1111,
/ ^ ^ / /N ^^ nl I
J3 I lu
1—k \I (11(1 ft li. Inl. Dmc'l iiim
Sf f l ION
--
F IN \L 5 \\II'L f;
UNI I ISI I If IM1
U,pu..d nl.n,.,.l -. -.. - - - - b,p„^ I ^^ - -
-
-
Uaie I ne
,u o q
i- ^x
of
i y...a..

Environmental
Restoration ERC Team
Contractor 1>.D. WA
CCN: 055088
fob Vo.2zt72
W^^A^ a
Interoffice Memorandum a' ^'' w° iWA w^ ran ^
S C
SMw•CoA 11!0
TO: D. A. St. John LO-19 °ATE: I ebnwy 27. 1999
Scc Bclow MO.% S. L. Winsl ow
RadCuu Engine ering
X3-41/531-0706
suuecT: CURIF. ESTIMATE FOR SJUPPINCCONCRETFE, CORE SAMPLES
The following calculation simw that core sampleswith a direct reading of equal to or less IlLin
400.000 dpm/1 00cm'will be below the definition ofradivactive material as de fi ned in 49 CFR 173.40;
of 70 Bq/g (2F3 pCl/g). Lach sample will consistofeoncrete mate rial from flour, two inch core
samples and enough water to make a slurry consisrncy. 'fhe distrihutiun of radionuclides is hased ern
previous concrete samples taken front the below gmdt! Fuel Storage Basin that would also be
represcniative of these cunercic samples.
'iven:
Cylinder Volume = nih Radius of co acte core (r) = I inch
Concrete Density = 1 35 g/cm' height of care sample taken (h) - 0.25 inches
27 pC; i =13q Maximum Jana reading on core = 400,000 dprni i UUcni'
2?2 dpm = pCi
Calculations
V — (3.14) (I in.)'(U._5in) = 0.78 in' (16.4 ctrl'/in^ (4 care santplcs) = 51? cm
(400.000 dpni/5 L2 cm') (cm'2.35 g) = 3.32E3 dim/g
3.32L3 dpin"l; (pCi2 2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g
SINAld
Percent Distribution(%) Conceatration (VOW,
nCo 0.17 2.55 pCi/g
"'Cs 82 1.2F.3 pCilg
'''lEu 0.33 4.95 pCi/g
"'Eu 0.05 7.5E-1 pC ilg
°"Sr 1 7 2.55E2 pCi/g
SA'Atn 0.005 7.5E-Z pCi/g
'39n 'Pu 0.1 1 5 nCU
Co ics:
S. G. lvlarske X5-53
P. A. Newnlatt X:>-4 1
RadCon Enginee ri ng FildlLB X0-23
Document and Into Services 110- 0 1)
TU'fAL_ 1.46U3 pCi/g
61 115

Figu re 1
SAMPLE CHECK-IN LIST
DateTme Received: d 3 51 Sc'k W uOb/^2 S
Work Order Number.
0^
Shipping Container ID: '^ ^ Chain of Custody #
SAF # 13 I JGG-QP
RFSH-SOW-93-0003
Revision 5
1. Custody Seals on shipping container inta ct? Yes ( q-,K o
2. Custody Seals dated and signed? Yes (q- o
3. Chain-of-Custody record present?^ Yes ( o ( ]
4. Cooler temperature
5. Vermicurde/packing mate ri
als is Wet (] D ry
6. Number of samples in shipping container.
7. Sample holding times exceeded? Yes [I No 14--'
8. Samp have:
tape _hazard labels
custody seals !approp riate sample labels
9. Samp are:
ii^n good condition leaking
broken have air bubbles
10. Where any anomalies identified in sample re ceipt? Yes [ I No [q--^
11. Descrip tion of anomalies (in cl
ude sample numbers):
Sample ate: 6
Telephoned
?4
G.

H
Client Sample Screening Results
13-Mar-98
l3-Afar-98
03^^3 LIB i^ 03,E 40 ".
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
Blil BON690 3/13/1998 QUA 1324B 3/13/1998 1:15:37 PM BON690 30 7 0.17619048 71 1.3838095
D' LIQUID Ilkg: 3/13/1998 1:30:14 AA1 BKG 700 40 0.05714286 688 0.9828571
Anl Dale: 3/13/1998 Tot So, Alq: 1.00E+00 1.00E+00 Alp; (Dpi/ 5.84E-0 1 (uCB 2.63E-04 (pCl/ 2.63E+02 ± 2.6E+02 CAT 9.5E-02 Lab
Ppt me: 1 1 5 Unib: L MI Bet; Alq): 2.64E+00 So): 1.19E-0 3 LI8): 1.19E+03 ± 2.5E +02 I / 4.2E-02 Alq
LIE
Bill 13ON691 3/13/1998 QUAD24C 3/13/19981:15:37PM BON691 30 2 0.00666667 30 -0.002857
dZ- LIQUID Bkg: 3/13/19981:30:14 AM BKG 700 42 0.06 702 1.0028571
AM Dote: 3/1 3/1998 Tot So, Alq: I.00E+00 LOOE+00 Alp; (Dpm/ 2.02E-02 (uCV 9.12E-06 (pCU 9.12E+00 + 2.0E+02 CAT 2.7E+00 Lab
PplmB: 1.5 / UNin: L / , ml Be(; Alq): -9.36E-03 So): -4.21E-06 LI8): 4.21E+00 + 1.6E+02 I I.OE+00 Mq
LIE
Quanterra Environment Se rvices, SCP V2. 0 3
p

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES T B98-061 -I6 PaRe
Collector/ /
a/t r4 J1 RAld
Project Dealgnation
105 -C Phase 1 R Phase II - Concrete Samples
Conlini ('unlact 7 elepbonr No.
Steve Maroc J7J-4716
ampling Location
I OO Atea
Project Cnordinalnr
W11S. S, lit.
AF No.
1198-061
I" Cheat Na Field Logbook No. .Method of Shipment
Mpped To
Quanterra Incorporate)
POSSIBLE SAMPLE IIAZARDS/REMARKS
Radloaetiv<
peclal Handling and/or Storage
{land deliver
Offsiie Properly No. hill of LadinR/Air hill No.
Prese rvation
T) or of Container
"°^°
No. of Cnnldner( s ) 7
Volume
s^^^ Ce)Da^7S
SAMPLE ANALYSIS
^03a ^'•I m g03X7,)- PC,4
Sample No. Matrix • Sample Date Sample lime
1. O Z Other Solid 3 —/6^ f U
CHAIN OF POSSESSION Sign/Print Names

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-14 Page 1 of !
Collector company Contact Telephone No. Project Coordinator Data 'turnaround
to o+Mhrr 3 A!11 /1 Steve Marske 3734316 WEISS. RI.
4 I
Project Designation /'\,
Sampling Location SAF No.
105-0 Phase 1 & Phase 11 - Concrete Samples 100 Area B98-061
Ice Chest No. Field Logbook No. Method of Shipment
Hand deliver
- hipped To Offske Property No. Bill of Lading/Air Bill No.
Quanterm Incorporated
POSSIBLE SAMPLE HAZARDS/REMARKS
Radioactive
S pecial Handling and/or Storage
S.-vNIPLE AN'AIA SIS
Preservation
Nape
T) pe of Container P
No. of Container(s1
A'olume
u.
sec eem al i ^^
Special
Inswnlo^.
Sample No. Matrix Sample Date Sample How .. .»r a __ .., ^
BON693 02 Other Solid ._ 6 p
21 Days
CII N OF P SS.FSS ON
R
^ery^^ pl
y D
^ ^
I?/ C
Sign/Print Names
A ^
h^
IJate'I c
2
/
?/
//'
/_
SPECL%L INST] tIONS
fll lU'Meia6-bU1041Jupenrao 1, 1.cad;-Memw.-74-1- ICVL Chronmunlie'- 71 96.
PCBs roscopv Q,smm-137_ Cobalt-60, Lawtalim-152.
Furop um I ^1 Cumpwm I n Ai enaum-?GI Imtopie Plwmuum. Isotopic lJrann lm_ Sale
^ /
/^
(Aj"V( — /^/3^ 9
s
St
s0
Si
Matrix
Snit S.Emc^
-- Solid
= Sluay.^
6v Relinquished By Ua le71lnc Rece . ced B1 ^ryVL'^
lI..CC.. t_
)ale.Time l
^^—^ ^^— ^^_ ^r -
1)
t
- N'a^a
- Olt
Reli ted BS hale I mx Rewncd Bc Dale-lime
echne-h'urv^ - `I q
J
r, 4

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-15 F! ,f 1
Collector /^^ 7
ISr1`fq .v+
^,y {^ (
Project Designation Sampling Location
1051' Phase I & Phase II -Concrete Samplcs
100 Area
Compa nN Contact Telephone No.
Steve Marske 373-4316
Project Coordinator
WFISS. RL
'AF No.
B98-061
Ice Chest No. Field Logbook No. Method of Shipment
Hand deliver
Shipped I o
Quanterra Incorporated
POSSIBLE S,\htI'Lf: 11:\Z.\RDS/Kt:\I:\1265
Radioacinc
)(life Propert N .N o. Bill of Lading/Air Bill Nn.
I'rescn'alion
Tcpe of Container
No. of Cunlainer(s)
pecial Ilandling and/or Storage \. 1 rent
nonr --
II.
s.e urin U i ^
spe^al
SA M P[ E ANA 1.1 S IS °51N°°°`
^03^? X11 Cl^ rti1 ^D^^^^^ ^^(
Sample No Matrix " Sample (late Sample Time J- .. --
BON694 03 Other Solid
l)
S G
N
Data I urnaround
S / }L
21 Days
SPECI:A1, IN'STRt'CI IONSNtaulx
CI P IN OF 'OSSESSION Sign/Prins Names
F / _ IulclNt 1 i. e 1 A.NI, ", - I I( I a rr,.
s. ,.a,,.
Sel ui' ^
I
N.^^,^J
qq pp )a l e linen kece b, Ual is I'( 11 41 80 1io i 1 Cin AI CCrtrs op C Is'. t b h 60 ( uuopiiiiii I'' so s.^
I.i ,hr .............^.:, ni..ic ._'41. I. n.pJlrno 6nopicLen n
N-CLLL /b ^p'lyC^ lZ/5 C
SJ< SI ,i1ue
^7 q
keLnquahed lac __-- Uom llmc aca-n u113.Deie'Iim^
--7,7.
^^
l/lM
rl f "^ {
CC..^^ I
clinqunacd I{, iLeo Ilwa kecur cJ b, Uam linen °`'r r { l//ti-e b^r / -
ehnyuuhN U. Unir lnr,^ Remir ad I4 hntc lnn^
S1. C [ ION
FIN.AI. tiA AII'Lt_ U I d Ata h o a
DISPOSII ION
_
1—all-
/ A G^ 3 , cJ//.^
_ Unl .cJ B Uuc I unc
Ua In.

Res Environmental
Hestoratlon
Contractor
^^^ Team
Interoffice Memorandum
M D. A. ^4. John 1.0-19
t 0M.N.
See Below
t'"TE:
IRON:
373 c'.17g
1^cbruary 27. 1999
S. L. Winslow AV
RadCun Engineering
X3-41/531-0706
SUBJECT. CURIF ESTIMATE FOR SHIPPING CONCKETE CORE SAMPLES
Job No. 22172
D. D. »-A
OC 10.c
q w
suww. cod. IM
C C N: 055OHN
The following Calculations show that core !iampleswith a direct reading of equal to or less than
400.000 dpm/l 00cm'will be below the definition ofradivactive material as defined in 49 CFR 173.40;
of 70 Bq/g (2F.3 pCi/g). Lerch sample will consist of concrete material Bonn four, two inch core
samples and enough water to make a slurry consistency. 'Fhe dist ri bution al radionuclides is based on
previous concrete samples taken from the below grade Fuel Storage Basin that would also be
representative of these concrete samples.
"vet :
Cylinder Volume _ nr'h Radius of concrete core (r) = I inch
Concrete Density = 2.35 g/Cm' Height of core sample taken (h) - 0.25 inches
27 pCi = Bq Maximum tfrrect reading on core = 400.000 dpm/ 100cm1
2.21 2 dpm = pCi
Calculations:
V - (3.14) (1 in.) 4(U.25in) = 0.78 in' (16.4 cot'/irrj (4 care samples) = 51.7-1 cm'
(400.000 dpnl/5 1. 2 cm) (cm'/2.35 g) = 3.32EI dtm/g
3.320 dpm/g (pCi/2.2 dpm) = 1.5E3 pCUg or 55.4 Bq/g
SI . W Ald
Percent Distribution(%) Cortcentration (VCi/g)
"Co 0.17 2.55 pCi/g
137
Cs 82 1.2E3 pCi/g
02Eu 0.33 4.95 pCi/g
`Eu 0.05 7.5E-1 pCi/g
"'Sr 17 2.55E2 pCi/g
Z41
Ain 0.005 7.5F.-2 pCi/g
2J'U2 4U
Pu 0.1 L5 .i/
Co ies:
S. G. Marske X5-53
P. A. Newman X3-41
RadCun Enginee ring File/LB XO-23
Document and Into Services 110- 09
TD'fAL: 1.4683 pCUg
G1^1

