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Quanterra Incorporated<br />
13715 Rider Trail North<br />
Earth Citv, Missouri 63045<br />
314 298-8566 Telephone<br />
314 298-8757 Fax<br />
Bechtel <strong>Hanford</strong> Incorporated<br />
3350 George Washington Way<br />
Richland, Washington 99352<br />
April 21, 1998<br />
Attention: Joan Kessner<br />
Project Number<br />
Date Received by Lab<br />
Number of Samples<br />
Sample Type<br />
SDG Number<br />
Data Deliverable<br />
I. Introduction<br />
CASE NARRATIVE<br />
^$9501112 >b<br />
do,<br />
ti<br />
Environmental<br />
Services<br />
0(14.`332<br />
^' R ^ ^^ ^ p<br />
PR 1993 ^<br />
RECEIVED i<br />
550.260"—^<br />
March 09, 10, 11, 12, 13 and 16, 1998<br />
Fifteen (15)<br />
Other Solid<br />
W02275<br />
Summary<br />
le Ab<br />
" OL 6 19 L95^<br />
Between March 9 and 16, 1998, a total of fifteen (15) other solid samples were received by<br />
Quanterra, Richland and was transferred to Quanterra, St. Louis for chemical analyses. Upon<br />
receipt, the samples were given the following laborato ry ID numbers to correspond with the<br />
specific client IDs:<br />
The samples were filtered to separate the liquid phase from the solid phase. The solid phase<br />
sample IDs are listed below:<br />
St. Louis ID BHI ID Richland ID Matrix Date Receipt of<br />
17199-001<br />
BON680 80316001 Solid 09-MAR-98<br />
17199-002 BON681 80316002 Solid 09-MAR-98<br />
17200-001 BON685 80320501 Solid 11-MAR-98<br />
17200-002 BON686 80320502 Solid 11-MAR-98<br />
17200-003 BON687 80320503 Solid 11-MAR-98<br />
17202-001 BON682 80318301 Solid 10-MAR-98<br />
17202-002 BON683 80318302 Solid 10-MAR-98<br />
17202-003 BON684 80318303 Solid 10-MAR-98<br />
17203-001 BON688 80322101 Solid 12-MAR-98<br />
17203-002 BON689 80322102 Solid 12-MAR-98<br />
17221-001 BON690 80324301 Solid 13-MAR-98<br />
17221-002 BON691 80324302 Solid 13-MAR-98<br />
17224-001 BON692 80327101 Solid 16-MAR-98<br />
17224-002 BON693 80327102 Solid 16-MAR-98<br />
17224-003 BON694 80327103 Solid 16-MAR-98<br />
o0006'L
Bechtel <strong>Hanford</strong> Incorporated<br />
April 21, 1998<br />
Project Number: 550.260<br />
SDG: W02275<br />
Page 2<br />
imbanterra<br />
Emironmental<br />
Services<br />
The liquid phase of the samples were placed in containers and put on hold for the following<br />
sample IDs:<br />
St. LouisID BHI ID Richland ID Matrix Date of Receipt<br />
17199-003 BON681 FILTRATE 80316002 Liquid 09-MAR-98<br />
17221-003 BON690 FILTRATE 80324301 Liquid 13-MAR-98<br />
17221-004 BON691 FILTRATE 80324302 Liquid 13-MAR-98<br />
17224-005 BON693 FILTRATE 80327102 Liquid 16-MAR-98<br />
17224-006 BON694 FILTRATE 80327103 Liquid 16-MAR-98<br />
1I. Analytical Results/ Methodology<br />
The analytical results for this report are presented by analytical test. Each set of data includes<br />
sample identification information, analytical results and the appropriate detection limits.<br />
Analyses requested<br />
PCBs (Aroelor-1254) by EPA 8080. ICP-Trace Metals (Lead) by EPA Method 6010. Mercury<br />
by EPA Method 7471.<br />
III. Quality Control<br />
A Laboratory Control Sample and Method Blank were analyzed with each preparation batch<br />
MatrixSpike and Matrix Spike Duplicate analyses were performed per the protocol for each<br />
analyte in this SDG.<br />
IV. Definitions<br />
The following codes were used to denote laboratory quality control samples and can he found in<br />
the data summary secti-)n of this report:<br />
QCBLK- Quality Control Blank, Method Blank<br />
QCLCS- Quality Control Laborator y Control Sample. Blank Spike<br />
V. Comments<br />
0 000 63
Bechtel <strong>Hanford</strong> Incorporated<br />
April 21. 1998<br />
Project Number: 550.260<br />
SDG: W02275<br />
Page 3<br />
f,mbanterra<br />
Environmental<br />
Som, e,<br />
Shipping and Receiving<br />
There are no comments or nonconformances associated with the shipping and receivin g of these<br />
samples.<br />
Wet Chemistry<br />
Percent Moisture analyses for the solid phase samples were requested after the priority results<br />
were reported. A Percent Moisture report was transmitted by facsimile on April 13, 1998.<br />
PCBs<br />
There are no comments or nonconformances associated with this analysis.<br />
Metals<br />
Percent solids was not determined for the samples in SDG W02275. Due to software<br />
configuration, the CLP forms list solid sample result units as " dry weight" and `7 solids as "<br />
100 ". The results on the forms are actually mg/Kg as is and are not corrected for percent<br />
solids. The figure of 100 was used as percent solids for calculation purposes only and does not<br />
represent measured solids content of the samples.<br />
The percent difference for the Lead serial dilution (12.9) was greater than 10. therefore all<br />
associated data was flagged with a "E".<br />
I certify that this data package is in compliance %vith the SOW. hoth technically and for<br />
completeness, for other than the conditions detailed above. Release of the data contained in this<br />
hard copy data package has been authorized by the Laboratory Manager or a designee. as<br />
verified by the following signature.<br />
Reviewed and approved:<br />
Robert E. White<br />
Project Manager<br />
000-00y
Control #: B98-043<br />
Sample Disposition Record Revisionu: O<br />
Section 1 - BACKGROUND<br />
SAF#: B98-061<br />
OU: N/A<br />
Project ID: 105-C Reactor<br />
Task ID: 9<br />
Sampling Event: 105-C Phase I & Phase If<br />
Laboratory: Quanterra Incorporated<br />
Project Coordinator: WEISS, RL<br />
Task Manager: ARMATROUT. JF<br />
Section 2 - SAMPLE INFORMATION<br />
Number of Samples: 15<br />
Date Initiated: 3/17/98<br />
ID Numbers: BON680, BON681, BON683, BON684, BON686, BON687, BON688. BON691, BON692, BON693. BON694,<br />
BON682, BON685, BON689, BON690<br />
MATRIX:<br />
Collection Date:<br />
Section 3 - ISSUE<br />
N/A<br />
Class: Lab Direction<br />
NCR Number: N/A<br />
Type: Multiple Phase Sample<br />
Description: Concrete samples were wet ground in the field. The procedure resulted in too much liquid for analysis of the<br />
samples as a single phase<br />
NCR Validation (Print/Sign) Date<br />
Section 4 - DISPOSITION<br />
Type: Use As Is<br />
Description: For all samples, separate liquid from solid phase and analvze liquid for CrVI. For the following, assign new<br />
sample numbers as shown to liquids and analvze liquid for all other consitituents identified for solid.<br />
BON680(solid) to BON894 (liquid), BON683(solid) to BON895(liquid ). BON686(solid) to BON896(liquid),<br />
BON68 (solid)<br />
to BON897(liquid), BON692(solid) to BON898(liquid)<br />
ol L '<br />
Project Coordinator (^^PnL""Sign) Date<br />
ARMATROUT, JF<br />
Task Manager (Print/Sign Date<br />
N/A<br />
QA (Print/Sign) Date<br />
Section 5 - INSPECTION (Issue Class: Nonconformance Onlvl<br />
N/A<br />
Inspection Number: N/A<br />
Inspection Results: N/A<br />
Inspector (Print/Sign) Date
Ouanterra April 13, 1998 10:47 am<br />
Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev.<br />
Master Sample Login: 17199<br />
Project Manager: N. Price<br />
Draft: final: Entered and Reviewed by:<br />
{,M^<br />
L^J ^{-^ PM Review:<br />
Sample Header Template:<br />
WO 22 75IAJC 2P,6<br />
y<br />
2 ,^^fy<br />
Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Rad Category Red Semple ND.<br />
Comments<br />
# Container Type Analysis Class Preservative AnaL. Due Date Hold Date <strong>Site</strong> (Container Numbers:% Filled)<br />
Data:<br />
17199-001 BON680 Solid 09- 14AR-98 10:30 09-MAR-98 13:42 27-MAR-98 AIRBORNE 3<br />
RICHLAND I.D. 80316001///ICAPT = PS ONLY.<br />
1 PH - Plastic-250m1 HG/7471/04 S COLD 23-MAR-98 06-APR-98 R58<br />
1 ICAPT/6010/04 S COLD 23-MAR-98 05-SEP-98 R5 11<br />
1 PCB/8080/04 S COLD 23-MAR-98 23-MAR-98 R58<br />
1 PM/17/04 S COLD 23-MAR-98 05-SEP-98 R58<br />
17199-002 DON681 Solid 09-MAR-98 13:45 09-MAR-98 15:15 27-MAR-98 AIRBORNE 1<br />
RICHLAND I.D. 80316002///ICAPT = PB ONLY.<br />
1 PN - Ptastic-250mL HG/7471/04 S COLD 23-MAR-9B 06-APR-98 R5B<br />
1 ICAPT/6010/04 S COLD 23-MAR-98 05-SEP-98 R5B<br />
2 PCB/8080/04 S COLD 23-MAR-98 23-MAR-98 R5 1;<br />
1 PM 1 IT/04 S COLD 23-MAR-98 05-SEP-98 R56<br />
17199-003 SON681 FILTRATE Liquid 09-MAR-98 13:45 09-MAR-98 15:15 27-MAR-98 AIRBORNE 1<br />
RICHLAND I.D. 80316002///ICAPT = PB ONLY.<br />
1 PM - PlastiC-1 1- HOLD//04 S COLD 23-MAR-98 19-MAR-98 R5B<br />
17199-004 SON894 Liquid 09-MAR-98 10:30 09-MAR-98 12:15 27-MAR-98 AIRBORNE 1<br />
RICHLAND I.D. 80321501///ICAPT = PB ONLYWUSE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17199-001.<br />
1 PH - Plastic-1 1- HG/7470/04 S COLD 23-MAR-98 06-APR-98 EMPTY<br />
1 ICAPT/6010/04 S COLD 23-MAR-98 05-SEP-98 EMPTY<br />
1 PCB/8080/04 S COLD 23-MAR-98 16-MAR-98 EMPTY<br />
O C<br />
3- =Sample has not been rad screened.<br />
R7045-001 tv 8 -2 2 -7`<br />
(364122:20) J<br />
Page 1<br />
(364122:20)<br />
(364123:21)<br />
(364122:20)<br />
Screening not Required<br />
(364312:2D)<br />
(364312:20)<br />
(364313:21 364323:22)<br />
(364312:20)<br />
(364316:99)<br />
Screening not Required<br />
Screening not Required-<br />
(364317;99) (J<br />
(364317:99)<br />
(364317:99)<br />
'fJ
Chain of<br />
Custody Record<br />
QUA 4124 0797<br />
Client<br />
gS^ 7 e p^ °^ ^C ^t K<br />
IYU^S!<br />
Project Manager<br />
Dale<br />
C#^l,^Q<br />
1 ^^'C^<br />
,^ SIG ^ R<br />
Address Telephone Number (Area Code) ax Number Lab Number<br />
City Slate Zip Code S ite Contact Lab Contact Analysis<br />
s p (A ttach list if<br />
ace ce is needed<br />
Project Name( /^ ^ 0G<br />
Con(rac t/PUrchasJrderlQu u 00lee No.<br />
S<br />
(4//,(^(I<br />
Sample I.D. No. and Description<br />
(Containers for each sample may be combined on one line)<br />
GO<br />
CarnerANaybdi Number<br />
Matrix<br />
Containers &<br />
Preservatives<br />
Date Time = a ° o o<br />
Posslele na2ara ltlenbhCatlenJ npre ursposar<br />
U<br />
^.<br />
-<br />
Q'banterra<br />
Chain of Custody Numbe<br />
Page of<br />
Special ions ru ec<br />
Conditions of Receipt<br />
(A lee may be assessed i/samples are retained<br />
El Non -Hazard q Flammable El Skin le-dan( El Poison B Unknown Relurn To Chen l q Disposal By Lab q Archive For Months longer than 3 months)<br />
Turn Around Time Required OC Requirements (Speci fy)<br />
l /^ ) ^"J<br />
q 24 Hours J [1 48 Hours q 7 Days q 14 Days V21 Days q Other<br />
^ReMrqu a y' I 1 I^ r - lane 1. ecerved D e Time<br />
—<br />
If<br />
Relinquished By Date Time . Received By Date Time<br />
G elrnquished By Dale Time 3. Received By Date Time<br />
DISTRIBUTION. WHITE - Slays with the Sample, CANARY - Returned to Cleat with Report, PINK - Field Copy<br />
I<br />
I`<br />
I
I<br />
Chain of<br />
Custody Record<br />
S I CDJa'D<br />
QUA 4124 0797<br />
Client Project Manager 1<br />
1 Q^^^<br />
of<br />
Address Telephone Number (Area Code)/F Number Lab Number<br />
C it<br />
y State Zrp Code <strong>Site</strong> Contact Lab Contact<br />
Project Name J ]\ ! Carner/Waybill Number<br />
Contract/Purchase Order/Quote No.<br />
Sample 1. 0. No. and Description<br />
(Containers for each sample maybe combined on one line)<br />
Matrix<br />
Containers &<br />
Preservatives<br />
Date Time o _ "e n el `^ o = 0 a s 0<br />
N i<br />
Analysis<br />
more space<br />
^3 -1ZS1<br />
(Att<br />
ach list if<br />
is needed<br />
^iivanterra<br />
Chain of Custody Numbe<br />
Page o1<br />
Special Instructions/<br />
Conditions of Receipt<br />
9L 8 g ---<br />
ra v 3 v q C^ ^/ v l^ 8<br />
L1 Non -Hazard q Flammable El Inifant El Poison B<br />
I p<br />
Unknown<br />
rpie lapVSa1<br />
7 Realm Io Client q Disposal By Lab q Archive For Months<br />
(A lee maybe assessed it samples are retained<br />
longer than 3 months)<br />
Turn Around Time Required\^ /<br />
-/<br />
--D o! hlours El Hours El 7Days El 14 Days ^J 21 Days<br />
'Alh fy<br />
l<br />
q I Ulher f I ^ I IJ Kn<br />
J<br />
QC Requirements (Speci fy)<br />
I 5 n( /.k:r 1<br />
LO<br />
..- .. .............. ..r 3are<br />
1. l (/Ll^'V<br />
elinquisheOBy Date Time 2 Received By Data Time<br />
Relinquished By Date Time 3. Receiver) By I Date I Time<br />
DISTRIBUTION: WHITE - Stays with the Sample; CANARY - Returned to Client with Repo"; PINK - Field Copy
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-01 page I of<br />
Collector Company Contact 'Telephone No. Project Coordinator Data Turnaround<br />
R. Fahlberg Steve Marske 373-4316 WEISS, RI.<br />
Project Designation<br />
105C Phase I k Phase If -Conc<br />
Sampling Location AF No.<br />
21 Days<br />
re te Samples 100 A re a B98-061<br />
fee Chest No. Field Logbook No. Melbod of Shipment<br />
_ 3 [land deliver<br />
Shipped To<br />
Quanteria Incorporated<br />
POSSIBLE SAMPLE HAZARDSIREMARKS<br />
0.adiasetive<br />
Special Handling exciter Storage<br />
31 LD<br />
SAMPLE ANALYSIS<br />
T . to I<br />
U^V<br />
Bslte Property No.<br />
N /.^<br />
Preservation<br />
Type of Container<br />
No. of( onlainer(s) 2<br />
^<br />
21<br />
Volume<br />
l^<br />
IL<br />
See item(I)in<br />
Sp«ial<br />
Waiom<br />
SOI[^<br />
^I<br />
Bill of fading/Air illll No.<br />
Ali /!,J<br />
Sample No. Metric • Sample Dale Samplc'1lme *,5^ e<br />
ON680 D I Other Solid -^ y-^ e 10 3 J LCC44 0N k 4 0 1<br />
rI b<br />
x^So r, l- /+ Ce, Fws^ 7wbo<br />
SPECIAL INSTRUCTIONS / _- / Malris-<br />
CHAIN OF POSSESSION Sign/Print Names s<br />
s.,,i<br />
(1)ICP Metals- 6010A(Sigxi 1race) l l-eadl, Mvauy-7471- ( CV) , Chmmiom 11, 7196. '1 t..i.^,ra<br />
ehnquisbedB DalNrime ei By 1^ I Time PCB, X080 JArocl°r-1254 J, Gamma SpecnoscopY ((^"noo 117,C, ,hA60,Furapiuo M, 5p - c°hd<br />
3^ 'a l Aril ^'-7 ( Europium-154, Europium-1551: Amencium- 2 41, Iso topic Plutonium, Isotopic Uranium: Sele sl. - o"J"<br />
9 ^P.^CRIw I-.-t -l9<br />
e q Mime R edBY 1 f Datc/T^me<br />
NI alff -^03 Sf^ 1,9 - j7j/za 5 o wl•<br />
teJ — a I'9( T^t^<br />
y9 mot, ^o I l¢ Av; S^ IJ, 111 opt lnlida<br />
in wished By Daleffime Recei ed By Dalc/linen ] n1 u . 1 .pinr<br />
Nl Wipe<br />
inquished By Dale/rime Received By Date/rim, I I " z<br />
-J<br />
^.eeiau„<br />
nme,<br />
LABORATORY Received By<br />
SECTION<br />
—'lisle<br />
-__ _.. Uatu lime<br />
FINAI.SMIPLE<br />
DISPOSITION<br />
IXsptnal Method - U sposed Bs --------<br />
_<br />
Uatclllme<br />
__<br />
--<br />
1<br />
1
Y<br />
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES T 1198-061-02<br />
Collector Company Contact 'I elephant No. Project Coordinator DATA "I urnaround<br />
R. Fahlbcrg Steve Manske 3734316 WEISS, RL<br />
21 Days<br />
Project Design ation Sampling Location AF No.<br />
105-C Ph as e 1 R Phase II - Concrete Samples 100 Area B99-061<br />
Ice Ch est No. Field Logbook No. Method or Shipment<br />
Iland deliver<br />
Shipped To Mile Property 1. Bill of Ladin A BIII No.<br />
Quanterra In co rporated<br />
POSSIBLE SAMPLE IIAZARDS/REMARKS<br />
Radioactive<br />
Special Handling And/or Storage<br />
SAMPLE ANALYSIS<br />
903W -burin 6031(^I - ILLcr-<br />
Prae vAlinn<br />
Type of Container<br />
No. of Container(s)<br />
Volume<br />
Sample No. Matrix • Sample Dale Sample Time<br />
ONSB1 N Other Soliq<br />
P<br />
2<br />
IL<br />
6m imm,l, in<br />
Specid<br />
^o/^ D3/,<br />
3 /x/ Z- ^\Ir/ ^^ /d A ^ I<br />
SPECIAL[ TRUC'IIONS Q tau is<br />
CHAIN OF POSSESSION Sign/Print Names Vd ^.,. i<br />
(I)ICI'Meais- 6010A ISupenrace) 1[rid), 7471 (CV) Cluumimn Ile.-7196.<br />
e[i<br />
e'<br />
uished<br />
y<br />
Dale/Time<br />
^ ^ p/<br />
G<br />
DAINI'ime<br />
Reuiv<br />
ive<br />
B<br />
Y On<br />
Date/Time<br />
151<br />
- s<br />
PCBs-80801Atoclor 12541, Gamma Spectnosc. py(Cesium-U7. Cohxll-60, Europium-152,<br />
r-opium; 154, Eumpimm-1551; Amencium-241. Isotopic Plutonium; Isotopic IIranium, Sele<br />
SdPnl sn -^9<br />
r Ni[J^N (03 i Sr- $9 9a-- 7G I S^ "<br />
T h 9 q^, b0fl<br />
1 c-C7<br />
gl<br />
a<br />
tc<br />
"hat<br />
'^t3^.<br />
j<br />
'nquished By Date/Time Received By DaterTime !'^ 1<br />
ZD<br />
'ntonshed By Dalelfime Received By Dalerlime<br />
BORATORY 0.euived By<br />
SECTION<br />
Tine naie'I une<br />
FINAL SAMPLE<br />
DISPOSITION_<br />
Diallo»I Mahod<br />
--<br />
Uisrysscd -- By -- -<br />
- W(" (une<br />
1<br />
s•<br />
-<br />
_.<br />
r<br />
I<br />
^ra.,t,><br />
I<br />
Iv i<br />
I<br />
^ ;;'-?<br />
l
Client Sample Screening Results<br />
!0-Mar-98<br />
CLIE14TCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCPMB<br />
B M4CI /9/15981:42:00 PM 21A 7/10/199811:27:38 BOM4C1 30 16 A9^3777 e41 27.23 313<br />
IQUID Bk . 3/10/1998 :51 AM BKO 100 4 0.04 0 0.8<br />
AN Do /Ia1998 Alq: 3.00E-01 LDOEMI (DpM 3 .49E-01 (uCl/ 1.24E-05 CU 2.47E+01 ±2.3E+01 QA 0E+00 1.a0^<br />
t mLt 2.1 UdU: L Bet; 3.42E+01 So):fl. 2E-03 LIL): +03 ±8.7E+OI I 2.0<br />
Ue 'ylaq^<br />
BHI BOM4 422<br />
LIQUID<br />
3/9/1998 1:42:00 PM QUAD I 3/10/199811:23'38 AM<br />
7-. 3/10/19988:43:5 998 9:43<br />
BOM4C2<br />
IIK<br />
30<br />
100<br />
6<br />
3<br />
.17<br />
0.03<br />
202 3 937333 -<br />
/<br />
95/ 0.95<br />
AdD 3/1 Tol S., Alq: 3.00E-0 ^O^<br />
E401 Alp; (Dp 0 (uCU 807E-06 (p 1.6 01 ± 2. 4E4 01 AT E+00 Lob<br />
pt mR 2.6<br />
BHI BON680S<br />
NV: L<br />
3 /9/1998 1:42:00 PM QUAD24D<br />
Bel/Alq): /I.IIE I.1+OI<br />
c<br />
3 1 101 1998 11:23:51 AM BON690S<br />
Ljll):<br />
30<br />
3.01E+02 3 +01<br />
1130 37.6066667<br />
I<br />
124390<br />
Alq<br />
1.0E-0<br />
e<br />
4145, 4 333<br />
SOLID Bkg: 3/10/1998 8:43:35 AM BKO 100 6 0.06 90 0.9<br />
Ad Dol es 3/10/1998 To1Ee,Alq: 1.63E+02 9.81E401 Alp; (Dpm/.1.71E401 (uCU . 1.27E-02 (pCU -7.83E+01 ±9AE400 CAT 1.6E402<br />
Lab<br />
Pp/mp 88,1 / UNb: L me Bolt Alq), 9.19E+03 eo): 6. 116E+00 t4e)t 4.22E404 f 1.2E+02<br />
111 /<br />
2.48-03 Alt<br />
1•IL<br />
BHI BON681F 3 /9/19983:13:00 PM QUAD2 1 A 3/10/199811:54:54AM DON681F 30 3 0.12666667 96 2.4<br />
LIQUID like: 3/101 1998 8:43:51 AM BKO 100 4 0.04 8o 01<br />
Ad Delet 3/10/1998 Tot S., Alq: 1.80E+00 1.00E+01 Alp; (Dpm/ 3.23E-0 1 (uCU 2.62E-03 (pCU 1.45E+01 ± 2.4E+01 CAT 1.7E+00 Lab<br />
PptmL: 6.9 U nite: L / ml Bel; Alq): 4.79E+00 So): 3.88E-04 LIL): 2.16E+02 ±3.IE+01 I I 2.3E-ul Alq<br />
LIt<br />
BHI BON6919 3/9/I9983:I 3 :00 PM QUAD2 1 B 3/10/199811:54:54 AM BON691S 30 13 0.40333333 234 6.55<br />
SOLID BkL: 3/10/1998 8:43:31 AM BKO 100 3 0.03 95 0.95<br />
Ad Dole: 3/10/1998 Tot Se, Alq: 1.90E+02 1.15E+02 Alp; (Dpm/ 2.38E+00 (uCU 1.93E-03 (pCU 1.02E+01 +5.3E+00 CAT 49E400 L.b<br />
Pp/ me: 114.3 / Units: g i mg Bet; Alq): 1.35E+01 Sa): 1.16E-02 Lit): 6.08E+01 ± 4.6E+00 1 1.6E+00 Alq<br />
ide<br />
BHI BON69OF 3 /9/19981:42:00 PM QUAD24C 3/10/199911123:51 AM BON68OF 30 43 1.39333333 3426 113.39<br />
LIQUID Blig: 3/10/19989:43:55 AM BKG 100 4 0.04 81 0.81<br />
A nt Dole: 3/10/1998 Tot Se, Alq: 1.80E+00 1.00E+01 Alp; (Dpn3 4.48E-0 1 (uCU 3.64E-0 5 (pCl/ 2.02E401 + 2.2E+01 CAT L2E400 I..b<br />
N P t m 3.4<br />
P P Units; 1, ml Bet; AI 2.14E402<br />
9):<br />
n<br />
So :<br />
) 1.74E-02 L C): 9.66E+03 ± 1.7E+02 1 / 5.2E-03 Alq<br />
Ide<br />
10-Mar-98 Quan(erra Environment Se rvices, SCP V2.03 1
OateRme Received:<br />
FIVISM t<br />
SAMPLE CHECK-IN UST<br />
y J^/3 S start (^(/0^1^<br />
o<br />
Work Order Number 0 ^0 ^^ SAF i J 11S - " t<br />
Shipping Cantainv I-l<br />
1f<br />
b fain of Custody rt<br />
fi ^1<br />
RMSOW-43 -0003 -<br />
1. Custody Seals oosttpp- g mr I iietibf ? Yes [pw[ I<br />
Z<br />
Custody Seals dated and signed?<br />
Yes.H', [ I<br />
3. Chain-d-Custodf rer 9 d preswe Yes [ I<br />
1 t GC<br />
4. Cooler temperature<br />
5. VermicufiWpaddm materials is Wet [ j 'rl<br />
6. Number of samples in shipping =muter.<br />
Revision 5<br />
YT'^ ^'<br />
7. Sample holding 5nes exceeded? Yes [ ; uo [ }^<br />
8. Sampws have:<br />
pe hazard labels<br />
dy seats maple labels<br />
9. Sam s are_<br />
__,Lim good mrdifiaon kalong<br />
broken _gave air bubbles<br />
10. Where any anomalies identified in sanpte receipt? Yes (j No<br />
11. Description of anoma lies (utc'.ude sample numbers):<br />
Sample Custcdia n/Laboatnrf.* —X. LL LIu.^ Date:<br />
Telephoned To: Dn^_By<br />
0000 11
Five* 1<br />
SAMPLE CWCK4N UST<br />
DatePrme Received:^ J 1 `J7S SGS W(),U7J<br />
RFSHSOW 93-4003<br />
Revision 5<br />
ak<br />
Work Order Number 86310 + 164 1 SAF * e9<br />
g<br />
A -<br />
y<br />
Shipping Container 10:W635 a%& of Custody * Imo( (1 - U.9 1 - 0a<br />
1. Custody Seals an sltippi 9 container irfart? Yes Hl c ( ]<br />
2 Custody Seals dated and signed? Yes ( No ( ]<br />
3. Chain-of-Curb* n=rd present? Yes ]<br />
4. Cooler temperak re<br />
5. Vermiculite/pacidng materials is Wet [ Dry [ Y, /-A<br />
6. Number of swoes in shipping ccldai er<br />
7. Sample holding Imes exceeded? Yes [ ] No [ 9^<br />
8.<br />
3 '<br />
have:<br />
tape<br />
custody seats<br />
9. Sam are<br />
in good con diti<br />
on<br />
broken<br />
hazard lab els<br />
?ppo¢iate sample Labels<br />
kaking<br />
Rave air bubbles<br />
10. Where any anoma lies identified in sample receipt? Yes [ ] No [-]------<br />
11. Description of anomalies (in clude sample manbers):<br />
l eiepnui i^ 1 u. w by<br />
0<br />
Y<br />
600012
Environmental<br />
Contractor<br />
Contractor ERC Team<br />
Interoffice Memorandum<br />
M. A. St. John x.0-19<br />
40mm` Scc Below<br />
°"7e l;ebruary 27.1999<br />
0-o' S. L. Wi^ow<br />
RadCun Eaginceriag<br />
X3411531-070,<br />
wuEcr. CVHlF FSTTMATE FOR S111PP1NC CONCRFTF. CORE SAMPLES<br />
CCN: 055088<br />
Job So. n1 92<br />
W", O.P. Xft.I w<br />
w<br />
Oil a 1«c<br />
MA w<br />
$<br />
C. !LO<br />
The 1•olluwing calculations show that cvn: satnplawith a direct reading of equal to or less than<br />
400.000 dpm/100cm' will be below the de fi nitionafradimttive mate rial as defined in 49 CFR 173.40 3<br />
of 70 Bq/g (2F.3 pCi/g). L'ach sample will consistofcoacrcte mate rial from Ibur, two inch co re<br />
samples and enough wat er to make r slum consiotocy. The distrihution of radionuc lides is bussed tin<br />
previous concrete samples taker from the below grade Fad Storage Basin that would also he<br />
representative of these cuncrcte samples.<br />
iven:<br />
Cylinder Vulurrtc = ttr'h Radius ofcaocrcte core (r) = I inch<br />
Concrete Density = 2.35 g/cm' Height of care sample taken (h) - 0.25 inches<br />
27 pCi = Dq Maximum & Lt Wading on core = 40,000 dpm/ 1 UUcm'<br />
2?2 dpm = pCi<br />
Calculations:<br />
V - (3.14) (1 in.)'(U 25in) =0.78 in' (16.4 cm'/irrl(4 mix samples) = 51.2 cm,<br />
(400,000 dpm/51.2 cm') (cm'1235 g) = 3.32E3 dpdg<br />
3.32ED dpm/g (pCi/2.2 dpm) = 1.SE3 pCi/g or 9.4 8419<br />
SI.W:did<br />
Percent Distribution(7) Concemratina (oC: i/c)<br />
ACo 0.17 2.55 pCi/g<br />
'rrCs 82 1.2F3 pCi/g<br />
131 E 0.33 4.95 pCi/g<br />
134 E 0.05 7.5E-1 pCi/g<br />
'Sr 17 2.55E: pC ilg<br />
741 Am 0. W5 7.5F Z pCi/g<br />
n9 210p u 0.1 1.5<br />
TOTAL: 1.460 PCi/g<br />
C(2 j! 5E<br />
S. 6. Marske X5 -53<br />
P. A. Newman X3-41<br />
RadCun Enginee ring File/LB X0-23<br />
<strong>Document</strong> and into Se rvices 1 10-09 00001)
eo-Z/-7b 11=ZBA RAOCC" 373 an7o n - C.<br />
Environmental<br />
Restoration =RC Team<br />
Contractor<br />
Interoffice Memorandum<br />
To` D. A. St. John 1.0-19 da:<br />
`o^''`` Sec Below nmr:<br />
Concentration (vCi/e)<br />
2.55 pCi/g<br />
1.2F3 pCi/g<br />
4.95 pCi/g<br />
7.5E-1 pCi/g<br />
2.55E2 pCi/g<br />
7.5F.-2 pCilg<br />
1.5 '/<br />
I.46L3 pCi/g<br />
February 27. 1999<br />
S. L. Winslow<br />
RadCon Engineering<br />
X3-41/531-0706<br />
suwzcr: CU141F FSTIMATE FOR SHIPPING CONCRETE CORE SAMPLES<br />
Job N9.22192<br />
DrOr,. ww<br />
^Y^r ww<br />
a^. ieec<br />
AA<br />
S w,<br />
ww<br />
ibwl CeA. 41W<br />
CCN: 055088<br />
The following calculations show that cu re samples with a direct reading or equal to or less than<br />
400,000 dpm/100cm = will be below the de finition ol'radivactive mate rial as de fined in 49 CFR 173.40 1<br />
of 70 Bq/g (2F.3 pCi/g). Each slugrle will consist of comrctc material from tiour. two inch core<br />
samples and enough water to make a slur ry consistency. The distri bution of radionuc lides is based tun<br />
previous concrete samples taken f ro m the below grade Fuel Storage B asin that would also be<br />
representative of these concrete samples.<br />
"ven:<br />
Cylinder Volurnc = nr'h Radius of concrete core (r) = I inch<br />
Concrete Density = 2.35 g/cm' l leight of core sample taken (h) = 0.25 inches<br />
27 pCi = Bq Maximum direct reading on core = 400.000 dpm/lOUcm1<br />
2.22 dpnn = pCi<br />
Calculations:<br />
V = (3.14) (1 in.)'(0.25in) = 0.79 in' (16.4 em'/in) (4 mn; samples) = 51.2 cm'<br />
(400.000 dpm/51.2 cm) (cm'12.35 g) = 3.32E3 dpm/g<br />
3.3213 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 BWg<br />
S1. W AId<br />
"'Ca<br />
Percent Distribulion( 7o )<br />
0.17<br />
[IT<br />
CS 82<br />
12Eu 0.33<br />
"°Eu 0.05<br />
°0Sr 17<br />
7°'Am<br />
ZJ<br />
"PU<br />
0.005<br />
0.1<br />
TOTAL:<br />
C(! ics:<br />
S. G. Mtuske X5-53<br />
P. A. Newman X3 -4 1<br />
RadCun Enginee ring File/LB XO-23<br />
<strong>Document</strong> and Info Se rv ices HO-09<br />
GOOOi4
Quanterra 6W V S 014488<br />
Effiroameattl<br />
Son=<br />
Condi ti on Upon Receipt Variance Report<br />
St. Louis Laboratory<br />
3<br />
Client. _ Daze:_<br />
Project No: -Sz) 2- Initiated by: oz,<br />
f<br />
Shipper/No: A i r b• rrt C RFA/COC Numbers: l Q y L4<br />
Condition/Variance (Check all that apply):<br />
1. q Sample received b roken leaking.<br />
2. q Sample received without proper prese rv ative.<br />
q Cooler temperature not within 4C ± 2C<br />
q pH<br />
q other:<br />
Record temperature:<br />
3. q Sample received in improper con ta iner.<br />
4. q Sample received without proper paperwork. Explain:<br />
5. q Paperwork received without sample.<br />
6. q No sample ID on sample con tainer.<br />
7. q Custody tape disturbed broken/missing.<br />
q No variances were noted during sample receipt. Cooler<br />
/<br />
Login No.: / ^7/9'<br />
8. q Sample ID on con tainer does not match sample ID<br />
on paperwork. Explain:<br />
9. q III coolers on airbill not received with shipment.<br />
10. q Other (explain below!:<br />
Temperature Upon Receipt:<br />
Notes: C^ ' /, 5 ^— CJrt ^G(/t-e..s, So /cJl-I<br />
Corrective Action:<br />
A F C 0 1<br />
CL I/,<br />
/ L( 0 Lc t >fX<br />
v=<br />
q Client's Name: Informed verbally on: By:<br />
q Client's Name: Informed in writing on: By:<br />
q Sample(s) processed "as is".<br />
q Sample(s) on hold unt il : If released. notify<br />
Sample Control Supe rvisor Review: (or desienat Date<br />
Project Management Review: (A— 71 G.,i^,— Date: 3 — If — ^.3<br />
SL-ADMIN-0004. Rev¢ed 1121;95<br />
SIGNED ORIGINAL xIL:ST BE RETAI N-ED IN THE PROJECT FILE<br />
(p<br />
^rC—<br />
^i,Ji5
O<br />
C<br />
L=,<br />
C<br />
r4<br />
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-qb't'-0I<br />
Collector Company (outnel I elrphone No. Project f nnrdinalor Wim I or11Nr n11111I<br />
R. rahlberg Sieve Mnrske 171-411 1, WrISS, lll.<br />
Project Designation<br />
105-0 Ph ase 1 k Phase 11 -Concrete Samples<br />
Sampling Lo ca tion<br />
100 Area `<br />
'AF No.<br />
1198-0(I3<br />
Ice Ch iral No. Field Logbook No. Method of Shipment<br />
_ Iland deliver<br />
3<br />
fL<br />
Shipped To )Belie Property No. 11111 of LadInR/Al, IIIII No.<br />
Quenterra Incorporated N<br />
POSSIBLE SAMPLE IIALARDS/RE AIARKS<br />
Radioactive<br />
Special Handling and/or Storage<br />
8032150) G,<br />
g o3aic^oi<br />
I j^<br />
(S<br />
Preservation<br />
Type of Container<br />
No. of Conlabrer)s)<br />
Volume<br />
N°^r I -I<br />
P<br />
2<br />
IL<br />
5
1<br />
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST<br />
Collec tor<br />
R. 1'ahlhera<br />
Project Design ation<br />
105-C Ph ase I R Phase 11 - Concrete Samples<br />
Ice Chesl No.<br />
Shipped To<br />
Quanleres Incorporaled<br />
POSSIBLE SAMPLE IIAZARDS/REIIIARKS<br />
Radioactive<br />
Con+pany /'u ntact '1 e""'eNo.<br />
Alcvc 1,10,4C:171-4716<br />
Sampling Location<br />
100 Aren<br />
Field Lagbooh No.<br />
L: -- L — l r ,. `<br />
I<br />
Project (bnrdin ldw<br />
wFlxs. Ill.<br />
SA F No.<br />
I19 9 -01" 1<br />
Nlethad of Shipment<br />
(land deliver<br />
Offislic Properly No.. BIII of lading/Alr Bill Nn.<br />
il.i<br />
Prtacnalion<br />
I ype of fbnlRiner<br />
No. of Conlalner(s)<br />
Special llandlag end/or Storage<br />
go3a^ ^ &YPU oa<br />
SAMPLE ANALYSIS<br />
Volume<br />
Q^<br />
L<br />
BOA) 89<br />
%^I LL I r 1 UIL41--1 ID 11 1\-LUll<br />
p<br />
2<br />
IL<br />
a«^ Ii5 in<br />
063<br />
u9x-Iwt o4 i ' ' ye !n' !<br />
DAN 'l urnnnnmd<br />
'n'l^o'•a' +<br />
Sample No. Ma (rla• Semple Date Sample IIme N .. } vTe!.^. CVas , jl+^:n,tl ;]'-;a1 tf+ l! p^ ' sn-^<br />
Othar6eRd-<br />
1)<br />
^- /Q " 9 cT<br />
IAIN OF POSSESSION SIgNPrint Names<br />
R npuhhed ^<br />
/ '<br />
S O<br />
aldflm^ R ived By Daleyl irne<br />
el uished8 By DnNllme<br />
ReceNed0By Dat ime -G /<br />
Impoished By Wicnime Received By Wlerlime<br />
npuished By Dalerlime Received By Dale/lime<br />
BORATORY<br />
SECTION<br />
FINAL SA pIP1.E<br />
DISPOSITION<br />
21 Days<br />
Oft ^l y y^ x.,^%.- "7 _ +<br />
SPECIAL INSI RUCTIONS<br />
O ICP McWk 60104 S.. ( Pubacel lLeaJ), Mvcuq-7471-(CVI. Chromium tic.-7196,<br />
PCI]s; 1100.0 254 1. Omnma Speetrnscq, ICesimn-117, COWL-60. r:uropium 157,<br />
L.,.pmm . 134, Ellropium-1511, Amtpcitim-24 I', Isowrie Phllnili mn, knlnplc Upnnim, 5ele<br />
Q n+hc/ -^ 9 /l/r-l.Kel (o3 Sf -&'9 50-- yp,^ /jr•<br />
fi2o1299 ' Ci rbo t ^¢ ' 4c -iVr SCaot<br />
/<br />
Retsived By title Dam/lout<br />
Disposal Mtlhod UispuuJ Uy<br />
(^<br />
_—_—___<br />
Ualc/Iona<br />
hSAllli<br />
s s...l<br />
to o,6,1<br />
11 bade[<br />
u - ol<br />
4<br />
Ill<br />
WI<br />
u,<br />
q',re<br />
\, \f4' r<br />
^<br />
..