Figure 1
SAMPLE CCK-IN LIST
Date/TlmeReceived: ^^ ^^^^^ SG#:
Work Order Number. 0 ^3 7
r
RFS H-SOW-93-0003
Revision 5
^ ^^0^ SAF #: oU^i -
Shipping Container lD: O) Chain of Custody # /^0 "(',&/-
1. Custody Seals on shipping container intact? Yes eNo
2. Custody Seals dated and signed? Yes KNo [ ]
3. Chain-of-Custody record present? Yes [>r No [ ]
O
4. Cooler temperature
5. Vermiculite/packing mate rials is Wet [I Dn/^^
6. Number of samples in shipping container.
7. Sample holding ti
mes exceeded? Yes [ ] No [4---
8. Samples have:
_ Llape
custody seals
hazard labels
appropriate sample labels
9. Samp s are:
n good condition leaking
broken have air bubbles
10. Where any anomalies identified in sample receipt? Yes [ ] No
11. Desc ription of anomalies (include sample numbers):
Sample Custodian/Labor/ UL ^^ Llj4
Telephoned To: On C/
I

Client Sample Screening Results
17-Mar-98
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
Bill B0HJI0 3/17/1998 QUAD21B 3/17/19989:38:04AA1 BOH1I0 30 11 0.32 107 2.6266667
SOLID Bkg: 3/17/199812:19:30 A61 BKG 600 28 0.04666667 564 0.94
Ant Date: 3/17/1998 Tot Sa, Alq: 5.00E+02 1.02E+02 Alp; (DpM 2.10E+00 (uC7/ 4.66E-03 (pCU 9.33E+00 ±5.3E+00 CAT 5.4E+00 Lab
Ppt mg: 101.6 / );nits: G mg Bet; Alq): 5.73E+00 Sal: 1.27E-02 LIg): 2.54E+01 ± 3.4E+00 I 3.9E00 Alit
Dill 13011/11 3/17/19')8 QIJAD21C 3/17/I9989:38:04AM 8011111 30 13 0.37333333 308 9.2816667
SOLID Bkg: 3117/1998 12:19:30 A11 BKG 600 36 0.06 591 0.985
An] Date: 3/17/1998 Tot Sa, Alq: 5.00E+02 9.95E+01 Alp; (Dpm/ 1.90E+00 (uCV 4.31E-03 (pCU 8.62E+00 ± 5.4E+00 CAT 5.8E+00 Lab
Ppt mg: 99.5 Units: g mg Bet; Alq): 2.06E+01 Sa): 4.66E-02 Llg): 9.32E+01 +5.9E+00 I , LIE+00 Alq
"It
BHI BOHJI2 3/17/1998 QUAD21D 3/17/19989:38:04Abi BOHJI2 30 12 0.34666667 212 6.1383333
SOLID Bkg: 3117/1998 12:19:30 A.\I BKG 600 32 0.05333333 557 0.9283333
And Date: 3;17/1998 Tot Sa, Alq: 5.00E+02 9.91E+01 Alp; (DpM 1.98E+00 (uCU 4.50E-03 (pCU 8.99E+00 ±5.4E+00 CAT 5.6E+00 Lab
Ppt me: 99.1 Units: g mg Bet; Alq): 1.36E+01 Sa): 3.10E-02 Llg): 6.20E+01 +4.9E+00 I ,- 1.6E+OU Alq
LIg
Bill BOHJ13 3/17/1998 QUAD22A 3/17/19989:38:08 AM BOH113 30 1 -0.0183333 346 10.638333
SOLID Bkg: 3/17/1998 12:19:41 AM BKG 600 31 0.05166667 537 0.895
Ant Date: 3/17/1998 Tot Sa, Alq: 5.00E+02 9.87E+01 Alp; (Dpm/ -7.95E-01 (uCU -1.81E-03 (PC[/ -3.63E+00 ±4.6E+00 CAT 5.0E+02 Lab
Ppt me: 98.7 Units: g mg Bet; Alq): 2.30E+01 Sa): 5.25E-02 LIg): 1.05E+02 +6.IE+00 I 9.5E-01 Alq
LIg
Bill BOHJ 14 3/17/1998 QUAD22B 3/17/19989: 38: 08 AM BOHJ14 30 20 0.59666667 670 21.385
SOLID Bkg: 3/17/1998 12:19:41 AM BKG 600 42 0.07 569 0.9483333
And Date: 3/17/1998 'rot Sa, Alq: 5.00E+02 LOSE+02 ,Up; (DpM 2.83E+00 (uCi/ 5.91E-03 (pCU 1.18E+01 +S.IE+00 CAT 4.2E+00 Lab
Ppt mg: 107.8 ))nits: g m g Bet; AI9h 4.74E+01 Se ) : 9.90E-02 L e): 1.98E•+02 ± 8.0E+00
I
S.IE-01
LIC
LIg
Bill BON692 3/17/1998 QUAD22C 3/17/19989:3808AId BON692 30 7 0.19166667 310 9375
LIQUID Bkg: 3/17/1998 12:19:41 AM BKG 600 25 0.04166667 575 0.9583333
AN Date: 3'17'1998 Tot Sa, Alq: 100E+00 1.00E+00 Alp; (Dpn,/ 2.40E-01 (uCV 1.08E-04 (pCU 1.08E+02 + 1.9E+02 CAT 2.3E-01 Lab
Ppt mg: 04 Units: I, ml Bet; Alq): 1.73E+0i Sa): 7.81E-03 LIg): 7.81E+03 +4.9E+02 1 64E-03 Alq
LIg
CI
F-+
T 17-Afar-98 Quanterra Environment Services, SCP V2.03
C.7

L^
T J
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B
BHI BON693 3/17/1998 QUAD22D 3/17/19989:38:08 AM BON693 30 7 0.16166667 117 2.96
LIQUID Bkg: 3/17/1998 12:19:41 AM BKG 600 43 0.07166667 564 0.94
Ant Date: 3/17/1998 Tot Su, Alq: 1.00E+00 1.00E+00 Alp; (Dpm/ 6.55E-0 1 (uCl/ 2.95E-04 (pCi/ 2.95E+02 ±3.7E+02 CAT 8.5E-02 Lab
Ppt mg: 512 / URNS: L -! ml Bet; Atq): 6.09E+00 So): 2.74E-03 Llg): 2.74E+03 ± 3.4E+02 I LSE-02
BID BON694 3/17/1998 QUAD23A 3/17/19989:38:12 AM BON694 30 6 0.11166667 57 0.8816667
G 3LIQUID Bkg: 3/17/1998 12:19:48 AM BKG 600 53 0.08833333 611 1.0183333
An] Date: 3/17/1998 Tot So, Alq: 1.00E+00 1.00E+00 Alp; (Dpm/ 5.45E-0 1 (uCV 2.45E-04 (pCl/ 2.45E+02 +3.8E+02 CAT 1.0E-0 1 Lab
Ppt mg: 5$. 1 UNta: L / ml deh, Alq): 1.78E+00 Sa): 8.02E-04 Lg): 8.02E+02 ± 2.4E+02
1
6.2E-02
LIIg
BHl B0N8616 3/17/1998 QUAD23B 3/17/19989: 38: 12 AM BON8M6 30 119 3.92 5799 192.32333
LIQUID Bkg: 3/17/199812:19:48 AM BKG 600 28 0.04666667 586 0.9766667
And Date: 3/17/1998 Tot Sa, Atq: 6.00E+00 1.00E+01 Alp; (Dpm/ 7.45E+00 (uCU 2.01E-03 (pCl/ 3.35E+02 +4.OE+01 CAT 7.5E-02 Lab
Ppt mg: 3.5 ,/ UNb: L ml Bet; Alq): 3.66E+02 So): 9.88E-02 Llg): 1.65E+04 ± 2.2E+02 1 , 3.0E-03
BHI BON8Af7 3/17/1998 QUAD23C 3/17/1998938- 1 2ANI BON8M7 30 23 0.71833333 107 2.6683333
LIQUID Bkg: 3 1 17/1998 12:19:48 AM BKG 600 29 0.04833333 539 0.8983333
And Date:
Ppt mg:
3/17/1998
5.9 !
Tot Sa, Alq: 6.00E+00 /
UNb: L
1.00 E+01
ml
Alp;
Bet;
(Dpm/ 2.18E+00
Alq): 4.79E+00
(uCl/ 5.89E-04
So): 1.29E-03
(pCl/
Llg):
9.81E+01
2.16E+02
±2.7E+01
+ 3.0E+01
CAT
I
2.5E-0 1 Lab
^-
2.3E-01
Alq
LIg
BHI BON8M8 3/17/1998 QUAD23D 3/17/199893812Abf BON 10,1 8 30 36 1.13666667 114 2.89
LIQUID Bkg: 3/17/1998 12:19:48 AM BKG 600 38 0.06333333 546 0.91
And Date: 3/17/1998 Tot So, Alq: 6.00E+00 1.00E+01 Alp; (Dpm/ 3.46E+00 (uCl/ 9.36E-04 (pCl/ 1.56E+02 + 3.0E+01 CAT 1.6E-0 1 Lab
Ppt mg: 3.5 / Un1b: I. / ml Bet; Alq): 4.83E+00 Sa): 1.31E-0 3 Lg): 2.18E+02 +2.9E+01
I /
2.3E-0 1
AI
Llg
17-,Liar-98 Quanterra Envi ronment Se rvices, SCP V2.03
!'^,71 i
LIg
LIg

1(`uanterra
Soria
BATCH SUMMARY/CHAIN OF CUSTODY
ANALYSIS A^ _MATRIX 0 TYW'R DUE DATE y -6 -`t
I^ R`t C-T--rnENr
WORK ORDER SEQUENCE # CLENT COMhom
J 03161 -1B
QCBATMFEACrENTMANK
6^+1
J N a. -ix QC BATCBMAIM BI ANK
J o b t b l -iM oQ
(circle)
J 2M or 2S
(fie)
D o3tbt -O^
!Sb3l6to\ J 1 `^
gu3 J$gO2
803 Zo(o O Z.
03 222.02
$03 Z'7 2_O1
Batched and QC updated bye on 3 •Z5-^
QC BATCHMAMUXREAC0;r
SPOM
QC BATC HMAIRDVREAGENT SPUKE
Duplicate ofSamo # $0 3 t b 1 01
Rec'd in Prep Lab by on Z" _W Sop# tLtF RCSot Rn'- 0 _
Rec'd in Sep Lab by v a/ on— Sop# Rn i
Rec'd in Sep lab by on Sop# Rte=
EDY ^P by
on `I - 3 - C
Sop# i^ i C h ,l C 5 U 0
^^ 11nn
rr %
by l an Sop# 6 ^Cl QQQ ^- Rid 6
Rec'd in C.R j 3 'T
Da ta Reviewed byon^ Sop# 6 Cr/ (sF?1^7. M-4 Z^
O riginal batch sheet complete akvl u n file to be filed with the FIRST listed work order number.
FORM NO.: RC-52.1/98. Rev. 8 2Faceo n^,G c
CRT
RPT u .TS = ^C^^S^ S(^ ^2u^ o s o^ O e yccw^ -^ nor rc 1 sA
CT
= \c0
GI^,,
c,T- =N 5 T = A-s p ^ ^ —

\^ ^c CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 10-Mar-1998
Page 1
' CUSTOMER: BHI SAMPLE DELIVERY GROUP
^p
11ATRIX OTHER ^ BATCH NUMBER
CUSTOMER
LIES ID DUP ACCOUNT ID COMMENTS
5A, A^
Ser)_
__°_______=====ESJA625 ---------- ==
To3^b1\S IQO129 )
1 ) 80316101 ESJA626 II BON680 O.000S6 8-
Pr.11/2 4 /91 91,11/29.98
2 ) sea t 6t62 6H f s vriooi
— '7t p?^16101
ESJA627 p.oco3' 73
J^AjCQTIONS (Initial !. Date)
9
1) INITIATED l ^ l !D 5) COUNTINC/MEASUREMENT LAB
SOPS) #
SOP (5) #
2) PREP LAB RECEIVED l9scY o.L 6) DATA REVIC:WED AND
ANALYTICAL_ PREP STORED
SOP(.`' .-) ;# {iy Np^So3 0
3) SAMPLE REMAINDER STORED 3-2S-7,y
SOP (s) I) , xo-
4) SEPARATION 1-AD RECEIVED
`iiiP i S) ,^
SOPS) #
_
--
UIZu

lV
V i
l ` ^Ulx CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 11-Mar-1998
1^I V Page 1
^Y •
CUSTOMER: DHI
SAMPLE DELIVERY GROUP (,^oaa-7.^
W0
j
MATRIX OTHER V -W/ HATCH NUMBER 03
1 )
2 )
3 )
CUS 1'OMER
OES ID DUP ACCOUNT ID COMMENTS
5 A, M*L
CS r^
80318402 E SJA628I BOP4's 3 0.00 0355
Pt.11 /24 / 91 81-11/24.98
863r "^' -I3PI^ 89)1684
ACTIONS (Initial & Date)
1) INITIATED
Wu-
^^
a) SCP(Si #
5) COUN T INWM-A- ,_RE', FNT . La
EDP (5) # _--
2) PREP LAD °E'`lVFD 6) 0-A-A R;-:'J(1- ED AND
- ---- ANfiLYT7CiiL FP,EP STORED
SCF(S) ff (^ H(mac SO 3^
Off,(• -
3) L E R E l , tA'_NDER S--0RE0 3.26siP - Qws
4) SEPAR?iTION LAC RE:_:=i`.'I)
soli (^) 's ..rte
iiUri 5; ii
V ti

CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1995
Page I
;j CUSTOMER: BHI SAMPLE DELIVERY GROUP 03 0,^
O
-a^/^/^-
MATRIX : OTHER ^ U -Ov I BATCH NUMBER 03 'a^
CUSTOMER
QES ID DUP ACCOUNT ID COMMENTS
SPrrwM
1 ) 0a296Q! — -BFII 900160w
2 ) 80320602 ESJAG29
Pr.11124/9' E%.11124.98
I BON636 0 .00083b
3 ) 80220 699 BI IT B6P 16E3
ACTIOj4S (Initial °. Date)
1) INITIATED ^A ^5) COUNTING/PIEASUREPIENT LAD _
nnj^
SOP (S) it /\j—) SOPS) #
2) PREP LAD RECEIVED 3-11^_ rl k a,< 6) DATA REVIEWED AND
ANALYTiCP,I. PREP STORED
SOP (S) 9t ?JSagC5o 'S--o
3) SAMPLE REMAINDER STORC{D -3 (,AP' °C
4) SEPARATION; LAO PECEIP -D
SO(' i S) It ... 4..
SOP (8) !1
SOP(S) #
Gl^^i

l)^-
G
U
CUSTOMER: BHI
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998
Page 1
SAMPLE DELIVERY GROUP
^(
MATRIX OTHER (^' BATCH NUMBER 03 o
CUSTOMER
QES ID DUP ACCOUNT ID COMMENTS
S ^ Aug
1 80322201
3 •^
2 ) 80322202 I BON689 0.000GS5
------------- --------- ------------ ----- - -- ------------- --
ACTIONS (Initial `z Date)
^^.)l/
1) INITIATED zo V1 ;51g9 5) C'UNTINC/MEA5UREi •1ENT LA3
SOP(S) # SDP(S) #
2) PREP LAB RECEIVED 3-L9- '^t 1' orc 6) DATA REVIEWED AND
ANALYTICAL PREP STORED
SOf (s) ;ir^ttg:cam
SOP(
3) SAMPLE REMAINDER STORED 3-_zb-Q Fos
4) SEPARATION 1- A0 RECEIVED
SOP(s) 4 J^
SOP(S? It
)n
6121

I ) ° 1 .
^1 -,CIlO
USTOMER: BHI
MATR D: : OTHER
- AMFL.E CELIVER' : .-R - 1 -11'
B A T:H NUM'-R
93
CUSTOMF_R
OES ID OUP ACCOUNT ID COMMEN-"5
Sl:- A JJ,4^
1 ) 80327201 D ' , - I 00116 172 C.000(o ^- 7
3 4 SQQQ' " a4 •arc n 01.i(-aa
--------
irtitiaL '< Dc'.:e
P, g L
1INITIATED Jo
"' S) C .^.^INTi": /;1-ASURE"iF_NT -`.3 —
EOP (5) # ^SOf (S `'.
2) FR=P LAB RECEIVED 1)-TA REVD: *WED AND
ANALYT'CiAl- PREP STORED
3) S-,^IPL.E R7- )T r•d nF--F c-I it L-
4) -cr ARri 1. i^fJ i_."' LV:_LJ
L6'^t W^
b0P(E` #
-
61;;0

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S^
BATCH SUMMARY/CHAIN OF CUSTODY
ANALYSISA--z-yr mmix dMINF-L DUE DATE -b- ct8
S w RRy
_ WORICORDER SEQUENM0 CLIENT coheAwn
J cJ-sI Fr 9 -IB QC BATCH REAG'FNT WAka
J N 14 ix QCBATCHMATRi 3-e&
I O 31&4 -IMot©
(ank)
j -2M or 2S
D O3 Zoe
(aide)
_off
QCBATCHMATRIX/R C NT
SPUM
^S 0:s t^401 03 zsR
^b -5 16102 1'4
$03 zo6ol b3 2 S^
^t7322201 -^' 1"
^O TJ 2'-1`l 01 bZ
$03 2 r ? bz
03
Batched and QC updated by ^ on 5-is -'JY
Rec'd in Prep Lab by -.p a on 3-t5 4
Rec'd in Sep Lab by > on-]?
Rec'd in Sep lab on
ED/^PP^y ^^ on Y- 3 -^^ S
^/ J
QC BATCH MATRDMMACENT SPHO
Duplicate of L ple #_3T3 zo 603
Sop# 1Z^cs1QCSr) Re47_
n,
Sop# ^1C^^C S^ Rn'^
Rev3
Sopy fZ i C N TIC JO^2 Retii
Rec'd in C.R. by on Sop# Red
Data Reviewed by on Sop#
L2Rna
^7y
Original batch shee and complete calculation file lobe Wed with the FIRST fisted work order number-
FORM NO.: RC-52,1/98, Rev. 8
IZ^ utj.T-s S PF 5^ ^^ 3/^UG^ C^
CT Tw nE = too Mw ^^G^ ^l _ p i /.
5'c__
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CT 1.rJS i = {^S Q^L
-
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l
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.
sA A.nK
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Sb3184i6 ESJA 6 13 -___-
___ 3o3 or LiL% IQ0188 1
ES JA614
Pr.11/24/97 81.11/24.98 _- --
5.LS
ESJA615 O.ou —
Pr.11/24/97 11.11/24.98
3'l9-zs DvL
(Z- mac. t"Z c So .3-0
3-25rih" oar
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ESJA616
Pr.11/24/97 EX. 11/24.98
' 0
w
S A, A.Ae-
rs
Gl 33

_ ^'^ ^'^ -GC S I D3- -
------- ------ -
ESJA617
__._ Pr.11124/91'5,11/24.98
SPF A^^
ESJA618 0•ozys --
ESJA61
Oo3Zo6o3 Pr 1112419'x•11124.98
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PA
ESJA620
Q ^
Pr. 11 124191II .11/24-98
^J(
3.x54('
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^QZSS
3-1911fi- out =
IZ ^Lh+RCSJ(Sb -- -
r
Odt------ - .
y
G1^^

^ Lk c^
U7^-ao j
ESJA621
Pr,11/24/91 88.11/24.98
ESJA632
Pr.11124197 81.11/24.98
On 1,
3— L'( —kt ouc,
R ^ N-2c So ^3^
3-251'i_Y p^^
G1-J6

cl
sp^ "A4-
ESJA623 O.C)?-Lk-7
Pr. 11/24/97 91.11124.98
ESJA624 0 - P- Z-14
Pr.11/24/97 81 .11/24.9 8
jo
2 5 --cL
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C%ivanterra
Emimnmlmd
Senxu
BATCH SUMMARY/CHAIN OF CUSTODY
ANALYSIS Peso MATRIX o ihF--e- DUE DATE q-C `t8
s^^ RRy
WORK ORDER SEQUENCE CLIENT COMMENTS
J oil Sr y -1B
bbl
QC BATCH REAGENT BLANK
1 f-i (4 -1X QC BATCH MATRIX BLANK
J t m l" -IM oQ
(Ckk)
J lq -2M or 2S
(cycle)
D 0 3 Z.ob ' 03
QC BATCH MATRDUREAGENT
SPIKE
So^1^401 03 zs A,
^b3l6toz
a la
$ p 3 z.obol 03 5 4
^IJTa?-Z2ol
N la
Fr 0 ,6 02
$03?rl?4b'z-
03
Batched and QC updated by w - on 3- 2. s-4X
Rec'd in Prep Lab by :]^ aL on-3 t°r 4d
Rec'd in Sep Lab by---O on ^' )
Rec'd in Sep lab by on
(E^/CPPT by Its on 3 C g
QC BATCH MATRM REAGENT SPIKE
Duplicate of Sample # %' 03 7. 06o3
S 0134 RICS-1QCSOV3 Rev#_
Sop#.0 ^r,^ ^'S 7
Sop#
Rev#
^/ 3/ ^t ( Rev#
Sop# _ !C ( (^ U 3 1 Rev#
Recd in C.R. by on^'^/9^ Sop#a1 C1711eDL,)X 9 Rev# J
Da ta Reviewed by on I I T Soo_ ^'C 2p-2— Rev#
Original batch sheet and omplete calculation fi le to be filed with the FIRST fisted work order number.
FORM NO.: RC-52,1/98, Rev. 8
Rf ^ urn= ^e_^(5r«
Lr T^ V-+^ = 2.00
C- T- =n 5T =
f-- L
G I J 8

-
3b3 fr`11B ESJA613
_ 3oswAIS I2HI225 1
ESJA614 p.pZio
Pr.11/24191 91.11/24.90
-Doc
"-° -
ESJA615 - _ -- --
Pr.11124191 6%.:1124.90
3-1q 1t F ova
^ \-ce+acSo%3-'Z:5
3•zs 1t^ o t
r^
p.ozi9
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ESJA616
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25 -`L
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-- - - ESJA617 - -- -p.OZd'1
Pr. 11/24/97 81.11/24.98
.---
_ - .5 zs ax
ESJA618
Pr.11/24197 81.11/24,98
-- - ESJA619
D032o603 Pr.11/24/97 81.11124.98
3 lg 'Uv-
c^^ ^H2cSOCs ^o
3^ZS-42r o^
N^
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- -----
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-- ESJA620
Pt,11/24/91 U.11/24.98
h I) S
R ^c uri c so ^S -o
J-zS `iFs^
O.O ZSS
Ll^^

-- -
_ ESJA621 O.OZ3`F
Pr.11/24/91 Br nne as
- -------- -. ESJA622
Pr.11/24/91 IX.11/24.98
R^ceF2c5a,3-^
3-2-5-tir o„ cl
N
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Olb /
3 -Zs 'Y
ESJA623 - --
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ESJA624
Pr.11124 191 31.11/24.98
R^^2cso^3^
3-25-`i e- out
5H- Avtm
Q' OZ^ 1
x_02 zV
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se.^
BATCH SUMMARY/CHAIN OF CUSTODY
ANALYSIS Pu00 MATRIX 0 TtW±j DUE DATE y-6-cLk
tip"( CS m wr
WORK CRDER SEQUA a # amir COmmem
J o 5 l b l -1B QC BATCH REA(EN M ANK
J N 1n. -ix QCBATCHMAMUSAW
J o 3 L 61 -imam
(dale)
J N 2M or 2S
(drde)
D o3ibt -Qt
p^Tj 16101 ^' 1"
go3 t8`{o2
8o3 Zob oZ
p3 22.Z02
$03 Z'7 L0^
Batched and QC updated by-^i ec on 3 Z5-%
3•
QC BATCH MATRDOMAGENT
SPIIKE
QC 13ATCH MA2RDORFAGENT SPM
Duplicate of Sample # $A 3 -IN lb
Rec'din Prep Lab by ^ on 3_ 19_4 Sop#RtCt Q-So13 Re,4 0
? C
Recd in Sep Lab by on 76 Sop# L' ^' C c yCJ
7 !^^IZ ^7 =e
/,'C S7v
Recd in Sep lab by on Sop# Rn:
PPTby
v
on-3 Sop# Zict^ t• 39 Rn= 1
Recd in C.R by on 31 3>1 14 Sop# r hi poa7 r R ^^
jptq-1- i--K
Data Reviewed by on 11' Sop#__ SC yam- JL,^i J
L
O riginal batch sheet complete calculation file to be filed with the FIRST Lsted work order number.
FORM NO.: RC-52, M8, Rev. 8
2^ w = e a-Z I SA
Gr S.v9 7 = i`kect
— { —
StH ^QAC ^, v.. ,S o^DRy cew.e...Tj ^o .— to Tel S-`/^^.^
6145

I
^3^^^
CHAIN-OF-CUSTODY B4TC1-i ANAL`(`.ilS RECORD 10-Mar-1998
D9Page 1
CUSTOMER: BHI E;At1P!_E DELIVEPY GROUP
MATRIX : OTHER ^ ^ BATCH NUMBER O^'Jbl
CUSTOMER
OES ID DUP ACCOUNT ID COMMENTS
.5,4 AuAI
( ^s"
__====3b3i6^=a ESJA625 _______-______-----=
So3i6l Ls14HI326 l
1 ) 80316101ESJA626 I BON6(30 p-0Ob36
ouStsio( ESJA627
2 ) F^p Pr.11/24/91 EI.11/24.98
3 •u
------------- ------ - ------------- --
ACTIONS (Initial & Date)
1) INITIATED^ 5) COUNTING/MEASUREMENT LAD _
SOP(S) # _ SOP(S) # —
2) PREP LAB RECEIVED 3 -09 4Y WI, 6) DATA REVIEWED AND
ANALYTICAL. PREP STORED
SOP(S) # ^icc+-¢cSO^b=o
SOPS) #
-3) SAMPLE REMAINDER STORED 3 -zc^r pn
4) SEPARATION LAD RECEIVED
90 p ( 01) f ^'^
S u p (F) 3
0146