Bechtel <strong>Hanford</strong> Inc. CHAIN Ole CUSTODY/SAMPLE ANALYSIS REQUEST u^xyet^Dt ! "' -'<br />
olleclnr Company /'onlacl 'I elephone Nn.<br />
Project ('oordinalor<br />
R. rahlhcrg ./] Steve Mw4c 171 -4116<br />
N119 1" S. It 1.<br />
Project Designation Sampling Loca tion<br />
'AF No.<br />
105-C Phase 1 k Phase If - Concrete Samples 100 Arcn 1398-061<br />
Ice Cheat No.^l /I^/^^^<br />
JM 15<br />
_<br />
Field Logbook No. v<br />
Method of Shipment<br />
1lnnd deliver<br />
Shipped To Offdle I'ropnly Nu 11111 of Lading/Air 11111 Nu.<br />
Quanlena Incorporated AJ<br />
OSSIBLE SAMPLE IIAYAR/RERIARkS<br />
OS<br />
RWIosed.8<br />
pedalItandlingand/orStorage<br />
^<br />
1 l^lf{<br />
SAMPLE ANALYSIS<br />
1'yuerral an<br />
Type of Container P<br />
No. of Contriner(s) _<br />
Volume<br />
SD3^JS0e3 ^,,... gD^JC^3^<br />
See 11em 1)' n<br />
SMW<br />
Sample No. Matrix • Sample Date Sample I une ) l^I - l} y}grrGr y, +1iA l. 4j j ^,f{P S!,.. T 5 5,1 : 4 t "` r<br />
$ 0,(18 9 b G V('f1<br />
Other Becht- ^^^- ff ^^^ CD<br />
AIN OF PO ION Sign/Print Names<br />
li ish By /] ime 1 Ree y Uaro/f lne<br />
e 1 YI 0 1<br />
/<br />
ellnqu ithed By J DMNrime Received By % D.Wl,.c<br />
eiinquished By DatdTime Received By Date/1imc<br />
elinquished By DodeoM a Received By WWI u,<br />
t"oNr"""<br />
G<br />
6<br />
Ditta I nrnaround<br />
21 Days<br />
-- --<br />
SPECIAL INSTRUCTIONS Liavis<br />
(1) ICP Metals- 6010A ISupMmcel l Lead l'. Mncury -7471-(CV), Chrmnimn lln -7196,<br />
PCBs - R080 lAroclor-11541; Gamrna Spectroscopy (Cesium-137, Cuhah-60, Europium-157,<br />
N ropio n-154, EuropiumAinericimnPiuwnin,n;<br />
-1551, -141; Isumpic Isrnnpic thorn mn; .Sete<br />
/<br />
^/Gl^l ( u-k'I -^9j /Ul (,^^ - r03 SV'- 8 Cf ^jQ<br />
l<br />
—tzek 99 . Carbon 4; 11C ¢,v1hJ'<br />
/<br />
LABORATORY Received By<br />
_--_—_<br />
role umdGmc ._<br />
SECTION<br />
FINAL SAMPLE<br />
DISPOSITION<br />
Dispovl Method Ustwsed By - llaic lime<br />
5 1.<br />
9p S„i,4<br />
°,<br />
n, u., I,^,m<br />
t ..<br />
Nl nTr<br />
1
C^<br />
C-3<br />
C)<br />
1"J<br />
Cz<br />
Client Sample Screening Results<br />
12-Mar-98<br />
12-Afar-98<br />
Quanterra Environment Se rvices, SCP V2.03<br />
/ ^<br />
`N<br />
3I^ZI11^<br />
CLIENTCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCPMB<br />
Bill BON697 3/12/1998 QUAD2 1 A 3/12/1998 11:01:02 AM BON687 30 7 0.18 74 1.54<br />
LIQUID Bkg: 3/12/199812:01:04 AM BKO 600 32 0.05333333 556 0.9266667<br />
Ad Dole: 7/12/1998 Tot So, Atq: 1.00E+00 I.00E+00 ^ Alp; 3<br />
p; (Upm/ p - 8.19E-01 (uCU 3.78E-04 (pCU 3.78E+02 ±3.9E+02 CAT 6.6Ei..b<br />
-02<br />
Ppl mp 49 .6 / Units; 1 1 ml Bel; Alq): 3.27 E4 00 So): 1.48E-03 Leg): 1.48E+03 ± 2.8E+02 I 3.4E-0 2 X116
C<br />
U<br />
Client Sample Screening Results<br />
12-Mar-98<br />
v") ') 1 ^1 0<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM R<br />
POW BON0 119 3/12 1 1998 QUAD2 1 B 3/12/199811:01:02AM BON0 1-19 30 5 0.105 155 4 1733333<br />
LIQUID BkC: 3 1 12/1998 12:01:04 AM BKO 600 37 0.06166667 536 0.8933333<br />
And Date: 3 1 121 1998 Tot Sa, Alq: 1.60E+01 I.00E+OI Alp; (Dpm/ 2.08E-0 1 (uCi/ 1.50E-04 (pC'V 9.36E+00 ± 2.3E+01 CAT 2.7E+00 Lab<br />
Ppt mg: 7.4 i U nits: L ml Bet; Alq): 8.31E+00 Sa): 5.99E-03 LlC): 3.74E+02 ±3.7E+01 I 1.3E-01<br />
POW B0 1 , 1010 3/12/1998 QUAD2 1 C 3/12/199511:01:02 AM B0 1,10J0 30 7 0.18833333 148 4.0233333<br />
LIQUID RkC: 3/12/1998 12:01:04 A61 BKG 600 27 0.045 546 0.91<br />
An] Dale: 3/12/1998 Tot Sa,Adq: 1.60E+01 1.00E+01 Alp; (Dpm/ 4.81E-0 1 (uCV 3.47E-04 (pCt/ 2.17E+01 ±2.3E+01 CAT 1, 2E+00 Lab<br />
Ppt nil: 7.5 Units: L ! ml Bet; Alq): 7.89 E+ 00 Sa): 5.69E-03 LIC): 3.55E+02 + 3.6E+01 I 1.4E-01<br />
Iq<br />
Lit<br />
POW BONOJI 3/12/1998 QUAD2 1 D 3/12/199811:01:02AM BONO31 30 12 0.31166667 132 3 3 75<br />
LIQUID BkC: 3/ 12/199812:01:04 AAI BKO 600 53 0.08833333 615 1.025<br />
Ad Date: 3/12/1998 Tot Sa, Alq: 1.60E+01 / LOGE+01 Alp; (Dpm/ 9.54E-0 1 (uCV 6.88E-04 (pCi/ 4.30E+01 ± 2.7E+01 CAT 5.8E-0 1 lab<br />
P P1 m L 8.7 /<br />
Units: L ml Bet; AI9) 6.56E+00 Sal: ) 4.73E-03 L IL): 2.96E+02 + 3.4E+01 I 1.7E-01 Alq<br />
LIC<br />
POW B0 1,14 119 3/12/1998 QUAD22A 3/12 1 1998 10:40:55 Abt BON4119 10 2 0.14666667 10 0.135<br />
LIQUID BkC: 3/12.! 1998 12:01:14 MI BKG 600 32 0.05333333 519 0.865<br />
Ad Date: 3/12/1995 Tot Sa, Alq: 2.00E+00 I.00E+01 Alp; (Dpnd 4.31E-01 (uCV 3.88E-05 (pCi/ 1.94E+01 ± 3.4E+01 CAT 1.3E+00 Lab<br />
li ps ring: 2.7 / Units: L ml Bet; Alq): 1.65E-0 1 Sa): 1.48E-OS LAC): 7.41E+00 + 2.7E+01 I 6.7E+00<br />
POW BON541 3/12/1998 QUAD22B 3/12/1998 10:40:55 AM BON541 t0 2 0.15166667 22 1.2516667<br />
LIQUID BkC: 3. 12/199812:01:14 AM BKG 600 29 004833333 569 0.9483333<br />
,W Date: 3/12/1998 Tot Sa, Alq: 1.00E+00 / 1 OOF- 01 Alp; (Dpn t/ 4.34E-0 1 (uCV 1.95E-05 (pC'V 1, 95E+01 +3.6EWI UA2 13E+00 Lab<br />
Ppt ring: 2 / Unlls: L ml Bet; Alit): 2.30E+00 S.): 1 03E-04 LIC): 103C+02 + 4 .0E+01<br />
Alq<br />
N<br />
Lig<br />
1 Alq<br />
4 SE-01<br />
II I<br />
POW BON595 3/12/1998 QUAD22C 3/12/199810: 40: 55 ANI BON595 10 1 0-04333333 14 0.4783333<br />
LIQUID BkC: 3/12/1998 12:01:14 AM BKG 600 34 0.05666667 553 0.9216667<br />
0 Ant Date: 3/12/1998 Tot S&Alq: 2.00E+00 / I.00E+01 Alp; (DpnJ 1.14E-01 (uCV 1.03E-05 (p(-V 5.13E+00 +3.3E+01 CAT /4.9E+00 lab<br />
i<br />
C<br />
P Pt m G 2 / Units: L nil Bet, AI9h 8.68E-01 Sal: ) 7.82E-05 L IL ): 3 91E+01 + 3.2E+01 1 1.3E+00<br />
AIq<br />
1-IL<br />
12-Mar-98 Quanterra Environment Se rvices, SCP V2.03
K) 'ApItN<br />
CLIENT CODE ID MATRIXRECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
POW BON5 133 3 1 12/1998 QUAD22D 3/12/1998 10:40:55 AM BON5 133 10 1 0.055 22 1.2633333<br />
LIQUID Bkg: 3/12 1 1998 12:01:14 AM BKG 600 27 0.045 562 0.9366667<br />
AN Date: 3/12/1998 Tot Say Alq: 2.00E+00 1.00E+01 Alp; (DpM 1.27E-01 (uCV 1.14E-0 5 (pCV 5.71E+00 ± 3.5E+01 GAT 4.4E+00 Lab<br />
Ppt mg: 3.7 / units: ts: 1, ml Bet; Alq): 2.36E+00 So): 2.12E-04 Llg): 1.06E+02 ±4.OE1<br />
1<br />
4.7E-01<br />
AIy<br />
I-I[<br />
POW B01, 1589 3/12/1998 QUAD23A 3/12/1998 11:01:05 AM DON5 119 30 1 1 0.33166667 51 0.81<br />
LIQUID Bkg: 3/ 12/199812:0 1.20 AAI BKG 600 21 0.035 534 0.89<br />
AN Date: 3/12/1998 Tot Sa, Alq: 2.00E+00 1.00E+01 Alp; (DpM 937E-0 1 (uCV 8.80E-05 (pCV 4.40E+01 ± 2. 2E+01 CAT 5.7E-01 Lab<br />
Ppt P P mL 3.3<br />
Units: L ml Bet; AI9): 1.34E+00 Sa ) : 1.21E-04 L I[) 6.05E+01 + 2.0E+01<br />
1<br />
8.3E-01<br />
AN<br />
POW B0 1 , 1 50 3/12/1998 QUAD23B 3/12/1998 11:01:05 AM BONK5 30 5 0.09333333 40 0.3516667<br />
LIQUID Bkg: 3/12/1998 12:01:20 AA1 BKG 600 44 0.07333333 589 0.9816667<br />
Ant Date: 3/12/1998 Tot So, Alq: 2.00E+00 / 1.00E+01 Alp; (DpM 2.79E-0I (uCV 2.51E-0 5 (pCV 1. 26E+01 ±2.1 E+01 CAT 2.0E+00 Lab<br />
Ppt mg: 2 ,- U nits: L ml Bet; Alq): 6.12E-01 So): 5.51E-05 Llg): 2.76E+01 + 1.9E+01 I 1.8E+00 Alq<br />
POW B0N5D1 3/12/1998 QUAD23C 3/12/1998 11:01:05 Abl BON5D1 30 13 0.38666667 49 0.725<br />
LIQUID Bkg: 3/12/1998 12:01:20 AS1 BKG 600 28 0.04666667 545 0.9083333<br />
AN Date: 3/12/1998 Tot Sa, Alq: 200E+00 LOOE+01 Alp; (D i n/ 1.12E+00 (net/ 1.01E-04 (pC'I/ 5.05E+01 +2.3E+01 CAT 5.0E-0 I Lab<br />
Ppt mg: 2 / Units: L ml Bet; Alq): 1.17E+00 Sp: 1.06E-04 L [): 5.28E+01 ± 2.0E+01<br />
1<br />
9.5E-01<br />
AlqIt<br />
POW BON6 1`9 3/12/1998 QUAD23D 3/12/1998 11:01:05 AM BON6E9 30 8 0.21333333 32 0.1533333<br />
LIQUID Bkg: 3/12/1998 12:01:20 AAI BKG 600 32 0.05333333 548 0.9133333<br />
AN Date: 3/12/1998 Tot So, Alq: 1.00E+00 1.00E+01 Alp; (DpM 6.29E-0 1 (uCV 2.83E-05 (pCV 2.83E+01 ± 2.1E+0I CAT 8.8E-01 Lab<br />
Ppl mg: 0 Units: L ml Bet; Alq): 1.54E-01 So): 6.94E-06 LIg): 6.94E+00 + 1.6E+01 1 7.2E+00 AIq<br />
Id[<br />
POW BON6H0 3/12/1998 QUAD24A 3/12/199811: 00: 58 AM BON6110 30 4 0.06833333 36 0.2416667<br />
LIQUID Bkg: 3/12/199812:01:08 AAI BKG 600 39 0.065 575 0.9583333<br />
C^ Ant Dole: 3/12/1998 Tot Sa,Alq: 1.00E+00 I.00E+OI Alp; (Dpm/ 2.04E-01 (uCV 9.20E-06 (pCL/ 9.20E+00 +2.IE+01 CAT 2.7E+00 Lab<br />
(J<br />
Ppt mg: 0 Units: L ml Bet; Alq): 4.29E-01 So): 1.93E-0 5 Llg): I.93E+01 + I.BE+01 I 2.6E+00<br />
All "It<br />
12-Afar-98 Quanterra Environment Se rvices, SCP V2.03 2<br />
AIL<br />
1.1[
0uanterra March 23, 1998 03:02 pm<br />
Account: 10722 Project: 550.260 ouanterra-Richland OAS No. 550.26 Rev. 2<br />
Project Manager: N. Price<br />
Master Sample Login: 17200/1<br />
pf<br />
Draft: Final: Entered and Reviewed by PM Review: !/^/\—<br />
7^^1<br />
r 1 fw^<br />
Sample Header Template:<br />
.^ (`<br />
pll f,<br />
A j( 1'. F<br />
^'^ 1 - TOU^ 7<br />
+aT"rT'<br />
M^<br />
Of *007<br />
Sample No.<br />
Co<br />
Client ID C-Matrix Date: Collected Received Due Shipper Red Category gad SalRp(e No.<br />
mm ents<br />
N<br />
Data:<br />
Container Type Analysis Class Preservative Anal. Due Date Hold Date <strong>Site</strong> (Container Numbers:% Filled) I ,^ LZ-,^f<br />
L—<br />
17200-001 BON685 Solid 11-MAR-98 08;30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80320501//ICAPT = PIT ONLY//PCB 1254 ONLY///THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17200-005).<br />
1 PN - Plastic-1 1, HG/7471/Q4 S COLD 27-MAR-98 08-APR-98 R5B (364124:99)<br />
1 ICAPT/6010/04 S COLD 27-MAR-98 07-SEP-98 R5B (364124:99)<br />
1 PCB/8080/04 S COLD 27-MAR-98 25-MAR-98 R5B (364124:99)<br />
17200-OOIMS BON685 Solid 11-MAR-98 08:30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80320501//ICAPT = P8 ONLY/(PCB 1254 ONLY.<br />
1 PN - Plastic-1L HO/7471/Q4 $ COLD 27-MAR-98 08-APR-90 R58 (3641Z4:99)<br />
1 ICAPT/6010/04 S COLD 27-MAR-98 07-SEP-98 R58 (364124:99)<br />
1 PCB/8080/Q4 S COLD 27-MAR-98 25-MAR-98 R5B (364124:99)<br />
17200-OOlMSD BON685 Solid 11-MAR-98 08:30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80320501//ICAPT = PB ONLY//PCB 1254 ONLY.<br />
1 PH - Plastic-1 1. NG/7471/04 S COLD 27-MAR-98 08-APR-90 R56 (364124:99)<br />
1 ICAPT/6010/04 S COLD 27-MAR-98 07-SEP-98 R58 (364124:99)<br />
1 PCB/8080/04 S COLD 27-MAR-98 25-MAR-98 R5B (364124:99)<br />
17200-002 BON686 Solid 11-MAR-98 10:00 11-MAR-98 11:57 31-MAR-98 AIRBORNE 3 87042-001<br />
RICHLAND I.D. 80320502//THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17200-004).ICAPT = PIT ONLY.//PCB 1254 ONLY;<br />
1 PH - Plastic-1L HG/7471/Q4 S COLD 27-MAR-98 08-APR-98 R5B ' (364125;:99)<br />
1 ICAPT/6010/04 S COLD 27-KAR-98 07-SEP-98 R5B (364125:99)<br />
1 PCB/8080/Q4 S COLD 27-MAR-98 25- 14AR-98 R5B (364125:99)<br />
17200-003 BON687 Solid 11-MAR-98 13:05 11-MAR-98 14:20 31-MAR-98 AIRBORNE 1<br />
RICHLAND I.D. 80320503//ICAPT = Pit ONLY//PCB 1254 ONLY///THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17200.006)<br />
1 PN - Plastic-1 1.HG/7471/Q4 S COLD 27-MAR-98 08-APR-96 R5 0<br />
1 ICAPT/6010/Q4 S COLD 27-MAR-98 07-SEP-98 R58<br />
i PCB/8080/04 S COLD 27-MAR-98 25-MAR-98 R58<br />
,1-200-004 BON896 Liquid 11- 140 -98 10:00 11-MAR-98 11:57 31-MAR-98 AIRBORNE<br />
G RICHLAND I.D. 80321503//ICAPT = PS ONLY//AROCLOR 1254 ONLY///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17200.002.<br />
1 PN - Plastic-1 1.HG/7470/04 S COLD 27-MAR-98 08-APR-98 R5B<br />
d 1<br />
J i<br />
ICAPT/6010/04<br />
PCB/8080/04<br />
S<br />
S<br />
COLD<br />
COLD<br />
27-MAR-98<br />
27-MAR-98<br />
07-SEP-98 R5 11<br />
18-MAR-98 R5B<br />
3 - =Sample has not been rad screened.<br />
Page 1<br />
(364126:99).<br />
(364126:99)<br />
(364126:99)<br />
Screening not Required<br />
1 Screening not Required<br />
(364324p99)<br />
(364324:99)<br />
(364324:99)<br />
^^UO2LG^
Project Manager: N. Price<br />
Ouanterra March [3, 199B US:UC pm<br />
Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev. 2<br />
Master Sample Login: 17200<br />
Draft: Final: Entered and Reviewed by: PM Review:<br />
Samp le Header Template:<br />
Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Red Sample No,<br />
Comments<br />
p Container Type Analysis Class Preservative Anal. Due Date Hold Date <strong>Site</strong> (Container Numbers:% Filled)<br />
Data:<br />
17200-005 DON685 FILTRATE Liquid 11-MAR-98 08:30 11-MAR-98 11:57 31-MAR-98 AIRBORNE<br />
RICHLAND I.D. 80321501///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17200-001.<br />
1 PN - Plastic-1L HOLD//04 S COLD 27-MAR-98 21-MAR-98 R58<br />
17200-006 BON687 FILTRATE Liquid 11-MAR-98 13:05 11-MAR-98 14:20 31-MAR-98 AIRBORNE<br />
RICHLAND I.D. 80321503///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17200-003.<br />
1 PN - Plastic-1 1.HOLD//04 S COLD 27-MAR-98 21-MAR-98 R58<br />
r-,<br />
U<br />
C^<br />
3 - = Sample has not been red screened.<br />
Page 2<br />
t screening not ..R" !red<br />
(365372:99)<br />
1 Screening not Required<br />
(365373:99).