)CUSTOMER- BHI
MATRIX : OTPER
OES TD
PUI;,O#
CHf;IN-OF-C'_! STODY SWCH ANALYSIS RECI ]RD 11-Mar-1998
^
q
SAMPLE DELIVERY GROUP
ID[ BATCH NUMBER
CUSTOMER
DUP ACCOUNT ID
S h Awe
1 ) BB8iB4i1 8i-ITr^OC BA^!E}-:^
^ .L 6 4Y
2 ) 80318402 ESJA628 I 1301,4 683 0.0003155
Pr.11/24/9 1 91.11/24.98
3 ) 8A8184HS 43itI3 ,-, --"-'3d
JJ^^^^//'^^
4it^ ^?S
Page 1
OL^Ts7F—
COMMENTS
RC TIONS (Initial !, Date)
Q
1) INITIATED ^^^ 5? c; UNTI'i^/MEASURE:`?ENT LAD
SOPS) # SOP (S) #
2) FREP LAB RE(,E T_ V F.) T S- k9 Y orL_-
SUP (`:) , ._ R^trf^4So ^3 o
3) 5=MPLE REi4Fl 17 ii'^:!* ST,-RF_O 3!Lb•^Y^ 4
4) SEPARATION t.:=,C RF.0=IV.0
,'tNALYTIC:'I_ PRE? STORED
SOPS) #
Ci^i

0 /qg
CUSTOMER: BHI
MATRIX : OTHER
1 )
QES ID
*41 PUISO 4-"
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1999
Page 1
^/^ SAMPLE DELIVERY GROUP
1319-v" ) BATCH NUMBER
booms
03 -xi.10
CUSTOMER
DUP ACCOUNT ID COMMENTS
SA- AWAi
------------------------
3-Lb
2 ) E303206O2 ESJA629 I BON6360.0O0£eb6
Pr.11/24191 8.11124.98
3 ) "QO32 B er6 5 514 r-^nTeaa^
3,Zy
------ ----------------------------------
A(^ TIGHS (Initial Datc)
1) INITIATED
l
1^l^D `a) COUNTINO/MEASUREMENT LAB
SOPS) 4k '/U1/V S7i'(S? m
2) PREP LAB RECE' !)ED 75-t- p yvc 6) DATA P.EVI.vJEE AND
ANALYTICAL_ PREP STORED
3) SAI•iPLE REiMAIitD'i--F ST'JR' r) S,Z6-9S
4) SEFARATION LAP RECEP.: L`
SOP (3) #
6:.40-

(^ ^Q
*#* PUISO*#
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998
Page I
CUSTOMER: BHI
SAMPLE DELIVERY GROUP
MATRIX
Q /p
OTHER Koo
/ BATCH NUMBER 03'(29,;?
1 ) s2ee
CUSTOMER
GES ID DUP ACCOUNT ID COMMENTS
SR A+A,l
3-x6 ,W
2 ) 80322202 I BON6E90.00o655
- -- ------- ------------------- - ----- ---------------- --
ACTIONS (Initial '< Date)
3
1) INITIATED "1^^ 5? t:'UPITINr/M,=AStRci iENT - 8 __
SOPS) if SOPS' it -
2) PREP LAB RECEIVED _3- (gkY o^ h) DATA REVIEWED AND
ANALYTICAL ?REP STORED
90F(S) is _1Z cH?cS^^3a
SOPS; #
3) SAMPLE REMAINDER STORFD 3 -26 -2 P c-t^
4) SEPARAT I ON _1;B PFi;= :`Jta;
9 0P(S) it ^A
SOP (3) ;i
6149

^ CHAIN- O=-CUST77-`'( B?TCI- ANAL''P'iS RECORD 17-Mar-1995
i l
Page 1
CUSTOMER: BHI SAMPLE DELIVERY GROUP
/I)/^ ^f
W(/^/
MATRIX OTHER kJ `s - Ob / BATCH NUMBER Oc/ -az l OS
CVSTOm
GES ID DUP ACCOUNT ID
5A. ANA-,
COMMENTS
(D rr>
1 ) 60327201 J " I BON692 0 •ooa^ 7
2 ) 80'12720 2 BI iI 3 uAYBON69a
3 )^B09272 39 BH; °"` 80W.694
'ur
6'4
3•zc
------ -------------------------------
ACTiO 0IS (Initial & Date)
1) INITIATEDO 5) C UN-I".=%i9EASURE''EMT Lr;3
SOPS) # __.J>!^ SOP(-) #
2) PREP LAB RECEIVED 3-( 9t -iY - 71^^ .
SOPSS) i) ^tc^+ac5y3 ^
3) SAMPLE REi"RI !')EP °.TOR-n
4) SEPARATION L.-'
:;C AP i ::^) nJ ^
r_ rc":; )
f,) 0,T„ REV r -_JED nMD
Ai'iALY-iCAI- PREP STORED
50f iS) #
Gl;,o

RPj
R 1'. ,'uanterra
s^
BATCH SUMMARYICHAIN OF CUSTODY
ANALYSIS o-o MATRIX 0M %V*, DUE DATE 4A-b-aS
S t-v RRy
WORK ORDER SEQUMgCE 0 C[ma COMMe (g
J-:3-S1&`4 4B3
O ^l I
QCBATCHREAGe rffiAW
J N 14 -I% QC BATCH MATRM SAM
1 031Fsy -1M ot©
(dide)
QC BATCHMATRUVRFACENr
SPIIM
J 2M or 2S QC BATCH MATRDORFAGENr win
D O 32'1 z..
Z Duplicate of Sample# $032'^ Zo z
80 TS 1t4o1 03 zsR
Fo3lbloZ
a la
$03 zo601 03 2 SA
^032Z201
.^ la
Fr0b z yy ol oZ
^03 Z'12bZ
03
Batched and QC updated by -DVc on 5-is-qY
Recd in Prep Lab bY- oc- on 3 -ter 4d
Sop#- '-uC C -U
Rev# Q_
Rec'd in Sep Lab by ^ .^ one^ - 36 SF Sop# &i &kf ,S 6 3 6 R--v# C`
Recd in Sep lab by
/CPPT by
pp
on
^
Sop#
Sop#
Rev#
i 3) Rev#
Rec'd in C.R. by f j ' a0 an Vw ^t Sop# a0»> r Rev# o
^n
Data Reviewed by i^ on' (^ GI gyp#
O ri ginal batch sheet an complete calculation file to be filed with the FIRST fisted work order number.
FORM NO.: RC-52,1/98, Rev. 8 S^
t ^x^ra c ^^ 2 ti c-Ait1C ^u3
= po- L /S ic^
LT S tV 5T = At5 PEC-
0151

_
S A-AuA-L
_-_-__ESI27495 --
X31 y`
` --
s_o y9
EQIE316
\
---__ So3 y _os
^fr`1_ 0.03^34ode,
lS .._... . _..,..,, fs a 1 -__ _ _-----_----- 5.ov^
—
ESI27496Ci•ozv3
_ ,. _
Pr. 73113/97 8x.:'_!13/9A 5.0 op 8
s ss•t
- ESI27497 6.0?z6 5 ^-7 1 ^ —
P [.1?! 13 / 91 3x,'.2!' 3'9B
2^c \+ec5^ \3 ^
r ^-
_
-
_-
G15

ESI27498
9r.12/13197 31.12 /13/9 2
r^
e+C
'-QUO 1
-vU •. JF;^ ^^ lrC _—__
5 A An Al
SPe
S-061-7
-
FE
c153

AN+_'.,1 PECCPD—filar-194(3
5 P, P ~ AIL
ESI27499 -- — o.ozS7
Pr,"/:: /97 ?a./:3133
S-ZA4r
ESI27500 - -- — -
_ O .o^4Z
l9 -4k
V^^c rFecSo i3-o
3-L6 ALP
61-34

^1 v F7- 1 ,f -
^cl C^
5{f A.AI
ESI27501 O•oab l -
Pr.12/ 11 '3,1
--- --- -
1 3a:12/13/98
..
S- 0 5 9 So
OdC-
- - - - - - - - ---
•xL'E1'
nl^^
- - - 3-Zl-q-a'
{ZlCµ2CSo^3^ ---- -- -
tiw
C 15

- _ ESI27502 0.0ZS1
Pr,12/13/97 Ba,12!13/93
ES I27503 G
Pr.;J'3/97 s"a 12/13/?8
3 -4t c^^
`tZ is t+^CCSa rS-o
_ —_ _ 3-^b 2k art
N ^'
S o(o 17
s 91 ^^
-.
_..---- -
6156

---------- ESI27504
..___L7o32'r ZO2 ESI27505
_
ESI27506
1-2b-4Y o«
^v
$ k "At
------ --- —
p.oz a6

BATCH SUMMARY/CHAIN OF CUSTODY
4 0 A A31s ut y0 MATPJX on-WA DUE DATE 9-6-9
T5R`( Cam WT-
_ F9 )P% CstDER
1 Va __._ _ _- —
l0 3 t 6 t -1M oQ
SEQUFNM# QgNf COMMENTS
-1B QC BATH REAGENT BLANK
-IX QC BATCHMATRIX BLANK
(arcle)
I -2M or 2S
(ar de)
Do3tbt -fit
^S17 -516 1 01 "' t °
gu3 1$`^oZ
8o3 Zob oz-
-6 2ZZOz
$03 Z'TZO\
Batched and QC updated by^cz_ on 3 -25-alr/
Rec'd in Prep Lab by on
Rec'd in Sep Lab by
74
Rec'd in Sep lab by on
3-
_ onoa -a C -9 F
Re
(EL)/CPPT by /b on q /3'q g
QC BATCH MATRDUREAGFNP
SPDM
QC BATCH MATRUMA(ENI SPUM
Duplicate ofsample #X03 t b t o l
Sop#RK-t''RCSot^ ReO Q
Sop^^IC,.^P[' .sago R^?Q
sops >2i CL-ec 57 3q Rcn'-
Rec'd in C.R by on Sops Rte=
Data Reviewed by / ' ^C^ ' p ^^
Cl k y Sops -1 L I ^^ C E ^c Z R-
Original batch sheet and mplm ration file to be filed with the FIRST' rioted work order number.
FORM NO.: RC-52. 1/98. Rev. 8 1 ^— Qxtr 2^- ., ,^
i
4 z w 5 R,CNQ^_ °3•.
5ET fRA^-no.J iS OF PRy ^c.w,a-..^^ n^oT 0^" l^rn{ SR.5-L6-`LS^
C^T^-J i2a D.ru.o c0`3"- -
R.PT llwtn = FCi-`spt CTTtw.Ec200 = IBS L G158

CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 10-Mar-1998
Page 1
CUSTOMER: BHI SAMPLE DELIVERY GROUP
MATRIX OTHER
N-1611
BATCH NUMBER (/'
CUSTOMER
GES ID DUP ACCOUNT ID COMMENTS
SA-AuAL
SI 7507
^3 \61^^ ` ._
_______=_______-___________________________
i S.oS fG
503161LS EQIE317 ^S_p3S'o•^26797 l 1 .5.03^"J.
1 ) 80316101 ESI27508 Pr.1211?191 37.1211i/9P
I BON680 C^-oOV376
S_ 0 S ]lp
2 RWI 89N68}
ESI27509
_____ O03t6101_?r..2113/97_°1.:2i'.'.r 19_____________
ACTIONS (Initial & Date)
1) INITIATED III 5) COUNTING/MEASUREMENT LAB
SOPS) # SOP (s) #
2) PREP LAB RECEIVED 3 _l q a k oc r- 6) DATA REVIEWED AND
ANALYTICAL PREP STORED
SOPS) #6 ^^t42LSo^3^
SOP (9) #
3) SAMPLE REMAINDER STORED
]UI ' 1 ^J ) iI N
4) SEPARATION LAD RECEIY[-D
^)O('iS? tt
6150

^CUSTOMER:
CHAIN-DP-CUSTODY BATCH ANALYSTS RECORD 11-Mar-1998
Page 1
BHI^^//
SAMPLE DELIVERY GROUP ^Oa375
MATRIX : OTHER 8q S-aj I BATCH NUMBER
CUSTOMER
GES ID DUP ACCOUNT ID COMMENTS
SA- A+.JkIL-
-------------- ------- -- ----------====^sr^^===___-----------------____
1 ) A01 8401SHI -- bo'^
2 ) 80316402 ESI27510 I BON603 0 -000 -6-70
3 )
Pr,1211 3 '7 7 38.11!11/P2,
3 ;4tY
S_ 05 7(p
---- - - ------ ----- - ------------------------
ACTIONS (Initial '< Date)
1) LNITIATED
SOPS) #t
3^^i I
^O
io— Y l
5) (;DtJNTIN>;'i1EAStJREPii_NT LaB
COPS) #
2) PREP LAB RECEIVED h) DATA RE4'I`. WED AND
AtdAL'f 1 lC A(_ PREP STORED
SOP (S) is 50k3--p
so? (5) #
3) SAMPLE REMAINDER STOR-D 3.2k_ -q^tPlk,
SOP (3) ii
4) SEPARATION LAB RECEIVED
FjOF' (3 ) ;i
^it;lJ

CUSTOMER BHI
MATRIX OTHER eq -G(; J
CHAIN—OF—CUSTODY BATCH ANALYSIS RECORD 12—Mar-1998
Page 1
SAMPLE DELIVERY GROUP -75
QES ID CUP ACCOUNT
1 ) sum
2 ) S0330602 ES I27511 I BON-5,96 0 -000 1r 'S9
raft
BATCH NUMBER O3 ^ T^ r
CUSTOMER
ID COMMENTS
so, ai m-
======
61- 71-01-45 (init=_a1 & Cate) -------- —
1) INITIATEC ^_^^^[^^ S) CCUNTI'dG%P! cA URE`IEiiT L:1L+
SOP(S) ii ^l/^ScP(5;
2) PREP LAD RECEI`.'ED, 6) PATH REVI:..iE_, AND
3) SAMIPLE iENl ii!DFR STORCn
`iOP(^ ) 4S I\ -
4) SEPARATION L A'_1 REi- El')' L)
u-,P(°!
G161

^ 3 CH A IN-OF-C'.JST^=^DY BATCH AN ALYSIS RECORD 13-i1ar-199 8
' `^
Page 1
` CUSTOMER: BHI
SAMPLE DELIVERY GROUP ^-Z5
MATR I X : OTHER
QQ ^n
l u w BATCH NUMBER
1 )
CUSTOMER
DES ID DUP ACCOUNT ED COMMENTS
32,i,R^'
2 ) 803?2202 ESI27512 I BQi•46og 0•0006(-2
v., 2i?' :1. 121 :3/ca
S,o3^a
— ---- — —ACTiDidB (Inii;iai '< Date) ------------ —
1) INITIATED h"_/ 5? C UNTi' ;MEAS)REi1ENT LAB
SOP(S) g 11^^ ^SGT ;Si k
2) PREP LAB RECEIVED 7 _' 1'1-1Y_16) UAia 'EviF:' E7 FiN_
Ai.IN^'r'T; ^AL °JE? STCRD __..__._
3) SAMPLE REMr^ T.N i )ER STORCO
4) SEPARA T: I,;N !. RCEI ij_i)
SOPS) #A —^'-
5CJl(cl. ^
50F'iSi sk ___
G16C.

II
CHr+I N -OF-C':JSTODY BaT(;H AN-CYSTS RECORD 17-Mar-199£;
Pa a 1
CUSTOMER: BHI SAMPLE DELIVERY GROUP W 0020
MATRIX OTHER( v" I BATCH NUMBER Da ^^
CUSTOMER
GES ID DUP ACCOUNT ID COMMENTS
SA• PNni
1 ) 80327201 ESI27513 I SON692 0-00066
2 )
3 Roaa7292 Bill--SON", ^4
-- - --
/r
03 i
ACTIONS (Initial & Date) -- --------- -
1) I NITIATED ^ ^. :' _ „'i1 ---
SOP(S) # 4 --
2) PREP LAB P,ECEIYED 3:x`1 F h) OAT= PEYI WED AND
ANALY 7 ICA1_ PREP STORED
SOP (S) R Ott 2C 13^
SOP (S) #
3) SAMPLE PENAINDEFR S?OR D __Zb_^LY OTC
4) SEPAR I) TION LAP, RECF-:IVF-0
GOYO i; ^
i70P (t ) i!
ciss

uanflerra
J o3I bt
S riaa
BATCH SUMMARY/CHAIN OF CUSTODY
AC ALYSIS MATRIX OTrWA DUE DATE y-6-9--
-r!,2Y CS=m Ekm
WORK OMM SEQUE NCE # CUENr COM1mm
QCBATCHREAGENTHIAMC
Afl, IX
EAC3- 26 -4 1
J N %x -1X QCBATCHMAIRIXEILM
1 o b t 61 -1M oQ
(fie)
on
I}
QCBATCHMATRDURFAGWr
2IM 844 C-oo 1
J N tA. -2M or2S QC BATCH MATRDURF GWr SPUM
Do3tbt _Ot
DSO -St6lo1 "' 1 a
gv3 L$`ao2
803 Zo(o pZ
03 2-2.?-Oz
$O3 z-7Z.0 \
Batched and QC updated by- - ^Dvt on 3 -Z5-ul
Rec'd in Prep Lab by -err— on 3 -w
Rec'd in Sep Lab
Dapii eate of Sample #g0 3 t 61 01
R tC+eCs0t-7 1
W-' R tc-t 5() Rn'--^_
Rec'd in Sep lab on Sop# Rey;
ED/CPPT by on Sop# Rn:
Rec'd in C.R- by / oa 3 2G Q Sop#
Data Reviewed by
Rev-,-
RIC /f 7 Reo O
n
r/ Sop#_f'(ZC Low) ^ ^
C-
O riginal batch sheet and mplete calculation fi le to be filed with the FIRST rived work order number.
FORM NO.: RC-52- IM, Rev. 8 C 00 nT -r k yr E = 4500jo u n., =m S:r= C ^ 2
JP, ^ tarn trs = ^CC / SA G-Lc Z5
CR'1
SR k pRy ^^ ^..- X02 ^, „o- ^^ s^
G1G^

CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 10-Mar-1998
Page 1
Li CUSTOMER: BHI SAMPLE DELIVERY GROUP
MATRIX OTHER BATCH NUMBER
QES ID
06% Ix
1 ) 80316101
2 )
ACCTIONS (Initial & Data)
1) INITIATED p^'I ' l 5) COUNTING/MEASUREMENT LAD
SOP(s) 0 IJ SOP(3) #
2) PREP LAD RECEIVED 6) DATA REVIEWED AND
RK rrR^SO^?'1 ANALYTICAL PREP STORED
SOP(s) # R \cHtccSo 13-0
SOP (S) #
3) SAMPLE REMAINDER STORED 3- 2-S-4Y o.^,
SOP(s) if r
4) SEPARATION LAB RECEIVED
L
DUP ACCOUNT
CUSTOMER
ID COMMENTS
SA oncE..+,y' (S i})
iw ====o..ems====e—=itai==o------s^^==o^
K FahE O rMr+h
SOP( cl ) 4
CO r\r Tiw f- _ 5 ) , I e-O =ZS) PC, /S^
1030
NfG cool 0-1 w.*. 91 %L" LSt (^N L6/y1fjP Q^^91D
BHI BON680 o4vruMtYY 103,0 C,z355 /-G zeoe "e
G. 16

Q^^- q' ^
CUSTOMER: BHI
MATRIX : OTHER
1 )
OES ID
CHAIN-OF-CUSTODY BAT -, F l ANALYSIS RECORD 11-Mar-1998
Page 1
^
j
SAMPLE DELIVERY GROUP
II BATCH NUMBER Vt/
CUS I'OMER
DUP ACCOUNT ID Sq COMMENTS
s A A. AA. aRTc
2 ) 80310402 BHI B01•4683 0.2z4utomacggottSG L( ^09^1
3 ) -86^^946aS•s5-tc OUTPn i n
1 , 14
i ON5 (I 1 1 i t i a l '. Date)
1) INITIATED _^/ 0 5) C7UNTIN,/MEASUREMENT LAB
SOP (5) # Xa E A SOPS) #
2) PREP LAD RECEIVED 3_IQ--4-K off_ 6) DATA REVIEWED AND
ANALYTICAL PREP STORED
SOPS) R __R>^+44 0 -^
3) SAMPLE REMAINDER STORE;U 3_25-4Y oaf
SOP ( S ) SI
4) SEPARriTIOfd LAB RE;; ['':) --
(,OVv7T T/ 01 e = 5U)
b, eo = 2s ) P G^S^
SOi'(^) #
6166

I J
CHAIN-OF-CUSTOD`' BAI --,- ANAL' . ' 'l i S RECORD 12-Mar-1998
Page 1
/ CUSTOMER: BHI Elid'IPI_E :DELIVE` : Y GROUP
MATRIX : OTHER p'(i(1 BATCH NUMBER d3-^
C US'r OMER
GES ID DUP ACCOUNT ID SA
1 ) X93=^ r_nt c 3.2.SA' NW; $HHthF3^
sR
COMMENTS
2 ) 80320602 BHI BON6061 (M' X 1wo o•'k 107 G3 Z6rh,^R9 g I /03
3 ) 89829 92 yHf E) E)
ACT! DO , ' ( Initial & 0.3t2)
J 7'
1) INITIATED ^^((^^ / ^^U 5) COUNTINOiMEASUREMENT LAD _
SOP(S) 4 _ND S^F'(5) #
2) PREP LAB RECEIVED 3_L^_Q o_rL_ 6) DATA REVI WED AND
2^rtac So Z-I ANALYTICAL PREP STORED
SOP (S) # _ i^kr^?CSo^3 0
SOP(°„ #
3) SAMPLE REP1ATMrEP STDPI-') ^^zs 4t__os^
4) SEPARATION LAD RECL-l ki: D
c16

CHAIN-OF-CUSTODY B%T." ANAL'ii S RECORD 13-Mar-1998
Page 1
/ ^^^
I V t CUSTOMER BHI SAMPLE OELIVEFiV GROUP L(J(
27s-
MATRIX : OTHER BATCH NUMBER 03 d^
OES ID DUP ACCOUNT
CUSTOMER
ID
SA-
i ) '^922e^^.=`^'}^e^s•z $fIF $9HiS8B
s P. rw^C
2 ) 80322202 BHI BON689t2'^"* l3`S O.vzco
ACTIONS (Initial & Date)
COMMENTS
1) INITIATED `// "/^ Gl 5) C,OUNTIN9/MEASL'REt1ENT LAB
SOPS) # IJ 117v^ SOPS) ;!
2) PREP LAD RECEIVED _

AUSTOMER
MATRIX
BHI
rAi".'A -x :^
CHAIN-OF-CL B,4TC1' ANAL' `.aIS RECORD 17-Mar-1998
OTHER j-/ &W
SAMPLE:'JELIVER`/ GROUP
BATCH NUMBER
Page I
D^^ S
o ^5-;rZa
CUSTOMER
OES ID DUP ACCOUNT ID COMMENTS
SA SR- n^n^
---------------------------------------- ^^ _____ `SIN- )
1 ) 803E720t CHi EOi964211oh'+HR. o83a O.4oyS(^ ^
G )
3 ) —eose-7,R
oar - Z -c
HT 1391v69q
1) INITIATED - 1 -' F 'NT LAG
2) PREP L.rQ "c: is iE T'dED 3 -49 AY - 9v5 h) OATA RE`.-'IF:'AED AN'_)
F2.c rt 2a5o 1-7-1 AN-?LY-iC at_ = RE= ST )R=D
3) =, 7 NFI_E i;Eit.f Ir;:,. .r S' I?+.) _3 -25 Y
/
Co^^^ ^rrc r = soy G^^ - zs c, ^^ C,^ se
2,/4141P9^
^_
6161

^!s'aanf-errs
F nimnn
S nim
BATCH SUMMARYICHAIN OF CUSTODY
AtIALYSIS n .' MATRIXo=_DUE DATE
Sw RRy
PORK ORDER SEQUENM # Q1EN7 cch owlem
1 oil& y -IB
6
QC BATMREAGENrN AW
1 N Iq -IX QC BATCBMATRIXB[Aw
1 031&H , -1moom
( cirde)
1 t4 -2M or 2S
(drdc)
QC BATCBMATRDUREAGENr
SPUM
QC BATCBMATRDQREAGENr SPIKE
D 03 bolo "Ol -
Dupli=cofSample # go3zo601
Ff 03 I LA 01 03 Z SR
$b31blOZ
a la
$Ozo6ol b3 2 s^
$0322201
FfOb 2'-1`i 0\
$03 Zr12bZ
la
p'Z
03
Batched and QC updated by Atli` on -5-aS-4Y
- 3• 5-4d'
12\LC{-RCSo ^7 \
Rec'd in Prep Lab by a or.- on 3 -1°r 2 Sop#3 tCN --X Reo C)
Rec'd in Sep Lab on Sop# Re+
Rec'd in Sep lab on Re%-J
ED/CPPT byon Sop# R e%-J
Rec'd in C. R. by
on-— Sop#-KCN200 )O Z ReO^_
Data Reviewed by on ^/ ? lip# ^C^^12^7 Rn^^
O riginal batch sheet
lT-'T^' `77-^^^ y -U^
complete calculation file to be tSlMed \vrth th j
e FIRST fisted work order number.
FORM NO.: RC-52,1/98, Rey.$
/ ^Q (^ 7 ( n /
(Coo
(T^ o = too
c r s ,j s-F =GAR
UUl
G ^ i J