^<br />
Chain of<br />
Custody Record<br />
UOA 1134 11 19 7<br />
Cleat<br />
f3f^ l,lf^<br />
51<br />
Project Manager<br />
L 6 0^S^;C^<br />
t<br />
Dal<br />
I-Izr1^<br />
Address Telephone Number (Area Code)/F Number Lab Number<br />
Qty State Zip Code <strong>Site</strong> Contact Lab Contact<br />
Prolecl NameA ' -<br />
1<br />
Contract Purchase Order/Quo te No<br />
Sample 1. 13. No. and Description<br />
(C:onldumas for each sample may be combined on ono line)<br />
Date Time<br />
Carder/WaybIll Number<br />
Ma trix<br />
1 wh. - i a,ard munnncen m pyrnple rn 1-0 al<br />
^.-y I Non Hazard<br />
q Flam m able f] Skm hrifanf q Poison B Unknown I<br />
L ^XI<br />
f<br />
-Iurn Around Time Requeed<br />
^<br />
_<br />
--<br />
gefurn To Glianf<br />
4 flours q 4 8 Hours q 7 Days q 14 Days 21 Days q ^ Iher ^^ ^^ ^_<br />
„ q^ e N y<br />
Date ,^e<br />
h<br />
l<br />
^ y r ^ ^_^^^—<br />
I
Ilecldel Ilan ford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES T u9a-Obi-ul 1''b` !<br />
Collec for Counpauy Cnulocl 'I vlrphone No. Project l'unnlblalur I).Ia I or'us roond<br />
It I uhiber8 slave KSnu.ske 171-4116 VVV.1.SX, Ill.<br />
foujoel Designation Sampling Location<br />
105-4' Phase I & Phase II -Concrete samples<br />
100 Area `<br />
AFNo.<br />
1.—d)73<br />
lu Chest No. Fi eld Logbook No. Method of Shipment<br />
_ Iland deliver<br />
hipped To ORaI(e 1'rnperty Nu. IIIII of Ladil KIA it 11111 No.<br />
Qumncrra Incorporated N ^f- N 3f<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
RWlaanva<br />
pedal Handling and/or Sto rage<br />
A03^1 Sol /1 WmI<br />
^D 3^1^/I ^lGl<br />
SAMPLE ANALYSIS<br />
Preservation<br />
Type of Container P<br />
21 Days<br />
No. of Conlaiucr(s) 7 _.<br />
Volume<br />
IL<br />
Sn ium I , In<br />
I^^"^`I^°^•<br />
"'"o,<br />
sample No Matrix • Sample Da te sample'l imc ^`, ^", ', {^. ' 3g{ payenn '^ k 9 d 1<br />
LN-<br />
x"689- Other 6elirY<br />
S -^ C^^ /[^ ,^ L^ LCK,1!1<br />
e)N8 N L1eJ" 1<br />
l—L<br />
CILUN OF POSSESSION Sign/Print Names<br />
Reliogai.hed 05 r Dwe/yLne<br />
J -4'-Y a<br />
Iq c 1<br />
I P 2^^_, ^5 —<br />
Ic/time<br />
I<br />
eel d 0y<br />
l., A<br />
I /rim.<br />
I -1<br />
R edgy 1- ` / Ua1e/I'ime10'-<br />
eiu niched By UaWI...m Recei ed By WWI im. //<br />
ioquishcJ By Dwcil ne Received By D.ICIFimc<br />
IAIIOIIATORV<br />
SECIIt1N<br />
FINAL. SAKIPLE<br />
DISPOSII ION<br />
SPECIAL. INS'fRIICI'IONS<br />
I ICP Mail. - 6010A S,, nuce Leal ' Merco 7471 - CV Chromium Ilea 7196;<br />
NCB. - 8080 1Aroclor-13341; Gamma Spearosoupy IC.s om-137. Coba1660, Earopiwm 153,<br />
liuopiwm 154. Luopiow 1351. A... oral-741; 1.°mpic Plwmmun; bolapie Unnlmn: S ol e<br />
SeleR,w&- -'t9^ MLtCI-63 Sr- 5 5^ •<br />
3ri, o -- tDrn-1<br />
}Ee^t7^ - G0. r{J Uvl l¢ Fl cliv, t^ s^«-.,<br />
Received By Title Dmdfimc<br />
e•<br />
—<br />
f Q<br />
1,5 A..<br />
DL u,<br />
T 1.:<br />
W I W."<br />
I. Ilq.i J<br />
V yew^°n<br />
x 0Lh,<br />
I<br />
1_.<br />
l<br />
1<br />
Manix<br />
1LIDI<br />
so - Sa6d<br />
SL - 5;-1,<br />
w"`<br />
Di.po..I Mahal —. .-_<br />
- -- Urs 1,used o y Dale/1'imc --<br />
l=11<br />
4<br />
y
Iicchlel IlBnford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST lil8•h(fioI .,<br />
'ulleclor<br />
R Pnld6c tp<br />
Project D es ignation<br />
105 C Phase I & Phase 11 - Concrete Samples<br />
Coulpuly Con fact<br />
.1<br />
hour Nn.<br />
Slew Mnrskc :171-4116<br />
Sampling Location<br />
IDO Arco 1<br />
Ice Ch es t No. Field Logbook No.<br />
Shipped To<br />
Quanleua Incorpo rated<br />
POSSIBLE SAMPLE IIAZARDS/REAIARKS<br />
RaJioanirc<br />
peclal llandiing and/or Storage<br />
1: - L- — / I o ^ `<br />
Offrlle Proper ly No<br />
`Q<br />
Preservalion<br />
'Iypc of Container<br />
^60301^^ -m x,27 Da y<br />
SAMPLE ANALYSIS<br />
N^^•<br />
No. of Conlainer(s) 1<br />
Volume<br />
IL<br />
P<br />
,..3'nW a<br />
Project Courdlnalur or<br />
WI T S$, Ill.<br />
•AF No.<br />
1198- 061<br />
Alelhod of Shipment<br />
hand deliver<br />
Bill of LadinWAir Bill Nn.<br />
iV A<br />
fl urnaruund<br />
No....O^a 1<br />
21 Days<br />
Sample No Matrix • Sample Dare Sample ' I hoc 4y i -...<br />
Ilf 1Sk+x yux6^/3 eJ;<br />
gef^.I4I<br />
/5,;1'.^lfq ^' 1.<br />
60.1. -64 Other 6elicY ^- /o- 9v" t7 fl s'^ `^ ^<br />
..<br />
/<br />
x.o/^. , -•" 7 Yl t<br />
onl8 q S<br />
^'^'"<br />
IAIN OF POSSESSION Sign/Print Nunn<br />
R inquirhned 'pn\1 alelfim<br />
1L^5°, S^^ 3 I^ ' ^3<br />
R ived Dy Dalell'iine<br />
_ r,<br />
du uishcd DY Uale/Time R
0 J<br />
d<br />
^I<br />
C)6-3<br />
Ilechlel Ilanforll Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B9XybrBI<br />
Collector ,y-<br />
R. ISddhcrg 13I- ./(.J<br />
Project Designation<br />
105-C Phase I & Phase 11 -Concrete Samples<br />
Company Conlacl 'P
C^<br />
G<br />
LJ<br />
C%<br />
ry<br />
00<br />
Client Sample Screening Results<br />
12-Afar-98<br />
CLIEN'1' CODE 11) AIATIUX RECEIVED DETECIOB ACQ DATE SAMPLE<br />
DIII I1ON687 3/12 1 1998 QUAD21A 3/12/199811:O 1:02AM BON687<br />
LIQUID Bkg; 3/12/199012:01:04 AM BKO<br />
MINUTES CNTS A NET CPAI A CNTS 8 NET CPA1 B<br />
n<br />
30 7 0.18 74 1.54<br />
600 32 0.05333333 556 0.9266667<br />
Aid Ilde: 3/12/1998 To1 So, Alq: 1.00E +00 3 IAOE400 Alp; (Dyad 8 .39E-0 1 (uCll 3 . 78E-04 (pCU 3 .78E+02 ± 3 .9E+02 CAT / 6 .6E-02 Enk<br />
Ppl uq: 49.6Units; 1. nil Bel; M q): 3.27E+00 Su ) : IABE-03 uv: 1.48E+03 f 2.8E+02 1 3.4E-02 M<br />
q<br />
18<br />
12-Afar-98 Quamerra Environment Se rvices, SCP V2.03 1
Client Sample Screening Results<br />
12-A far-98<br />
CLIENT CODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
PGW BON0119 3112/1998 QUAD21B 3/12/199811:01:02AM BON0119 30 5 0.105 155 4.2733373<br />
I.IQIIIU BUZ: 3/12/1998 12.01:04 AM DKG 600 37 0.06166667 536 0.8933333<br />
Ad Dole: 3/12/1998 Tul Sy, AIq: 1.60E+01 1.00E+01 Alp; (Dpi./ 2.08E-0l (uCU 1.50E-04 (pC1/ 9.36E+00 ± 2.3E+01 CAT 2.7E+00 Lob<br />
1'07 me: 7.4 ! U.N.. L / ,.,1 U... el..+• v atc+nn co+. c ooc na .1-1. a an c.na - a I.,., I / , ac n<br />
. ALI<br />
l`G\V BONOJO 3/12/1998 QUAD21C 3/12/199811:01:02 AM UONOJO 30 7 0.18833333 148 4.0233333<br />
LIQUID 868; 3/12/1998 12:01:04 AM BKG 600 27 0.045 546 0.91<br />
AW hole: 3/12/1998 Tut So, Alq: 1.60E+01 1.00E+01 Alp; (Dpnd 4.81E-01 (uCV 3.47E-04 (pCY/ 2.17E+01 ±2.3E+01 CAT / 1.2E+00 Lob<br />
Ppl me: 7.5 Ud13: 1, / ml Bet; Alq): 7.89E+00 So): 5.69E-03 LIC): 3.55E+02 ± 3.6E+01 I 1.4E-0 I<br />
Alq<br />
LIJJ<br />
POW BONOJI 3/12/1998 QUAD2ID 3/12/199811:01:02 A t BONOJI 30 12 0.31166667 132 3.373<br />
I-lQU1U DUB: 3/12/1998 12:01:04 AM BK(J 600 53 0.08833333 615 1.025<br />
Ad Dote. 3/121998 Tut So, Alq: 1.60E+01 / LOGE 101 Alp; (Dpnd 9.54E-01 (uC'U 6.88E-04 (p(-'U 4.30Et0l ±2.7E+01 CAT S.SE-01 Lob<br />
Pptmt: 8.7 / Udta; L ml Bel; Alq): 6.56E+00 So); 4.73E-03 LIZ): 2.96E+02 f3.4E+01 I ! 1.7E-0 1 AN<br />
Ids<br />
POW BON4119 3/12/1998 QUAD22A 3/12/199810x40: 55 AM 13ON4119 10 2 0.14666667 10 0.135<br />
I.IQOID IIUZ: 3/12/1998 12:01.14 AEl IJKG 600 32 0.05333333 519 0.565<br />
AM Dole: 3/12/1998 Tut So, Alq. 200E+00 I.00E,01 Alp; (Dpnd 4.31E-01 (uC1/ 3. SSE-05 (pCU 1.94E+01 ±3.4E+01 CAT 1.3E+00 Lab<br />
Ppl mZ: 2.7 / IIn11o: L / ml Bel; Alq): 1.65E .01 So): 1.48E-05 LIZ): 7,41 E+00 f 2.7E+01<br />
I<br />
/ 6.7E+00 Alq<br />
148<br />
POW BON541 3/12/1998 QUAD22B 3/12/199810:40:55 AM BON541 10 2 1E 15166667 22 1.2516667<br />
LIQUID BUZ: 3/12/1998 12:01:14 AEI BKG 600 29 0.04833333 569 0.9483333<br />
Aul hole: 3/12/1998 - -- 'I'ul So, Alq. 100E+00 IO0Ei01 Alp; (Dpnd 4.34E-01 (ICY/ 1.951:05 (pCU I95E101 ±3.6Ef01 CAT 1.3E+00 I.ab<br />
Ppl n,Z: 2 ,/ UWte: L ml [let; Alq): 2.30E+00 So): 1.03E-04 J.IZ): 1.03E+02 ± 4.OE+01 1 4.8E-0 1<br />
KAV IJON585 3/12/1998 QLJAI322C 3/12/1998 10:40:55 AEI BON595 10 1 0.04333333 14 0.4783333<br />
(-_' LIQUID B4Z: 3/12/199812:01:14 AM BKG 600 34 0.05666667 583 0.9216667<br />
l<br />
AWnote: 3112/1998 '1'o1SO,Alq: 2.00E+00 IOOLM Alp; (Dpnd 1.14E-01 (ICU 1.03E-05 (pCY/ 513E+00 +3.3E+01 CAT 4.9E+00 Irb<br />
Ppl mZ: 2 / Units: I. ml Bel; Alq): 8.68E-01 So): 7.82E-05 Ilit): 3.91E+0I ± 3.2E+01<br />
I<br />
1.3E100 Mq<br />
Ile<br />
%2-Afar-98 Quanterra Environment Services, SCP V2.03<br />
y<br />
/<br />
LIL
C LIEN 'f('ODE 11) MATRIX RECEIVED<br />
PGW BONSBS 3/12/1998<br />
LIQUID<br />
Aul Dule: 3/12/1998 Tut Sa, Alq: 2.00E100<br />
C ='<br />
U<br />
Ppl me: 3.7 - Unllr, 1 1<br />
12-.A far-9H<br />
DETECTOR ACQ DATE SAMPLE MINUTES CN 'I'S A NET CPM A CNTS B NET CPbt B<br />
QUAD22D 3/12/199810:40:55 AM BON5B3 10 1 0055 22 1.2633333<br />
BkB; 3/12/199812:01:14 AM BKG 600 27 0.045 562 0.9366667<br />
LOOEt01 Alp; (B lind 1.27E-01 (uCV 1.14E-05 (p(-'V 5.71E100 ± 3.5E-1 01 CAT 4.4E+00 IAIJ<br />
ml Bel; Al 2-36E-100 So :<br />
9Y• ) 2.12E-04 1. 1.06Ei02<br />
ID:<br />
QDanlerra Environment Se rvices, SCP V2. 0 3<br />
t 4.0E+01<br />
I / AN<br />
4.7E-01<br />
1.18<br />
PGW 13ON5B9 3/12/1998 QUAD23A 3/12/199811:01:05Aki BON5B9 30 11 0.33166667 51 0.81<br />
LIQUID BkB: 3/12/1998 12:01:20 AM BKO 600 21 0.035 534 0.89<br />
Ail Dole: 3/12/1998 Tut So, Alq: 200E-100 LOOEi01<br />
1- pt 1n8: 3.3 ! 11 11113: 11<br />
Alp; (Dpnd 9.77E-01 (uCV 8.80E-0 5 (pCV 4AOE101 ± 2.2E+01 CAT 5.7E-0 1 l.ab<br />
Bel; Al it); 1.34E-100 So): 1.21E-04 1.18): 6.05Ei01 +2.OEi01 I 8.3E-01 Alq<br />
PGW BON5C5 3/12/1998 QUAD23B 3/12/199811:01:05AA1 BON5 42 5 30 5 0.09333333 40 0.3516667<br />
LIQUID BkB: 3/12/199812:01:20 AM BKG 600 44 0.07333333 589 0.9816667<br />
Aul Dune: 3/12 1 1998 '1'ol Sa,Alq: 2.00Ei OO / LOOE401<br />
Ppt m8: 2 / Un113: 1- ml<br />
PGW BON5U1 31 12/1998 QUAD23C 3/12/199811:01:05 AM BON5D1 30 13 0.38666667 49 0.725<br />
LIQUID BkB: 3/12/199812:01:20 AM BKG 600 28 0.04666667 345 0.9083333<br />
And Dole: 3 1 12/1996 Tut Sr,Alq: 2.00E+00 LOOEi01 Alp; (Dpm/ 1.12E+00 (uCV 1.01E-04 (pCV 5.05E+01 ±2.3E+01 CAT 5.0E-0 1 Lob<br />
Ppl nq,: 2 / Units; I- -/ ml Bet; Alq): 1.17E+00 So): 1.06E-04 1.^8): 5.26E+01 ± 2.0E+01<br />
1-18<br />
1 Alq<br />
/ 9.5E-01<br />
118<br />
POW BON6F9 3/12/1998 QUAD23D 3/12/199811:01:05AM BON6F9 30 8 0.21333333 32 0.1533333<br />
LIQUID BkB: 3/12/199812:01:20 AM BKO 600 32 0.05333333 548 0.9133333<br />
And Dote: 3/12/1998 'Iu1Su,Alq: 100E-100 1OOL101<br />
Ppi nq: 0 , Anita: L nit<br />
Alp; (Dpn3 2.79E-01 (uCB 2.51E-05 (pCV 1.26E+01 +2AE+01 CAT 2.0E+00 Lab<br />
Bet; Alq): 6.12E-01 So): 5.51E-05 1.18): 2.76E+01 ± 1.9E01 I 1.8E+00 Alq<br />
1-18<br />
Alp; (Dpn3 6.2913.01 (u( 'V 2.831:05 (pCV 2.83E101 ± 2.IEf01 CAT 8.8E-01 IAIJ<br />
Bet; Al it): 1.54 E-01 So): 6.94E-06 L1B): 6.94E+0U + 1.6E+01 I 7.2E+00 Alq<br />
1-18<br />
PGW BON6110 3/12/1998 QUAD24A 3/12/199811:0058AAI BON6110 30 4 0.06833333 36 0.2416667<br />
LIQUID BkB: 3/12/1998 12:01:08 Ali] BKO 600 39 0.065 575 0.9583333<br />
Aid D.w 3/12 1 1998 3'u1 So, Alq- LOOS+00 1.00E+01 Alp; ( Dpnd 2 .04E-01 (uCV 9 . 20E-06 (pCV 9 . 20E+00 + 2 . IE+01 CAT 2.7E+00 Lab<br />
Ppt ut8: 0 Un113: I. , ml Bel; Alit): 419E -01 So); 1.93E-05 LAB): 1.93E-1 01 ± L8E+01 I 2.6E-100 All<br />
1-18
uuanterra March e3, Tenn ua:ul pm<br />
Project Manager: N. Price<br />
Account: 10722 Project: 550.260 Ouanterra-Richland QAS No. 550.26 Rev. 2<br />
Master Sample Login: 1720<br />
1(^<br />
Draft: Final: Entered and Reviewed by: c<br />
///{//n)/
(l7<br />
Chain of ^,; . Qivanterra<br />
Custody Record<br />
OHA 41-A msr<br />
L c C'<br />
CbeN _ .^<br />
Project Manager<br />
C 6 a 1- ^C^<br />
Dat<br />
7-1 Z- e-1 ^<br />
AAdress Telephone Number (Area Code)/F Number Lab Number<br />
Ciry Stale Z1p Code See Contact Lab Contact<br />
Project Name . 0 / -- `<br />
C...Wact Purchase Ordedouote No<br />
r<br />
^) (^ '^'^^^ 1<br />
Sample 1, D. No. and Description<br />
(Gonlainers for each sample maybe combined on one line)<br />
Date Time<br />
Carne rlWayblll Number<br />
Matrix<br />
$ m y<br />
tL I _ _ I t ^l .^,?<br />
3<br />
^<br />
d<br />
`^<br />
Containers s<br />
Preservatives<br />
o<br />
i i<br />
o<br />
2<br />
o<br />
ti i<br />
L, _<br />
Analysis (A ttach list it<br />
mores ace is needed<br />
-<br />
`<br />
Chain of Custody Numbe<br />
Page o!<br />
0131<br />
Special Instructions/<br />
Conditions of Receipt<br />
rossm;a rruam mennncaoon a1 7ple Disposal<br />
_ (A lea maybe assessed it samples a re retained<br />
Nun-f fazanl q Flarmnabla q SkWn I...1, - q Poison B Llnknuwn H turn 10 Clent q Disposal By l ab q Arcbrvu Tor _. _ Months longer than 3 months)<br />
_-<br />
n AO,<br />
u round limo Regwred `pC Regmren^enls / (SpeutyJ r<br />
aft q aeROUm q 0ays [71a Days z1Days 11 her ^^ ^^ ^ (-^^'> of<br />
i ;had 3y^ -- -f -^<br />
-<br />
Date 1 _ Receued By Date Time<br />
- - -- - - -<br />
linq^ ^ncd Hy j -- ^ Date ^ Lrno 1. Received By -- --- - I Date I Time<br />
--<br />
9 ...... l¢'d B V<br />
-- - - ^ Dal -j e 7inm - 3. nor ceivod By OBIa Time<br />
Conmienis<br />
DISTRIBUTION: WFIITE SIeVS wnh the Sample. CANARY - Retumetl to Client with Report; PINK -Field Copy
Bechtel <strong>Hanford</strong> Inc. I<br />
'olleclor<br />
Il.I ,Iilbcfg<br />
Yo)ttl Iletgnallon<br />
105-C Phase 1 A Phase II - Concrete Samples<br />
cc Chest No.<br />
CHAIN OF POSSESSION<br />
^&.goohcd By<br />
J<br />
T.AIIOI1.51(1111' SVC- I ION<br />
FINAI. SARIPI E<br />
DISPOS1114 ON<br />
Incorporated<br />
POSSIBLE SAMPLE IIAZAHUS/a EMAn6S<br />
Ndloacdva r<br />
fly<br />
CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES'1<br />
Company ('nnlxrl ,'I el, phon y No. P rolerl Conr.11nxlnr<br />
slevc Mnrske 111 4116 wpISS. 111 ^J<br />
wrpling L oration -- AF NsS_<br />
fT^<br />
100 Arco 1195-1113<br />
Field Logbook No. McOlod of Shipment<br />
_- _ (-' Iland deliver<br />
Offdle Properly No. 1101 of Lading/Air 111<br />
N/ 1T ti /31<br />
Name<br />
`^<br />
I ,<br />
Preservation<br />
Type of Container P<br />
No. of ConlahrerlQ 2<br />
Special Handling and/or Slonge ^ _ ^<br />
Volume<br />
I'^-•<br />
/^ i M<br />
srr iom 111 in<br />
CSN<br />
^<br />
Il/IhLe• -, / i ^<br />
sryctid<br />
^0^2<br />
f^ SANIPL E ANALYSIS ^.,.--, cam lyn `li^^<br />
sample NO mairlx Sample [)are Sample 1111 I<br />
Other Sehd- S ^ C^ .^/<br />
I1 ^^ ^,'5)I<br />
I<br />
f- l4<br />
ime<br />
(1<br />
i 1)alc/lime<br />
DaINI c //<br />
Dmerime<br />
SPECIAL INSTRUCA IONS Matrix<br />
(<br />
s s.,d<br />
l) ICPMdAI - 60101 IS upcnrecel lLcadl; Aicrany-7471-ICV1;Chromiom Ilex-7196;<br />
S[ - s^^^^^.i<br />
PCnr- 110801Arociur 12541. Gamma Spcmmf
Uechlel <strong>Hanford</strong> Inc. CHAIN Ole CUSTODY/SAMPLE ANALYSIS Itl:QUES'1'<br />
Collector Company /'oulxcl 'I c1cphune Nu.<br />
R I :nhlherp<br />
Slcve Mprskc 371-1316<br />
Prnlrxt Ilaignallun<br />
105 C Phase I & Phase 11 - Concrete Samples<br />
smulpling Localion<br />
100 Area I<br />
Ice Chest No. Field Logbook No.<br />
(,-L _ I<br />
Shipped I<br />
1)uenlun Incnrpnu (ed<br />
Poss l"LL SAMPLE IIAZanusntEMARKS<br />
RaJiwclive<br />
Special llandling and/or Storage<br />
&^kooa e<br />
SAMPLE ANALYSIS<br />
Ondte 1'rup,rty No..<br />
A i/`J<br />
1'reservaliun<br />
ra, `<br />
e7<br />
'i ype of Container 1'<br />
No. of Containers)<br />
Volume<br />
IL<br />
,..,P.<br />
Sample No Matrix • Sample Date Sample 'I'6nc ° ^'<br />
7111<br />
3^'r als x,{S ee<br />
. -7<br />
'S P,? F x 5 ±•'SA<br />
^r 3-,<br />
: r<br />
Project Coordinator<br />
wFiss. RI.<br />
SAF No.<br />
1198-061<br />
Method of Shipment<br />
Iland deliver<br />
(sill of Lading/Alr 11 111 Nn.<br />
w<br />
8m6" -Q7 Other 6eRd- ^- /Q- iJ (!t'r7 K.a<br />
130AJ?q<br />
ILUN OF POSSESSION Sign/Print Nunn<br />
R inquished ll}<br />
\,,r<br />
"^ S •'<br />
c S oi,eJRy<br />
L',<br />
am/fim q1<br />
R ived Ry<br />
^^ ^^ 305 4<br />
Damn'imc<br />
Received By<br />
Dalen i1ne<br />
Dal nine,<br />
Rckslnls islmJ try<br />
Dalc/l unc<br />
ReccivcJ By Ila1c/I hnc<br />
U<br />
R ish
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST ^<br />
1198y<br />
!<br />
"olleclnr ,/- Company Contact 'Iclephnnt Nu.<br />
Project Coordinator<br />
Data Turnaround<br />
H. Iahlhcrg G . ^jl'j /(ter<br />
.s(eve hlnlske 171-4116<br />
wl;I%N. It<br />
1•rolal Iltsignal un Sampling Location i 'AF Nu.<br />
105 .0 Phasc I & Phase II - Concrete Samples 100 Area 1198-061<br />
Ice Chest No.l yJ p /^ G/ Field Logbaok No. hiclhnd of Shipment<br />
J M ^<br />
^1J{O _ hand deliver<br />
Shipped To Offsltt<br />
Quanlxn• Incorporated<br />
POSSIIILI: SAMPLE IIA7.AIInS/ItEhIAR6S<br />
NaJluadbe<br />
Special handling and/or Storage<br />
j<br />
-<br />
I<br />
pSAMPLE<br />
ANALYSIS<br />
Properly Nu<br />
I,^d<br />
1'rraerval nra<br />
'i'ype of Coulnbmr<br />
N11e<br />
No. of Canlalner( . ) )<br />
Vulwne<br />
P LI<br />
II,<br />
See Oem (I I in<br />
Special<br />
I."'."i°"^<br />
Sangdc No Matrix • Sample Dale Sample T rate l^ 5r , I '(rl,w<br />
}'I}) ^, ^r ll lr i ,;1'li ^<br />
I I ,111.<br />
Other Selhf- ^ -/^_ ^ ^(^O (D<br />
11 ^I i!: p1 1 ) 1 1<br />
E^ ^ _I +':13 :.!>
V<br />
CG<br />
C7<br />
Client Sample Screening; Results<br />
l3-,Igor-98<br />
QDanlerra Envi ronment Se rv ices, SCP V2.03<br />
(F-ji ,^I1^I1^'<br />
LIEN F( ME, 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPAIA CNTSU NETCP111B<br />
Bill 130N687 3/12/1998 QUAD2IA 3/12/199811:01:02 AM BON687 30 7 0.18 74 1.54<br />
uQIOD Bke: 3/12/199812x01:04 AM BKG 600 32 0.05333333 556 0.9266667<br />
Aid Dale: 3/12/1998 'ru(Sa,Aly; IOOE100 I.00Ei00 Alp; (Dpad 8. 39E-01 (uCV 3.78E-04 (pCl/ 3.78E)02 ±3.9Et02 CAT6.6E-02 Lab<br />
Ppl me: 49.6 Ihdb: L nd Bet; Alq); 3.27E400 Sa); 1.48):03 Lie): I48EiO3 ±2.SE402 I 3.4E-02<br />
Alq<br />
IAg<br />
1
Client Sample Screening Results<br />
12-A1ar-98<br />
(3d EN "I'CODE 11) MATRIX RECEIVED BET ECI'Olt ACQ BATE SAMPLE MINUTES CNTSA NETCPNIA CNTSB NETCPMB<br />
PGW BON01 1 9 3 1 12/1998 QUAD2 1 B 3/12/199811:01:02 AA1 BON0119 ---- _ 30 5 0.105 155 42733333<br />
LIQUID Bbe: 3/12/1998 12:01:04 AM BKO 600 37 0.06166667 536 01933333<br />
Aul Date: 3/12/1998 Tut Sa, Alq: 1.60E+0I I . 00Ei OI Alp; (Dpad 2.08E -0 1 (uCV 1 . 50E -04 (pCV 9 .36E+00 ± 2. 3Ei01 CAT 2 .7Ei00 Lab<br />
1-p1mt: 7. 4 ml Bel; Alq): 8.31E+00 Sal: 5.99E-03 1.18): 3.74 E+02 f 3.7Ef01 I ^ 1.3E -0 I<br />
P(iW BONOJO 3/12/1998 QUAD2IC 3/12/19981LO1.02AM BONOJO 30 7 0.18833333 148 4.0233333<br />
LIQUID Bbt: 3/12/1998 12:01:04 AM BKG 600 27 0.045 546 0.91<br />
AM Dule; 3 1 12/1998 T.1 Su, Alq: 1.60E-t01 1.00E+01 Alp; (DpnV 4.81E-0 1 (uCV 3.47E-0a (p(-'I/ 2.17E101 ±23E+01 CAT 1.2Ei00 Lab<br />
Ppt me: 7.5 Unk.; I- ! nO Bet;Alq): 7.89E + 00 Sa); 5.69&03 I.Ie): 3.55E +02 ± 3.6E +01 I IAE-01 AIq<br />
PGW BONOJI 3/12/1998 QUAD2ID 3/12/199811.01:02 AM BONOJI 30 12 0.31166667 132 3.375<br />
1.1Quil) B4t: 3/12/1998 12:01 04 AM 11KO 600 53 0.08833333 615 1.025<br />
Aul Dule: 3/12/1998 To1 Sa, Alq: 160E +0I / IOOEt01 Alp; (Dpud 9 . 54E-01 (uCV 6 . 88E-04 (pCV 4 . 30E101 ± 2.7E+O1 CAT 5 . 8E -0 1 Lab<br />
Ppt 1nt: 8.7 - Unit.: 1 1 111 1 11,1; Alq): 6.56E+00 SO 4.731: 03 I. le): 2.96Er02 ± 3.4E+01 I 1.7E-0I AN<br />
PGW BONAU<br />
AM DUle: 3/12/1998<br />
Ppl mt: 2.7<br />
I.IQIIID<br />
T.1 Sa, Alq:<br />
hull.:<br />
3/12/1998<br />
200E+ 00<br />
I.<br />
QUAD22A<br />
Ilbt:<br />
IDOf1 OI<br />
al l<br />
3/12/199810:40:55 A61 BON-0 1 9<br />
3 1 12/1998 12:01:14 AM BKG<br />
Alp; (OpnV 431E-01 (uCV 3.SHE-05<br />
BeQ AI 1.65E-01 Sa : 1.48E 05<br />
4)1 )<br />
10<br />
600<br />
( pCV<br />
llel:<br />
2 0.14666667<br />
32 0.05333333<br />
1.94Et01 ± 3AE+01<br />
741E+00 S 2.7E 101<br />
10<br />
519<br />
CAT<br />
1<br />
0.135<br />
0.865<br />
IIC<br />
1•le<br />
1 .3E100 Lab<br />
Alq<br />
6.7E 100<br />
1dt<br />
POW BON5 4 1 3/12/1998 QUAB22 11 3/12/199810: 41055 AM BON541 10 2 0.15166667 22 1.2516667<br />
I.IQ(IIO Bbt: 3/12/1998 12:01:14 AM BKO boo 29 004833333 569 0.9483333<br />
Aull).W 3 1 12/1998 1'u 1 Sa, Alq: IO01i+00 / I.00h WI Alp; (Dpud 4.34 E-01 (u('I/ 1.95E-05 (pCV 195Ef01 ±3.6E+01 CAT 1.3Ei00 Lab<br />
1'pt u1t; 2 Unll.: I. all Bet; Alq): 2.30E+00 Sa): 1.03E-04 1.18): 1.03E+0] ± 4.0Et01 I 4.8E-0I<br />
Aiq<br />
Idt<br />
POW BON585 3/12/1998 Ql1AB22C 3/12/19981OAU:55 AM BON585 10 1 004333333 14 0.4783333<br />
O I.IQIIID Itbt: 3/12/199912:01:14 AM BKO 600 34 005666667 553 0.9216667<br />
W AalD.Ie; 3/12/1998 '1.1 Sa, Alq: 2.001:100 100E-01 Alp; (Dpn) L14E-01 (u('U 1.03E-05 (pCV 5.13EfOO ±3.3Ei01 CAT / 49E+00 Lab<br />
PPI mg: 2 / lJnlla: I. al l llel; AI4) :) 8.68E-OI Sa : 7.82E-(15 LIt): 391E+101 ± 7.2Er01<br />
I<br />
1.3E 100 ` Iq<br />
4t<br />
1 2-Afhr-971 Quanterra Environment Se rvices, SCI' V2.03 1
CLIEN"1' CODE IB MATRIX RECEIVED<br />
POW BON5153 3/12/1998<br />
LIQUID<br />
And UWe: 3/12/1998 To( So, Alq: 2.00E+00<br />
Ppl n, g: 3.7 (Inlly: I.<br />
(') •Al212N<br />
DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
QUAD22D 3/12/1998 10:40:55 AM BON5113 10 1 0.055 22 1.2633333<br />
Bkg: 3/12/199812:01:14 AM BKO 600 27 0.045 562 0.9366667<br />
1.00E+01 Alp; (DpnV 1.27E-01 (uCV 1.14E-05 (pC•V 5.71E+00 ±3.5E101 CAT 4AE+00 Lob<br />
nd Bel; AI43: 2.36E+00 Sr ) : 212E-04 1. Ig): 1.06E+02 t 4.0E+01<br />
I • i<br />
4.7E-01<br />
Alq<br />
1.11<br />
PGW 11ON589 3/121998 QUAD23A 3/12/199811:01.05 AM BON589 30 11 0.33166667 51 0.81<br />
LIQUID Bkg: 3/121199812:01:20 AM BKO 600 21 0,035 534 0.89<br />
And Dute: 3/12/1998 Tot Se, Alq: 2.00E+00 1.00E+0I Alp; (DpnJ 9.77E-01 (UCU 8.80E-05 (pCV 4440E+01 +2,2E+01 CAT 5.7E-01 Lob<br />
Pp1 ntg: 3.3 Ihdis: 1- nd Bel; Alq): 1.34E+00 So): 1.21E-04 Ljg): 6.05E+01 ± 2.0E+0I 1 8.3E-01<br />
POW BON5C5 3/12/1998 QIJAD238 3/12/199811:01:05 AM DON50 30 5 0.09333333 40 03516667<br />
LIQUID Bkg: 3/12/199512.01:20 AM BKG 600 44 0.07333333 589 0.9816667<br />
And Dule: 3112/1998 3'u1 Se, Alq: 200E+00 / I.00Et01 Alp; (DpnV 279E-01 (uCV 2.51E-05 (pCV 126E+01 ±2AE+01 CAT 2.OEi00 Lob<br />
PpI mg: 2 / Uld1r: L m1 Bel; Alq): 6.12E-01 So): 5.51E-05 LIg): 2.76E101 ± I.9Et0(<br />
1<br />
1.8E+00 Alq<br />
Is<br />
POW BON5D1 3/12/1998 QUAD23C 3/12/199811:01:03 AM BON5D1 30 13 0.38666667 49 0.725<br />
LIQUID Bkg: 3/1211998 12:01.20 AM BKG 600 28 0.04666667 345 0.9083333<br />
AW nwe: 3/12/1998 '1'u1 S., Alq: 200E+00 1.00E+01 Alp; (DpL/ 1.12E400 (uCV 1OIE-04 (pCV 5.05E+01 ±2.3E+01 CAT 5.0E-01 Lob<br />
1-pt mg; 2 / troll.: L / ml Bel; Alq): 1.17E+00 Se): 1.06E-04 LIg): 5.28E +01 12.0E+01<br />
1<br />
9.5E-01<br />
Alq<br />
1-Ig<br />
PGW BON6i9 3/12/1998 QUAD23D 3/12/199811:01:05 AM BON61;9 30 8 0.21333333 32 0.1533333<br />
LIQUID Bkg: 3/12/1998 12:01:20 AM BKG 600 32 0.05333333 548 0.9133333<br />
Ant Dole; 3/12/1998 'IWS.,Alq: IOOE+00 LOOE101 Alp; (I)pm/ 6.29E-01 (uCV 2.83E-05 (pCV 2.83E+01 ±2.IEt01 CAT 8.8E-01 Lob<br />
Pp1 m g; 0 1 Una; ll<br />
1- ml Bel; Alq): 1.54E-01 So): 6.94E-06 LIg): 6.94E+00 ± 1.6E+01 I 7.2E+00<br />
PGW BON6110 3/12/1998<br />
LIQUID<br />
Aid D.1,; 3/12/1998 1n1 S., Alq: I.VV1.100<br />
CJ PlIt mg: 0 Unit.; L<br />
G<br />
QUAD24A 3/12/199811:00:58 AM BON6110 30 4 0.06833333 36 03416667<br />
Bkg: 3/12/199812:01:08 AM BKG 600 39 0.065 575 0.9583333<br />
1.000+01 Alp; (Dp / 2.046:-0I (tICV 9.20E-06 (pCV 9.20EWO ±21Et01 CAT 2.7E+00 Lob<br />
nd Bel; Alq): 4.29E-01 So): 1.93E-05 I.Ig): 1.93E+01 ± I_SEW)<br />
1<br />
2.6E/00 Alq<br />
LIg<br />
12-A/nr-98 Quanterra Environment Services, SCP V2.03 ?<br />
mq<br />
Ids<br />
A19<br />
LIg
uuanterra march ca, ivvo uo:ur pm<br />
n<br />
Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev. 2<br />
11 11<br />
Master Sample Login: 17203 ^Q.n is r1q<br />
".1,<br />
Pr ject Manager: U. Price ^^<br />
Fp4 o t<br />
Draft: Fine L- Entered and Reviewed by: PM Review:<br />
Sample Header Template:<br />
Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Red Sample MD...<br />
Cements:.<br />
# Container Type Analysis Class Preservative Anal. Due Date Hold Date <strong>Site</strong> (Container Nudaers:% Filled) 1 1^ ?-I ^S<br />
Data: W<br />
17203-001 BON688 Sot id 12-MAR-98 09:15 12-MAR-98 13:53 01-APR-98 AIRBORNE Screening note. Required<br />
RICHLAND I.D. 80322101//ICAPT = PH ONLY///PCB r S = AROCLOR - 1254///THIS SAMPLE MUST BE FILTERED TO CREATE FILTRATE SAMPLE 17203-004.<br />
1 PH - Plastic-1 1 - HG/7471/g4 S COLD 26-MAR-98 09-APR-98 R108 (364154¢99) .<br />
1 ICAPT/6010/04 S COLD 26-MAR-98 08-SEP-98 R108 (364154:99)<br />
1 PCB/8080/04 S COLD 26-MAR-98 26-MAR-98 R10B (364154:99)<br />
17203-002 BON689 Solid 12-MAR-98 13:15 12-MAR-98 14:30 01-APR-98 AIRBORNE. 3 R7043.001<br />
RICHLAND I.D. 80322102//THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17203-003).ICAPT =.PB ONLY///PCB r S = AROCLOR - 1254.<br />
1 PH - Plastic-1 1 - H 61 7471/g4 S COLD 26-MAR-98 09-APR-96 R108. (364155:99)<br />
1 ICAPT/6010/04 S COLD 26-MAR-98 08-SEP-98 R10B (364155:99)<br />
1 PCB/8080/04 S COLD 26-MAR-98 26-MAR-98 R10B (364155:99)<br />
17203-003 BON897 Liquid 12-MAR-98 13:15 12-MAR-98 14:30 01-APR-98 AIRBORNE 1. Screening not Required<br />
RICHLAND I.D. 80324101//ICAPT = P8 ONLY//AROCLOR 1254 ONLY///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17203-002.<br />
1 PN - Plastic-IL HG/7470/04 S COLD 26-MAR-98 09-APR-98 RIOS (364325;99)<br />
1 ICAPT/6010/04 S COLD 26-MAR-98 08-SEP-98 R10B (364325:99) ^.VO L L<br />
_a<br />
b11<br />
1 PCB/8080/04 S COLD 26-MAR-98 19-MAR-98 R10B (364325:99)<br />
17203-004 BON688 FILTRATE Liquid -. 12-MAR-98 09:15 12-MAR-98 14:30 01-APR-98 AIRBORNE 1 Screening not'; Required.<br />
RICHLAND I.D. 80322101///USETHIS EMPTY BOTTLE FOR ` FILTRATE FROM SAMPLE 17203.00 1.<br />
1 PN - Plastic- 1 1. HOLD//04 S COLD 26-MAR-98 22-MAR-98 R108: (365376:99)<br />
r-.<br />
._ l<br />
CG<br />
3 . 4$amipte has not been rad screened.<br />
Page 1
Chain of<br />
Custody Record<br />
QUA 4124 0797<br />
S1 ^ N_^` 1)<br />
Client ^ ^ Project Manager ^ ^ Date _ ^ ^7<br />
Address Telephone Number (Area Code)/ ax Number Lab Number<br />
City State Zip Cotle <strong>Site</strong> Contact Lab Contact<br />
Pooled Name /"^ r/ /' f- ^-^ ^ ^<br />
I('<br />
/fi<br />
Contract Purchase Order/Quote No<br />
` Sample 1. D. No. and Description<br />
(Confamen for each sample maybe combined on one line)<br />
C/^/^//A<br />
Date Time<br />
^ I C^ ^° '7 C'^^l In ^<br />
CarrienWaybill Number<br />
Matrix<br />
gg<br />
g<br />
a m y j<br />
y<br />
=<br />
Containers &<br />
Preservatives<br />
"o<br />
i =<br />
o<br />
2<br />
^o<br />
^'<br />
u Q L (/tl (1JC<br />
Analysis (A ttach list if<br />
mores ace is needed<br />
Qi^uanterra<br />
Chain of Custody Numb<br />
I I<br />
Page 1 of 1^<br />
Special Instructions/<br />
Conditions of Receipt<br />
t`oss,ole Hazard lde identification I Saprple Disposal<br />
—t^ DC1J<br />
1t^l ^ Non<br />
lee may be assessed it samples are retamed<br />
q Non Hazard q Flamma ble [ImSk Initanf q Poison B Unknown 1 Be(,, Return , To Client q Disposal By Lab q Archive For Months longer than 3 months)<br />
Tum Around Time Required OC Requirements (Specify)<br />
q 4 Hnprs q 45 Hours q T Days q 14 Days W,<br />
..._....^ _.. _r<br />
C`)<br />
I Days q<br />
Olhor I<br />
L^<br />
1. Received By<br />
.... ..,, .. r<br />
eLnquuhed By IDate<br />
Time 3. Received By<br />
DISTRIBUTION WHITE Stays with the Sample. CANARY - Returned to Client with Report; PINK - Field Copy<br />
0 too<br />
Date I Time<br />
^..
Bechtel HanforJ Inc. CHAIN OF CUSTODY/SAMI'Lle ANALYSIS REQUEST' 119A ^ 111 • 1•"e I d I<br />
Collector longsanp ('onlaC( 'Velephone Nu, Project Coordlnalor Ilala 'Fonurnund<br />
R. Foblbcrg<br />
Project D esignation<br />
105 .0 Phase 1 k Phase 11 - Concrete Samples<br />
Steve Marskc<br />
SamplingLocation<br />
100 Area<br />
1373-4316<br />
-<br />
WEISS, RI.<br />
SAF Nn.<br />
IIUR-11(/-g<br />
21 Days<br />
let Chest No. Field Logbou l, No. Method of Shipment<br />
.133 _Z (land deliver<br />
Mpped'i a<br />
Quanlerra Incorporated<br />
Ilfraile 1•roprrly Nu. But of L..il It1A Ir 11111 Nu.<br />
•OSSIIII.E SAMPLE IIA%ARDS110:141ARKS<br />
RWltsacllve<br />
1're.ervalnn<br />
7)penf Conbiner<br />
N"ne<br />
P<br />
Special Ilandling and/or Storage<br />
1/<br />
7(03^^' ► L/1`-
^^^ tr al<br />
Restoration Reatoratlon<br />
Team<br />
CCN: 055088<br />
Jo ^ IItn<br />
Contractor %.0W "^^"'r<br />
Interoffice Memorandum aI{y W<br />
TP D.A. St, Jahn 1.0-19 sac February 27.19%<br />
Cnrua!<br />
Scr Below pp1t S. L^i^ow<br />
Ra dCun Eagim coat<br />
)C,-41/531 -0700<br />
suaaacr: CURIF. FSTIMATE FOR 51i1PPLN000lWRETE CORE SAMPLES<br />
W r<br />
II^Orr<br />
The rullowing calculations show that cue somplawiih a direct reading of equal to ur lesis lhaa<br />
400.Uou dpm/1 o0em r will be below the definitiaoafrar liu=tivc material as defined in 49 CFR 173.40<br />
of 70 Bq/g (2>; pCi/g). Lath sample will cunsistof cm=ctc material from ruur. two inch ton<br />
samples and enough water to ma4 a shiny constancy. *Me distribution of radionuclides is bar d tin<br />
previous concrete samples Ld= fmm the belowgrr)e Ferl Storage Basin that would also Ix:<br />
Nprescntative of these cuncrae samples<br />
iver,<br />
Cylinder Vulunie nth Radius of cwa= core (r) = I inch<br />
Concrete Density = 2.35 g/cm 116ght of mwswoc taken (h ) - U15 inches<br />
27 pCi = Dq<br />
2?2 dprn = pCi<br />
Mxdmtun di nt among on tort = 400.000 dpr. 3 :UUcm<br />
Calculations:<br />
V - (.-,. 1 4) (1 in.) '(U 25 in) = 0.78 m' (16.4 cm%'iu1 (4 am: samples) = 511 cm'<br />
(400.000 dpm/51.2 cm) (cm'2.35 g) = 3-32E3 dp dg<br />
3.320 dp rn/g (pCi2 2 dpm) = 1SE3 pCi/g or 514 kg<br />
51.W:dld<br />
Percent D'tstribution(V Cotmeration (VO/F.1<br />
,.I Cc<br />
0.17 255 pCV9<br />
137 Cs<br />
82 1 m pCi/g<br />
132 E 0.33 4.95 PU3<br />
"'Eu 0.05 7.5E-1 PCi/g<br />
"'Sr 17 2.55E2 pCi/g<br />
741 Ain<br />
'<br />
0.005 7.5F.-2 pCi/g<br />
3 91tie'Pa 0.1 1.5 .J<br />
(te n its:<br />
S. (J. Marske X5-53<br />
P. A. Newman X3-41<br />
RadCun Engineering File!LB XO 23<br />
floeumcnt and Into Services 110-09<br />
TOTAL: 1.460 PCi/g
t e,<br />
CIO<br />
RFSH-SOW-93-0003 -<br />
rJRevision 5<br />
Figu re 1<br />
SAMPLE CHECKA LIST<br />
Dat&Mme Received ! `1 r) Mt .. ()Oa).29'<br />
Work Order Number. bU3., I v^4a SAF #- _((^<br />
Shipping Cbntainer ID: w Chain atCustody I wIk-Q(^ / - /G<br />
1. Custody Seals on shipping contanrr intact? Yes I l<br />
2. Custody Seals dated and signed? Yes [ No (1<br />
3. Chain-d-Cuddy rec ord present? Yes No I 1<br />
• e ^<br />
4. Cooler terrmperatore<br />
5. Vermicufdelpadcrg materials is Wet [ j C ry 13<br />
6. Number of samples in shipping cmtainer. 1<br />
7. Sample holding fines exceeded? Yes [ J No ( j<br />
F Sa leshave<br />
custody seals<br />
hazard labels<br />
,appropriate sample labels<br />
9. -e6mples are:<br />
in good otindi5on<br />
leaking<br />
broken have air bubbles<br />
10. Where any anomalies identified in sample receipt? Yes (J No<br />
11. Description of anoma lies (include sample numbers):
Client Sample Screening Results<br />
13-Mar-98<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPAIA CNTSB NETCPIIIB<br />
Bill BON688 3/13/1998 QUAD2IA 3/131199810:21:17 AM BON689 30 9 0.241428 $7 57 0.96<br />
LIQUID Bkp 3 1 13/1998 1:30:18 AM 13KG 7110 41 0.05857143 638 094<br />
An[ Dole: 3/13/1998 Tot Sa, Atilt 1.00E+00 , 1.00E+00 Alp; (Dpnd 1.21E+00 (uCV 3.43E-04 (pCl/ 5.43E402 ±4.1 E+02 CAT 4.6E-02 Lab<br />
Pplmp 31.3 Unitas L n11 Bell Alq): 1.98E+00 Sap 8.94E-04 Leg): 8.94E+02 12.5E+02 I / 3.6E-02 Al"<br />
/ Bill DON689 3/13/1998 QUAD2 1 B 3/13/199810:21:17 AM BON689 30 661 21.9790476 47333 1576.8733<br />
(?On I gq '7 LIQUID Bkgt 3/13/19981:30: 18 AM BKO 700 38 0.03428371 672 0.96<br />
Anl Datat 3/13/1998 T04 list, Algd 1.00E+00 , 1.00E+00 Alp; (Dpnt/ 2.196401 (uCV 9.84E-03 (pCl/ 9,84E+03 18.3E402 CAT 2.5E-03 Lab<br />
Ppt mg: 30 / Unlbt L /, ml Bet; Alg )j 3.30E403 Sap 1.49E+00 Leg): 1.49E406 ±6.8E103<br />
III /<br />
3.4E-09,<br />
Alq<br />
Ids<br />
BIII BON733 3/13/1998 QUAD2 1 C 3/13/199810:21:17 AM DON753 30 0 -0.0371429 84 1.9037143<br />
SOLID Bkg: 3 1 13/1998 1:30:18 AM BKO 700 40 0.03714286 626 0.8942837<br />
Asst Dates 3/13/1998 Tot So. Algt 2.50E +02 , 9.77E+01 Alp; (Dpm/ -5.47E-0 1 (uCV -6.30E-04 (pCi/ -2.52E400 ± 4.8E+00 CAT 2.3E+02 Lab<br />
P itt mg: 97.7 / Units: g / mg Bet; Alq): 4.30E+00 So): 4.96E-03 Leg): 1.98E+01 ± 3.2 E+00<br />
I<br />
/ 3.0E+00 Alq<br />
ug<br />
BII( DON754 3/13/1998 QUAD2 1 D 3/13/199810:21:17 AM 13ON754 30 8 0.20666667 77 1.4709524<br />
SOLID Bkg: 3/13/19981:30:18 AM BKO 700 42 0.06 767 1.0937143<br />
And Dole: 3/13/1998 Tot Sa, Alq: 2.50E+02 Alp; (Dpm/ 1.31E+00 (uCV 1.34E-03 (pCl/ 6.16E+00 ±5.6E+00 CAT SJE400 Lab<br />
Fist Mgt 96 Un11at g , mg Bet; Alq): 3.19E+00 So): 3.74E-03 Llg)t 1.49E+01 ±3.1 E+00<br />
I /<br />
6.7E+00<br />
a`<br />
Bill 13ON753 3/13/1998 QUAD22A 3/13/1998 10:21:21 AM BON753 30 3 0.05571429 70 1.4004762<br />
SOLID Bkes 3/13/1998100:26 AM BKO 700 31 0.04428371 633 0.9328571<br />
Aid Dates 3/13/1 Tot So, Alq: 2.50E+02 / 9.61E+01 Alp; (Blind 2.80E-0 1 (uCV 3.2SE44 (pCl/ 1.31E+00 14.3E+00 CAT^ 3.8E+01<br />
Ppt mgt 96.1 holds g<br />
mg Bet; Alq)s 2.98E+00 So): 3.50E-03 Leg): 1.40E+01 3 2.8E+00<br />
7.2E+00<br />
La Alit<br />
I Ig<br />
BIII BON736 3/13/1998 QUA1322B 3/13/1998 10:21:21 AM BON756 30 S 0.20952381 66 1.2314286<br />
C AN Dates 3/13/1998<br />
SOLID<br />
Tot Sa, Alq: 2.30E+02<br />
Bkg:<br />
9.73E+0(<br />
3/13/1998 1:30:26 AM BKO<br />
Alp; (Dpnd 1.32 E+00 (uCV 1.53E-0 3<br />
700<br />
(pCl/<br />
40 0.05714286<br />
6.12E+00 ±5.OE+00<br />
678<br />
CAT<br />
0.9685714<br />
8.2E400 Lab<br />
G<br />
Nip<br />
P itt mg: 97.3 / Units: g / , mg Bel; Alq): 2.57E+00 So): 2.97E-0 3 144): 1.19E+01 ± 2.8E+00<br />
I /<br />
8.4E+00<br />
Adg<br />
Lle<br />
M<br />
I3-Mar-98 Quanlerra Environment Se rvices, SCP V2.03 I
Project Manager: U. Price<br />
wuanterra March 18, 1YYB 1(i am<br />
Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev. 3<br />
Master Sample Login: 17221<br />
^/'^J ((^^<br />
Draft: ina L Entered and Reviewed by: C5 PM Review: (y Qom_ ^ L^<br />
Sample Header Template:<br />
Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Red Sample No.<br />
Comments<br />
p Container Type Analysis Class Preservative Anal. Due Date Hold Date <strong>Site</strong> (Container Numbers:% Filled)<br />
Data:<br />
17221-001 BON690 Solid 13-MAR-98 08:15 13-MAR-98 10:35 OZ-APR -96 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80324301//ICAPT = P8 ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17223 .003.<br />
1 PN - Plastic-1L HG/7471/Q4 S COLD 27-MAR-98 10-APR-98 R10A (364654:99)<br />
1 ICAPT/6010/04 S COLD 27-MAR-98 09-SEP-98 R10A (364654:99)<br />
1 PCB/8080/04 S COLD 27-MAR-98 27-MAR-98 R10A (364654:99)<br />
17221-002 BON691 Solid 13-MAR-98 09:00 13-MAR-98 10:35 02-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80324302//ICAPT = P8 ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17221.004.<br />
1 PH - Plastic-1 1- HG/7471/Q4 S COLD 27-MAR-98 10-APR-98 R10A (364655:99)<br />
1 ICAPT/6010/Q4 S COLD 27-MAR-98 09-SEP-98 R10A (364655:99)<br />
1 PCB/8080/04 S COLD 27-MAR-98 27-MAR-98 R10A (364655:99)<br />
17221-003 BON690 FILTRATE Liquid 13-MAR-98 08:15 13-MAR-98 10:35 02-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80324301.<br />
1 PN - Plastic-1 1- HOLD//04 5 COLD 27-MAR-98 23-MAR-98 R10A (364656:99)<br />
17221-004 BON691 FILTRATE Liquid 13-MAR-98 09:00 13-MAR-98 10:35 02-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80324302, -<br />
C.<br />
1 PN - Plastic-1 1E HOLD//04 B COLD 27-MAR-98 23-MAR-98 R10A (364657:99)<br />
^ l<br />
G<br />
G7<br />
3 •= Sample has not been Pad screened.<br />
Page 1<br />
O<br />
^d<br />
Z ^.^
Chain of<br />
Custody Record<br />
QUA 4124 0]9]<br />
/^ o —r e-r" r Y<br />
C^<br />
iiivanterra<br />
Clienl Project Manager Date Chain of Custody Numb<br />
101143<br />
Address Telephone Number (Area Code)/F Number Lab Number<br />
City<br />
Project Name^^<br />
C<br />
Slate Zip Code<br />
/^ (399 -(X p<br />
<strong>Site</strong> Contact<br />
Carrie rrWaybill Number<br />
Lab Contact<br />
Conlrac0'Purchase Order/Quote No<br />
Matrix<br />
Containers &<br />
preservatives<br />
Sample I. D. No and Description<br />
(Conlaviers for each sample may be combined oil line)<br />
Date Time<br />
e vi 9i<br />
v 8<br />
2 i 2<br />
°° a?<br />
to Analysis ace<br />
(Attach list if<br />
is needed<br />
Page of<br />
Special Instructions/<br />
Conditions of Receipt<br />
Possible Hazard Identilication<br />
q Nom Haza rd q Flam mable q Skin Irmant q Poison B Unknown<br />
a ple Disposal<br />
Return To Chem El Disposal By Lab El Arch,,, For Months<br />
(A lee may be assessed if samples are retained<br />
longer than 3 months)<br />
L-Jyrm Around Time Required -- OC Requirements (Specify) - c<br />
VR<br />
urs q 48 Hours q 7 Days q 14 Days 21 Days q Other<br />
uisDale<br />
5<br />
ished By Date<br />
Time<br />
Time<br />
I- Received<br />
eceived B<br />
l // i` ^<br />
D to<br />
9-17-99<br />
Date<br />
Time<br />
Time<br />
i -lb 1b OD O g 2-0<br />
3. Relmgmshed By Dale Time 3. Rererved By Date Time<br />
Commonly<br />
DISTRIBUTION: WHITE Slays with the Sa 1pir. CANARY - Relurned to Client with Repo rt ; PINK - Field Copy
Bechtel <strong>Hanford</strong> Inc. CHAIN Or CUSTODY/SAMPLE ANALYSIS, REQUEST B98-061-11 fare or<br />
Collector "^<br />
.o _c,.. 6jh"'<br />
pjV Ikn+ {^gsrAl<br />
Project Designation<br />
105-C Phase I & Phase 11 - Concrete Samples<br />
Campion) Contact 'Telephone No.<br />
Steve Merskc 077-4316<br />
n m pling Luution<br />
100 Area l OS -C 1\P 4('^d 3<br />
Project Courdinalnr<br />
WIBSS, III.<br />
AF No.<br />
B98-061<br />
Ice Chest No. Field Logbook No. Niched of Shipment<br />
" L- I3U( — U7/<br />
Iland deliver<br />
hipped'To<br />
Quen lcna Incorporated<br />
POSSIBLE SAMPLE I IAZARDS/REIIIARKS<br />
Radioactive<br />
Special I landling and/or Storage<br />
SAMPLE ANALYSIS<br />
1Rdte Property Na.<br />
w 1l<br />
Preservatlon<br />
None<br />
Type of Container P<br />
NB. of Coniainer(s) (<br />
Volume<br />
S!X G()/ s^<br />
/,-)h^l7<br />
d D3,;24^'2r- -C"w, 96<br />
Sample No. - 'mo nts etrix • Sample Date Sample Time<br />
I L<br />
Seelmmlll in<br />
i.e.(l<br />
In,smcli.n,<br />
hill of La li /Air Bill No.<br />
^ ^.<br />
Data 'I urnarouod<br />
21 Days<br />
BON690 01 Other Solid MA2g6 IS c 1XI /<br />
CIIAIN OF POSSESSION SIg ntPrint Names<br />
Rellnquidr D.N?hna Red Dala i<br />
p<br />
iaNgT+B /O J S ^/T A<br />
inquhhcJ BY Dete/rim. Received By OD emlfln^c<br />
lingwshcd BY UalJrime Received BY DatefTimc<br />
elinquith
CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-12 r•ae ! ar !<br />
R ct 4<br />
Company Conracl<br />
Sieve 6lurske<br />
'I'cieplunm No.<br />
3734316<br />
project Coordinator<br />
wlgsS, Rl.<br />
Dols Turnaround<br />
'amplhlg Location<br />
AF No.<br />
Phase II - Concrete Samples<br />
100 Arca — I OS C. R e a e iuv 1199-061<br />
ke a. Field Logbook No.<br />
F—L-13U<br />
Method of Shipment<br />
p I oL<br />
1 land deliver<br />
'hipped '1' t,<br />
Quanterr9 in corporated<br />
Offalle Property No.<br />
MA<br />
(fill of Lading/Air hill Nu.<br />
I,vA<br />
POSSIBLE SAMPLE IIAZARDSlREMARKS<br />
Rdiwaim<br />
'perial Handling and/or Storage<br />
SON691<br />
SAMPLE ANALYSIS 4_<br />
So3a4 CkM 9o3^4 -r-«<br />
Semple No.<br />
01OR<br />
f10^<br />
Preservation<br />
'type of Container<br />
a^^•<br />
Nu. or Containers) 2<br />
Volume<br />
P<br />
II-<br />
.See imm I q in<br />
Sp
cc*<br />
Environmental<br />
Job Vo.22172<br />
Restoration<br />
Contractor ERC Team u. c.. rw<br />
Interoffice Memwandum a' 1 91C<br />
TO D. A. St. John x.0-19 MTL Febmary 27,1999<br />
nru:tc<br />
See Below mc"' S. L. Winslow<br />
RadCun Engineering<br />
X.1-41/531-0700<br />
suarecr: CVIAIF FSTIMATEFOR SWPING CONCRF•TF. CORE SAMPLES<br />
.0 w<br />
Sw.^Cnr !fib<br />
The fulluwing calculations shoe that cure samples with a direct reading of equal to or less than<br />
400,000 dpm/l00cm' will be bdow the definition ofralivactive mate rial as defined in 49 CFR 173.403<br />
of 70 Bq/g (2F.3 pCi/g). Lachmmple will consistofcoacrete material from four, two inch co re<br />
samples and enough water to mAe a slurry consi s:cary. The distribution of radionuclides is bused an<br />
previous concrete samples wkm from the below grade Fuel Storage Basiu that would also be<br />
representative of these concrete samples.<br />
••von:<br />
Cylinder Volume - nrh Radius of cam= core (r) = 1 inch<br />
Concrete Density = 2.35 g/cm `Ileight of cure swrtple taken (h) — U.25 inches<br />
27 pCi = Dq Maximum d irect reading on core = 400,000 dpm/IUUcat'<br />
2.22 dpm = pCi<br />
Calculations:<br />
V — (3.14) (1 in.)'(0 25in) = 0-79 in' (16.4 cm `/irr) (4 cure samples) = 512 cm'<br />
(400.000 dpm/5 L2 cm`) (cm'235 g) = 3.32E3 dpm/g<br />
3.32L3 dpm/g (pCi/2.2 dpm) = 1.5 113 pCi/g or 55.4 E4'g<br />
SLW:dld<br />
Percent Distrtbation(%) Cong=ration (vCi/e )<br />
"Co 0.17 235 pCi/g<br />
17Cs 82 13F3 pCilg<br />
WEu 0.33 4.95 pCi/g<br />
"°Eu 0.05 7.5E-1 pCi/g<br />
"ST 17 2.55E2 pCi/g<br />
241<br />
Ain<br />
Z3912<br />
'pu<br />
0.005<br />
0.1<br />
7.5F.-2 pCi/g<br />
1.5 -<br />
Co ies:<br />
S. 0.lvdarske X5-53<br />
P. A. Newman X 3-41<br />
RadCun Engineering File/LB X0-23<br />
<strong>Document</strong> and into Serv ices 130.09<br />
TUrAI-: 1.460, pCi/g<br />
(-U00049
9.<br />
Samp are:<br />
'Ries<br />
in good condition<br />
broken<br />
Figure t<br />
SAMPLE CHECK-IN LIST<br />
Date/rme Received: nn221 ^Y D 3 ^l srrr.<br />
FF<br />
Work Order Nurnber. & 42Z SaF # ^O -GYP<br />
Shipping Container 10: ru -0 ^ C^ Chain dQatody #<br />
leaking<br />
lave air bubbles<br />
RFSH-SOW-93-0003<br />
Revision 5<br />
1. Custody Seals on 9**g cont*w intact? Yes (q' o [ ]<br />
z Custody Seals dated and signed? Yes [^}'^io ( ]<br />
3. Chain-of-Custody record preset Yes . o [ J<br />
4. Cooler temperature<br />
5. Vermiculite/packing materials is Wet [ ] Cry 4/(yL<br />
6. Number of samples in shipping container.<br />
7. Sample holding times exceeded? Yes [ ] No<br />
S.<br />
Samp have:<br />
tape _hazardbabeis<br />
wstody seals _apprgsafe sample labels<br />
10. Where any anomalies identified in sample receipt? Yes [ ] No [^<br />
11. Descrip ti<br />
on of anomalies ( include sample n abers):<br />
Sample<br />
Telephoned To:<br />
r_=
C^<br />
C-J<br />
CG<br />
L7<br />
Client Sample Screening Results 1,<br />
13-Mar-98<br />
1,<br />
0, 3, 10<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
Blll BON690 3 1 13/1998 QUAD24B 3/13/19981; 15:37 PM BON690 30 7 0.17619048 71 1.3838093<br />
LIQUID Rks: 3/13/1998 1:30:14 AM DKO 700 40 0.03714286 688 0.9829571<br />
And Date: 3/1311998 Tot Se, AIq; 1.00E+00 , 1.00E+00 Alp; (Dpm/ 3.84E-0 1 (uCV 2.63E-04 (pCl/ 2.63E+02 ± 2.6E+02 CAT 9.3E-02 Lab<br />
Ppl mp 13.5 Units: L ml Bet; AIq): 2.64E+00 So): 1.19E-03 I 48): 1.19E+03 ± 2.5E+02 I / 4.2E-02 AIq<br />
BHI 13ON691 3/13/1988 QUAD24C 3 1 1311998 1:15:37 PM SON691 30 2 0.00666667 30 -0.002857<br />
LIQUID BkSs 3 1 13/1998 1:30:14 AM BKO 700 42 0.06 702 1.0028571<br />
AM Dale: 3/13/1998 Tot So. Alq: I.00E+00 1.00E+00 Alp; (Dpm/ 2.02E-02 (uCV 9.12E-06 (pCV 9.12E+00 ± 2.0E+02 CAT 2.7E+00 Lab<br />
Pptm8: 1.5 / Uatta: L / , ml Bel; Alq); -9.36E-03 Saj: -4.21 E-06 L f8): 4.21E+00 ± 1.6E+02 I / 1.0E+00 AIq<br />
Lis<br />
13-Afar-98 Quanterra Environment Se rvices, SCP V2.O3 /<br />
1.18
(Ruanterra G w ^- 5L 014514<br />
EoAroommtar<br />
sermw<br />
Condition Upon Re ce<br />
ipt Variance Repo rt<br />
St. Louis Laboratory<br />
Client. r`i ^}6 Date:<br />
Login No.:<br />
7<br />
? — 1 / " U Time:<br />
Project No: Initiated by:<br />
Shipper/No: 9 3 5 2 2- 1 1 RFA/COC Numbers: ^^^/[/ 7<br />
ConditionNari ce (Check all that apply):<br />
L q Sample received broken/leaking. S. q Sample 0) on container does not match sample ID<br />
3. q Sample received without proper prese rv ative. on paperwork. Explain:<br />
q Cooler tempera ture not within 4°C --- ?•C<br />
Record tempera ture:<br />
q pH 9. q All coolers on airbill not received with shipment.<br />
q other. 10. q Other (explain below)<br />
3. q Sample received in improper container.<br />
4. q Sample received without proper paperwork. Explain:<br />
5. q Paperwork received without sample.<br />
6. q No sample ID on sample container.<br />
7. q Custody tape dis turbed/broken/missing.<br />
—@'- No variances were noted during sample receipt. Cooler Temperature Upon Receipt: yr^-<br />
Notes:<br />
Corrective .action:<br />
q Client's Name: Informed verbally on: By:<br />
q Client's Name: Informed in writin g on: BV:<br />
q Sample(s) processed 'as is".<br />
q Sample(s) on hold until: f released. noufv:<br />
\<br />
-7 g I,<br />
Sample Control Supe rv isor Review: or desi gnate) I cc : 37 — [ / _<br />
Project Mana gement Review: 7\ t—L—<br />
SL-ADMIN-0003. Revised :1!'_4/95<br />
q<br />
Date: 3 — ^ I --v<br />
SIGNED ORIGINAL MUST BE RETAINED IN THE PROJECT FILE
Q'Auanterra 014501<br />
Condition Upon Receipt Variance Report<br />
St. Louis Laboratory<br />
Client: t/GC'^ Date: 3 — 7 , `!<br />
Project No: 5250 -2(G 6 Initiated by: o-. A-Pi<br />
Shipper/No: RF VCOC Numbers: /7 0 C sL<br />
Condition/Variance (Check all that apply):<br />
'1<br />
Login No.: / 72-2-/<br />
I. q Sample received broken/leaking. 8. q $am pie ID on container does not match sample ID<br />
2. q Sample received without proper preservative. onn paperwork. Explain:<br />
q Cooler temperature not within 4-C t 2°C<br />
Record temperature:<br />
q pH 9. q All coolers on an-bill not received with shipment.<br />
q other: 10. q Other (explain below)<br />
3. q Sample received in improper container.<br />
4. g/ Sample received without proper paperwork. Explain:<br />
5. q Paperwork received without sample.<br />
6. q No sample 1D on sample container.<br />
7. q Custody tape disturbed/broken/missing.<br />
^d No variances were noted during sample receipt Cooler Temperature Upon Receipt:<br />
Noes:<br />
Corrective Act on: t<br />
Q^I., (" ?3) t II !<br />
q Client's [me: Informed verbally on: By:<br />
q Client's Name: Informed in writine on: By<br />
q Sample(s) processed "as is".<br />
q Sample(s) on hold until If released. notify<br />
Sample Control Supervisor Review: (or desi gnate) Date:<br />
Project Management Review: L— " I tN^ Date: J _ (^/ 79<br />
SL-AD?dIN:)004. Revised I1;--1/95<br />
SIGNED ORIGINAL ^',IL'ST BE RETAINED IN THE PROJECT FILE<br />
_-7<br />
tme:<br />
(1 00 053<br />
lozr
— - - --- --- - -- -- WO 2?^ s Q-- - -<br />
' L Qanterra Q April O8, 1998 02:33 pm<br />
Ac count: 10722 Project: 550.260 QunterrRichland<br />
a a- OAS No. 550.26 Be,, 3<br />
Master Sample Login: 172<br />
Project Manager: W. Price<br />
222J4<br />
Draft: Final: Entered and Reviewed by: S^^`^Q^, n'/^'. ^ PM Review: I/C07`^//^<br />
Sample Header Template:<br />
Sample No Client ID C-Matrix Date: Collected Received Due Shipper Bad Category Rad Sample No,<br />
Comments<br />
N Container Type Analysis Class Preservative Anal. Due Data Hold Date <strong>Site</strong> (Container Numbers:& Filled)<br />
Data<br />
17224-001 BON692 Solid 16-MAR-98 08:30 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80327101//ICAPT = PB ONLY//AROCLOR 1254 ONLY"<br />
' FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECO ME S SAMPLE 17224-004.<br />
LJ v L 2")<br />
PN - Plast ,ll, HG/7471/Q4 S COLD 30-MAR-96 13-APR-98 R10A (364686:99)<br />
1 ICAPT/6010,'24 S COLD 30-MAR-98 12-SEP-98 R10A (364686:99)<br />
1 PCB/8080/Q4 c COLD 30-MAR-98 30-MAR-98 R10A ( 364686:99)<br />
17224-002 BONG93 Solid 16-MAR-98 09:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND i - D. 80327102 !; ICAPT = PB ONLY//AROCLOR 1254 ONLY/ !iFlLiER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOME S SAMPLE 17224-005.<br />
- IN Plastic-1L HG/1471 1I Q4 S COLD 30-MAR-98 11-APR-98 R10A (364687:99)<br />
1 ICAPT/6010/Q4 S COLD 30-MAR-98 12-SEP-98 RIGA (364667:99)<br />
1 PCB/8080/Q4 S COLD 30-MAR-98 30-MAR-98 R10A (364687:99)<br />
17224-003 BONG94 Solid 16-MAR-98 10:25 16-MAR-98 12:15 03-APR 4d AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 803271031/ SOAP: = PB ONLY,'/AROCLOR 1254 ONLY///F'ILtER AND ANALYZE SOLID PORTION ONLY, ;SQUID PORTION BECOME S SAMPLE 17224-006.<br />
1 IN Plastic 11, NO, 7471/Q4 COLD 30 MAR-96 13 APR 98 R10A 1364688:99)<br />
1 ICAPT'/a010iQ4 .. COLD 30-MAR-98 b'LP 98 R10A (364688:99)<br />
PCB/8 '",80;Q4 5 COLD 30-MAR-98 30 MAR-98 R101. 68<br />
11224-004 BJPB9b Liquid 16 MAR-9 8 08:30 16-MAR-98 12:15 03 APR 0 AIRBORNE 1 Screening noL Requilad<br />
RICHLAND I.D. 80327801;'1/ICAPT = PB ONLY'/AROCLOR 1254 ONL Y iTH: SAMPLE IS THE FILTRATE FROM SAMPLE 17224-001-<br />
. FN - 2)est 1 c- :L r 147. 04<br />
ICAPT 6010; Q4 _<br />
COLD<br />
(101D<br />
,- APR-9n<br />
_)i-APR 98 1Z<br />
.Pp,8 R10A<br />
- EP -98 R10A<br />
1364689,99)<br />
1364689:99)<br />
1 PCB/8C80/Q4 _ COLD p1-APR-98 MAF 98 R10A !364689:991<br />
X 229-OJS B ON,,, FILTRATL' Liquid -6 -MA.-, , 9 25 16 Mild ,8 12 :15 ciI( ':E Ai3 BORNE 1 Screen il4 1r.. krq..0 ed<br />
'v 1(t `.AN: 1 327102:'/lI^AnT - . -_._!:AR 1254 ONL ..^ ^Ah CLe i= THE FILTRATE FROM SAM; E . 7 229 u02.<br />
i YL 1L 1 .- ,.ti CGLD _ -AFR-9' .,r.., od RI'A ',364690:99, W O<br />
:<br />
17224 CL6 F(N 6 94 FILTRATE L q,i7 MAR 36 10 c :6 MAN 5 F _ RBOR1; _<br />
RICHLrU F 2 1 1'3"-ICAPT rP.. i ARJ( LO R 2. 4 ONL^ _..__ FP^PLE 1 5 THE FILTRATE FROM SAMPLE 2 _t3.<br />
O<br />
G<br />
CG<br />
cl(<br />
.R.<br />
1 t a, JLS .. , .., ,. „ .. RIOA i364,4, 991<br />
/<br />
1^<br />
( V<br />
-2<br />
t<br />
t^^^<br />
Sc eeci^y n t kequll^d<br />
L e ) S<br />
)<br />
V '/<br />
7 1^ Y-0
Dr a f tM<br />
W. Price<br />
Quanterra April 13, 1998 10:36 am<br />
Account: 10722 Project: 550.260 Ouanterre-Richland OAS No. 550.26 Rev. 3^^^<br />
Master Sample Login:<br />
Our"<br />
'^ifr^<br />
D ref t: Final Entered and Reviewed by:<br />
PM Review: ^s^fA<br />
Samp le Header Template:<br />
1722224777<br />
^^y^—in<br />
1.<br />
Q'"A lye r^0i^"<br />
Semple No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Rad Sample No.<br />
Comments<br />
N Container Type Analysis Class Preservative Anal. Due Date Hold Date <strong>Site</strong> (Container Numbers:% Filled)<br />
Data:<br />
17224-001 SON692 Solid 16-MAR-98 08:30 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80327101//ICAPT = PB ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17224-004.<br />
1 PN - Plastic-1 1. HG/7471/Q4 S COLD 30-MAR-98 13-APR-98 R10A (364686:99)<br />
1 ICAPT/6010/04 S COLD 30-MAR-98 12-SEP-98 R10A (364686:99)<br />
1 PCB/8080/04 S COLD 30-MAR-98 30-MAR-98 R10A (364686:99)<br />
1 PM/IT/Q4 S COLD 30-MAR-98 12-SEP-98 R10A (364686:99)<br />
17224-002 BON693 soLid 16-MAR-98 09:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80327102//ICAPT = PS ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17224.005.<br />
1 PN - Plastic- 11 HG/7471/Q4 S COLD 30-MAR-98 13-APR-98 R10A (364687:99)<br />
1 ICAPT/6010/04 S COLD 30-MAR-98 12-SEP-98 R10A (364687:99)<br />
1 PCBi8080/Q4 S COLD 30-MAR-98 30-MAR-98 R10A (364687:99)<br />
1 PM/IT/04 S COLD 30-MAR-98 12-SEP-98 R10A (364687:99)<br />
17224-003 DON694 Solid 16-MAR-98 10:25 16-MAR-9812:15 03-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80327103//ICAPT = PB ONLY//AROLLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17224.006.<br />
1 PN - Plastic-1L HG/7471/04 S COLD 30-MAR-98 13-APR-98 RIUA (364688:99)<br />
1 ICAPT/6010/04 S COLD 30-MAR-98 12-SEP-98 R10A (364688:99)<br />
1 PCB/8080/04 S COLD 30-MAR-98 30-MAR-98 RiOA (364688:99)<br />
1 PM/IT/Q4 S COLD 30-MAR-98 12-SEP-98 R10A (364688:99)<br />
17224-004 BOB898 Liquid 16-MAR-98 DB:30 16- 14AR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND I.D. 80327801///ICAPT = P8 ONLY//AROCLOR 1254 ONLY///THIS SAMPLE I $ THE FILTRATE FROM SAMPLE 17224-001. W02281<br />
1 PN - Plastic-IL HG/747D/Q4 S COLD 01-APR-98 13-APR-98 R10A (364689:99)<br />
1 ICAPT/6010/04 S COLD 01-APR-98 12-SEP-98 R10A (364689:99)<br />
1 PCB/8080/04 S COLD 01-APR-98 23-MAR-98 R10A (364689:99)<br />
17224-005 0ON693 FILTRATE Liquid 16-MAR-98 09:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required<br />
RICHLAND J.D. 803271021//ICAPT = PB ONLY//AROCLOR 1254 ONLY///THIS SAMPLE IS THE FILTRATE FROM SAMPLE 17224-002.<br />
1 PN - Plastic-11. HOLD//04 S COLD 01-APR-98 26-MAR-98 R10A (364690:99)<br />
( .-17224-006 BON694 FILTRATE Liquid 16-MAR-98 10:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required<br />
C-., RICHLAND I.D. 80327103///ICAPT = PB ONLY//AROCLOR 1254 ONLY///THIS SAMPLE IS THE FILTRATE FROM SAMPLE 17224-003.<br />
J 1 PN - Plestic-1 1. HOLD//04 S COLD 01-APR-98 26-MAR-98 R10A (364691:99)<br />
Ci<br />
LI<br />
UI<br />
3-=Sample has not been cad acreened.<br />
Page 1
Chain of<br />
Custody Record<br />
QUA 4124 07 97<br />
S i Io<br />
L't LO 10"banterra<br />
Client<br />
d , _.<br />
'lfXn^'l n Project Manager Oaf I ^—<br />
C<br />
Address Telephone Number (Area Code) Fax Number Lab Number<br />
City State Zip Code <strong>Site</strong> Contact Lab Contact<br />
Project Name<br />
Contract'Purchase Order/Quote Noo -<br />
Sample I.D. No and Description<br />
(Containers for each sample may be combined i on one line)<br />
7 V l 1^<br />
^2 3<br />
VI<br />
-<br />
— / n / CarrierlWaybill Number<br />
Date Time<br />
Matrix<br />
gg<br />
3 E - 3 a<br />
Containers 8<br />
Preservatives<br />
°<br />
i o 6 ^o<br />
N i<br />
Analysis<br />
more s ce<br />
(Attach list if<br />
is needed<br />
Chain of Custody Numb P,t<br />
1 o -<br />
Page of<br />
Special Instructions/<br />
Conditions of Receipt<br />
P >a,<br />
(A lee may beetl if samples are retained<br />
El No,, Hazard q Flammable q Sbn Irnlan( L1 Poison B Vonknowi, Return To Client El Disposal By Lab q Archive For Months longer than 3 months)<br />
Turn Around Time Required OC Requirements (Specilyr<br />
q 24 tVrirs q 48 Hours q / Days q 14 Days y21 Days q Other<br />
in uished Date Tema 1. Re ed By s Date Time<br />
`-- 2. Relinquished By Dale Time 2 Received By Date Time<br />
- J<br />
R ^.^n uished q BY ^ Dale f Time — 3. Received BY<br />
I Dale I Time<br />
GominenR<br />
DISTRIBUTION: WHITE - Slays with the Switch,, CANARY - Returned 10 Client with Report PINK - Field Copy<br />
1<br />
4 6
Chain of<br />
Custody Record<br />
OIIA- Al 24 n>G]<br />
loo [D<br />
Client Prolecl Manager<br />
c^<br />
Dat<br />
3111- 9<br />
Address Telephone Number (Area Code) Number Lab Number<br />
City Zip Code <strong>Site</strong> Contact Lab Contact<br />
Project Name<br />
^^,y ^' (/<br />
L^r I I<br />
C<br />
^"<br />
ContrectPurchase OrderlQuote No<br />
Sample 1. D. No. and Description<br />
Coma, ners for each sample maybe combined on one line)<br />
^<br />
CarriegWaybill Number<br />
Matrix<br />
Date Time °m - o =<br />
Containers 8<br />
Preservatives<br />
ei<br />
OX,<br />
=<br />
0 30 m<br />
Analysis<br />
more spa<br />
r<br />
(A ttach list A<br />
is needed<br />
CO"'banterrla<br />
Chain or Custody NumbC(<br />
11 0450<br />
Page ^ of<br />
Special Instructions/<br />
Conditions of Receipt<br />
rossore nezam Idenuncanon<br />
q NonHaeard q Flammable El Skin Initant El Poison B nknuwn<br />
a' nPie "bposai<br />
Return To Client El Disposal By Lab El Archive For Months<br />
(A lee me<br />
longer fh n 3<br />
ssessed if samples are retained<br />
onths)<br />
Turn Around Time Regmree OC Requirements (Specify) ///<br />
q 4 Hours<br />
in quishe<br />
P.^<br />
q 4 8 Hours El Days El 14 Days 21 Days q Other<br />
D e<br />
1 3<br />
T<br />
l 66<br />
Received By<br />
w ^^D /<br />
Date<br />
1<br />
1190quished By Date Hme 2 Hecervad fly<br />
C<br />
^Aelingwshed By Date Time 3. Received By<br />
Commerns<br />
DISTRIBUTION: WHITE Slays mIh Ibo Sarnple. CANARY -Returned to<br />
1<br />
Time<br />
— —_ — I Date I Time
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUE'S1' B98- 061 -16 rase ! "' !<br />
ollector^5/ Q4r.4 ., ,/ /<br />
KAIU f<br />
Company C'nnlecl 'I'tlrydmnr No.<br />
Steve Mnrskc ,171-4114<br />
Project Coordlnalur<br />
WP]SS, R1,<br />
Project D esignallon unpling Location 'AP Nn.<br />
105C Pha se I & Phase 11 - Concrete Samples 100 Area 1598-001<br />
Ire Cheat No. Field Logbook No. Method of Shipment<br />
I land deliver<br />
Shipped To<br />
Quanlcr ts Incorpo rated<br />
Offailc Property No. 15111 ur Ladin g/Air 0111 No.<br />
POSSIBLE SAMPLE IIA7ARDS/REMARKS<br />
Radlosclive<br />
Preservation<br />
"""•<br />
Special Handling and/or Storage<br />
SAMPLE ANALYSIS<br />