SA
SR Av RL -
Soat&4i8 - -- -: _--- 7 ----
25Ntk22045 1 --^j.^ 7- /77R ^ 7^0^
Sob1FSN15 QCAG387 o9FEBgK?zap 1 (ZL McvgY oil<
..... - ..; lO rrN^t41f eg35 0.0537
3-lq
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a-asac
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BATCH SUMMARY/CHAIN OF CUSTODY
ANALYSIS^ MATRIX DUE DATE 444-8
S LV RRy
_ WORK ORDER SEQUIIAM / CLIENT combaRm
I v3l&y -1B
6 H-t
QC BATCH REAGENT MAW
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^b3 16102
a IA.
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Ala
Fs03R 14'1 oZ
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QC BATCHMATRDURFAWIT
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Recd inR C. by on N GfJ Sop#_f.'1^N2^ Rn3 C^
Da ta Reviewed by ! on 7 3-if Cnml 11^
9 CIFAAZ
sY-' J q I. l y 3 ^.
QC BATCH MATRDJRFAGeTr SPIIM
Duplicate of Sample # %702 Lt uc t
Recd in Prep Lab by at on 3-tit Qd Sop# -IS: ZO-- RM 0_
Rec'd in Sep Lab by
Op
7.T n 1 on Sop# i t ti R c 00 E
RL,-4
Rec'd in Sep lab by on Sop# ReS i
O riginal batch sheetAnd complete calculation file to be fi led with the FIRST rested work order numb,
FORM NO.: RC-52. 1/98, Rev, 8
X: PrnQ- dI A PR '^. 1 3: U
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BATCH SUMMARY/CHAIN OF CUSTODY
ANALYSIS -7-sr MATRIX DUE DATE y-6-4.R-
T1tN !'fenEntr
WORKORDER SEQUENCE# MINT CODS
1 161 -1B
^t+1
QC BATC HREAGEN T W A M
J nj1A -1X QC BATCH MAMIX ff-ea
J - 0 3161 -1M aim
(°=IC )
J 2M or 2S
(aide)
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SPUM EQGp;(, 9 'ec-193f 1.1ti349^^
QC BATCH MATRM71AGENP SPUM
Duplicate of Sample #S0 3 1 b 10 1
x'0316 1 01 "' 1 °' _
gv3 l$`{02
803 i;o^ oZ
a3 2zZ.oz
X03 ^'7 ZO1
Batched and QC updated by^vt on 3 -Z5-%K
Rec'd in Prep Lab by ^ on -3 -n -w SVOJR ^^ t* Q-S O t Red n
Rec'd in Sep Lab by - 12on ;1 1 $^¢ , S c }L ^^'[' Rn -Z
Recd in Sep lab by on Sop3 r " / F R^
ED/CPPT by
.4
1 on
sopit_—L-_ R
Recd in C.R. by / on Sopd^iC f^/^L^^n ^ -4 ,
Data Reviewed by a3-Y^ $opi frJ^C^" AZ- Re,'^
O riginal batch sh and complete calculation file to be filed with the FIRST listed work order number.
17MM NO.: RC-51 1/98, Rev. 8
SA fRM-na ^ ^S off' aRy C.evre.^Z^ No: of TOM1 SA Ij yJ h (•^
3/ 3i^4 Y
5 R s^9
x;18

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CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 10-Mar-1998
Page 1
CVSTOMER: BHI SAMP1- DELIVERY GROUP ( D f^J^^^
MATRIX OTHER n r BATCH NUMBER 111
^/Ixv CUSTOMER
GES ID DUP ACCOUNT ID
PVT „n Sft a„^
COMMENTS
]0316\^$ ESF?4_51 =__----___________-------
G^.C, (
____(ofCIA
IOAgg )/Z3
So3lbttS EQGF264
1 ) 80316101 ESF '_ 42,' 2 I BON680 q-).D bL
-Do3l6\ol ESF14253 QS.! n.000366 (ip
ACTIONS (Initial & Date)
1) INITIATED ^^ 5) COUNTING/MEASUFEF'ENT LAD
SOP(S) # 40 SOPS) #
2) PREP LAB RECEIVED 6) DATA REVIEWED AND
ANALYTICAL PREP STORED
SOP (S) # Q^L+-2^ 50 ^^-7
SOP (S) #
3) SAMPLE REMAINDER STORED 3_Zb^Lt^
4) SEPARATION LAD RECEIVED
SOP (S) 4 - \°
SOP(5) 4
G
1
C18J

CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 11-Mar-1998
1 Page 1
11,
CUSTOMER: BHI
J SAMPLE DELIVERY GROUP
MATRIX : OTHER
^^((
U-^t BATCH NUMBER O j
1 )
CUSTOMER
GES ID DUP ACCOUNT ID COMMENTS
P P'r w'f- s R ^
S•u
2 ) 80318402ESF142^4 II BON633 G^.^ o -oou3V9 (.¢ 1,410R4^1 /lli
3
iq
AC
3u^
IONS ( 1:111: a1 0: T)-1
------ ---
T
1) INITIATED 5) COUNTiNC/NEASURENENT LAB
SOP(S) 0 jVnD SOPS) #
2) PREP LAB RF_CEIVED 3 •19_TY_ wet b) DATA REVIEWED AND
ANALYT?CAI_ PREP STORED
3) SAMPLE REi`1A'NDER STOR 1) -z6-LR Ot
4) SEPARATION L 4 3 RECEIV(I)
SOP (5) #
GIS5

CHAIN-OF-CUSTODY BATCH AID.-,LYS;IS RECORD 12-Mar-1998
I tq)
Page 1
fvfL CUSTOMER: BHI
/I)
SAMPLE DFLIVERY GROUP IND ]^7
MATRIX
n^
OTHER ^ /^ lJ1 BATCH NUMBER 0^ r
CUSTOMER
0ES ID DUP ACCOUNT ID P T.,c Sar ^^ COMMENTS
1 j—ffB3Re6ei A(+1 5 B6WbE35
2 ) 80320602 ES-14265
v. ^o • , ..
I
,:a
BON686 ZF j.j O coOF5 7 0bg 8' / Zz-
3) L-893@ B 60 3 BI I I O1^ B II 'J^
AC-IONS (T t i d a l '< Date) ------ -------
I
1) INITIATED LAB
2) PREP LAB RECEIVED 3_,l9_•9P.^^ 6) DATA REVD=tiED AND
`ur(S) 4S Fjv_-*,^C J\3^
3) SAMPLE REN(kiN i)E:R ST P Pt=D _ -2b-z% oJ^
4) SEFARATION L.AE Ri:CEiV>.D
SOP (S) if _-------
Ocf' (0) iF
ANALYTIC I_ PREP STORED
SOP(Si

-$*t _-AL-SR c44
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998
l) Page 1
1 2CUSTOMER: BHI
SAMPLE DELIVERY GROUP
MATRIX : OTHER
_/)/p v^-^' I BATCH NUMBER D3'a3^
GES ID DUP ACCOUNT
CUSTOMER
ID
wZ' SA- ANA^
APT
COMMENTS
1 ) 80322201 ---81i^ `"--a te B^eH6c65
2 ) 80322202 °SF14_5o lI BON639 Gy.Z 0. 000"6 6C. i ApR 1zz^
------------ --------- ------ - ------ --
ACTIONS CTIOi JS (Initial & Date) -----------
1) INITIATED < 3 5) COUNTING/MEASUREMENT LAL+
2) PREP LAB RECEIVED aL-t9-9g _ 5) DATA FEVIE-WED AND
A.NALYTI;P.I_ PRE° STDRED
3) SAMPLE REMAINDER STOR. D 3_Z6=4T _p^
4) SEFARATiOi: LAP RECEI'-TGh
SOp(G) R
Gigs

3 l / CUSTOMER
MATRIX
-** TOTAL-SR # -I*
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 17-Mar-1998
9 e
EHI SAMPLE DELIVERY GROUP
OTHER rl -LV I BATCH NUMBER
CUSTOMER
OES ID DUP ACCOUNT ID COMMENTS
r ^r
Lh.r.^ CsA^ -------
1 ) 80327201 BHI BON692 Q3.1 O-0006&T^ 6D //}iie4$ 12.Zl
2
3 )
f ------ - -ACTIG10S (Initial & Date) - ------- --
1) INITIATED 1) GOUPJTiPJG/hIEASUREi`f:-NT LAP
SOP(S) 4 SOP (5) t --
2) PREP LAB RECEIVED 6) DATA PEV1EWED AND
r`.NALYTICAL PREP STCRED
501 1 (S) # $_^^±^2c So i3^
SuP(5) #
3) SAMPLE RENAI-'NDER STCRPn 3 Lb-4g out
4) SEPARATION! LAD P.ECEIV'_D
-
cis, j

%uanterra
.Sb.iCV
BATCH SUMMARY/CHAIN OF CUSTODY
ANALYSIS C-1 q MATRIXo+DUE DATE y -6-9k
t!^R`( r-rr-mEnlr
WORK ORDER SEQUENCE a amir CONAENIS
J- 03161 -10 Wj,;AJ QCBATC$REAGEM'BIAW
J . ^U. D^ I (ro iX QC BATCHMAMUX IS AIS
J o 316 t IM oQ
J-
D o31b1
(dtde)
2M or 2S
(dude)
01
^'p3161o1 '^ 1 "
gn3 LB^oZ
g03 F-06 pZ
b3 Z? 02
$03 z-2z0^
Batched and QC updated by-^i e^ on 3 -2
3•
QC BATCH MATRDUREAt3Nr
SPUM
QC BATCHMATRUMEAG NT SPUCE
Dupticade of Sample H 8`0 3 t 61 01
Rec'd in Prep Lab by on 3- H -w S0 05L1C- C-So 1 i Rn,= 0
Rec'd in Sep Lab by uM , on #-G fe Sop#12(_ e-- SG,2.) Rni /
Rec'd in Sep lab by on 41 SOP# _ RnLj—
ED/CPPT on Sop# Rni
Rec'd in C.R by on yl, l+r So p(__,
Data Reviewed by - ^`^ l^ Sop# e- ^4 Z
O riginal batch sheet an complete calculation file to be filed with the FIRST Esttd work order number.
FORM NO.: RC-52. I/98. Rev 8
S4 FRAc c10
i s 0-^ O R y 5 0 L- o, Nor o^ 1 S;
&L-L- s 02 1 = Gi9i1
Rn

CHAIN-OF-CUSTODY BATCH ANALY;l S RECORD 10-Mar-1998
Page 1
'J
CUSTOMER: BHI
SAMPLE DELIVERY GROUP I/ ^^
MATRIX
Q
OTHER ^ ^ u -D0 l
/`^)
BATCH NUMBER ll -0I
CUSTOMER
OES ID DUP ACCOUNT ID COMMENTS
sa aaa^
---------------- ----------------------------
1 ) 803161010.000 1040 BHI SON660
2 ) 80216192 Biii 130H681
^..3•i6
1) INITIATED
D031b 4o l 0_•000blg
it
3
ACTIONS (Initial & Date)
^ 5) COUNT IN /MEASUREi•4ENT LA3 ___
SOPS) # SOP(S) i4
2) PREP LAB RECEIVED 3_-v =L -ci^j^.^ Ei) 4)jT;n REVIh.WED ANO
,04l%LY I i L FRS? STGRcD
SOP ( ) ) if R -
SOP (S) #
3) EA'NPLE REf!AINiiER SIOR I=D s-2S-qY _o L
4) SEPAROTION LAB RECEIVED
SOH (5 i 4
L191

CHAIN-OF-CUSTODY BATCH ANAL`SIS RECORD 11-Mar-1998
1 3 ^1 Page 1
CUSTOMER: BHI SAMPLE DELIVERY GROUP ^
Q
MATRIX : OTHER f ^ lam' i BATCH NUMBER o3'IS
CUSTOMER
GES ID DUP ACCOUNT ID COMMENTS
gp dal
1 ) 603E 8481 7" ac 3-zs
I?I13 $9PF6^^
2 ) 80010402 0.0006\ 7 DHI BON6 33
3 ) ^ BE)S I BR6S T'°` 3 ' Fill! BER16 j4
----------------------------------------nr
I%i') ri
1) INITIATED `) CCUNTI'?G!i IcA5UREi`lEi T L.AB
SCP ( S ) 4 SOP (S) ##
2) PREP LAD ^.__ :." - 5-t5 9^ S___ b) hATA REVIEWED AND
t^.iINALYTICAI_ PREP STORED
SOt' (5 i ;E Ri^H RC S9 ^3 -o —
GOP (7)
3) SAMPLE RE?A 7 ^'0^° '-TSJ,;" h 3_z5- ciY O(t --
4) E /?i i,l IiJIli L.'?L' FL t.t I'i -11
--
619

1 / 1
CHAIN—OF—CUSTODY BATCH ANAL"S IS RECORD 12—Mar-1998
Page 1
I/ CUSTOMER: BHI SAMPLE DELIVERY GROUP
MATRIX : OTHER HAW BATCH NUMBER
(,^
CUSTOMER
OES ID DUP ACCOUNT ID COMMENTS
SR AUkI
%A
2 ) 60320602 0 .00 1 1 4c BHI BON686
3 ) (36226692 _
i-u ^Lr _R 41 uQW687 -
- -- ------- -------- -- ---- ------------------------------- ----
IJACTIONS (Initial ?< Date)
ff
1) INITIATED ^ t _ vC 5) COUNTiW,/M=ASURE;'lENT LAI3
SOP(S) 4 SOP(S) #
2) PRE? LAD REC E IVED 3=1.^^K. D^^ 6) DATA RE'J[t_WED AND
IgALYTIC `)L PREP STORED
SOP (5) t# ^t^So ^3
3) SAr.PLE REMAINDER STOR^_0
4) SEPAR A TION L=° 9E-,-E`4's_,)
SC P 13) 4 wW.
F)
(JigJ

CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998
Page 1
31 / CUSTOMER: BHI SAMPLE DELI`,lERY GROUP WQ^^^^
MATRIX : OTHER M8-bul BATCH NUMBER
1 )
CUSTOMER
QES ID DUP ACCOUNT ID COMMENTS
5 A Au A^
zs
2 ) 80322202 0. 00 t O 2S l BHI BON639
------------- ----------- --------------- — --
ACTIONS (Initial & Date)
1) INITIATED(-1 U) COUNTING/MEASUREMEidT LA3
2) PREP LAB RECEIVED -j°1-gH_°nc S) DATA REVIEWED AND
ANALYTICAL PREP STORED
SOPS) H Rjct"
SOP (3) n
3) SAMPLE REMAINDER STORED 3_ zS '^K Oaf
4) SEFARATION LAD RECEP;`;i)
SUP (5 ) ;' _ _ —^W----
SCP (^:) It
61,9,1

CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 17-Mar-1998
Page 1
/ CUSTOMER: BHI WIPLE DELIVERY GROUP
MATRIX OTHER -oCQ, BATCH NUMBER
CUSTOMER
QES ID DUI' ACCOUNT ID COMMENTS
-SA AmPrc_
1 ) 80327201 (0 .00lozz DHI BON692
2 ) , 20=7202 VY^-3 . 2 5 tL1( 8 1693
3 ) —Be -327E 3 ° L4 -Hi BON694
719g
1-a'
`^J ^
1) INITIATED _ 3 > CuUid^ ;'=Ci IG1SU°EPIE^JT Ld7
2) PREP LAD RECEIVED 3-l^L-RY_D _ > DATA REV IE!:ED AND
Arl.ALYTICAI_ FRET STCt?HD
3) SAMPLE R i''.,a;i;L'=R ".: i_'I

i..T":}1M1frt::l
Sen+:rx
BATCH SUMMARY/CHAIN OF CUSTODY
ANALYSIS 5F.-77 MATRIX C) T^ DUE DATE_a -6 -Ur
^R`( CS=m Etvr
WORK ORDER MQMCE s CENT Comme T$
J 03161 - 113 QC BATCiREAGUITBtANK
J ^ tw -1X QC BATCH MAT= BLANK
J o 3 t 61
J N In
- 1m aim
(code)
-2M or 2S
(mde)
QC BATCH MAIMMAGENT
SPUCE
QC BATCH MATRDUREACENT SPLICE
Do-6tb1 -01 -_
Dt>Q lirate of Saittple B g0 3 l 61 01
FSb3l6 l o1 '^ 1 `^
gub l$ 1oZ
8o3 zob oZ
03 2ZZ02
$03
Hatched and QC updated by-^dt on 3 LS-LJ
Rec'd in Prep Lab by ean 3 A _ Sopiig tL g-SO t 3 Re%-
Recd in Sep Lab by l A on ^^ ^^ Sop3 C^ ^^ L ` R n^
Rec'd in Sep lab by on Sop# Rcv
ED/CPPT by on SopB p Rn
Recd in C.R. by !^ on 3 31 SOP# 7^ Ic- ^G l R^ ^^
3,70-,-
Da ta Reviewed by on Sop! ^^^' Cc [ R^
O riginal batch sheet add complete calculation file to be filed with the FIRST Eved work order number.
FORM NO.: RC-52.1/98. Rev. 8
50. tS of 1 {Lj CS-,: WN ') tvoT of- set
CWT 1^^ -. Rab^•F ^ a.LQ.
Li^U

I
CHAIN-OF-CUSTODY B,4TCFi ANAL Y 51S RECORD 10-Mar-1998
Page 9 1
CUSTOMER: BHI ^/'y SAMPLE DELIVERY GROUP W D ^^
MATRIX : OTHER I3 ^ (/ {may I BATCH NUMBER
CUSTOMER
0ES ID DUP ACCOUNT ID COMMENTS
S(} Auk
1 ) 80316101 ° _ _ = ' )' _JN680 o-oco3 ra
2 ) 863t6ie _ _ I e
1) INITIATED
13^ti6a
ACTIONS (Initial & Date)
^ ^5) CSUNTIN•f,/MEASURE-,KENT LAB
SOPS) # 410- i^ SUP(S) ?k _
2) PREP LAB RECEIVED 6) DATA REVIEWED AND
ANALYTIC ;)_ PREP STnRED
SOP (S) Sk ^^tE2C5 o^T»
SOP(S) u
3) SAMPLE REMAINDER STDREO 3-Z6 0.8 q^
SOF'(S) i; V-
4)
n
SEPARATION LAB RECEivi -0 ^^^(^^!^ ^^^^\\
SOP3,^^IT^4^
^^19,

!
**^^ SE-79 ***
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 11-Mar-1998
CUSTOMER BHI
Page 1
SAMPLE DELIVERY GROUP (,voa07
MATRIX OTHER I BATCH NUMBER 03-1
CUSTOMER
GE3 ID DUP ACCOUNT ID COMMENTS
5{} A"4tz-
1 ) 3,Lb
3
80318402 I BON633 O •oeo357
----Y
5
-- ------ ^ ^ir T I OI •aS (I n i t i a 1 `. D.^ ^: a) ------------
1) INITIATED / ` )^ :) COUNTI`JG/i`IaASUREi`IENT LAB
SOPS) # SOP (s) #
2) PREP LAB RECEIVED 3-g-9^0^_ 6) DATA nEVIEWED AND
3) SAMPLE REMAINDER STORED _3-26 `^k_OyC
4) SEPARATION LAB RECEI'V,
n^
ANALYTICAL PREP STORED
SOP(S) #
G L J ,j

*n 5F-79#r
I,^
^
V
q li^
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1998
Page 1
CUSTOMER: BHI
V hf'
MATR IX OTHER /y . 1
I'\ l
SAMPLE DELIVERY GROUP OQQ7.S
BATCH NUMBER O3 -°Cy
CUSTOMER
GES ID DUP ACCOUNT ID COMMENTS
S!! AwA -
1 ) 805Efto s'f c5
2 ) 80320602 -- I B 0N61360. 000 rs50
3) eeszewe Bi )l3 "^- BE)H687
- -- ----------------- -------
ACTION-- (Iuitiai & Date)
1) INITIATED _ ^(^?7D^ 5) COUNT iNC!t1EAS'.JRE'tENT LAB
SOP(S) # S010 (S) t#
2) PREP LAB REC_eVEG 3 _lg _fig ,_ 6) DATA REVD - WED AND
FiN.^- Y i.AL =RE P STOR E71)
SOPS) 4 F^^Cti C50^3 0
Soe (s) #
3) SAMPLE REMAIfdDER ST07v:D 3.26-`^rr
4) S EE cAR.fTI^CN
Sr)^ c :^) ,i ,^^
l
^l l n i^

^CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998
Page 1
CUSTOMER: BHI SAMPLE DELIVERY GROUP
MATRIX : OTHER ^(^ ^ BATCH NUMBER 0v _Z/92
CUSTOMER
QES ID DUP ACCOUNT ID COMMENTS
S tOr AN A k-
---------------------------- -----
1 ) C $
3.7bRTf
2 ) 80322202 - - : II BON 639 0.000657
1 CTIOi.3S (Initial Data)
1) INITIATED / ^1 `) CCUNT?NC;/ IN IEASUREPIC 'i\iT LAD
2) P R EP L AB R EI` iEC 3.1^g$ b) I IATA ,EVI; WED AID
SOP (S) # R'CH-Re5013-0
3) SAMPLE REMAIPIDER STOR'1) 3_- 26 "2'? r--A.
4) SEPARATIuP"! LAL
AiNALYTICAI.. P R EP °_.T04Ei
^Pc
G; 3 0

W A^
CUSTOMER
MATRIX
EHI
OTHER ^U cb I
h^^ SE:-!9
^^n
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 17-Mar-1998
SAMPLE DELIVERY GROUP
BATCH NUMBER
^^(^ ^7 Page 1
I.W^ I
o3-a7a
CUSTOMER
QES ID DUP ACCOUNT ID COMMENTS
5^4 ANR^
1 ) 80327201 ' " eC= ` ' I BON692 O-0006°tb
3.26'45 "
3 ) ^69327^ P+f 13—^^tl^`^Q ^'.At'^,5^4
------ -- - --- ---- ---- -- - ---------------------------
'^CTI0PJ:3 (Inibxal ', Dace:
1) INITIATED 5) COVivT-NS/MEASUREMENT LAD
SOP(S) J^'3 5i7P(5) R
2) PREP LAB RE Ei•1 D 3-)5_= jy^ 6) DATA REV!'-W;ED AND
(`,N1LY7-,-j`j PREP STORED
Sop 1. 3 i K R%L'wfC 4501 3 -i7
SOP ( 0 )
3) SAMPLE Ri_i', i' i;GP STOP! D 'b -26-43 V+
4) EEPARAT10iI LA-r `?=r'EIY,-D
G^G^

(j..%"uanterra
BATCH SUMMARY/CHAIN OF CUSTODY
ANALYSIS TL . Q MATRIX O TlifA DUE DATE L -6 `Lk
r,a`4 rV-rn FIUT
WORK ORDER SEQUENCE # CLINT
J-. 0316 1 -1B QC BATCHREAGE"NP BLANK
J - N ^ k -ix QCBATCHMATMBLANK
1 0 3161 -1M 0(a)
(circle)
1 -ZM or 2S
(aide)
Do3tbt -fit
^Sb-Sl6lo1 "' 1 °'
QC BATCHMA
SPDM
p GEgr
QC BAT CHMATROGRFAGENT SPIKE
Duplicate of Sample # $0 3161 01
gv3 tB^lOz I -
g03 i_06 02
go3 2zZO2
$-03 Z: '7Z0\
Hatched and QC updated by^_ on 3 -2 5-%^
Rec'd in Prep Lab by -- vr.- on 3 -H -W Sop>9RtCttRCSoI^ M-2 C)_
Rec'd in Sep Lab by 6TL1)
on 312- 411 Y
Rec'd in Sep lab by /L( — on SOP# Rte:
ED/CPPT on SOP# R.t -
Rec'd in C . R_ by---4- on 'f I i k r SOpag _ tZ r tilts, 7 ,o t Rn-4 o
Da ta Reviewed by on
sop# t^
^F`T^ ^Re1d
O riginal batch sh t and complete calculation file to be filed with the FIRST Gsted work order num be r.
FORM NO.: R -52. 1/98_ Rev 8
SCE ^--RA

J r
CHAIN-OF-CUSTODY HATCH ANALYSIS RECORD 10-Mar-1998
ql/1 Page 1
1) INITIATED
SOP (S) #
"Do3 16) b 1 O-00038Z
ACTIONS (Initial & Date)
oaa^7
CUSTOMER: BHI SAMPLE DELIVERY GROUP
MATRIX OTHER VuI BATCH NUMBER
/,
_1(^I
CUSTOMER
QES ID DUP ACCOUNT ID COMMENTS
SA, Afjn^
1 ) 80316101 0.000yrt BHI BON680
2 ) R0314410:2 LZtc 5-25 9d I I BON 681
5) COUNTING/MEASUREi`1ENT LAB
SOP (5) #
2) PREP LAB RECEIVEll 3-i9 - CC _ 6) DATA REVIEWED AND
ANALYTICAL PREP STORED
SOP (S) # ^R-L4A^\J^:^)
SOP (s) #
3) SAMPLE REMAINDER STORED•z51t
4) SEPARATION LAB RECEIVED
SOPS) B J w
SOP' (S) !k
vL,.^J

n/ ^j\x CHAIN-OF-CUST011`r' BAICFi ANAL`iTiIS RECORD 11-Mar-1998
UU ,J` U
Page 1
, I TOMER: BHI
-j
501PLL DELIVERY GROUP W6422 /
llV// MATRIX OTHER g- BATCH NUMBER LCJ
1 )
CUSTOMER
OES ID SDAU pACCOUNT (D COMMENTS
2 ) 60318402 0-00034Z BHI BONE03
3 ) sea^a4e^ 0at3•z54k -IT
1) INITIATED
/
tiC
01dS (Tuitial I< Date)
-1
U 5) COUNTING/MEASURE4IENT L D
SOPS) # r-! SOPS) 4
2) PREP LAD RECEIVED 3-Ict-4^^SL 6) DATA =.EVCEWFID AND
ANALYTICAL PREP STORED
SOP (s) 4 R1ctFScL^i^^-o
3) SAMPLE REMAINI)ER STOR`--r )
C^ ^^ (J i If rJ
4) ===;RATIO;•! L B RE.C==VC0
o^(s a
L20el