I y'pe of Con tamer<br />
Nu. o(l'0nleiner ( s)<br />
volume<br />
S06- tooa^7S<br />
IL<br />
S. in<br />
sr«id<br />
momuiom<br />
Data 'Turnaround<br />
21 D21yS<br />
^03a I CIS m gD3^ r1 (Zc^c<<br />
Sample No. Matrix • Sample Dale Sample Time 1<br />
I' os•...'•' j '^V<br />
^•^..<br />
1. O 2 Other Solid 3 -/6-^8 (^ 3 -^ e, o -<br />
SPECIAL INS"TRIK-1 IONS<br />
CIIAIN OF POSSESSION Sign/Print Names<br />
(II ICI• MeW,-6010A (S.patmce) 11.< ad), hlercwy-7471 (CV), C1. ....mm Ilse 7196,<br />
di<br />
Q.e ,<br />
Relinquished By<br />
Dats?ims<br />
^6 f{A ?9>3 /2 / S<br />
Ualdfime<br />
R e By<br />
Recei) ve Y ^I<br />
imc<br />
`<br />
Uale imc<br />
I'CBs,1080(Aivd,)rr 12541, Gainu Spccouv
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST 1198- 11 61 - Id<br />
ollector<br />
Q C.hlh.r<br />
Project Designalian<br />
3 ^N<br />
ompany Contact<br />
' Steve Marske<br />
Sampling Location<br />
'Telephone No.<br />
373-41IG<br />
Project Coordinator<br />
wl;lSS, fit-<br />
'AF No.<br />
Dalo Turnaround<br />
2I<br />
105 -C Phase 1 & Phase II - Concrete Samples 100 Area 1198-061<br />
fee Chest No. Field Logbook No. Method of Shipment<br />
I land deliver<br />
'hipped To Offsinr Properly No. Rill of Lading/Air Dill No.<br />
Qulnterra Incorporated<br />
POSSIBLE SAMPLE IIAZARDS/RERIARKS<br />
Radloacdn<br />
Special Ilandling and/or Storage<br />
SAMPLE ANALYSIS<br />
1'reservalloo<br />
7 ype of Container<br />
Nn. of Container(s)<br />
g o3 ^1 I G^-t r -, g o3a^a P-6,d<br />
Sample No Matrix • Sample Date Sample Timc<br />
"""•<br />
Volume IL<br />
P<br />
2<br />
See item (1) In<br />
Speaid<br />
Inanu,"on. -<br />
ON693 Q 2 Other Solid _ 6 _ O Ja — ( /^<br />
Clit OFP SSfS ON Sign/Print Names - ( 1) ICP McUk - 6010A (Supunace) 11 cadl. Mercury - 7471 -(CV), Chrommm Ilex - 7196,<br />
el 'uis By DaIHTime<br />
iengte 98 S<br />
R B' Uale i c<br />
Relinquished BY Date/filne Received BY (N,L 7ale/iinle<br />
(CLY 1<br />
Rflinquidled By Daldllnm Received By Damn nm<br />
^rilrf^JVi-79' /V rC(Cel-(a3 •Y= S ^1, 90- TdfLiSr' echnei,'uwt 99 C^ubo l c /`<br />
J h ^ ^/ / 3-,-”<br />
l<br />
Days<br />
.<br />
SPECIAL INS I'BUCI IONS Man, ,<br />
PCBs - 8080 (Aunt., -1254 ) , Gamma 5penmscopy ICevum-137, Coha 11-60, Europium-152,<br />
Europium-154, Lnopwm-1551, Anmunu nr 241. Isotopic Plulounnn; Isotopic Uranium; Sete<br />
5<br />
SL<br />
so<br />
51<br />
-<br />
-<br />
-<br />
-<br />
Sem,„mt<br />
S„ im<br />
Sn.Jye<br />
'uished By DaldGne Received By 1lale 7 lint<br />
1. - qwa<br />
Bdumn<br />
U, X - OiAu<br />
L ORATORY Received By ]ide DaldTime<br />
SECTION<br />
FINALSAMPLE Mspwd Me1hm1 Disposed By -- -- Date'lbur<br />
DISPOSITION<br />
o A<br />
Ps<br />
D1.<br />
- oJ1el<br />
11,,,,ns„nJ,<br />
u,,,m I,ywm
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS KEQUIsS'f B98- 061-15 " vc ! "r i<br />
olleclorpp p<br />
('nm pp ny (^nslacl 'I clephmle No.<br />
Mp "^^<br />
A4,,4<br />
Steve Manske 3.73 4116<br />
Project Designation Sampling Location<br />
105-C Phase 1 k Phase II - Concrete Samples<br />
100 Area<br />
Projerl ( -uordinator<br />
WII ISS. Hi<br />
'AF No.<br />
1198-061<br />
I ce Chest No. Fi eld Logbook No. Method of Shipment<br />
Iland deliver<br />
- hipped To<br />
Qllmnella lncurpormcd<br />
POSSIBLE SAMPLE IIAZARIIS /RF-hIARKS<br />
Radipanive<br />
Special Dandling and/or Storage<br />
SAMPLE ANALYSIS<br />
ORaile Properly No. Hill of Lading/Air (till No.<br />
I'rcservpllnn<br />
'T ) pe of ( nnialner 1<br />
No. of ('onldner( s)<br />
\'ulunm<br />
^o3an 1 U^ L.enti go3 a ^<br />
2<br />
IL<br />
Scc non I I l m<br />
Strcatl<br />
I^'r'11e"""a<br />
flala I ornaruund<br />
Sample No Matrix a Sample Dale Sample Time ,}^INe s^„ u s ^, - r es 'j" r ; It r:, ., 1 ~,r f "<br />
BON694 03 Other Solid<br />
CI IN OF 'OSSFS'ION<br />
F<br />
0.el ' BIY'o Dalelfime<br />
/6 AtA R9B ^Z ^^<br />
Relin fished B Date/ 1anc<br />
yrr y<br />
Sign/Prim Nunes<br />
Ra U rT r<br />
T214 ^-<br />
Received B '\ Dam/tim e<br />
Relui4uisheJ - By UauRirne Receircd By hale/I nne<br />
Inthatitoshed Ua¢fflme Recdred By Ua1ell in¢<br />
LABORATORY<br />
SF.(TI ON<br />
TINA S<br />
-SAhIPLE<br />
IIISP(ISIII(1N<br />
Y<br />
SPECIAL INS I' RUC" I' IONS<br />
11)Is- a08 01roclor 12 5upallncc111cadlAkmup-7J]I-(CVI. Clllomiwu 111%-)196.<br />
Ls CB -. 154, oclnr-23J1, Gn11nnn Spenrosc'+Py IC esvum 117. Cnbah-60. burnpiva+-132,<br />
I:mupiuurl3J. llumpuumlSS;,An¢uamm241. lsnl upic l'Lilunmin. 11 0111,1 11 ILaniunr. Selc<br />
^/ ^<br />
5_/e111 jU"1^ -79 / / ,<br />
/vfC / Qy ^^a / ^r<br />
^ ^^-f[A O /, / — /O"'rtt^<br />
^<br />
ec / 9 ,/(h<br />
y^<br />
^ (/&r o/<br />
- l¢' ^^ ^3 S41)<br />
Received By lisle Daelunc<br />
Dn sd Mnbod -"-- ---__-'-<br />
1 S UIdl uu<<br />
21 Days<br />
I<br />
St_<br />
So<br />
Matrix<br />
s,,<br />
5'^.<br />
%Id"d<br />
%t.<br />
w<br />
'v<br />
s<br />
- II I.nly<br />
scud<br />
tr,l<br />
^<br />
Il,<br />
UL<br />
- I4wn 5.IW.<br />
leiiio l ..p,w,<br />
Ripe<br />
1. t ignW<br />
v - rcra+11,.,,<br />
% +nnr+
CCN: 055088<br />
Environmental<br />
Job No. 22192<br />
Restoration<br />
Contractor ER^ Team o. ' MO<br />
Interoffice Memorandum<br />
7O I). A. St. John LO-19 DAM I;ebruary 27.1998<br />
I nPI"-5!<br />
*<br />
Scc Bclow "o"r` S. L. Winslow<br />
RadCun Engineering<br />
X3-41/531 40706<br />
suuEcT. CURT F: FSTTMATE FOR S111PP1NG (-VNCRFTF. CORE SAMPLES<br />
r.... w^<br />
OIL"IW<br />
IAA ww<br />
Liloc . !1O<br />
The Following calculation show that curt: samples with a direct rending of equal to ur less than<br />
400.000 dpm/I0(kan = wllbcbclow the definition ofratlivactive matcrialas defined in 49 CFR 173.403<br />
of 70 By/g (2F3 pCi/g). L•ach sample will consist of concrete mate rial from four - two inch core<br />
samples and enough waterto make a slurry consisxmy. The dist ri hution of radionuclides is based tin<br />
previous concrete samples tak«t from the below grade Fuel Slortge Basin that would also lx;<br />
representative of these concede samples.<br />
'iven:<br />
Cylinder Volume - nr'h Radius ofcowxte core (r) = 1 inch<br />
Concrete Density = 2.35 glom' Height of cmL^s_ample taken (h) - U25 inches<br />
27 pC:i = Dq Maximum ilkeet reading on core = 400,000 dpm/1 UUcm'<br />
2.22 dpm = pCi<br />
Calculations:<br />
V - (3. 14) (1 in.)'(0 25in) = 0.78 in' (16.4 cm J/irrj (4 cure samples) = 511 cm'<br />
(400.000 dpm/51 2 cm) (='2.35 g) = 3. 3 2E3 d;m/g<br />
3.32L I dpm/g (pCi2.2 dpm) = 1.5E3 pCi/g or 55.4 By/g<br />
SI.W:dld<br />
'OCo<br />
Percent Disr ributionMo<br />
0.17<br />
IJ7cS 82<br />
'uEu<br />
033 0<br />
I"Eu 0.05<br />
o'Sr 17<br />
'°'Ain 0.005<br />
'J91'"pu 0.1<br />
TOTAI-:<br />
Cn ics:<br />
S. (J. Nlarskc X5-53<br />
P. A, Newman X3-4 1<br />
RadCun Engineering File LB XO-23<br />
Doeumen: and Info Services 110-09<br />
Coetrntration (oC:i/e)<br />
2.55 pCi/g<br />
1.2F3 pCi/g<br />
4.95 pCi/g<br />
7.5E-1 pCi/g<br />
2.55E2 pCi/g<br />
7.5F.-2 pCi/g<br />
1.5 nCi/e<br />
1.4603 pCi/g
Figure 1<br />
SAMPLE CCK-IN LIST<br />
DateMme Received: l^ ^0^^^ SG#: &ZQQ7,-^<br />
RFSH-SOW-93 -0003<br />
Revision 5<br />
Work Order Number. 0 ^3c^^ 0^ SAF #: -<br />
ShippingContainerID: -0 ChainofCustody# ' gW^J^^v<br />
1. Custody Seals on shipping container intact? -<br />
Yes [ 1<br />
2. Custody Seats dated and signed? Yes No [ )<br />
f t^^<br />
3. Chain-of-Custody record present? Yes Cij /No [ )<br />
4. Cooler temperature<br />
^O<br />
5. Vermiculitefpaci ing mate ri<br />
als is Wet [ ] Dr/—{ ^^^^<br />
6. Number of samples in shipping container.<br />
(<br />
r'<br />
7. Sample ho&q times exceeded? Yes [ ] No (^<br />
8. Samples have:<br />
--^Zape<br />
custody seals<br />
9. Same are:<br />
in good condition<br />
brdm<br />
hazard labels<br />
appropriate sample labels<br />
leaking<br />
have air bubbles<br />
10. Where any anoma lies identified in sample receipt? Yes [ I No Cl/<br />
11. Descrip tion of anomalies (include sample numbers):<br />
Sample CustodiargUbo<br />
Telephoned To:<br />
7<br />
o^<br />
/<br />
Date: ^O/C)
Client Sample Screening Results<br />
17-Mar-98<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
B ill BOIU10 3/17/1998 QUAD2IB 3/17/19989:38:04AM 0011110 30 11 0.32 107 16266667<br />
SOLID Bbg: 3/17/199812:19:30 AM BKO 600 28 0.04666667 364 0.94<br />
AN Dale: 3/17/1998 Tot Sa, All: 3.00E+02 , 1.02E+02 Alp; (DpM 2.10E+00 (uCV 4.66E-03 (pCU 9.33E+00 f 5. 311+00 CAT 3.4E+00 I.b<br />
Ppl mgs 101.6 Unita: O / , mg Bel; All): 3.73E+00 So): 1.27E-0 2 LIE): 2.34E+01 ± 3.4 11 +00<br />
1 ",<br />
3.9E+00<br />
All<br />
Bill BOHJII 3/17/1998 QUADZIC 3/17/19989:38:04AM B011111 30 13 0. 37333333 308 9.2816667<br />
SOLID Bbg: 3/17/199812:19:30 AM BKO 600 36 0.06 391 0.983<br />
Ad Dote: 3/17/1998 Tot So, Alls 3.00E+02 , 9.93E+01 Alp; (DpM 1.90E+00 (uCV 4.31E-03 (pCU 8.62E+00 f 3.4E+00 CAT 3.8E400 Lab<br />
PPlmgt 99.8 Unite: 8 mg Dell Alq)i 2.068+01 5.): 4.668-02 1,11)1 9.338+01 S f.98+00 1 " 1.18i U0 All<br />
• 1.18<br />
Bill B0H112 3/17/1998 QUAD2 1 D 3/17/19989:38:04AM B011112 30 12 0.34666667 212 6.1383333<br />
SOLID mist 3/17/1998 12:19:30 AM BKO 600 32 0.03333333 557 0.9283333<br />
Ad Dalai 3/17/1998 Tot Ba, Atli 3.00E+02 , 9.91E+01 Alp; (DpnJ 1.98E+00 (uCV 4.30E-03 (pCU 8.99E+00 13.4E+00 CAT 3.6E+00 Lab<br />
Ppl mp 99.1 i - Udb: g ^'- mg Bet; All): 1.36E+01 Sa): 3.10E-02 LIE): 6.20E+01 f 4.9E+00 1 / 1.6E+00 All<br />
4E<br />
Bill BOIU13 3/17/1998 QUAD22A 3/17/19989:38:08 AM BOIIJI3 30 1 -0.0183333 346 10.638333<br />
SOLID Bbg: 3/17/1998 12:19:41 A61 BKO 600 31 0.05166667 337 0493<br />
AM Dalai 3/17/1998 Tot So, Atilt 3.00E+02 9.87E+01 Alp; (DpM 4.95E-01 (uCV -1.81E-03 (pCU -3.63E+00 ± 4.6E+00 CAT 3.0E+02 Lab<br />
Ppt mg: 98.7 - U nitas g , mg Bel; Alq): 2.30E+01 So): 5.25E-02 LIE): I.03E+02 ± 6.1E+00 I 9.3E-01<br />
Bill 80}1114 3/17/1998 QUAD22B 3/17/19989:38:OSAb/ 0011114 30 20 0.39666667 670 21.383<br />
SOLID Bbg: 3/17/1998 12:19:41 AM BKO 600 42 0.07 569 0.9483333<br />
Ad Dotes 3/17/1998 Tod Sa, All: 3.00E+02 , 1.08E+02 Alp; (Blind 2.83E+00 (uCV 3.91E-0 3 (pCU 118E+01 f5.1E+00 CAT 4.2 E+00 Lab<br />
Ppt mgt 107.8 i Unites g / , mg Bell Alq): 4.74E+01 50), 9.90E-02 1-10 1.9 11 E+02 S t.0E+00 1 /<br />
Bill BON692 3/17/1998 QUAD22C 3/17/19989:38:08 AJ.1 BON692 30 7 0.19166667 310 9.375<br />
LIQUID Bbg: 3/17/1998 12:19:41 AM BKO 600 23 0.04166667 373 0.9383333<br />
i Ani Dote; 3/17/1998 Tot Sa, All: 1.00E+00 , 1.00E+00 Alp; (Dpnd 2.40&01 (uCV 1.08E-04 (p(V 1.08E+ 02± 1.9E+0I CAT 2.7E-0I Lob<br />
Ppt mg: OA Ulnas L ml Bet; All): 1.73E+01 So): 7.8,E-03 LIE); 7.81E+03 ±4.9E+02<br />
1<br />
/6AE-03<br />
All<br />
17-Mar-98 Quanlerra Environment Se rvices, SCP V2.03 /<br />
^3<br />
3.1E-0I<br />
All<br />
All<br />
tat
C ^'<br />
U :7)<br />
.A<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR % ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
Bill BON693 3/17/1998 QUAD22D 3/ 17/19989:38:08AM BON693 30 7 0.16166667 117 296<br />
LIQUID BLS: 3/17/199812:19:41 AM UKO 600 43 0.07166667 564 0.94<br />
AM Date: 3 1 17/1998 Tot Se, Alq: 1.00E+00 , 1.00E+00 Alp; (Dpm/ 6.55E-0I (uCV 2.95E-04 (pCl/ 2.95E+02 ±3.7E+02 CAT 8.5E-02 lab<br />
Ppt m8: 53.2 / Units: L ! ml Bet; Alq): 6.09E+00 Sa): 2.74E-03 40): 2.74E+0l ± 3.4E+02 I LBE-03 Alq<br />
LI S<br />
Bill BON694 3/17/1998 QUAD23A 3/17/19989:38:12 AM DON694 30 6 0.11166667 57 0.6816667<br />
LI<br />
QUID Bkg: 3/17/1998 12:19:48 AM BKO 600 53 0.08833333 611 1.0183333<br />
AM Date: 3/17/1998 Tot Sa, Adq: 1.00E+00 , 1.00E+00 Alp; (Dpm/ 5.45E-0 1 (uCV 2.45E-04 (pCV 2.45E+02 ± 3.8E+02 CAT LOE-0 1 Lab<br />
Pplmp 55.1 ./ Units: L ml Bel; Alq): 1.78E+0O Sa):<br />
I<br />
/ q<br />
8,02E-04 48): 9.02E402 4 2.4E+02<br />
6.2E-0 2<br />
Ill[<br />
BBf BONSM6 3 1 17/1996 QUAD23B 3/17/1998 93 8:12 AM BONSM6 30 119 3.92 5799 192.32333<br />
LIQUID Blq: 3/171 1998 12:19:48 AM BKO 600 28 0.04666667 586 0.9766667<br />
Aal Dal es 3/17/1998 Tel Se, Allis 6.00E+00 , 1.006101 Alp: (Upm/ 7.45E+00 O,CV 7.01 H4A (pCV 1.376+07 14 09 401 CAT 7.3E-07 14,16<br />
Pplmp 3.5 ,/ UNta, L ml Bell Alq), 3.66E+02 Sa); 9.88E-0 2 14 8): 1.65E+04 3: 2,2E+02 I 3 .0E-0 3 Alq<br />
,^<br />
L18<br />
Bill BONSM7 3/17/1998 QUAD23C 3/17/19989:38: 12 AM 130NIN17 30 23 0.71833333 107 2.6683333<br />
LIQUID 848: 3/17/1998 12:19:48 AAI BKO 600 29 0.04833333 539 0.8983333<br />
And Dale, 3/17/1998 Tot Sa, Alq: 6.00E+00 / 1.00E+01 Alp; (Dpm/ 2.18E+00 (u (-V 5.89E-0 4 (pCV 9.81E+01 ±2.7 E+01 CAT 2.5E-0 1 Lab<br />
Ppl mp 5.9 i Unlla, L , ml Bel; Alq): 4.79E+00 Sa); 1.29E-03 40 2,16E+02 ± 3.0E+01 I - ^- 2.3E-01<br />
Bill B0N8M8 3/17/1995 QUAD23D 3/17/19959:38:12AM BONSMS 30 36 1.13666667 114 2.89<br />
LIQUID 848: 3/17/1998 12:19:48 AA1 BKO 600 38 0.06333333 346 0.91<br />
Anl Dale: 3/17/1998 Tot Sa, Mq: 6.00E+00 1.00E+01 Alp; (Dpnd 3.46E+00 (uCV 9.36E-04 (p(-'V 1.56E+02 + 3.0E+01 CAT 1.6E-0 1 Lab<br />
Piss mg: 3.5 / Units: L ml Bel; Mq): 4.83E+00 Sa): 1.31E-03 LIZ) : .18E+02 ± 2.9E+01<br />
I<br />
2.3E-01 Alq<br />
1.15<br />
17-Mar-98 Quanlerra Environment Se rvices, SCP V2.03 2<br />
Lis LIB
A,, -i/I fIY6<br />
—1 ` c,ir3<br />
Beclael llRnforfl Inc. CHAIN Ol e CUS'I'ODWSAMPLE ANALYSIS ItEQOES'I' I 1j9NjIM-L6<br />
'a1lrslnf f Cuwpni y CoMmirl lrlrphnue Nu. 1'rulrrl f'enrdln^lur Ibb - 1 car n[. uand<br />
R Rr.4 1 2Aidt<br />
SlcvcMarske 171-4716 WIIY1.Irl.<br />
2I I)i<br />
Project Designation Sasnph"It Lo ca tion tiAF No. ,(j^^J11 Ins<br />
105C Phase I R Phase II • Concrete Samples 100 A,ca ' Will. 3 1 fl.J(I(/r''^I<br />
Ice Cheal No. Held Logbook No, Method of Shipment<br />
Ilend deliver<br />
Shipped To Uffrllr 1'rmpaly Nu. 11111 of Lullnµ/Air 11111 Nu.<br />
Quanlerrs Incorporated<br />
POSSIBLE SARIPLE IIAZARnS/REMARKS — "M•<br />
1 1rnrrrallon i r i<br />
Rrdioaclive<br />
Special llandling and/or Storage<br />
S03a 79 - ►^ g o3a^ - /<br />
SAMPLE ANALYSIS<br />
I y'pe of Coulainer<br />
No. of Contalnerls)<br />
Volume<br />
P<br />
-_...<br />
7<br />
—<br />
—^ ^.. _.. I<br />
IL - ^-<br />
Srrihrmll,ha<br />
sp«i.1<br />
ImWmom .<br />
/<br />
3 `6 y` 5F-)6— to oa3^i<br />
sample 140 Matti. Sample [talc Songdc lime ♦.bl fr^ 5 '.:I^I j alYhi, "'.k: .i'^ ,1 (I'j j)lp rl',YF4':)ia': hr •f 1 ,h rll, o'I I,m,Ct 1 j •i s;C+ n •II' _.<br />
N 898<br />
.01ha, So<br />
w TL<br />
CIIAIN OF POSSESSION S ign/Prin t Nunes<br />
Rdr ) 1)aterfime Be [ a Bj I /lime/<br />
R f' /e Hq?9B /I i $ G<br />
Client Sample Screening Results<br />
l7-Mar-98<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR AC'Q DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
BIII B0H110 3/17/1996 QUAD2 1 B 3117/19999:38:04AM 8011110 30 II 0.32 107 2.6266667<br />
SOLID Bkg1 3/17/1991112A9:30 AM BKO 600 28 0.04666667 564 0.94<br />
Ad Dole, 3/17/1998 Tot Se, AIq, 3.00E+02 , 1.02E+02 Alp; (Dpm/ 2.10E+00 (uCU 4.66E-03 (pCU 9.33E+00 ± 5.3E+00 CAT 5AE+00 Lob<br />
Ppt mip 101.6 Udb, 0 j mg Bel; Alq): 5.73E+00 Sep 1.27E-02 LIg): 2.54E+01 3 3.4E+00<br />
i '<br />
3.9E+00 Alq<br />
1•le<br />
BIII 8011111 3/171 1998 QUAD2 1 C 3/17/19989:38:04AM 8011111 30 13 0.37333333 308 9.2816667<br />
SOLID Bkp 3/17/1998 12:19:30 AM BKO 600 36 0.06 391 0.983<br />
Ad Dates 3/17/1998 Tot Sa,Algl 5.00E+02 , 9.95E+01 Alp; (Dpn,/ 1.90E+00 (uCl/ 4.31E-03<br />
Pplmg: 99.5 Udla: g mg Bel; Alq): 2.06E+01 So): 4.66E-0 2<br />
Bill 6011112 3/171 1998 QUAD2 1 D 3/17/19989:38:04AM B011J 1 2<br />
SOLID Bkgt 3/171 1998 12:19:30 AM BKG<br />
Ad D ole: 3 1 17/1998 Tot Se, Mq: 5 .00E+02 9.91E,01 Alp; (1)p,N 1.981:+00 (.Cl/ 4.301:03<br />
Ppe mg: 99.1 i - Units: g / mg Bel; Alq): 1.36E+01 So): 3.10E-02<br />
(pCU 8.62 E+00 ± 5.4E+00 CAT 5.8E400 Lob<br />
I.Ig): 9.32E+01 ± 5.9E400 1 1.1 E+00 Alq<br />
: IdL<br />
30 12 0.34666667 212 6.1383333<br />
600 32 0.05333333 557 0.9283333<br />
(pCU 8.99E+00 ± 5.4E+100 CAT 5.6E:00 Lob<br />
I,Ig): 6.20E+01± 4.9E+00 I j - 1.6E+00 Alq<br />
IAZ<br />
BIII 8011113 3/17/1998 QUAD22A 3/17/19989:38:OBAM B01IJ13 30 1 -0.0183333 346 10.638333<br />
SOLID Bkg, 3/17/1998 12:19:41 AM BKO 600 31 0.05166667 537 0.895<br />
Ad Dates 3/171 1998 Tot So, Alq, 5.00E+02 , 9. 117E+01 Alp; (Dpm/ •7.93E-0 1 (uCU . 1.81E-03 (pCV -3.63E+00 +4.6E+00 CAT 5.0E+02 Less<br />
Ppt mg: 98.7 Units: g mg Bel; Alq): 2.30E+01 So): 5.25E-02 Leg): 1.03E+02 j6.1 E+00<br />
1<br />
j" 9.5E-01 Alq<br />
1•le<br />
Bill BOIIJ 1 4<br />
3/17/1998 QUAD22B 3/17/19989:38:08AK1 B011114<br />
30 20 0.59666667 670 21 3 85<br />
SOLID<br />
Bkg; 3/171 1998 12:19:41 AKf BKO<br />
600 42 0.07 369 0.9483333<br />
Ad Dol e,3/17/1998 Tot Se, Alq: 3.00E+02 1.011E+02 Alp; (Dpm/ 2.83E+00 (UCU 3.91E-0 3 (pCU I.I&E101 ± 3.1E400 CAT 4.2E+00 Lob<br />
P iss mg: 107.8 . Udb: g^ , mg Bel; Alq): 4. 74E+01 Se): 9.90E-0 2 Ljg): 1.98E+02 ±B.OE too 1 / S.IE-01 AIq<br />
1•IL<br />
Bill BON692 3/17/1998 QUAD22C 3/17/1998 9:38:08 AK1 BON692 30 7 0.19166667 310 9.375<br />
LIQUID Bkg: 3/17/1998 12:19:41 AKI 13KO 600 25 0.04166667 375 0.9383333<br />
Ad Date: 3 1 17/1998 Tot Se, Alq: 1.00 V,+00 1.00E+00 Alp; (Dpn3 2.40E-01 - (uC'U 1.08E-04 -- (pCU -- 1.08E+02 -- -_<br />
± 1.9E+02 CAT 2.3E-0 1 Lab<br />
Piss mg: 0.4 Udb: L , ml Bel; Alq): 1.73E 101 So): 7.81E-03<br />
i<br />
LIg): 7.8IE403 ±4.9E)02<br />
i<br />
Alq<br />
6.4E-03<br />
IdL<br />
17-Afar-98 Ouanterra Environment Se rvices, SCP V2.03 J
Qyrhianterra<br />
;ter<br />
Sty<br />
orrecti Action<br />
(o<br />
Client's Name: G<br />
C Client ' s Name:<br />
Condition Upon Receipt Variance Report<br />
St. Louis Laboratory<br />
,tva Atot7lr.^.a.F.c,<br />
Informed verbally on: Bv:<br />
Informed in writin g on: By:<br />
014501<br />
Login No.: / 721-¢<br />
Client. Due: _ 7- `T,f Ime: 0 Y o<br />
Project No: S-50. 2G D Initiated by: o -A J—kh<br />
Shipper/No : -7<br />
ConditionNariance (Check all that apply): y):<br />
RFA/COC Numbers: /7 D C<br />
.. q Sample received b roken/leaking. 8. q Sample ID on container does not match sample ID<br />
2. q Sample received without proper preserva tive. on paperwork. Explain:<br />
•<br />
q Cooler tempera ture not within 4"C _ 2C<br />
Record temperature:<br />
q pH 9. q All coolers on airbiil not received with shipment.<br />
q other: 10. q Other (expla in below):<br />
.. q Sample received in improper container.<br />
j Sample received without proper paperwork. Explain:<br />
5. q Paperwork received without sample.<br />
6. q No sample ID on sample con tainer.<br />
-. q Custody tape dis turbed/brokervmissing.<br />
C No variances were noted<br />
Notes: ,3 -r- ^,l b ^ Z<br />
I^^^ 610<br />
Sample(s) processed "as is".<br />
\<br />
sample receipt Cooler Tempera ture upon Receipt.<br />
7 ?o3i^Pdi<br />
,P.ch/.2.0• t<br />
ll<br />
/-A CT e^ —/ ^^Q 4 / [Y rl Ss^^^i 3t ^^,<br />
C Sample(s) on hold unt il : If released. no tify<br />
Sample Control Supe rvisor Review: (or designate) Date: ?" ^ 7 —<br />
Project Management Review: ^ Date: 7 —/P -1Y<br />
SL.ADMIN-0004. Reviseo :! '24/95<br />
SIGNED ORIGINAL NR;ST BE RETALNED IN THE PROJECT FILE<br />
L
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON680<br />
OUanterra-Richlanci<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/09/98<br />
Receipt Date 03/09/98<br />
Report Date 04/08/98<br />
cuanterra ID 17199-001<br />
Blank Sample Prep. Analyses Detection<br />
Analyte CAS Number Name Date Date Result Unit Oual. Limit Dilution<br />
Aroclor-12 4 11097-69-1 QCRLK167668-1 03/18/98 0 / 0/98 63 UG/KG 33 .2<br />
DCS 2051-24-3 QCBLK167668-1 03/18/98 03/30/98 88 %REC .2<br />
TCM% 877-09-8 OCBLK167668-1 03/18/98 03/30/98 80 7.REC .2<br />
"11^^5
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON681<br />
Analyte<br />
Duanterra- Ri chI and<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/09/98<br />
Receipt Date 03109/98<br />
Report Date 04/08/98<br />
Duanterra ID : 17199-002<br />
Blank Sample Prep. Analyses Detection<br />
CAS Number Name Date Date Result Unit Dual. Limit Dilution<br />
Aroclor-1 54 11097-69-1 DCBLK167668-1 03/18/98 03/30/98 UG/KG U 33 .2<br />
DC8 2051-24-3 QCBLK167668-1 03/18/98 03/30/98 101 %REC .2<br />
TCMX 877-09-8 QCBLK167668-1 03/18/98 03/30/98 105 %REC .2<br />
"1 0
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: SON685<br />
Anal yte<br />
DCB<br />
TCMX<br />
Blank Sample<br />
CAS Number Name<br />
11097-69-1 OCBLK1681 3-1<br />
2051-24-3 QCBLK168133-1<br />
877-09-8 QCBLK168133-1<br />
Ouanterra-Richland<br />
3350 George Washington way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Semple Date 03/11/98<br />
Receipt Date 03/11/98<br />
Report Date 04/08/98<br />
Duanterra ID 17200-001<br />
Prep. Analyses Detection<br />
Date Date Result Unit Dual- Limit Dilution<br />
03/24/98 0 /2 /98 33 UG/KG U<br />
03/24/98 03/25/98 90 %REC 1<br />
03/24/98 03/25/98 103 %REC 1<br />
, 7.s
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON685<br />
Guanterra-Richland<br />
3350 George Washington Nay<br />
Richland, NA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/11/98<br />
Receipt Date 03/11/98<br />
Report Date 04/20/98<br />
Guanterra ID 17200-001MS<br />
Blank Sample Prep. Analyses Detection<br />
Analyte CAS Number Name Date Date Result Unit Qua(. Limit Dilution<br />
Aroclor-1016 12674-11-2 QCSLK16813 -1 03/24/98 0 /25/98 a6 %REC<br />
Aroclor-1260 11096-82-5 QCBLK168133-1 03/24/98 03/25/98 77 %REC 5<br />
DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 90 %REC 5<br />
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 106 %REC 5<br />
V _i"074
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client 10: 80X685<br />
Analyte<br />
Aroclor-1016<br />
Aroclor-1260<br />
DCB<br />
TCM%<br />
Blank Sample<br />
CAS Number Name<br />
12674-11-2 OCBLK168133-1<br />
11096-82-5 QCBLK168133-1<br />
2051-24-3 QCBLK168133-1<br />
877-09-8 QCBLK168133-1<br />
Duanterra-Richland<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Prep. Analyses<br />
Date Date<br />
03/24/98 03/25/98<br />
03/24/98 03/25/98<br />
03/24/98 03/25/98<br />
03/24/98 03/25/98<br />
Sample Date 03/11/98<br />
Receipt Date 03/11/98<br />
Report Date 04/08/98<br />
Duanterra ID 17200-OOIMS<br />
Detection<br />
Result Unit dual. Limit Dilution<br />
%REC 5<br />
%REC - - 5<br />
90 %REC 5<br />
106 %REC .5<br />
J 7'
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON685<br />
Duanterra-Richland<br />
3350 George Washington way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
sample Date 03/11/98<br />
Receipt Date 03/11/98<br />
Report Date 04/08/98<br />
Duanterra ID : 17200-GOIMSD<br />
Blank Sample Prep. Analyses Detection<br />
Analyte CAS Nunber Name Date Date Result Unit DuaL. Limit Dilution<br />
Aroclor-1016 12674-11-2 QCSLK168133-1 03/24/98 03/25/98 84 %REC .5<br />
Aroclor-1260 11096-82-5 QCBLK168133-1 03/24/98 03/25/98 81 %REC .5<br />
DC8 2051-24-3 QCSLK168133-1 03/24/98 03/25/98 91 %REC .5<br />
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 104 %REC .5<br />
.,0076
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: SON686<br />
AnaLyte<br />
DC8<br />
rCMx<br />
Blank SampLe<br />
CAS NLEber Name<br />
11097-69-1 QCBLK168133-1<br />
2051-24-3 QCBLK168133-1<br />
877-09-8 QC8LK168133-1<br />
Quanterra-Rich Land<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/11/98<br />
Receipt Date 03/11/98<br />
Report Date 04/08/98<br />
Quanterra ID 17200-002<br />
Prep. Analyses Detection<br />
Date Date Result Unit Qua L. Limit Dilution<br />
03/25/98 84 %REC<br />
03/25/98 89 %REC 9<br />
A077
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON687<br />
Analyte<br />
ouanterra-Richlana<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/11198<br />
Receipt Date 03/11/98<br />
Report Date 04/08/98<br />
0uanterra ID : 17200-003<br />
Blank Sample Prep. Analyses Detection<br />
CAS Number Name Date Date Result Unit Dual. Limit Dilute on<br />
Aroclor-1254 11097-69-1 OC8LK168133-1 03/24/98 03/25/98 33 UG/KG U 33<br />
Oc8 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 90 %REC<br />
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 105 %REC
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: SON682<br />
Ouanterra-Richland<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/10/98<br />
Receipt Date 03/10/98<br />
Report Date 04/08/98<br />
Duanterra ID 17202-001<br />
Blank Sample Prep. Analyses Detection<br />
Analyte CAS Number Name Date Date Result Unit Oual. Limit Dilution<br />
Aroclor-12 4 11097-69-1 QCBLK168133-1 03/24/98 03/25/98 33 UG/KG U 33 1<br />
DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 91 %REC 1<br />
TCMK 877-09-8 QCBLK168133-1 03/24/98 03/25/98 100 %REC t<br />
x,00079
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON683<br />
Analyte<br />
Duanterra-Richland<br />
3350 George Washington Nay<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/10/98<br />
Receipt Date 03/10/98<br />
Report Date 04/08/98<br />
Duanterra ID : 17202-002<br />
Blank Sample Prep. Analyses Detection<br />
CAS Number Name Date Date Result Unit Dual. Limit Dilution<br />
Aroclor-12 4 11097-69-1 DCBLK16 133-1 03/24/98 03/25/9 33 UG/KG U 33 1<br />
DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 91 %REC 1<br />
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 86 %REC 1
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON684<br />
Duanterra-Richland<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/10/98<br />
Receipt Date 03/10/98<br />
Report Date 04/08/98<br />
Ouanterra ID : 17202-003<br />
Blank Sample Prep. Analyses Detection<br />
Analyte CAS Number Name Date Date Result Unit Dual. Limit Dilution<br />
Aroclor-12 4 1 "<br />
07-69-1 QCBLK168133-1 03/24/98 03/ /98 33 UG/KG U 33 1<br />
DCB 2051-24-3 QCSLK168133-1 03/24/98 03/25/98 88 %REC 1<br />
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 94 %REC 1
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Duanterra-Richland<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/12/98<br />
Receipt Date 03/12/98<br />
Report Date 04108/98<br />
Client ID: BON688 Duanterra ID : 17203-001<br />
Blank Sample Prep. Analyses Detection<br />
Analyte CAS Number Name Date Date Result Unit Dual. Limit Dilution<br />
Aroclor-12 4 11097-69-1 QCBLK168133-1 03/24/98 03/25/98 33 UG/KG U 33 1<br />
OCS 2051-24-3 QCSLK168133-1 03/24198 03/25/98 92 %REC 1<br />
TCMK 877-09-8 QCBLK168133-1 03/24/98 03/25/98 105 %REC 1<br />
(J00S^:
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON689<br />
Analyte<br />
Blank Sample<br />
LAS Number Nam<br />
Ouanterra-Richland<br />
3350 George Washington Nay<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Prep. Analyses<br />
Date Date<br />
Sample Date 03/12/98<br />
Receipt Date 03112/98<br />
Report Date 04/08/98<br />
Ouanterra ID : 17203-002<br />
Detection<br />
Result Unit OuaL. Limit Dilution<br />
p roctor-1254 11097-69-1 QCBLK168133-1 03/24/98 03/25/98 UG/KG U 33 1<br />
DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 90 %REC 1<br />
TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 65 %REC 1<br />
^J
Duanterra-Richland<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Category: PCB's Sample Date 03/13/98<br />
Method: EPA 8080 Receipt Date 03/13/98<br />
Matrix: SOLID Report Date 04/08/98<br />
Client ID: BON690 Duanterra ID 17221-001<br />
Blank Sample Prep. Analyses Detection<br />
Analyte CAS Number Name Date Date Result Unit DuaL. Limit Dilution<br />
Aroclor-1254 11097-69-1 QCBLK16825 -1 03/25/98 03/29/98 33 UG/KG U 1<br />
DC8 2051-24-3 QCBLK168253-1 03/25198 03/29/98 94 XREC 1<br />
TCMX 877-09-8 QCBLK168253-1 03/25/98 03/29/98 73 XREC<br />
OS 6
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON691<br />
Duanterra-Richland<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/13/98<br />
Receipt Date 03/13/98<br />
Report Date 04/08/98<br />
Ouanterra ID 17221-002<br />
Blank Sample Prep. Analyses Detection<br />
Analyte CAS Number Name Date Date Result Unit DuaL. Limit Dilution<br />
Aroclor-1254 11097-69-1 QCBLK168253-1 03/25/98 03/29/98 33 UG/KG U 33 1<br />
DCB 2051-24-3 QCBLK168253-1 03/25/98 03/29/98 108 %REC 1<br />
TCMX 877-09-8 QCBLK168253-1 03/25/98 03/29/98 82 %REC 1<br />
, 6087
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: SON692<br />
Analyte<br />
Duanterra-Richland<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/16/98<br />
Receipt Date 03/16/98<br />
Report Date 04/08/98<br />
Duanterra ID : 17224-001<br />
Blank Sample Prep. Analyses Detection<br />
CAS Number Name Date Date Result Unit Dual. Limit Dilution<br />
Aroclor-1254 11097-69-1 QCBLK168253-1 03/25/98 03/29/98 33 UG/KG U 33 1<br />
DCB 2051-24-3 QCBLK168253-1 03/25/98 03/29/98 92 %REC 1<br />
TCMK 877-09-8 QCBLK168253-1 03/25/98 03/29/98 74 %REC 1<br />
tj
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client ID: BON693<br />
duanterra-Richland<br />
3350 George Washington Nay<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date 03/16/98<br />
Receipt Date 03/16/98<br />
Report Date 04/08/98<br />
duanterra ID 17224-002<br />
Blank Sample Prep. Analyses Detection<br />
Analyte CAS Number Name Date Date Result Unit dual. Limit Dilution<br />
ArocLor-1254 11097-69-1 QCBLK168253-1 03/25/98 03/29/98 33 UG/KG U 3 1<br />
DCB 2051-24-3 QCBLK168253-1 03/25/98 03/29/98 95 %REC 1<br />
TCMX 877-09-8 QCBLK168253-1 03/25/98 03/29/98 87 %REC 1<br />
J08 9
Category: PCB's<br />
Method: EPA 8080<br />
Matrix: SOLID<br />
Client 10: SON694<br />
Anatyte<br />
Aroclor-<br />
DCB<br />
TCMX<br />
Quanterra-Richland<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Stank Sample Prep. Analyses Detection<br />
CAS Number Name Date Date Result Unit Qua L. Limit Dilution<br />
2051-24-3 QCSLK168253-1<br />
877-09-8 QCBLK168253-1<br />
03/29/98 98 %REC<br />
03/29/98 93 %REC<br />
Saapie Date 03/16/98<br />
Receipt Date 03/16/98<br />
Report Date 04/08/98<br />
Quanterra ID 17224-003<br />
^i.,^J0
Lab Name: OUANTERRA.MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 6.0 (g/ml) G<br />
Level: (low/med) LOW<br />
Moisture: not dec. dec.<br />
Extraction: (SepF/Cont/Sonc) Sonc<br />
GPC Cleanup: (YIN) N pH:<br />
CAS NO. Compound<br />
1D EPA SAMPLE NO.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
SAS No.: SDG No.: W02275<br />
EONG80<br />
Lab Sample ID: 17199-001<br />
Lab File ID:<br />
Date Sampled: 03-09-98<br />
Date Extracted: 03-18-98<br />
Date Analvzed: 03-30-98<br />
Dilution Factor: 0.2<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 63<br />
U Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
"j0J X93
1D EPA SAMPLE NO.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
I<br />
BONG81<br />
Lab Name: OUANTERRA.MO Contract 550.260<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 6.0 ('g/ml) G<br />
Level: (low/med) LOW<br />
% Moisture: not dec.<br />
Extraction: (SepF/font/Sonc)<br />
GPC Cleanup: (Y/N) N<br />
CAS NO. Compound<br />
dec<br />
pH:<br />
Sonc<br />
SAS No.: SDG No.: W02275<br />
Lab Sample =D: 17199-002<br />
Lab File ID:<br />
Date Sampled: 03-09-98<br />
Date Extracted: 03-18-96<br />
Date Analyzed: 03-30-98<br />
Dilution Factor: 0.2<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 33 U_<br />
U: Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
j0O94
Lab Name: OUANTERRA MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matr_%: (soil/water) SOIL<br />
Sample wt/vol: 30.0 (g/ml) G<br />
eve_: flow /med) LOW<br />
% Moisture: not des. dec.<br />
Extraction: (SepF/font/Sonc) Sonc<br />
GPC Cleanup: (YIN) N pH:<br />
CAS NO. Compound<br />
11097-69-1 ------ Aroclor-<br />
1D EPA SAMPLE NO.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
SAS No.: SDG No.: W02275<br />
BON685<br />
Lab Sample 1D: 17200-001<br />
Lab File ID:<br />
U Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
Date Sampled: 03-11-96<br />
Date Extracted: 03-24-98<br />
Date Analyzed: 03-25-98<br />
Dilution Factor: 1<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) UG/KG Q<br />
33 1 U<br />
1, -J0095
Lab Name: OUANTERRA MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 30.2 (g/ml) G<br />
Level: (low/med) LOW<br />
Moisture: not dec. dec.<br />
Extraction: (SepF/Cont/Sonc) Sonc<br />
GPC Cleanup: (YIN) N pH:<br />
CAS NO. Compound<br />
1D EPA SAMPLE NO.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
SAS No.: SDG No.: W02275<br />
BONG86<br />
Lab Sample ID: 17200-002<br />
Lab File ID:<br />
Date Sampled: 03-11-98<br />
Date Extracted: 03-24-98<br />
Date Analyzed: 03-25-98<br />
Dilution Factor: 1<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 33 U<br />
U Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
"j<br />
I
Lab Name: OUANTERRA,M0 Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 30.2 (g/ml) G<br />
Level: (low/med) LOW<br />
W Moisture: not dec. dec.<br />
Extraction: (SepF/Cont/Sonc) Sonc<br />
GPC Cleanup: (Y/N) N PH:<br />
CAS NO. Compound<br />
1D EPA SAMPLE NO<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
550.260<br />
SAS No. SDG No. W02275<br />
BONG97<br />
Lab Sample ID: 17200-003<br />
Lab File !D:<br />
Date Sampled: —03----1-98<br />
Date Extracted: 03-24-98<br />
Date Analyzed: 03-25-98<br />
Dilution Factor: 1<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kq) UG/KG<br />
11097-69-1 ------ Aroclor-1254 33 -U--<br />
U: Concentration of analyte is less than the value given,<br />
FORM I PEST<br />
1- U009 "1
Lab Name: QUANTERRA,MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 30.1 jg/ml) G<br />
Level: (low/med) LOW<br />
°s Moisture: not dec. dec.<br />
Extraction: (SepF/font/Sonc) Sonc<br />
GPC Cleanup: ,Y/N) N pH:<br />
CAS NO. Compound<br />
ID EPA SAMPLE NC.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
iBON682<br />
SAS No.: SDG No.: W02275<br />
Lab Sample ID: 17202-001<br />
Lab File ID:<br />
Date Sampled: 03-10-98<br />
Date Extracted: 03-24-98<br />
Date Analvzed: 03-25-98<br />
Dilution Factor: 1<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 33 ^—U_i<br />
U: Concentration of analvte is less than the value given.<br />
FORM I PEST<br />
00098
Lab Name: QUANTERRA,MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: (scii/water) SOIL<br />
Sample wt/vol: 30.0 (g/ml) G<br />
Level: (low/med) LOW<br />
% Moisture: not dec. dec.<br />
Extraction: (SepF/font/SOnc) Sonc<br />
GPC Cleanup: (Y/N) N pH:<br />
in EPA SAMPLE NO.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
550.260<br />
SAS No.: SDG No.: W02275<br />
Lab Sample ID: 17202-002<br />
Lab File ID:<br />
Date Sampled: 03-10-98<br />
Date Extracted: 03-24-98<br />
Date Analvzed: 03-25-98<br />
Dilution Factor: 1<br />
BONG83 -^<br />
CONCENTRATION UNITS:<br />
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 33 1 U<br />
U: Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
(:00099
Lab Name: OUANTERRA,MO Contract<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 30.1 (g/ml) G<br />
Level: (low/med) LOW<br />
% Moisture: not dec.<br />
Extraction: (Sep F/font/SOnc)<br />
GPC Cleanup: (YIN) N<br />
CAS NO. Compound<br />
1D EPA SAMPLE NO.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
dec.<br />
pH:<br />
Sonc<br />
550.260<br />
SAS No.: SDG No.: W02275<br />
SON684<br />
Lab Sample iD: 17202-003<br />
Lab File ID:<br />
Date Sampled: 03-10-98<br />
Date Extracted: 03-24-98<br />
Date Analyzed: 03-25-98<br />
Dilution Factor: 1<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) UG/KG 4<br />
11097-69-1 ------ Aroclor-1254 33 U<br />
U: Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
"00100
Lab Name: OUANTERRA MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 30.2 (g/ml) G<br />
Level: (low/med) LOW<br />
% Moisture: not dec. dec.<br />
Extraction: (SepF/font/SOnc) Sonc<br />
GPC Cleanup: (Y/N) N pH:<br />
ID EPA SAMPLE NO.<br />
PCP ORGANICS ANALYSIS DATA --HEST<br />
550.260<br />
SAS No.: SDG No.: W02275<br />
SONG88<br />
Lab Sample ID: 17203-001<br />
Lab File ID:<br />
Date Sampled: 03-12-98<br />
Date Extracted: 03-24-98<br />
Date -nalvzed: 03-25-98<br />
Dilution Factor:<br />
CONCENTRATION UNITS:<br />
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 33 U<br />
i<br />
U: Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
:. V V i V l
Lab Name: OUANTERRA,MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: !Soil /water) SOIL<br />
Sample wt/vol: 30.2 (g/ml) G<br />
Level: (low/med) LOW<br />
% Moisture: not dec. dec.<br />
Extraction: (SepF/font/Sonc) Sonc<br />
GPC Cleanu p : (YIN) N pH:<br />
1D EPA SAMPLE NO.<br />
PCB ORGANICS ANALYSIS DATA SHEET.<br />
550.260<br />
SAS No.: SDG No.: W02275<br />
BONG89<br />
Lab Sample =D: 17203-002<br />
Lab File ID:<br />
Date Sampled: 03-12-98<br />
Date Extracted: 03-24-98<br />
Date Analyzed: 03-25-98<br />
Dilution Factor: 1<br />
CONCENTRATION UNITS:<br />
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 33 U<br />
U: Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
100102<br />
—
Lab Name: QUANTERRA,MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 30.2 (g/ml) G<br />
Level: (low/med) LOW<br />
% Moisture: not dec. dec.<br />
Extraction: (SepF/font/Sonc) Sonc<br />
GPC Cleanup: (Y/N) N pH:<br />
1D EPA SAMPLE NO.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
550.260<br />
SAS No.:<br />
SDG No.: W02275<br />
3ON690<br />
Lab Sample ID: 17221-301<br />
Lab File ID:<br />
Date Sampled: 03-13-98<br />
Date Extracted: 03-25-98<br />
Date Analvzed: 03-29-98<br />
Dilution Factor: 1<br />
CONCENTRATION UNITS:<br />
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 1 33 1 U<br />
U: Concentration of analvte is less than the value given.<br />
FORM I PEST<br />
00103
Lab Name: QUANTERRA,MO Contract: 550.260<br />
1D EPA SAMPLE :70.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275<br />
Matrix: (soil/water) SOIL Lab Sample ID: 17221-002<br />
Sample wt/vol: 30.1 (g/ml) G Lab File ID:<br />
Level: (low/med) LOW Date Sampled: 03-13-98<br />
o Moisture: not dec. dec. Date Extracted: 03-25-98<br />
Extraction: (SepF/font/SOnc) Sonc Date Analyzed: 03-29-98<br />
CPC Cleanup: ;Y/N) N pH: Dilution Factor: _<br />
BON691<br />
CONCENTRATION UNITS:<br />
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 33 U<br />
U: Concentration of anal; ,te is less than the value given.<br />
FORM I PEST<br />
r u0iO4
Lab Name: QUANTERRA.MO Contract: 550.260<br />
1D EPA SAMPLE NO.<br />
POE ORGANICS ANALYSIS DATA SHEET<br />
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275<br />
Matr'_x: (soil/water) SOIL Lab Sample ID: 17224-001<br />
Sample wt/vol: 30.0 (g/ml) G Lab File ID:<br />
Level: (low/med) LOW Date Sampled: 03-16-98<br />
o Moisture: not dec. dec. Date Extracted: 03-25-98<br />
Extraction: (SepF/font/Sonc) Sonc Date Analyzed: 03-29-99<br />
GPC Cleanup : (YIN) N pH: Dilution Factor:<br />
EON692<br />
CONCENTRATION UNITS:<br />
CAS NO. Compound (ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 33 U<br />
U: Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
1 00105
Lab Name: QUANTERRA MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 30.2 (g/ml) G<br />
Level: (low/med) LOW<br />
Moisture: not dec. dec.<br />
Extraction: (SepF/Cont/Sonc) Son<br />
GPC Cleanup: (Y/N) N pH:<br />
CAS NO. Compound<br />
11097-69-1 ------ Aroclor-1254<br />
ID<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
EPA SAMPLE NO.<br />
BON693<br />
550.260 _!<br />
SAS No.:<br />
SDG No.: W02275<br />
Lab Sample ID: 17224-002<br />
Lab File ID:<br />
U: Concentration of analyte is less than the value given.<br />
FORM I PEST<br />
Date Sampled: 03-16-98<br />
Date Extracted: 03-25-98<br />
Date Anal y zed: 03-29-98<br />
Dilution. Factor: 1<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) UG/KG Q<br />
33 I-'J
Lab Name: OUANTERRA,MO Contract:<br />
Lab Code: ITMO Case No.:<br />
Matrix: (soil/water) SOIL<br />
Sample wt/vol: 30.0 (g/ml) G<br />
Level: (low/med) LOW<br />
% Moisture: not dec.<br />
Extraction: (SepF/font/SOnc)<br />
GPC Cleanup: (YIN) N<br />
CAS NO. Compound<br />
ID EPA SAMPLE NO.<br />
PCB ORGANICS ANALYSIS DATA SHEET<br />
dec.<br />
pH:<br />
Sonc<br />
550.260<br />
SAS No.: SDG No.: W02275<br />
SON694<br />
Lab Sample ID: 17224-003<br />
Lab File ID:<br />
Date Sampled: 03-16-98<br />
Date Extracted: 03-25-98<br />
Date Analvzed: 03-29-98 ._<br />
Dilution Factor:<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) UG/KG Q<br />
11097-69-1 ------ Aroclor-1254 33 U<br />
U: Concentration of analyte is less than the value given.<br />
FORM I PEST
Category: Mercury<br />
Method: EPA 7471<br />
Matrix: SOLID<br />
ouanterra-Richland<br />
3350 George Washington Way<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Semple Date 03/09/98<br />
Receipt Date 03/09/98<br />
Report Date 04/20/98<br />
Client Ouanterra Blank Saapte Prep. Anityses Detection<br />
ID ID Analyte CAS Number Name Date Date Result Unit Ouai. Limit Dit.<br />
BON680 17199-001 Mercury 7439-97-6 OCBLK168655-1 03/30/98 03/30/98 0.10 MG/KG 0.033 1<br />
BON681 17199-002 Mercury 7439-97-6 OCBLK168655-1 03/30/98 03/30/98 0.03 MG/KG B 0.033 1<br />
BON685 17200-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
BON685 17200-001M5 Mercury 7439-97-6 OCSLK168333-1 03/25/98 03/25/98 116 XREC 1<br />
BON685 17200-001MSD Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 111 %REC 1<br />
BON636 17200-002 Mercury 7439-97-6 OCBLK168333-1 03/25198 03/25/98 0.13 MG/KG 0.033 1<br />
BON687 17200-003 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
BON682 17202-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
BON683 17202-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.10 MG/KG 0.033<br />
BON684 17202-003 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
BON688 17203-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
BON689 17203-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.04 MG/KG 0.033 1<br />
BON690 17221-001 Mercury 7439-97-6 OCSLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
BON691 17221-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
SON692 17224-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.16 MG/KG 0.033 1<br />
SON693 17224-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
BON694 17224-003 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
NA OCLCS168655-1 Mercury 7439-97-6 OCBLK166655-1 03/30/98 03/30/98 116 %REC 10<br />
NA OCBLK168655-1 Mercury 7439-97-6 OCBLK166655-1 03/30/98 03/30/98 0.017 MG/KG U 0.033 1<br />
25
category: Mercury<br />
Method: EPA 7471<br />
Matrix: SOLID<br />
QUanterra-Richland<br />
3350 George Washington Nay<br />
Richland, WA 99352-1613<br />
Project: 550.260<br />
Sample Date NA<br />
Receipt Date NA<br />
Report Date 04/08/98<br />
Client Quanterra Blank Sample Prep. Analyses Detection<br />
ID ID Analyte CAS Number Name Date Date Result Unit Qua L. Limit Dil<br />
NA QCLCS168333-1 Mercury 7439-97-6 QCBLKI 33-1 03/25/98 03/25/98 107 KREC 10<br />
NA QCBLK168333-1 Mercury 7439-97-6 QCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1<br />
^^ 6
Category: ICAP Metals<br />
Method: EPA 6010<br />
Matrix: SOLID<br />
Duanterra-RichLano<br />
3350 George Washington way<br />
RichLand, WA 99352-1613<br />
Project: 550.260<br />
Sample Date NA<br />
Receipt Date NA<br />
Report Date 04/08/98<br />
CLient Duanterra Blank Sample Prep. Analyses Detection<br />
ID ID Analyte CAS Number Name Date Date Result unit Oual. Limit Dil<br />
NA OCLCS168299-1 Lead 7439-92-1 OCOLK168299-1 03/25/98 03/25/98 100 %REC 1<br />
NA QCBLK168009-1 Lead 7439-92-1 QCBLK168C09-1 03/23/98 03/23/98 0.21 MG/KG B 0.30 1<br />
NA QCBLK168299-1 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 0.16 MG/KG B 0.30 1<br />
BON680 17199-001 Lead 7439-92-1 QCSLK168009-1 03/23/98 03/23/98 10.9 MG/KG E 0.30 1<br />
BON681 17199-002 Lead 7439-92-1 QCHLK168009-1 03/23/98 03/23/98 3.7 MG/KG E 0.30 1<br />
BON685 17200-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.2 MG/KG E 0.30 1<br />
BON685 17200-OOlMS Lead 7439-92-1 QCSLK168299-1 03/25/98 03/25/98 90 XREC 1<br />
SON685 17200-OOlMSO Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 88 %REC 1<br />
BON686 17200-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 11.8 MG/KG E C.30 1<br />
SON687 17200-003 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.7 MG/KG E 0.30 1<br />
8ON682 17202-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.7 MG/KG E 0.30 1<br />
SON683 17202-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 7.6 MG/KG E 0.30 1<br />
BON684 17202-003 Lead 7439-92-1 GCBLK168299-1 03/25/98 03/25/98 3.3 MG/KG E 0.30 1<br />
BON688 17203-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.0 MG/KG E 0.30 1<br />
9ON689 17203-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 9.0 MG/KG E 0.30 1<br />
SON690 17221-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.4 MG/KG E 0.30 1<br />
SON691 17221-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 2.9 MG/KG E 030 1<br />
BON692 17224-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 10.6 MG/KG E 0,30 1<br />
BON693 17224-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 4.2 MG/KG E 0.30 1<br />
BON694 17224-003 Lead 7439-92-1 OCBLK168299-1 03/25/98 03/25/98 3.6 MG/KG E 0.30 1<br />
NA QCLCS168009-1 Lead 7439-92-1 OCOLK168009-1 03/23/98 03/23198 102 %REC 1
U.S. EPA - CLP<br />
COVER PAGE INORGANIC ANALYSES DATA PACKAGE<br />
Lab Name: QUANTERRA MO Contract: 550.260<br />
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275<br />
SOW No.: SW846<br />
EPA Sample No.<br />
_BON692<br />
_2 0 11 680<br />
_BON681<br />
BON682<br />
_B0N683<br />
_BON684<br />
_BON685<br />
_BON685SD<br />
_BON685S<br />
_BON686<br />
_BON687<br />
_B0N688<br />
_BON689<br />
_BON690<br />
_BON691<br />
_BON693<br />
BON694<br />
Were ICP interelement corrections applied ?<br />
Were ICP background corrections applied ?<br />
If yes - were raw data generated before<br />
application of background corrections ?<br />
Comments:<br />
Lab Sample ID<br />
17224-001_<br />
17199-001<br />
17199-002<br />
17202-001<br />
_17202-002<br />
17202-003<br />
17200-001<br />
_17200-OO1SD_<br />
17200-OO1S<br />
17200-002<br />
_17200-003^<br />
17203-001_<br />
17203-002<br />
17221-001<br />
17221-002J<br />
17224-002<br />
17224-003<br />
Yes/No YES<br />
Yes/No YES<br />
Yes/No 7C<br />
I certify that this data package is in compliance with the terms and<br />
conditions of the contract, both technically and for completeness, for<br />
other than the conditions detailed above. Release of the data contained<br />
in this hardcopy data package and in the computer-readable data submitsed<br />
on floppy diskette has been authorized by the Laboratory Mana ger r -he<br />
Manag er's designee, as verified by the following signature.<br />
Signature: Name:<br />
Date Title:<br />
COVER PAGE - IN SW-^46<br />
7 A<br />
, - J 1
U.S. EPA - --LP<br />
INORGANIC ANALYSES DA '.-=ET<br />
^<br />
BON692<br />
Lab Name: QUANTERRA MO<br />
Lab Code: - TMO Case No.:<br />
Matrix (soil/water): SOIL<br />
Level (low/med): LOW<br />
Solids: 100.0<br />
Contract:<br />
SAS No.: SDG No.. W02275<br />
Sample ID: 17224-001<br />
-,--e Received: 03/15/98<br />
Concentration Units (ug/L or mg/kg dr.; :oeight)<br />
CAS No. Analyte Concentrat Q<br />
7439-92-1 LeaT 1C._^^ E<br />
7439-97-6 Mercury-0.15– — -<br />
Color Before: Clarity Before:<br />
Color After: Clarity After:<br />
^7omments:<br />
-<br />
^I<br />
I<br />
P<br />
CV<br />
MG/KG<br />
=1<br />
-<br />
-I<br />
SW-84h
Color Before:<br />
Color After:<br />
Comments:<br />
I- . .EPA - =<br />
1 --PA :SAMPLE No.<br />
INORGAN_ - ANALYSES -ATA. -HEET I<br />
BON630<br />
Lab Name: QUANTERRA MO<br />
Lab Code: ITMO Case No.:<br />
Matrix (soil/water): SOIL<br />
Level (low/med): LOW<br />
Contract:<br />
SAS No.:<br />
5 .26G<br />
SDG No.:<br />
Lab Sample ID:<br />
Date Received:<br />
W02275<br />
17199-001<br />
03,`(J9/9 c<br />
% Solids: 100.0<br />
Concentration Units "ug/L or mg/kg dry weight): MG/KG<br />
CAS No.<br />
7439-92-1<br />
7439-97-6<br />
Analyte Concentration C Q IM<br />
LeadI 10.9<br />
Mercury_ O.lO CV<br />
I-<br />
i<br />
—<br />
I-<br />
. ,<br />
.<br />
Clarity Before : TP_xr^:^e.<br />
Clarity After: Art-facts:<br />
_ ten,•, _ - _^^<br />
i<br />
SW-n46
U.S. EPA CLP<br />
1 EPA SAMPLE NO -<br />
INORGANIC ANALYSES DATA SHEET<br />
BGN631<br />
Lab Name: QUANTERRA MO Contract: 550.260<br />
Lab Code: ITMO Case `To.: SAS No.: —I SDG o.: ;102275<br />
Matrix (soil/water): SOIL<br />
Sample ID: _7199-00:<br />
Level (low/med) LOW Date Received: 3;09/98<br />
s Solids: 100.0<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
CAS No.<br />
7439-92-1<br />
7439-97-6<br />
Analyte<br />
Lem<br />
Mercury<br />
Concentration Q<br />
i– i<br />
3.7 E<br />
0.03 B<br />
Color Before: Clarity Before: Text re:<br />
Color After: Clarity After:<br />
Comments:<br />
i<br />
–i<br />
N<br />
5<br />
_V<br />
i<br />
SW-146<br />
131<br />
i
U.S. EPA --LP<br />
1 EPA SAMPLE NO.<br />
INORGANIC ANALYSES DATA SHEET<br />
20N682<br />
Lab Name: QUANTERRA MO Contract: -750.260<br />
Lab Code: ITMOCase No.: SAS No.: SDG No.: W02275<br />
Matrix (soil/water): SOIL Lab Sample ID: 17202-001<br />
Level ;low/med): LOW Date Received: 03/10/98<br />
Solids: 100.0<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
CAS No. Analyte Concentration C Q M<br />
7439-92-1 Lead 3.7 E P<br />
7439-97-6 Mercury_ 0.02 U ^CV<br />
Color Before: Clarity Before:<br />
-<br />
exture:<br />
Color After: Clarity After: = -facts: -<br />
Comments:<br />
I_<br />
-<br />
SW-846<br />
r. 2
U.S. EPA --LP<br />
1 EPA SAMPLE NO<br />
INORGANIC ANALYSES DATA SHEET<br />
3ON683<br />
Lab Name: QUANTERRA MO<br />
Lab Code: ITMO Case No.:<br />
Matrix (soil/water): SOIL<br />
Level (low/med): LOW<br />
% Solids: 100.0<br />
Contract:<br />
SAS No.:<br />
550.2 6 0<br />
SDG `:o.:<br />
Lan Sample ID:<br />
Date Received:<br />
W02275<br />
17202-002<br />
03!10/98<br />
Concentration Units (ug/L or mg/kg dry weight)<br />
CAS No. Analyte ( Concentration C<br />
7439-92-1 Le —a—(l Le 7.6<br />
7439-97-6 Mercury_ 0.10<br />
Color Before: Clarity Before:<br />
Color After: Clarity After:<br />
Comments:<br />
Q<br />
'— I<br />
M<br />
CV<br />
—<br />
MG/KG<br />
^'extnre<br />
rt -acts.<br />
SW-846<br />
^33
U.S. EPA - CLP<br />
1 EPA SAMPLE 70<br />
INORGANIC ANALYSES DATA SHEET<br />
30N634<br />
Lab Name: QUANTERRA MO Contract: 550.260<br />
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275<br />
Matrix (soil/water): SOIL Lab Sample 1D: !7202-20<br />
Level !low/med): LOW Date Received: 03/10;98<br />
Solids: 100.0<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
CAS No. Analyte Concentration . 0 Q M<br />
I<br />
7439-92-1 Lem—3.3 E P<br />
7439-97-6 Mercury_ 0.02 U A<br />
Color Before: Clarity Before: 7extsre:<br />
Color After: Clarity After: Artifacts:<br />
Comments:<br />
-34<br />
SW-&4F
U.S. EPA _LP<br />
i EPA SAMPLE NO.<br />
INORGANIC ANALYSES DATA SHEET<br />
BONG85<br />
Lab Name:QUANTERRA MO Contract: 550.250<br />
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275<br />
Matrix (soil/water): SOIL<br />
Lan Sample ID: 17200-001<br />
Level (low/med): LOW Date Received: 03/11/98<br />
°a Solids: 100.0<br />
Color Before:<br />
Color After:<br />
Ccmments:<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
CAS No.<br />
7439-92-1<br />
7439-97-6<br />
Analyte Concentration<br />
Lead 3.2<br />
Mercury_ 0.02<br />
Clarity Before:<br />
Clarity After:<br />
C Q M<br />
E P<br />
U ACV<br />
—<br />
–i —<br />
i<br />
– —<br />
I<br />
Texture:<br />
art «acts<br />
" ^.i -J5<br />
SW-646
U.S. EPA - CLP<br />
1 EPA SAMPLE NO.<br />
INORGANIC ANALYSES DATA SHEET<br />
BON685<br />
Lab Name: QUANTERRA MO Contract: 550.260<br />
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275<br />
Matrix !soil/waterj: SOIL Lan Sample ID: 17200-002<br />
Level (low/med): LOW Date Received: 03/11/99<br />
Solids: 100.0<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
CAS No. Analyte Concentration C Q M<br />
7439-92-1 Lear 11.8 _E_ P<br />
7439-97-6 Mercury—0.13 Cv<br />
Color Before: Clarity Before: Texzure:<br />
Color After: Clarity After: Art __`acc3:<br />
Comments:<br />
I<br />
SW-846<br />
136
U.S. EPA CLP<br />
1 EPA SAMPLE NO<br />
INORGANIC ANALYSES DATA SHEET<br />
BON687<br />
Lab Name: QUANTERRA MO Contract: 550.260<br />
Lab erode: ITMO Case No.: SAS No.: S D G No.: W02275<br />
Matrix (soil/water): SOIL — Lab Samp le ID: 17200-00:'<br />
Level (low/med): LOW Date Received: 03/11/98<br />
Solids: 100.0<br />
Color Sefore:<br />
Colcr After:<br />
Comments:<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
CAS No.<br />
7439-92-1<br />
7439-97-6<br />
Analyte<br />
Lea^—<br />
Mercury_<br />
Concentration C Q<br />
Clarity Before:<br />
Clarity After:<br />
3.7 - E -<br />
0.02 U<br />
–I<br />
M<br />
P<br />
CV<br />
I — I<br />
I<br />
i<br />
ext. _:<br />
Artifacts:<br />
" 13 '7<br />
SW-946
U.S. EPA - CLP<br />
1 EPA SAMPLE NO.<br />
INORGANIC ANALYSES DATA SHEET<br />
BON688<br />
Lab Name: QUANTERRA MO<br />
Lab Code: iTMO Case No.:<br />
Matrix (soil/water): SOIL<br />
Level (low/med): LOW<br />
Solids: 100.0<br />
Contract: -^_ .260<br />
SAS No.: SDG No.:<br />
Lan Sample ID:<br />
Cate Received:<br />
W02275<br />
17203-001<br />
03/12/98<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
CAS No.<br />
7439-92-1<br />
7439-97-6<br />
Analyte<br />
Leaa-<br />
Mercury_<br />
Concentraticn.0 Q<br />
3.0^ E<br />
0.02 U<br />
Color Before: Clarity Before: Texture:<br />
Color After: Clarity After: Artifacts:<br />
Comments:<br />
FORM I - IN<br />
i<br />
—I<br />
M<br />
P<br />
CV<br />
ff.<br />
l) ^J i J<br />
SW-846
Color Before:<br />
Color After:<br />
Comments:<br />
CAS No.<br />
7439-92-1<br />
7439-97-6<br />
J.S. EPA CLP<br />
'<br />
1<br />
INORGANIC ANALYSES DATA SHEET<br />
EPA SAMPLE NO.<br />
BON6c9<br />
i<br />
Lab Name: QUANTERRA MO<br />
Lab Code: ITMO Case No.:<br />
Matrix (soil/waer): t SOIL<br />
Level (low/med): LOW<br />
Solids: 100.0<br />
Contract: 550.260<br />
SAS No.: SDG No.:<br />
n Sample La ID:<br />
Date Received:<br />
W02275 _<br />
17203-002<br />
03/12/98<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
Analyte Concentration Q<br />
Lead -9.0 _ I _E<br />
Mercury_ 0.04<br />
Clarity Before:<br />
Clarity After:<br />
i<br />
—<br />
—I<br />
M<br />
P<br />
CV<br />
Texture:<br />
Art--`acts:<br />
SW-=46<br />
139
U.S. EPA CLP<br />
1 SPA SAMPLE '7j 0<br />
INORGANIC ANALYSES DATA SHEET<br />
BON690<br />
Lab Name: QUANTERPA MO Contract: 550.250<br />
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275<br />
Matrix (soil/water): SOIL Lab Sample ID: 17221-007<br />
Level (low/med): LOW Date Received: 03/13;'98<br />
°s Solids: 100.0<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
CAS No. Analyte Concentration , (- Q ^M<br />
7439-92-1 Lem— 3.4 E P<br />
7439-97-6 Mercury 0.02 U CV<br />
I_<br />
I<br />
I I<br />
— I<br />
– i -<br />
-I —<br />
Color Before: Clarity Before: Texti:re:<br />
Color After: Clarity After: Art_-acts:<br />
:7 omments:<br />
sw---;6
U. E. EPA - CT<br />
1 EPP_ SAMPLE NO.<br />
INORGANIC ^,NALYSES DATA -HEET<br />
Lab Name: QUANTERRA MO<br />
Lab Code: _TMO Case No.:<br />
Matrix (soil/water): SOIL<br />
Level (low/med): LOW<br />
o Solids: 100.0<br />
Contract:<br />
SAS No.:<br />
X20 260<br />
SDG No.:<br />
Lan Sample ID:<br />
Date Rece_ved:<br />
BON691<br />
W02275<br />
17221-,702<br />
03/13/58<br />
Color Before:<br />
Color After:<br />
Comments:<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
CAS No.<br />
7439-92-1<br />
7439-97-6<br />
i<br />
Analyte I Concentration!CI Q M I<br />
Lear—2 . 9 E P<br />
Mercury_ 0.02 U CV<br />
Clarity Before: exture<br />
Clarit y After: Artifacts:<br />
vO141<br />
SW-c}6
CAS No. Analyte<br />
7439-92-1 Lem<br />
7439-97-6 (Mercury_<br />
U.S. EPA - CLF<br />
1 EPA SAMPLE NO<br />
INORGANIC ANALYSES DATA SHEET<br />
-N69_<br />
Lab Name: QUANTERRA MO Contract: 000.260 _1<br />
1<br />
Lab Code: ITMO Case ^;o.: SAS No.: SDG No.: ::02275<br />
Matrix (soil/water): SOIL _L__aE Sample ID: 17224-00<br />
Level (low/med): LOW Date Received: 03/16/98<br />
% Solids: 100.0<br />
Concentration Units (ug/L or mg/kg dry weight): MG/KG<br />
Concentration C<br />
'3 c<br />
0.02 U<br />
_i<br />
–<br />
Q M<br />
Color Betcre: Clarity Before: Text r<br />
Color Af*_er. Clarity After: Art S: —<br />
Comments:<br />
E<br />
i<br />
P CVI<br />
SW- Hfir,
Color Before:<br />
Color After:<br />
Comments:<br />
U.S. EPA CLP<br />
1 -xPA ',AM P LE 0.<br />
INORGANIC ANALYSES DAT I SHEET<br />
SONG 741<br />
Lab Name: QUANTERRA MO Contract: 550.260<br />
Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275<br />
Matrix soil/water): SOIL Lab Sampie ID: 17224-003<br />
Level ;low/med): LOW Date Received: 03!16/98<br />
% Solids: 100.0<br />
Concentration Units (ug/L or mg/kg dry weight): MG//KG<br />
CAS No. Analyte<br />
7439-92-1 LeacT-<br />
7439-97-6 Mercury_<br />
Concentration C Q M<br />
_ I<br />
3.6 E P<br />
0.02 U jCV<br />
Clarity Before:<br />
Clarit y After:<br />
I_<br />
i<br />
i<br />
"excure:<br />
Art '_facts:<br />
J i i<br />
SW-^4F
Bechtel <strong>Hanford</strong>, Inc.<br />
3350 George Washington Way<br />
Richland, WA 99352<br />
April 21, 1998<br />
Attention: Joan Kessner<br />
SAF Number<br />
Date First Sample Received<br />
Date SDG Closed<br />
Number of Samples<br />
Sample Type<br />
SDG Number<br />
Data Deliverable<br />
CERTIFICATE OF ANALYSIS<br />
B98-061<br />
March 9, 1998<br />
March 16, 1998<br />
15<br />
Other-Cement<br />
W02275<br />
21 Day Summary<br />
°ivanterra<br />
Emironmrnra7<br />
sen'u es<br />
lc^ In ti<br />
I. Introduction<br />
Between March 9, and March 16, 1998, 15 21-day TAT other-cement samples were received<br />
by the Quanterra Environmental Se rvices Richland Laboratory (QESRL) for radiochemical and<br />
chemical analysis. Upon receipt, the samples were assigned the following laborato r y ID<br />
numbers to correspond with the Bechtel <strong>Hanford</strong>, Inc. (BHI) specific IDs:<br />
QESRL ID Ji BHI iD# YIATRI% DATE OF RECEIPT<br />
80316101 BON680 Soil 3/9/98<br />
80316102 BON681 Soil 3/9/98<br />
80318401 BON682 Soil 3/10/98<br />
80318402 BON683 Soil 3/10'98<br />
80318403 BON684 Soil 3/10/98<br />
80320601 BON685 Soil 3111198<br />
803 2 0602 BON686 Soil 3i 11.'98<br />
80320603 BON687 Soil 3x 11 "98<br />
80322201 BON688 Soil 3/12x98<br />
80312 1_02 BON689 Soil 3.12.'98<br />
80324401 BON690 Soil 3J13^98<br />
80324402 BON691 Soil 3; 1?x98<br />
80327201 BON692 Soil 3.16,98<br />
80327202 BON693 Soil 3, 16,98<br />
80327203 BON694 Soil 3116,98<br />
r1<br />
G0I)..