:r Tr-99
CHAIN--OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1998
` Page 1
l•
/ CUSTOMER: BHI
SAMPLE DELIVERY GROUP
MATRIX
^Q
OTHER ^^ D` BATCH NUMBER LEA OWE
^-st
CUSTOMER
OES ID DUP ACCOUNT ID COMMENTS
5A AQ At
1 ) 9a-3:0601 --Z)0C -s•u Ski; BGW609
2 ) 60320602 0-00°6a6 BHI BON636
3 ) QQ-2ncn- 1 -pe 3 • 2,5 am;
_ ^l_Ap:T C1=5
13 ,90CA97
1) INITIATED _) t^b COUNTING !NEISUP,Ei'IEhIT LAB
SOPS) 4 oWG SOI'iS? T
2) PREP LAD RECEIVED ^_-1q-^^^` 6) DATA RE"'IcWEL' AND
ANALYTICAL PREP STDRED
90F`-) 4 R^t}iZC v\3 ^
SC i'' Ie/ '^
3) SAMPLE REMAIi`OEF ST7RL 1)
4) SEPARATION LAD RECEIV:T)
I 1 _`) 'It
LL-VJ

GvJ ^)
^
II
VIA//
CUSTOMER
MATRIX
BHI
CHAIN--OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998
Page 1
SAMPLE DELIVERY GROUP IJDo^^7S
OTHER IO^(/(^ I BATCH NUMBER
CUSTOMER
QES I 1) DUP ACCOUNT ID COMMENTS
'S4 quq^
1 ) 89a2229 } B)a4 BQW;$38
2 ) 80322202 0-00°6 77 BHI 13 01.4609
ACTIONS (ILtitial & Date)
^j
1) INITIATED 5) CUNTING/MEASUREMENT LAB
SOP(S) # SOP (S) #
2) PREP LAB RECE.'.VED ?Zlc]. ^
SOf' S) i5 _F
Ur TA di:b!ED %)i;-:
!i'1-'LYT.Gt\L PREP S 7 0R="D
c+ Q _ i3 -Q)
3) SAMPLE PENAI`CER STORi=O 3_ZS ^^^uL
G20G

C`IAIN-OP-CUSTODY BATCH ANALYSIS RECORD 17-Mar-1996
Page 1
1 i
CUSTOMER: BHI SAMPLE DELIVERY GROUP
MATRIX OTHER ^ BATCH NUMBER
OES Ill DUP ACCOUNT
CUSTOMER
ID COMMENTS
S y A+jf4fr
------------------ - --------------______________________________________
I ) 80327'-101 0_00ob !o BHI BON692
2 ) BHi
----------- -- -- -- ----- - --- - -------------- - -
lACCjTICNS (I) itiai D-i-)
1) INITIATED +)^ i ;_.H?_?I !NI \SURE`:1F.NT LAR
6OP(S) #_^ L ^! SO? (S)
21 PREP LAB :R c.(;=iVED I ` -`Z$ DDS b) i) ATA REV ( f:WFD AND
AidALV'_:AI_ of^cp ST'^ftED -__
3) SAMPLE F'EV-J ;Ii : i?E? S T OR :D 3.25-4^_f^t^
4) ScP:ARr1Ti:=?; _-- YD:C= ' .t:+:
SCf' (B i ;;
)!)
U2 o

' l i uani'erra
E _l,st8
S Tiv
BATCH SUMMARY/CHAIN OF CUSTODY
AVALYSIS TC -9 MATRIX DUE DATE LI -b-`c8
st_%j R-&y
19 ORK ORDER SEQUENM # QdENi' C lzg mm
1 oil&`V -1B
cs t+i
QCBATCHREAGENI'BLANK
J ata. _Ix QCBATCHMATRDMHIAMC
J O31 h-4 _IM 099)
J N
(dsde)
lq 2M or 2S
(drde)
D 03 iky -Ol
QC BATCH MATRI)WEACENT
SPUM
QC BATCH MAIRDUREAGENT SPIIM
Duplicate of San* #i $703 1840 1
^SO^I&4ol 03
-a la
Wn 227
^b3 1b102
$0b2.o6o1 b3 2- 5A
$03a22o1
S-0 -5 P- bZ
^ro3 Z 12b2
,., l a _.
OTC
Batched and QC updated by 'wL on 5-2--s-1Y
Rec'd in Prep Lab by -7z> eL on 3 -t°t Aqv
Rec'd in Sep Lab by_ 1Wl on >> 2 9 Si
Rec'd in Sep lab by on
ED/CPPT by on
Sop# a CtA 2CSbv3 RCO 0
Sop# A^ C I7 R C 1 6615 Rev*
{,
^ Rev#
Rec'd in C.R- by it on 3Sop# f` /c ,Q y^ryyl ) Rev
Data Reviewed by on ^- Z' Sop# f ` L W ( Ma 2Rn-4__ _ L
Original batch sheet and I
complete calculation file to be filed with the FIRST fisted work order number.
FORM NO.: RC-52,1/98, Rev 8
Revd
6 206

cclaq
w^'M t+s

_
SF^ Aa A^
Jll,! ''CUTS
G^1C

^!^ n"mil 12^^ 1 ?5
P, ^LrKZC S o i3 ^
5 25 -Z
^l

Get

SAr A-&) A^
621 J

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621=

CLIENT:
PROJECT ID:
BHI_45
SAP B98-061
Cr+6 CHAIN OF CUSTODY
MATRIX: OTHER DUE DATE: 03/31/98
SDG W02275 BATCH: 03-184
SAMPLE # CLIENT ID COMMENTS
W803184 01A BON682
W803184 02A BON683
W803184 03A BON684
Comments:
q QC REQUIRED
INITIALS DATE ^ SOP#
COC INITIATED L^ 7 , N/A
SAMPLE PREPARATION 3/1 1 gz RICHWC5003 Rev 2
SAMPLE ANALYSIS 3 ^ RICHWC5003 Rev 2
DATA REVIEW RICHWC5003 Rev 2
L^-1J

CLIENT:
PROJECT ID:
CS+6 CHAIN OF CUSTODY
BHI_15 MATRIX: OTHER DUE DATE:
SAP B98-063 SDG W02261 BATCH:
SAMPLE # CLIENT ID COMMENTS
W803216 01A BON894 (^, ^j b8,5)
W803216 02A BON895 (^Gy 3)
W803216 03A BON896 C' JG ,kj ypl
Comments:
El QC REQUIRED
04/01/98
03-216
INITIALS DATE SOP#
COC INITIATED ^j(C^ N/A
SAMPLE PREPARATION RICHWC5003 Rev 2
SAMPLE ANALYSIS RICHWC5003 Rev 2
DATA REVIEW
3 !^ Cyy RICHWC5003 Rev 2
C^lU

CLIENT:
PROJECT ID:
BHI_45
SAY B98-063
Cr+6 CHAIN OF CUSTODY
q QC REQUIRED
MATRIX: WATER DUE DATE: 03/31/98
SDG W02261 BATCH: 03-186
SAMPLE # CLIENT ID COMMENTS
W803186 01A BON783
Comments:
INITIALS DATE SOP#
COC INITIATE D N/A
SAMPLE PREPARATION
^
RICHWC5003 Rev 2
li
SAMPLE ANALYSIS RICHWC5003 Rev 2
DATA REVIEW 3 Q RICEWC5003 Rev 2
G

CLIENT:
PROJECT ID:
BHI_45
SAF B98-061
Ci+6 CHAIN OF CUSTODY
MATRIX: OTHER DUE DATE:
SDG W02275 BATCH:
SAMPLE # CLIENT ID COMMENTS
W803272 OIA BON692
El QC REQUIRED
04/06/98
03-272
W803272 02A BON693 ?o32,790/
W803272 03A BON694
Comments*
COC INITIATED
INITIALS DATE SOP#
'31 -7 /9 9
SAMPLE PREPARATION 36l RICHWC5003 Rev 22
SAMPLE ANALYSIS
a !6
N/A
RICHWC5003 Rev 2
DATA REVIEW RICHWC5003 Rev
G^:1^
it
it

CLIENT:
PROJECT ID:
Ci+6 CHAIN OF CUST0DY
BHI_45 MATRIX: OTHER DUE DATE:
SAF B98-063 8DG W02281 BATCH:
SAMPLE # I CLIENT ID ( COMMENTS
W803279 01A BON898 C ^0Y0 >
Comments:
COC INITIATED y _
El QC REQUIRED
04/06/98
03-279
INITIALS DATE SOP#
r/, `/ b
SAMPLE PREPARATION RICHWC5003 Rev 2
SAMPLE ANALYSIS RICHWC5003 Rev 2
DATA REVIEW RICKWC5003 Rev 2
N/A
^"^.j

CLIENT:
PROJECT ID:
Cr+6 CHAIN OF CUSTODY
BHI_45 MATRIX: OTHER DUE DATE:
SAY B98-061 SDG W02275 BATCH:
SAMPLE # CLIENT ID ( COMMENTS
W803206 01A BON685
04/01/98
03-206
QC REQUIRED
W803206 02A BON686
a-LD ^i41eL ,- 1ficGI uulwl-luL-( r3r) L
W803206 03A BON687 grj32^ld^^
Comments:
INITIALS DATE SOP#
COC INITIATED 7^= N/A
SAMPLE PREPARATION RICHWC5003 Rev 2
SAMPLE ANALYSIS RICHWC5003 Rev 2
DATA REVIEW RICEWC5003 Rev 2
G4.

CLIENT:
PROJECT ID:
Ci+6 CHAIN OF CUSTODY
BHI_15 MATRIX: OTHER DUE DATE:
SAP B98-063 SDG W02261 BATCH:
SAMPLE # CLIENT ID I COMMENTS
W803216 01A I BON894 C r3 .Qb8& l
W803216 02A BON895
(pO
W803216 03A BON896 C'JG/ l ^^^
Comments:
3 )
q QC REQUIRED
04/01/98
03-216
INITIALS DATE SOP#
COC INITIATED ^^ ^7 N/A
SAMPLE PREPARATION
SAMPLE ANALYSIS
3 ^z^ ^C
3/1
RICHWC5003 Rev 2
RICHWC5003 Rev 2
DATA REVIEW 3 / 4 Y RICHWC5003 Rev 2-
nn^
^^1

CLIENT:
PROJECT ID:
BHI_45
SAF B98-061
Cr+6 CHAIN OF CUSTODY QC REQUIRED
MATRIX: OTHER DUE DATE: 04/02/98
SDG W02275 BATCH: 03-222
SAMPLE # CLIENT ID I COMMENTS
W803222 01A I BON688
W803222 02A BON689
Comments:
80 A)
INITIALS DATE SOP#
COC INITIATED ^- __^( N/A
SAMPLE PREPARATION
3 13 1q - RICHWC5003 Rev 2
SAMPLE ANALYSIS Tfo 3 13 4 RICHWC5003 Rev 2
DATA REVIEW RICHWC5003 Rev 2
7 .^ r

CLIENT:
PROJECT ID:
Ci+6 CHAIN OF CUSTODY
BHI_45 MATRIX: OTHER DUE DATE:
SAF B98-063 SDG W02281 BATCH:
SAMPLE # CLIENT ID COMMENTS
W803242 01A I BON897
Comments:
QC REQUIRED
04/03/98
03-242
INITIALS DATE SOP#
COC INITIATED / N/A
SAMPLE PREPARATION RICHWC5003 Rev 2
SAMPLE ANALYSIS
DATA REVIEW
3/Na
RICHWC5003 Rev 2
M 3 9 1 ,^, IRICHWC5003 Rev 2 1

CLIENT:
PROJECT ID:
BHI_45
SAF B98-061
Cr+6 CHAIN OF CUSTODY QC REQUIRED
MATRIX: OTHER DUE DATE: 04/03/98
SDG W02275 BATCH: 03-244
SAMPLE # CLIENT ID I COMMENTS
W803244 01A BON690
W803244 02A BON691
Comments:
I IALS DATE SOP#
COC INITIATED ^' /,^ N/A
SAMPLE PREPARATION RICHWC5003 Rev 2
SAMPLE ANALYSIS 3r/9 RICKWC5003 Rev 2
DATA REVIEW 7j lb
^^ RICHWC5003 Rev 2
i

CLIENT:
PROJECT ID:
BHI_45
SAF B98-061
Cr+6 CHAIN OF CUSTODY
0 QC REQUIRED
MATRIX: OTHER DUE DATE: 03/30/98
SDG W02275 BATCH: 03-161
SAMPLE # CLIENT ID COMMENTS
W803161 01A BON680
W803161 02A BON681
Comments:
INITIALS DATE SOP#
COC INITIATED ^^ N/A
SAMPLE PREPARATION 3/Old RICHWC5003 Rev 2
SAMPLE ANALYSIS RICHWC5003 Rev 2
DATA REVIEW 34497 RICHWC5003 Rev 2

CLIENT:
PROJECT ID:
Ci+6 CHAIN OF CUSTODY
BHI_15 MATRIX: OTHER DUE DATE:
SAF B98 - 063 BDG W02261 BATCH:
SAMPLE # CLIENT ID I COMMENTS
W803216 01A BON894 l rJG/-) (a^GJ
W803216 02A BON895 ( J30 ^,-/ by3 )
W803216 03A BON896
Comments:
El QC REQUIRED
04/01/98
03-216
INITIALS DATE SOP#
COC INITIATED 7 N/A
SAMPLE PREPARATION 3/^^/ 8 RICHWC5003 Rev 2 II
SAMPLE ANALYSIS
31&
—
RICHWC5003 Rev 2
DATA REVIEW RICHWC5003 Rev 2
G^t_v
I