Bechtel <strong>Hanford</strong>, Inc.<br />
April 21, 1998<br />
Page 2<br />
II. Analytical Results/Methodology<br />
iivanterra<br />
EnOronmenral<br />
Souk ,<br />
The analytical results for this report are presented by laboratory sample ID. Each set of data<br />
includes sample identification information, analytical results and the appropriate associated<br />
statistical errors.<br />
The requested analyses were: Alpha Spectroscopy<br />
Americium-241 by method RICH-RC-5062<br />
Plutonium-238, -239/40 by method RICH-RC-5062<br />
Uranium-234, -235, -238 b_y method RICH-RC-5062<br />
Gamma Spectroscopy<br />
Gamma Scan by method RICH-RC-5017<br />
Gas Proportional Counting<br />
Total Strontium b y method RICH-RC-5006<br />
Liquid Scintillation Counting<br />
Carbon-14 by method RICH-RC-5022<br />
Nickel-63 by method RICH-RC-5069<br />
Selenium-79 by method RD-3253<br />
Technetium-99 by method RICH-RC-5029<br />
Chemical Analyses<br />
Chromium Hex by EPA method RICH-RC-5005<br />
III. Quality Control<br />
The analytical results for each analysis performed under SDG WO-2 -2 75 include a minimum of<br />
two Laboratory Control Samples (LCS) and one method (reagent) blank. Any exceptions have<br />
been noted in the "Comments" section_<br />
Quality control sample results are reported in the same units as sample results.<br />
(JO U.;
Bechtel <strong>Hanford</strong>, Inc.<br />
April 21, 1998<br />
Page 3<br />
IV. Comments<br />
Alpha Spectroscopy<br />
Q,P'uanterra<br />
Environmental<br />
Services<br />
Americium-241 by method RICH-RC-5062<br />
The LCS, batch blank, sample duplicate (BON680 and BON687) and sample results are within<br />
contractual requirements.<br />
Plutonium-238 -239/40 by method RICH-RC-5062<br />
The LCS, batch blank, sample duplicate (BON680 and BON687) and sample results are within<br />
contractual requirements.<br />
Uranium 234, -235 -238 by method RICH-RC-5062<br />
The LCS, batch blank, sample duplicate (BON680) and sample results are within contractual<br />
requirements. The RPD values for sample duplicate BON693 were slightly greater than the first<br />
level of evaluation criteria but the values met the second level evaluation criteria. Rich Weiss<br />
gave approval to report the data on 4/6/98.<br />
Gamma Spectroscopy<br />
Gamma Scan by method RICH-RC-5017<br />
The LCS, batch blank. sample duplicate (BON680 and BON685) and sample results are within<br />
contractual requirements_<br />
Gas Proportional Counting<br />
Total Strontium by method RICH-RC-5006<br />
The LCS, batch blank, sample duplicate (BON680 and BON690) and sample results are within<br />
contractual requirements.<br />
Liquid Scintillation Counting<br />
Carbon-14 by method RICH-RC-5022<br />
The LCS, batch blank, sample duplicate (BON680 and BON684) and sample results are within<br />
contractual requirements.<br />
Nickel-63 by method RICH-RC-5069<br />
The LCS. batch blank, sample duplicate (BON680 and BON688) and sample results are within<br />
contractual requirements.<br />
G0Oit
Bechtel <strong>Hanford</strong>, Inc.<br />
April 1-1, 1998<br />
Page 4<br />
^%%uanterra<br />
F.mironm
O<br />
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/9/1998 10:30:00 AM<br />
LAB SAMPLE ID: 80316101 REPORT NBR: 4835 RECEIVED DATE: 3/9/1998 1:42:00 PM<br />
CLIENT ID: BON680 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
COUNTING<br />
ERROR(2s)<br />
TOTAL ERROR<br />
(2s) MDA<br />
REPORT<br />
UNIT YIELD RST/MDA RST/CNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALQ<br />
UNIT<br />
DETECTOR<br />
ID<br />
METHOD<br />
NUMBER<br />
TC-99 -5.03E+02 1.5E+03 4.8E+03 3.63E+03 pCi/sam 95.10% -0.14 -0.33 4/2/98 0.000414 SA LSC RICHRC5078<br />
AM-241 6.72E+03 1.2E+03 1.7E+03 1.57E+02 pCi/sam 74-90% (429) (5.4) 4/3/98 0.000368 SA ALPHA-SPEC RICHRC5057<br />
HEXCHROME 4.00E-03 00E+00 0.0E+00 200E-03 mg/L N/A (2.) N/A 3/10/98 100.0 ML SPECPHOTO EPA7196<br />
U-234 8.61E+01 1.0E+02 1.0E+02 1.19E+02 pCi/sam 80.30% 0.73 0.84 4/3/98 0000376 SA ALPHA-SPEC RICHRC5030<br />
U-235 0.00E+00 0.0E+00 8.8E+01 7.98E+01 pCdsam 80.30% 0 N/A 4/3/98 0.000376 SA ALPHA-SPEC RICHRC5030<br />
U-238 8.37E+01 1.0E+02 1.0E+02 1.35E+02 pCi/sam 80.30% 0.62 0.82 4/3/98 0.000376 SA ALPHA-SPEC RICHRC5030<br />
PU-238 5.26E+02 2.4E+02 2.SE+02 7.49E+01 pCi/sam 62.20% (7) (2.2) 3/31/98 0000368 SA ALPHA-SPEC RICHRC5010<br />
PU239/40 1.82E+04 1.4E+03 2.8E+03 1.26E+02 pCi/sam 62.20% (143.6) (12.8) 3131/98 0.000368 SA ALPHA-SPEC RICHRCS010<br />
AM-241 6.78E+03 1.0E+03 1.2E+03 N/A pCi/sam N/A N/A (6.6) 3/26/98 0.2355 SA GAMMA RICHRC5017<br />
CO-60 4.21E+04 7.SE+02 4.3E+03 N/A pCi/sam N/A N/A (56.3) 3/26/98 0.2355 SA GAMMA RICHRC5017<br />
CS-137DA 1.49E+06 4.9E+03 1.5E+05 N/A pCi/sam N/A N/A (305.4) 3/26/98 0.2355 SA GAMMA RICHRC5017<br />
EU-152 4.14E+04 2.0E+03 4.6E+03 N/A pCi/sam N/A N/A (21.) 3/26/98 0.2355 SA GAMMA RICHRC5017<br />
EU-154 5.81E+03 8.0E+02 9.9E+02 N/A pCi/sam N/A N/A (7.2) 3/26/98 0.2355 SA GAMMA RICHRC5017<br />
EU-155 -1.37E+02 6.9E+02 6.9E+02 1.06E+03 pCi/sam N/A -0.13 -0.2 3/26/98 0.2355 SA GAMMA RICHRC5017<br />
STRONTIUM 4.67E+05 1.0E+04 1.7E+05 1.79E+03 pCi/sam 97.00% (260.4) (46.8) 4/1/98 0000367 SA AS RICHRC5006<br />
C-14 1.90E+02 1.0E+03 1.6E+03 2.40E+03 pCi/sam 100.00% 0.08 0.19 4/9/98 0.00064 SA LSC RICHRC5022<br />
NI-63 4.16E+06 2.1E+04 5.0E+05 4.48E+03 pCi/sam 76.70% (928.9) (1969) . 4/3/98 0.000367 SA LSC RICHRC5069<br />
O SE-79 2.01E+03 2.0E+03 7.3E+03 4.60E+03 pCi/sam 71.50% 0.44 (1.) 4/1/98 0.000372 SA LSC RICHRC5043<br />
C.<br />
Number of Results: '18<br />
Comments:
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/9/1998 1.45:00 PM<br />
LAB SAMPLE ID: 80316102 REPORT NBR: 4835 RECEIVED DATE: 3/9/1998 1:42:00 PM<br />
CLIENT ID: BON681 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
COUNTING<br />
ERROR(2s)<br />
TOTAL ERROR<br />
(2 s) MDA<br />
REPORT<br />
UNIT YIELD RST/MDA RSTICNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALQ<br />
UNIT<br />
DETECTOR<br />
ID<br />
METHOD<br />
NUMBER<br />
TC-99 352E+00 1.4E+01 42E+01 323E+01 pCi/sam 95.10% -0.11 -0.26 3/31/98 0.0458 SA LSC RtCHRCS078<br />
AM-241 319E+00 2-3E+00 2.3E+00 1.08E+00 pCi/sam 87.10% (3) (14) 4/4/98 0.046 SA ALPHA-SPEC RICHRC5057<br />
HEXCHROME 2.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3/10/98 100.0 ML SPECPHOTO EPA7196<br />
U-234 159E+02 2.5E+01 5.4E+01 4.10E+00 pCi/sam 19.80% (38.8) (6.2) 4/5/98 0.044 SA ALPHA-SPEC RICHRC5030<br />
U-235 8.15E+00 5.8E+00 6.3E+00 2.76E+00 pCi/sam 19.80% (3.) (1.4) 4/5/98 0.044 SA ALPHA-SPEC RICHRCS030<br />
U-238 1.83E+02 2.7E+01 6.2E+01 4.66E+00 pCi/sam 19.80% (39.4) (6.7) 4/5/98 0.044 SA ALPHA-SPEC RICHRC5030<br />
PU-238 0.00E+00 00E+00 5.2E-01 4.65E-01 pCi/sam 77.40% 0. N/A 4/3/98 0.046 SA ALPHA-SPEC RICHRC5010<br />
PU239/40 3.92E+00 1.6E+00 1.7E+00 7.84E-01 pCi/sam 77.40% (5.) (2.4) 4/3/98 0.046 SA ALPHA-SPEC RICHRC5010<br />
CO-60 4.22E+01 2.7E+01 2.8E+01 5.77E+01 pCi/sam N/A 0.73 (1.5) 3/27/98 0.0541 SA GAMMA RICHRCS017<br />
CS-137DA 4.95E+02 7.2E+01 8.7E+01 N/A pCi/sam N/A N/A (6.9) 3/27/98 0.0541 SA GAMMA RICHRCS017<br />
EU-152 1.87E+01 89E+01 8.9E+01 148E+02 pCi/sam N/A 0.13 0.21 3/27/98 0.0541 SA GAMMA RICHRC5017<br />
EU-154 1.14E+02 9.0E+01 91E+01 1.75E+02 pCi/sam N/A 0.65 (13) 3/27/98 0.0541 SA GAMMA RICHRCS017<br />
EU-155 -3.69E+01 65E+01 6.5E+01 101E+02 pCi/sam N/A -0.37 -0.57 3/27/98 0.0541 SA GAMMA RICHRCS017<br />
STRONTIUM 6.20E+02 3.2E+01 2.2E+02 1.34E+01 pCi/sam 9880% (46.3) (19.5) 4/2198 0.0476 SA AB RICHRC5006<br />
C-14 8.68E+00 1 4E+01 2.2E+01 3.30E+01 pCi/sam 10000% 0.26 061 4/2/98 0.0467 SA LSC RICHRC5022<br />
NI-63 4.47E+02 2.1E+01 8.1E+01 2.74E+01 pCi/sam 9930% (16.3) (21.6) 4/5/98 0.0458 SA LSC RICHRC5069<br />
SE-79 -5.63E+00 1.5E+01 5.6E+01 3.72E+01 pCi/sam 70.40% -0.15 -0.36 4/13/98 00464 SA LSC RICHRC5043<br />
C<br />
[Number of Results: 17<br />
C^<br />
Comments:
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/10/1998 8:35:00 AM<br />
LAB SAMPLE ID: 80318401 REPORT NBR: 4835 RECEIVED DATE: 3/10/1998 1:05:00 PM<br />
CLIENT ID: BON682 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
TC-99 -2.99E+01<br />
AM-241 4.68E+00<br />
HEXCHROME 2.00E-03<br />
U-234 2.85E+01<br />
U-235 4.09E-01<br />
U-238 3.68E+01<br />
PU-238 0.00E+00<br />
PU239/40 2.37E+00<br />
CO-60 -2.12E+01<br />
CS-137DA 3.28E+02<br />
EU-152 -1.29E+01<br />
EU-154 -4.98E+01<br />
EU-155 1.26E+01<br />
STRONTIUM 7.92E+01<br />
C-14 3.73E+01<br />
NI-63 2.42E+02<br />
SE-79 -1.33E+01<br />
dumber of Results: '17<br />
G<br />
Cl)<br />
Comments:<br />
COUNTING TOTAL ERROR<br />
ERROR(2s) (2 s)<br />
3.0E+01 9.3E+01<br />
4.3E+00 4.3E+00<br />
0.0E+00 0.0E+00<br />
8.3E+00 9.9E+00<br />
1.2E+00 1.2E+00<br />
9.5E+00 1.2E+01<br />
0 0E+00 1 2E+00<br />
2.0E+00 2.0E+00<br />
3.9E+01 3.9E+01<br />
6.5E+01 7.3E+01<br />
9 0E+01 9.0E+01<br />
1.2E+02 1 2E+02<br />
8.4E+01 8.4E+01<br />
2.1E+01 3.6E+01<br />
3 3E+01 5.1E+01<br />
3.2E+01 1.0E+02<br />
3.7E+01 1.3E+02<br />
REPORT<br />
MDA UNIT YIELD<br />
6.98E+01 pCi/sam 95.10%<br />
3.83E+00 pCi/sam 81.70%<br />
2.00E-03 mg/L N/A<br />
4.01 E+00 pCi/sam 56.60%<br />
3.21E+00 pCi/sam 56.60%<br />
4.14E+00 pCi/sam 56.60%<br />
1.10E+00 pCi/sam 74.40%<br />
1.85E+00 pCi/sam 74.40%<br />
6.47E+01 pCi/sam N/A<br />
N/A pCi/sam N/A<br />
1 .51E+02 pCi/sam N/A<br />
1.96E+02 pCi/sam N/A<br />
1.39E+02 pCi/sam N/A<br />
3.35E+01 pCi/sam 94.50%<br />
7.60E+01 pCi/sam 100.00%<br />
6.16E+01 pCi/sam 95.20%<br />
8.78E+01 pCi/sam 75.40%<br />
RSTIMDA RST/CNTERR<br />
-043 -(1-)<br />
(1.2) (1 1)<br />
1 N/A<br />
(7.1) (3.4)<br />
0.13 0.34<br />
(8.9) (3.9)<br />
0 N/A<br />
(1-3)<br />
(1.2)<br />
-033 -0.54<br />
N/A (5.)<br />
-009 -014<br />
-025 -0.42<br />
009 0.15<br />
(2A) (38)<br />
049 (L1)<br />
(39) (Z5)<br />
-0.15 -0.37<br />
ANALYSIS ALIQUOT ALQ DETECTOR METHOD<br />
DATE SIZE UNIT ID NUMBER<br />
3/31/98 0.0206 SA LSC RICHRC5078<br />
4/4/98 0.021 SA ALPHA-SPEC RICHRCS057<br />
3/11/98 1000 ML SPECPHOTO EPA7196<br />
4/4/98 0.0243 SA ALPHA-SPEC RICHRC5030<br />
4/4/98 0.0243 SA ALPHA-SPEC RICHRCS030<br />
4/4/98 0.0243 SA ALPHA-SPEC RICHRC5030<br />
4/3/98 0021 SA ALPHA-SPEC RICH RC5010<br />
4/3/98 0.021 SA ALPHA-SPEC RICHRC5010<br />
3/27/98 0.0537 SA GAMMA RICHRC5017<br />
3/27/98 0.0537 SA GAMMA RICHRC5017<br />
3/27/98 0.0537 SA GAMMA RICHRC5017<br />
3/27/98 0.0537 SA GAMMA RICHRC5017<br />
3/27/98 0.0537 SA GAMMA RICHRC5017<br />
4/2/98 0.0208 SA AB RICHRC5006<br />
4/2198 0.0204 SA LSC RICHRC5022<br />
4/5/98 0.0212 SA LSC RICHRC5069<br />
4/13/98 0.0183 SA LSC RICHRC5043
ISOTOPE<br />
TC-99<br />
AM 241<br />
U-234<br />
U-235<br />
U-238<br />
PU-238<br />
PU239/40<br />
AM-241<br />
CO-60<br />
CS-137DA<br />
EU-152<br />
EU-154<br />
EU-155<br />
STRONTIUM<br />
C-14<br />
NI-63<br />
SE-79<br />
Qlumber of Results<br />
G<br />
Comments<br />
RESULT<br />
-1.14E+03<br />
2 94E+03<br />
9 18E+01<br />
0 00E+00<br />
4 30E+01<br />
8 36E+01<br />
5.23E+03<br />
2 84E+03<br />
8.29E+03<br />
1 28E+06<br />
1 57E+04<br />
2 42E+03<br />
4 15E+02<br />
6 71 E+05<br />
7 01 E+02<br />
4.05E+05<br />
1.16E+03<br />
117<br />
FORM Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/10/1998 9:45:00 AM<br />
LAB SAMPLE ID: 80318402 REPORT NBR: 4835 RECEIVED DATE: 3/10/1998 1:05:00 PM<br />
CLIENT ID: BON683 ORDER NBR: B98-061 MATRIX OTHER<br />
COUNTING TOTAL ERROR<br />
ERROR(2s) (2s)<br />
1.8E+03 5.8E+03<br />
7.3E+02 8.5E+02<br />
9.8E+01 9.9E+01<br />
0.0E+00 7.3E+01<br />
6.9E+01 7.0E+01<br />
9.7E+01 9.7E+01<br />
7 6E+02 1.0E+03<br />
5.4E+02 6.1 E+02<br />
3.7E+02 9.1 E+02<br />
2.3E+03 1.3E+05<br />
2.1E+03 2.6E+03<br />
4.6E+02 5.2E+02<br />
7.1 E+02 7.1 E+02<br />
1.2E+04 2.5E+05<br />
1 1E+03 1 7E+03<br />
6.7E+03 5.2E+04<br />
1.9E+03 6.9E+03<br />
REPORT<br />
MDA UNIT YIELD<br />
4.39E+03 pCi/sam 95.10%<br />
1.23E+02 pCi/sam 98.10%<br />
1 22E+02 pCi/sam 92.90%<br />
6.61 E+01 pCi/sam 92.90%<br />
1.22E+02 pCi/sam 92.90%<br />
7 54E+01 pCi/sam 61.80%<br />
1.27E+02 pCi/sam 61.80%<br />
N/A pCi/sam N/A<br />
N/A pCi/sam N/A<br />
N/A pCi/sam N/A<br />
N/A pCi/sam N/A<br />
9.24E+02 pCi/sam N/A<br />
1.18E+03 pCi/sam N/A<br />
2.12E+03 pCi/sam 97.20%<br />
2 49E+03 pCi/sam 10000%<br />
4.29E+03 pCi/sam 8200%<br />
4.35E+03 pCi/sam 78.60%<br />
RST/MDA RST/CNTERR<br />
-0.26 -0.62<br />
(24-) (4)<br />
075 094<br />
0. N/A<br />
0.35 0.62<br />
(1.1) 087<br />
(41.1) (6.8)<br />
N/A (5.2)<br />
N/A (22.4)<br />
N/A (564.8)<br />
N/A (7S)<br />
(2.6) (5.3)<br />
0.35 0.58<br />
(3159) (54.2)<br />
0.28 065<br />
(94.6) (60.7)<br />
0.27 0.62<br />
ANALYSIS<br />
DATE<br />
4/2/98<br />
4/3/98<br />
4/3/98<br />
4/3/98<br />
4/3/98<br />
3/31/98<br />
3/31/98<br />
3/26/98<br />
3/26/98<br />
3/26/98<br />
3/26/98<br />
3/26/98<br />
3/26/98<br />
4/1/98<br />
4/9/98<br />
4/3/98<br />
4/1/98<br />
ALIQUOT ALQ<br />
SIZE UNIT<br />
0.000342 SA<br />
0.000355 SA<br />
0.00037 SA<br />
0.00037 SA<br />
0.00037 SA<br />
0.000355 SA<br />
0.000355 SA<br />
0.229 SA<br />
0.229 SA<br />
0.229 SA<br />
0.229 SA<br />
0.229 SA<br />
0 229 SA<br />
0.000349 SA<br />
0.000617 SA<br />
0.000359 SA<br />
0.000357 SA<br />
DETECTOR<br />
ID<br />
LSC<br />
ALPHA-SPEC<br />
ALPHA-SPEC<br />
ALPHA-SPEC<br />
ALPHA-SPEC<br />
ALPHA-SPEC<br />
ALPHA-SPEC<br />
GAMMA<br />
GAMMA<br />
GAMMA<br />
GAMMA<br />
GAMMA<br />
GAMMA<br />
AB<br />
LSC<br />
LSC<br />
LSC<br />
METHOD<br />
NUMBER<br />
RICHRCS078<br />
RICHRC5057<br />
RICHRC5030<br />
RICHRC5030<br />
RICHRC5030<br />
R ICHRCS010<br />
RICHRC5010<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRC5006<br />
RICHRC5022<br />
RICHRC5069<br />
RICHRC5043
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/10/1998 1:20:00 PM<br />
LAB SAMPLE ID: 80318403 REPORT NBR: 4835 RECEIVED DATE: 3/10/1998 1:05:00 PM<br />
CLIENT ID: BON684 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
COUNTING<br />
ERROR (2 s)<br />
TOTAL ERROR<br />
(2 s) MDA<br />
REPORT<br />
UNIT YIELD RSTIMDA RST/CNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALQ<br />
UNIT<br />
DETECTOR<br />
ID<br />
METHOD<br />
NUMBER<br />
TC-99 -1.93E+01 2.9E+01 90E+01 6.91E+01 pCi/sam 95.10% -0.28 -0.67 3/31/98 0.0214 SA LSC RICHRC5078<br />
AM-241 301E+00 31E+00 3.1E+00 3.09E+00 pCi/sam 92.60% 0.97 098 4/4/98 0.0219 SA ALPHA-SPEC RICHRC5057<br />
HEXCHROME 2.00E-03 00E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3/11/98 100.0 ML SPECPHOTO EPA7196<br />
U-234 4.07E+01 98E+00 1 2E+01 2.37E+00 pCi/sam 63.30% (17.1) (4.1) 4/4/98 0.0226 SA ALPHA-SPEC RICHRC5030<br />
U-235 3.45E+00 2.9E+00 3.0E+00 2.70E+00 pCi/sam 63.30% (1.3) (1.2) 4/4/98 0.0226 SA ALPHA-SPEC RICHRCS030<br />
U-238 3.57E+01 9.2E+00 1.1E+01 3.50E+00 pCi/sam 63 30% (10.2) (3.9) 4/4/98 0.0226 SA ALPHA-SPEC RICHRCS030<br />
PU-238 0.00E+00 0.0E+00 1.1E+00 9.66E-01 pCi/sam 76.10% 0. N/A 4/3/98 0.0219 SA ALPHA-SPEC RICHRC5010<br />
PU239/40 1.28E+01 4.3E+00 4.6E+00 1.44E+00 pCi/sam 76 1 0% (8.9) (3.) 4/3/98 0.0219 SA ALPHA-SPEC RICHRC5010<br />
CO-60 -1.94E+01 4.5E+01 4.5E+01 7.58E+01 pCi/sam N/A -0.26 -0.43 3/27/98 0.05 SA GAMMA RICHRC5017<br />
CS-137DA 1.37E+03 1.2E+02 1.8E+02 N/A pCi/sam N/A N/A (11.6) 3/27/98 005 SA GAMMA RICHRC5017<br />
EU-152 -3.76E+01 9.4E+01 9.4E+01 155E+02 pCi/sam N/A -0.24 -0.4 3/27/98 0.05 SA GAMMA RICHRC5017<br />
EU-154 1.52E+01 11E+02 1.1E+02 197E+02 pCi/sam N/A 0.08 0.13 3/27/98 0.05 SA GAMMA RICHRC5017<br />
EU-155 6.76E+01 80E+01 8.0E+01 1.31E+02 pCi/sam N/A 0.52 0.85 3/27/98 0.05 SA GAMMA RICHRC5017<br />
STRONTIUM 1.30E+03 7.1E+01 4.3E+02 3.26E+01 pCi/sam 87.40% (40) (18.4) 4/2/98 0.0218 SA AB RICHRC5006<br />
C-14 -2.42E+00 2.9E+01 4.6E+01 7.00E+01 pCi/sam 100.00% -0.03 -008 4/2/98 0.0223 SA LSC RICHRC5022<br />
NI-63 2.47E+02 3.1E+01 9.8E+01 593E+01 pCi/sam 94.30% (4.2) (7.9) 415/98 0.0223 SA LSC RICHRCS069<br />
SE-79 3.29E-01 3.1E+01 1.1E+02 7.38E+01 pCi/sam 73.70% 0. 0.01 4/13198 0.0223 SA LSC RICHRC5043<br />
C-)<br />
(_Number of Resu lts: 117<br />
^t<br />
C-e<br />
Comments:
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/11/1998 8:30:00 AM<br />
LAB SAMPLE ID: 80320601 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11:57:00 AM<br />
CLIENT ID: BON685 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
COUNTING<br />
ERROR(2s)<br />
TOTAL ERROR<br />
(2 s) MDA<br />
REPORT<br />
UNIT YIELD RST/MDA RST/CNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALQ<br />
UNIT<br />
DETECTOR<br />
ID<br />
METHOD<br />
NUMBER<br />
TC-99 -801E+00 2.9E+01 9.1E+01 6.98E+01 pCi/sam 95.10% -0.11 -0.27 3/31/98 0.0213 SA LSC RICHRC5078<br />
AM-241 3.65E+00 3.6E+00 3.7E+00 2.47E+00 pCi/sam 83.00% (1.5) 0 ) 4/4/98 00207 SA ALPHA-SPEC RICHRCS057<br />
HEXCHROME 2.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3/12/98 100.0 ML SPECPHOTO EPA7196<br />
U-234 3.50E+01 8.7E+00 1.1E+01 1.46E+00 pCi/sam 58.10% (24.) (4) 4/5/98 0.0257 SA ALPHA-SPEC RICHRC5030<br />
U-235 4.27E+00 3.1E+00 3.1E+00 2.17E+00 pCi/sam 58.10% (2.) (1.4) 4/5/98 0.0257 SA ALPHA-SPEC RICHRCS030<br />
U-238 5.12E+01 1.1E+01 1.4E+01 2.17E+00 pCi/sam 58.10% (23.6) (49) 4/5/98 0.0257 SA ALPHA-SPEC RICHRC5030<br />
PU-238 3.65E-01 8.0E-01 8.0E-01 1.59E+00 pCi/sam 80.20% 0.23 0.46 413/98 0.0207 SA ALPHA-SPEC RICHRC5010<br />
PU239/40 4.36E+00 2.6E+00 2.7E+00 1.07E+00 pCi/sam 80.20% (4.1) (1.7) 4/3/98 0.0207 SA ALPHA-SPEC RICHRCS010<br />
CO-60 5.67E+01 3.4E+01 3.4E+01 6.81E+01 pCi/sam N/A 0.83 (1.7) 3/27/98 0.0504 SA GAMMA RICHRC5017<br />
CS-137DA 2.82E+02 66E+01 7.2E+01 NIA PCs/Sam N/A N/A (43) 3127/98 00504 SA GAMMA RICHRC5017<br />
EU-152 6.01E+00 87E+01 87E+01 1.46E+02 pCi/sam N/A 0.04 0.07 3/27/98 0.0504 SA GAMMA RICHRC5017<br />
EU-154 689E+01 1.0E+02 1.0E+02 1.98E+02 pCi/sam N/A 0.35 0.66 3/27/98 00504 SA GAMMA RICHRC5017<br />
EU-155 3.04E+01 7.6E+01 7.6E+01 1.20E+02 pCi/sam N/A 0.25 0.4 3/27/98 0.0504 SA GAMMA RICHRC5017<br />
K-40 1.49E+03 12E+03 1.2E+03 NIA pCi/sam N/A N/A (1.2) 3/27/98 0.0504 SA GAMMA RICHRC5017<br />
STRONTIUM 4.78E+01 1.7E+01 2.3E+01 2.99E+01 pCi/sam 88.20% (1.6) (2.8) 4/2/98 0.0211 SA AB RICHRCS006<br />
C<br />
C-14 2.95E+01 3.3E+01 5.1E+01 7.60E+01 pCi/sam 100.00% 0.39 0.89 412198 0.0203 SA LSC RICHRC5022<br />
O NI-63 -303E-01 29E+01 89E+01 7.01E+01 pCi/sam 85.70% 0 -0.01 415/98 0.0208 SA LSC RICHRC5069<br />
F-^<br />
5E-79 -117E01 3.3E*01 1.2E+02 7.94E+ 01 pCi/sam 73.50% -0.15 -0.35 4/13/98 0.0207 SA LSC RICHRC5043<br />
Number of Results: 18<br />
Comments:
ISOTOPE RESULT<br />
TC-99 1 13E+02<br />
AM-241 3 74E+03<br />
U-234 7 12E+01<br />
U-235 5 94E+00<br />
U-238 2 27E+01<br />
PU-238 4 97E+02<br />
PU239/40 1 34E+04<br />
AM-241 3 72E+03<br />
CO-60 8.22E+03<br />
CS-137DA 1.36E+06<br />
EU-152 9 35E+03<br />
E U-154 1 85E+03<br />
E U-155 -1 56E+01<br />
STRONTIUM 4 33E+05<br />
C-14 6.59E+02<br />
NI-63 2.76E+05<br />
c1<br />
^ SE-79 7.68E+02<br />
~lumber of Results: '17<br />
Comments:<br />
COUNTING TOTAL ERROR<br />
ERROR(2s) (2 s)<br />
10E+03 3.2E+03<br />
5.3E+02 7.7E+02<br />
6.6E+01 6.8E+01<br />
2.8E+01 2.8E+01<br />
3 8E+01 3.9E+01<br />
1.6E+02 1.7E+02<br />
8.2E+02 1.9E+03<br />
2.5E+03 2.5E+03<br />
2.7E+02 8.6E+02<br />
1.4E+05 1.4E+05<br />
1 SE+03 1.7E+03<br />
3.8E+02 4.2E+02<br />
7.7E+02 7.7E+02<br />
6.3E+03 1.6E+0S<br />
5 9E+02 9.1 E+02<br />
3.7E+03 3.5E+04<br />
7.8E+02 2.9E+03<br />
FORM Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/11/1998 10:00:00 AM<br />
LAB SAMPLE ID: 80320602 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11:57:00 AM<br />
CLIENT ID: BON686 ORDER NBR: B98-061 MATRIX: OTHER<br />
MDA<br />
REPORT<br />
UNIT YIELD RST/MDA RST/CNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALQ<br />
UNIT<br />
DETECTOR<br />
ID<br />
2.40E+03 pCi/sam 95.10% 005 0.11 4/2/98 0.000626 SA LSC<br />
5.14E+01 pCi/sam 105.50% (72.8) (7.) 4/3/98 0.000836 SA ALPHA-SPEC<br />
898E+01 pCi/sam 73.10% 0.79 (1.1) 4/4/98 0.000839 SA ALPHA-SPEC<br />
8.35E+01 pCi/sam 73.10% 007 0.22 4/4/98 0.000839 SA ALPHA-SPEC<br />
7 20E+01 pCi/sam 73.10% 0.31 0.59 4/4/98 0.000839 SA ALPHA-SPEC<br />
5.00E+01 pCi/sam 6330% (9.9) (3.2) 3/31/98 0.000836 SA ALPHA-SPEC<br />
3.36E+01 pCi/sam 63.30% (398.7) (16.4) 3/31/98 0.000836 SA ALPHA-SPEC<br />
N/A pCilsam N/A N/A (1.5) 3/26/98 0.4107 SA GAMMA<br />
N/A pCi/sam N/A N/A (30.9) 3/26/98 0.4107 SA GAMMA<br />
N/A pCi/sam N/A N/A (10.) 3/26/98 0.4107 SA GAMMA<br />
N/A pCi/sam N/A N/A (6.4) 3/26/98 04107 SA GAMMA<br />
N/A pCi/sam N/A N/A (4.9) 3/26/98 0.4107 SA GAMMA<br />
1.25E+03 pCi/sam N/A -0.01 -0.02 3/26/98 0.4107 SA GAMMA<br />
8.16E+02 pCi/sam 99.90% (530.) (68.5) 4/1/98 0-000837 SA AB<br />
1.34E+03 pCi/sam 100.00% 0.49 (1 1) 4/9/98 0.001142 SA LSC<br />
2.00E+03 pCi/sam 76.00% (138.3) (74.3) 4/3/98 0.000831 SA LSC<br />
1.80E+03 pCi/sam 79.50% 043 0.99 4/1/98 0.00085 SA LSC<br />
METHOD<br />
NUMBER<br />
RICHRC5078<br />
RICHRC5057<br />
RICHRC5030<br />
RICHRCS030<br />
RICHRC5030<br />
RICHRCS010<br />
RICHRC5010<br />
RICHRC5017<br />
RICHRCS017<br />
RICHRCS017<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRCSW6<br />
RICHRC5022<br />
RICHRC5069<br />
RICHRC5043
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/11/1998 1:05:00 PM<br />
LAB SAMPLE ID: 80320603 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11'.57.00 AM<br />
CLIENT ID: BON687 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
COUNTING<br />
ERROR(2s)<br />
TOTAL ERROR<br />
(2s) MDA<br />
REPORT<br />
UNIT YIELD RSTIMDA RST/CNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALO<br />
UNIT<br />
DETECTOR<br />
ID<br />
METHOD<br />
NUMBER<br />
TC-99 -9.47E+00 2.5E+01 7.9E+01 6.04E+01 pCi/sam 95.10% -0.16 -0.37 3/31/98 0.0245 SA LSC RICHRCS078<br />
AM-241 3.43E+00 3.1E+00 3.1E+00 186E+00 pCi/sam 93.80% (1.8) (1.1) 4/4/98 0.0245 SA ALPHA-SPEC RICHRCS057<br />
HEXCHROME 3.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A (1.5) N/A 3/12/98 1000 ML SPECPHOTO EPA7196<br />
U-234 4.23E+01 1.1E+01 1.4E+01 282E+00 pCilsam 47.30% (16.1) (4.) 4/4/98 0.0272 SA ALPHA-SPEC RICHRCS030<br />
U-235 6.00E-01 1.3E+00 1.3E+00 2.62E+00 pCi/sam 47.30% 0.23 0.46 4/4/98 00272 SA ALPHA-SPEC RICHRC5030<br />
U-238 4.88E+01 1.1E+01 1.5E+01 2.98E+00 pCi/sam 47.30% (16.4) (4.3) 4/4/98 0.0272 SA ALPHA-SPEC RICHRC5030<br />
PU-238 8.22E-01 1.3E+00 1.3E+00 2.04E+00 pCi/sam 58.70% 0.4 0.65 4/3198 0.0255 SA ALPHA-SPEC RICHRCS010<br />
PU239/40 7.04E+00 3.6E+00 3.7E+00 2.23E+00 pCi/sam 58.70% (3.2) (2.) 4/3/98 0.0255 SA ALPHA-SPEC RICHRC5010<br />
CO-60 6.12E+00 3.9E+01 3.9E+01 6.99E+01 pCilsam N/A 0.09 0.16 3/27/98 0.0517 SA GAMMA RICHRC5017<br />
CS-137DA 1.48E+03 9.8E+01 1.8E+02 N/A pCilsam N/A N/A (151) 3/27/98 0.0517 SA GAMMA RICHRCS017<br />
EU-152 403E+01 9.2E+01 9.2E+01 1.59E+02 pCi/sam N/A 0.25 0.44 3/27/98 0.0517 SA GAMMA RICHRC5017<br />
EU-154 -4 46E+01 1.1E+02 1.1E+02 179E+02 pCi/sam N/A -0.25 -0.41 3/27/98 0.0517 SA GAMMA RICHRC5017<br />
EU-155 -1.89E+01 7.4E+01 7.4E+01 1 15E+02 pCi/sam N/A -0.16 -0.26 3/27/98 0.0517 SA GAMMA RICHRC5017<br />
K-40 1.91E+03 1.1E+03 1.1E+03 N/A pCi/sam N/A N/A (1.8) 3/27/98 0.0517 SA GAMMA RICHRC5017<br />
STRONTIUM 6.79E+02 5.1E+01 2.5E+02 3.46E+01 pCi/sam 86.30% (19.6) (13.3) 4/2/98 0.0241 SA AB RICHRC5006<br />
C-14 9.21E+01 3.0E+01 4.5E+01 6.40E+01 pCi/sam 100.00% (1.4) (3.1) 4098 00243 SA LSC RICHRC5022<br />
NI-63 1.60E+02 2.6E+01 8.0E+01 5.20E+01 pCi/sam 93.70% (3.1) (6.1) 4/5/98 0.0255 SA LSC RICHRCS069<br />
Fes+<br />
SE-79 8.50E-01 2.7E+01 97E+01 6.33E+01 pCi/sam 74.30% 0.01 0.03 4/13/98 0.0257 SA LSC RICHRC5043<br />
C.) Number of Results: 18<br />
Comments:
FORM Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/12/1998 9:15:00 AM<br />
LAB SAMPLE ID: 80322201 REPORT NBR: 4835 RECEIVED DATE: 3/12/1998 1:53:00 PM<br />
CLIENT ID: BON688 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
TC-99 -3.92E+00<br />
AM-241 1 42E+00<br />
HEXCHROME 2.00E-03<br />
U-234 3.81E+01<br />
U-235 1.44E+00<br />
U-238 4.34E+01<br />
PU-238 -5.63E-02<br />
PU239/40 1.06E+00<br />
CO-60 5.23E+01<br />
CS-137UA 6.18E+02<br />
EU-152 1 68E+01<br />
EU-154 -1.14E+01<br />
EU-155 2.57E+01<br />
K-40 5.80E+03<br />
STRONTIUM 2.08E+02<br />
C-14 2.28E+01<br />
c-) NI-63 7.60E+01<br />
C SE-79 -1.37E+00<br />
h-^<br />
"Number of Resu lts: 118<br />
Comments:<br />
COUNTING TOTAL ERROR<br />
ERROR(2s) (2 s)<br />
2.5E+01 7.7E+01<br />
2.1E+00 2.1 E+00<br />
0.0E+00 0.0E+00<br />
9.4E+00 1.2E+01<br />
2.0E+00 2.0E+00<br />
1 0E+01 1.3E+01<br />
8.0E-02 8.0E-02<br />
1.2E+00 1.2E+00<br />
3.6E+01 3.6E+01<br />
8.0E+01 1.0E+02<br />
86E+01 86E+01<br />
1.1E+02 1.1E+02<br />
7.5E+01 7.5E+01<br />
7.6E+02 9.6E+02<br />
3.1 E+01 7 5E+01<br />
2.6E+01 4.1E+01<br />
2.3E+01 7.1 E+01<br />
2 6E+01 9.4E+01<br />
REPORT<br />
MDA UNIT YIELD<br />
5.82E+01 pCi/sam 95.10%<br />
2.97E+00 pCi/sam 86.60%<br />
2.00E-03 mg/L N/A<br />
3.39E+00 pCi/sam 5480%<br />
3.39E+00 pCi/sam 54.80%<br />
2.61E+00 pCi/sam 54.80%<br />
1.61 E+00 pCi/sam 72.60%<br />
9.52E-01 pCi/sam 72.60%<br />
7.23E+01 pCi/sam N/A<br />
N/A pCi/sam N/A<br />
1.43E+02 pCi/sam N/A<br />
1.87E+02 pCi/sam N/A<br />
1.20E+02 pCi/sam N/A<br />
172E+03 pCi/sam N/A<br />
3.47E+01 pCi/sam 73.80%<br />
6.00E+01 pCi/sam 100.00%<br />
5.05E+01 pCUsam 95.10%<br />
6.14E+01 pCi/sam 76.70%<br />
RST/MDA RST/CNTERR<br />
-007 -016<br />
048 0.68<br />
1- N/A<br />
(11 2) (41)<br />
0.42 0.72<br />
(168) (4.3)<br />
-0.04 -0.71<br />
(i.t) 087<br />
072 (1 5)<br />
N/A (77)<br />
0.12 02<br />
-006 -01<br />
0.21 034<br />
(3.4) (7.6)<br />
(6.) (6-8)<br />
0.38 087<br />
(1.5) (33)<br />
-0.02 -005<br />
ANALYSIS<br />
DATE<br />
3131/98<br />
4/4/98<br />
3/13/98<br />
4/4/98<br />
4/4/98<br />
4/4/98<br />
4/3/98<br />
4/3/98<br />
3/27/98<br />
3/27/98<br />
3/27/98<br />
3/27/98<br />
3/27/98<br />
3/27/98<br />
4/2/98<br />
4/2/98<br />
4/5/98<br />
4/13/98<br />
ALIQUOT ALQ<br />
SIZE UNIT<br />
00254 SA<br />
00255 SA<br />
100.0 ML<br />
0.0264 SA<br />
0.0264 SA<br />
0.0264 SA<br />
0.0255 SA<br />
0.0255 SA<br />
0.0507 SA<br />
00507 SA<br />
0.0507 SA<br />
00507 SA<br />
0.0507 SA<br />
0.0507 SA<br />
0.0254 SA<br />
0.0257 SA<br />
0.0259 SA<br />
00257 SA<br />
DETECTOR<br />
ID<br />
LSC<br />
ALPHA-SPEC<br />
SPECPHOTO<br />
ALPHA-SPEC<br />
ALPHA-SPEC<br />
ALPHA-SPEC<br />
ALPHA-SPEC<br />
ALPHA-SPEC<br />
GAMMA<br />
GAMMA<br />
eIDLllr_1<br />
CeL1S11ra<br />
GAMMA<br />
GAMMA<br />
AB<br />
LSC<br />
LSC<br />
LSC<br />
METHOD<br />
NUMBER<br />
RICHRCS078<br />
RICHRCS057<br />
EPA7196<br />
RICHRCS030<br />
RICHRCS030<br />
RICHRC5030<br />
RICHRCS010<br />
RICHRCS010<br />
RICHRCS017<br />
RICHRCS017<br />
RICHRC5017<br />
RICHRC S017<br />
RICHRC5017<br />
RICHRCS017<br />
RICHRC5006<br />
RICHRC5022<br />
RICHRC5069<br />
RICHRCSO43
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/12/1998 1:15:00 PM<br />
LAB SAMPLE ID: 80322202 REPORT NBR: 4835 RECEIVED DATE: 3/12/1998 1:53:00 PM<br />
CLIENT ID: BON689 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
COUNTING<br />
ERROR(2s)<br />
TOTAL ERROR<br />
(2 s) MDA<br />
REPORT<br />
UNIT YIELD RST/MDA RSTICNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALQ<br />
UNIT<br />
DETECTOR<br />
ID<br />
METHOD<br />
NUMBER<br />
TC-99 2.45E+02 9.7E+02 3.0E+03 2.22E+03 pCi/sam 95.10% 0.11 0.25 4/2/98 0.000677 SA LSC RICHRC5078<br />
AM-241 313E-03 6.6E+02 8.4E+02 140E+02 pCi/sam 86.50% (22.4) (4.7) 4/4/98 0.000655 SA ALPHA-SPEC RICHRCS057<br />
U-234 266E+01 43E+01 4.3E+01 755E+01 pCdsam 8150% 035 0.62 4/4198 0.000662 SA ALPHA-SPEC RICHRC5030<br />
U-235 0.00E+00 0.0E+00 4.5E+01 4.10E+01 pCi/sam 81.50% 0. N/A 4/4/98 0.000662 SA ALPHA-SPEC RICHRC5030<br />
U-238 5.81 E+01 6.1 E+01 6.1 E+01 6.92E+01 pCi/sam 81,50% 0.84 0.96 4/4/98 0.000662 SA ALPHA-SPEC RICHRCS030<br />
PU-238 214E+02 1.1E+02 1.2E+02 6.59E+01 pCi/sam 70.80% (3.2) (1.9) 3/31/98 0.000655 SA ALPHA-SPEC RICHRC5010<br />
PU239/40 6.89E+03 6.3E+02 1.1E+03 7.19E+01 pCi/sam 70.80% (95.8) (10.9) 3/31/98 0.000655 SA ALPHA-SPEC RICHRC5010<br />
AM-241 2.75E+03 4.7E+02 5.4E+02 N/A pCi/sam N/A N/A (5.9) 3/26198 0.42 SA GAMMA RICHRC5017<br />
CO-60 3.83E+03 1.8E+02 4.2E+02 N/A pCi/sam N/A N/A (21.7) 3/26/98 0.42 SA GAMMA RICHRC5017<br />
CS-137DA 6.16E+05 1.9E+03 6.2E+04 N/A pCi/sam N/A N/A (320.5) 3/26198 0.42 SA GAMMA RICHRC5017<br />
EU-152 6.96E+03 8.6E-02 1.1E+03 WA pCi/sam N/A N/A (8.1) 3/26198 042 SA GAMMA RICHRC5017<br />
EU-154 1 74E+03 2.0E+02 2.7E+02 4.53E+02 pCUsam N/A (3.8) (8.7) 3/26/98 0.42 SA GAMMA RICHRC5017<br />
EU-155 1.34E+02 3.3E+02 3.3E+02 5.05E+02 pCi/sam N/A 0.27 0.41 3/26/98 0.42 SA GAMMA RICHRC5017<br />
STRONTIUM 4.06E+05 70E+03 1.5E+05 1.02E+03 pCi/sam 94.20% (3991) (58.2) 4/1/98 0.000661 SA AB RICHRC5006<br />
0-14 3.75E+01 6.0E+02 9.3E+02 1 42E+03 pCi/sam 100.00% 0.03 0.06 4/9/98 0.001081 SA LSC RICHRC5022<br />
c:<br />
NI-63 2.23E+05 3.7E+03 2.9E+04 2.42E+03 pCi/sam 77.30% (923) (60.) 413/98 0000675 SA LSC RICHRC5069<br />
O<br />
I,_<br />
SE-79 -6.38E+02 10E+03 38E+03 244E+03 pCi/sam 76.00% -026 -0.63 4/1/98 0000657 SA LSC RICHRC5043<br />
G Number of Results: 17<br />
Cov ents:
TC-99<br />
AM-241<br />
HEXCHROME<br />
U-234<br />
U-235<br />
U-238<br />
PU-238<br />
PU239/40<br />
CO-60<br />
CS-137DA<br />
E U-152<br />
EU-154<br />
EU-155<br />
-8 74E+00<br />
3 67E+00<br />
9 OOE-03<br />
3 48E+01<br />
6.02E-01<br />
3.72E+01<br />
3.57E-01<br />
1.28E+01<br />
3.99E+01<br />
9.23E+02<br />
1 09E+00<br />
-1 13E+02<br />
-1 46E+01<br />
K-40 1.18E+03<br />
STRONTIUM 6.13E+02<br />
C 14 5.30E+01<br />
C) NI-63 1.99E+02<br />
O<br />
1-+ SE-79 1.80E+01<br />
CT)<br />
Number of Results: 18<br />
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/13/1998 8:15:00 AM<br />
LAB SAMPLE ID: 80324401 REPORT NBR: 4835 RECEIVED DATE: 3/13/1998 10:35:00 AM<br />
CLIENT ID: BON690 ORDER NBR: B98-061 MATRIX: OTHER<br />
COUNTING TOTAL ERROR REPORT ANALYSIS ALIQUOT ALQ DETECTOR METHOD<br />
ISOTOPE RESULT ERROR(2s) (2 s) MDA UNIT YIELD RST/MDA RST/CNTERR DATE SIZE UNIT ID NUMBER<br />
Comments:<br />
2.7E+01 8.3E+01 635E+01 pCi/sam 95.10% -014 -0.33 3/31/98 0.0233 SA LSC RICHRC5078<br />
3.3E+00 3.4E+00 300E+00 pCi/sam 89.30% (1.2) (11) 4/4/98 0.0234 SA ALPHA-SPEC RICHRC5057<br />
0.0E+00 0.0E+00 2.00E-03 mg/L N/A (4.5) N/A 3/13/98 100.0 ML SPECPHOTO EPA7196<br />
9.2E+00 1.1E+01 2.75E+00 pCosam 54.00% (12.7) (3.8) 4/4/98 0.0251 SA ALPHA-SPEC RICHRC5030<br />
1.2E+00 1.2E+00 1.63E+00 pCi/sam 54.00% 0.37 0.5 4/4/98 0.0251 SA ALPHA-SPEC RICHRC5030<br />
9.5E+00 1.2E+01 2.75E+00 pCi/sam 54.00% (13.5) (3.9) 4/4/98 0.0251 SA ALPHA-SPEC RICHRC5030<br />
7.1E-01 7.2E-01 9.67E-01 pCi/sam 72.60% 0.37 0.5 4/198 0.0234 SA ALPHA-SPEC RICHRC5010<br />
4.3E+00 4.6E+00 1.44E+00 pCi/sam 72.60% (8.9) (3.) 4/3/98 0.0234 SA ALPHA-SPEC RICHRC5010<br />
4.2E+01 4.2E+01 7.63E+01 pCi/sam N/A 052 0.96 3127/98 0.0532 SA GAMMA RICHRC5017<br />
9.0E+01 1.3E+02 N/A pCi/sam N/A N/A (10.3) 3/27/98 0.0532 SA GAMMA RICHRC5017<br />
9.5E+01 9.5E+01 1.62E+02 pCi/sam N/A 0.01 001 3/27/98 0.0532 SA GAMMA RICHRC5017<br />
11E+02 1.1E+02 167E+02 pCi/sam N/A -0.68 -(1.1) 3/27/98 0.0532 SA GAMMA RICHRC5017<br />
8.7E+01 8.7E+01 1.42E+02 pCi/sam N/A -0.1 -0.17 3/27198 0.0532 SA GAMMA RICHRC5017<br />
8.4E+02 8.5E+02 N/A pCi/sam N/A N/A (14) 3/27198 0.0532 SA GAMMA RICHRC5017<br />
4.7E+01 2.3E+02 2.97E+01 pCi/sam 95.80% (20.6) (13.1) 4098 0.0234 SA AB RICHRC5006<br />
3.0E+01 4.6E+01 670E+01 pCi/sam 100.00% 0.79 (1.8) 4/2/98 0.0233 SA LSC RICHRC5022<br />
3.2E+01 9.8E+01 6.31E+01 pCi/sam 80.10% (3.2) (6.3) 46198 00246 SA LSC RICHRC5069<br />
3.2E+01 1.2E+02 7.52E+01 pCi/sam 69.20% 0.24 0.57 4113/98 0.0234 SA LSC RICHRCSO43
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/13/1998 9:00:00 AM<br />
LAB SAMPLE ID: 80324402 REPORT NBR: 4835 RECEIVED DATE: 3/13/1998 10:35:00 AM<br />
CLIENT ID: BON691 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
COUNTING<br />
ERROR(2s)<br />
TOTAL ERROR<br />
(2 s) MDA<br />
REPORT<br />
UNIT YIELD RSTIMDA RST/CNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALQ<br />
UNIT<br />
DETECTOR<br />
ID<br />
METHOD<br />
NUMBER<br />
TC-99 282E+01 28E+01 86E+01 6.38E+01 pCi/sam 95.10% 0.44 0 ) 3131/98 00232 SA LSC RICHRCS078<br />
AM-241 2.31E+00 2.7E+00 2.7E+00 2.08E+00 pCi/sam 86.20% (1.1) 0.87 4/4/98 0.0241 SA ALPHA-SPEC RICHRC5057<br />
HEXCHROME 200E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3113/98 100.0 ML SPECPHOTO EPA7196<br />
U-234 2.94E+01 7.9E+00 9.SE+00 2.12E+00 pCi/sam 65.10% (13.9) (3.7) 4/4/98 0.0249 SA ALPHA-SPEC RICHRC5030<br />
U-235 1.01E+00 1.5E+00 1.5E+00 2.12E+00 pCi/sam 65.10% 0.48 068 4/4/98 0.0249 SA ALPHA-SPEC RICHRC5030<br />
U-238 3.25E+01 8.3E+00 1.0E+01 2.81E+00 pCi/sam 65.10% (11.6) (3.9) 4/4/98 0.0249 SA ALPHA-SPEC RICHRC5030<br />
PU-238 0.00E+00 0.0E+00 1.2E+00 1.10E+00 pCi/sam 64.10% 0, N/A 4/3/98 0.0241 SA ALPHA-SPEC RICHRC5010<br />
PU239/40 6.11E+00 3.2E+00 3.3E+00 1.10E+00 pCi/sam 64.10% (5.5) (1_9) 4/3/98 0.0241 SA ALPHA-SPEC RICHRC5010<br />
CO-60 -276E+01 3.9E+01 3.9E+01 6.25E+01 pCi/sam N/A -0.44 -0.71 3/27/98 0.0504 SA GAMMA RICHRCS017<br />
CS-137DA 3.77E+02 8.5E+01 9.3E+01 N/A pCi/sam N/A N/A (4.4) 3/27198 0.0504 SA GAMMA RICHRC5017<br />
EU-152 1.70E+01 8.6E+01 8.6E+01 1.45E+02 pCi/sam N/A 0.12 0.2 3/27/98 0.0504 SA GAMMA RICHRC5017<br />
EU-154 344E+01 94E+01 9.4E+01 1 70E+02 pCi/sam N/A 0.2 0.37 3/27/98 00504 SA GAMMA RICHRCS017<br />
EU-155 2.20E-01 7.6E+01 7.6E+01 1.20E+02 pCi/sam N/A 0 0. 3/27/98 0.0504 SA GAMMA RICHRC5017<br />
STRONTIUM 1.36E+02 2.3E+01 5.1E+01 2.85E+01 pCi/sam 91.90% (4.8) (5.9) 4098 0.0241 SA AB RICHRC5006<br />
C-14 509E+01 30E+01 46E+01 670E+01 pCi/sam 100.00% 0.76 (L7) 412/98 00232 SA LSC RICHRC5022<br />
NI-63 8.95E+01 2.4E+01 7.3E+01 5.16E+01 pCilsam 102.30% (1.7) (3.7) 4/5198 0.0241 SA LSC RICHRCS069<br />
SE-79 -1.32E+01 3.3E+01 1.2E+02 7.98E+01 pCi/sam 68.00% -0.17 -0.4 4113/98 0.0223 SA LSC RICHRCSO43<br />
Qlumber of Results: 17<br />
O<br />
Comments:
C<br />
H<br />
FORM I Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: OUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/16/1998 8:30:00 AM<br />
LAB SAMPLE ID: 80327201 REPORT NBR: 4835 RECEIVED DATE: 3/16/1998 12:15:00 PM<br />
CLIENT ID: BON692 ORDER NBR: B98-061 MATRIX: OTHER<br />
ISOTOPE RESULT<br />
COUNTING<br />
ERROR (2 s)<br />
TOTAL ERROR<br />
(2 s) MDA<br />
REPORT<br />
UNIT YIELD RST/MDA RST/CNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALO<br />
UNIT<br />
DETECTOR<br />
ID<br />
METHOD<br />
NUMBER<br />
TC-99 -1.27E+03 92E+02 29E+03 224E+03 pCi/sam 95.10% -0.56 -(1.4) 4/2/98 0.00067 SA LSC RICHRC5078<br />
AM-241 7.76E+03 1.0E+03 1.7E+03 138E+02 pCi/sam 96.40% (56.4) (7.5) 4/4/98 0.000667 SA ALPHA-SPEC RICHRCS057<br />
U-234 2.97E+01 4.4E+01 4.4E+01 6.23E+01 pCi/sam 83.00% 0.48 0.68 4/4/98 0.000664 SA ALPHA-SPEC RICHRCS030<br />
U-235 -1.24E+00 2.5E+00 2.5E+00 6.23E+01 pCi/sam 8100% -0.02 -0.5 414/98 0.000664 SA ALPHA-SPEC RICHRCS030<br />
U-238 2.60E+01 4.4E+01 4.4E+01 8.27E+01 pCi/sam 83.00% 0.31 0.59 4/4/98 0.000664 SA ALPHA-SPEC RICHRC5030<br />
PU-238 4.46E+02 2.0E+02 2.1E+02 9.00E+01 pCi/sam 54.10% (5) (2.2) 3/31/98 0.000667 SA ALPHA-SPEC RICHRC5010<br />
PU239/40 1.53E+04 1.2E+03 2.5E+03 102E+02 pCi/sam 54.10% (150.2) (13.1) 3131198 0.000667 SA ALPHA-SPEC RICHRC5010<br />
AM-241 7.27E+03 4.1E+02 8.4E+02 WA pCi/sam N/A N/A (17.7) 3/26/98 0.4048 SA GAMMA RICHRC5017<br />
CO-60 6-13E+03 2.5E+02 6.6E*02 N pCi/sam N/A N/A (25.) 3/26/98 0.4048 SA GAMMA RICHRC5017<br />
CS-137DA 766E+05 1.2E+03 77E+04 N/A pCi/sam N/A N/A (618.9) 3/26/98 0.4048 SA GAMMA RICHRC5017<br />
EU-152 3.30E+04 1.4E+03 3.6E+03 NA pCi;sam N/A N/A (22.9) 3/26/98 0.4048 SA GAMMA RICHRC5017<br />
EU-154 601E+03 5.5E+02 8.2E+02 N/A pCi/sam N/A N/A (10.9) 3/26/98 0.4048 SA GAMMA RICHRC5017<br />
EU-155 3.25E+02 4.4E+02 4.4E+02 723E+02 pCi/sam N/A 0.45 0.74 3/26/98 0.4048 SA GAMMA RICHRC5017<br />
STRONTIUM 4.56E+05 7.2E+03 1.7E+05 1.06E+03 pCi/sam 93.90% (430.5) (63.) 4/1/98 0.000683 SA AB RICHRC5006<br />
C-14 467E+02 6.5E+02 1.0E+03 1.50E+03 pCi/sam 100.00% 0.31 0.72 4/9/98 0.001022 SA LSC RICHRC5022<br />
NI-63 3.44E+05 4.4E+03 4.3E+04 227E+03 pCi/sam 81.30% (151.7) (78.) 4/3/98 0.000684 SA LSC RICHRC5069<br />
SE-79 -2.43E+02 9.6E+02 3.5E+03 2.29E+03 pCi/sam 82.80% -0.11 -0.25 4/1/98 0.000646 SA LSC RICHRC5043<br />
Number of Results: 17<br />
Comments:
ISOTOPE<br />
TC-99<br />
AM-241<br />
HEXCHROME<br />
U-234<br />
U-235<br />
U-238<br />
PU-238<br />
PU239/40<br />
CO-60<br />
CS-137DA<br />
EU-152<br />
EU-154<br />
EU-155<br />
STRONTIUM<br />
C-14<br />
NI-63<br />
SE 79<br />
RESULT<br />
5 17E+00<br />
5 54E+00<br />
1 40E-02<br />
3 33E+01<br />
3 54E-01<br />
1 95E+01<br />
0 00E+00<br />
1 03E+01<br />
2.65E+01<br />
1 32E+03<br />
1 62E+01<br />
1 56E+02<br />
4 84E+01<br />
1 34E+03<br />
1.22E+02<br />
8 09E+00<br />
1.97E+00<br />
COUNTING TOTAL ERROR<br />
ERROR(2s) ( 2 s)<br />
2.6E+01 8.3E+01<br />
3.9E+00 4.0E+00<br />
0.0E+00 0.0E+00<br />
7.9E+00 9.8E+00<br />
9.4E-01 9.4E-01<br />
6.0E+00 6.9E+00<br />
0.0E+00 1.0E+00<br />
3.7E+00 3.9E+00<br />
3.7E+01 3.8E+01<br />
1 .3E+02 1 9E+02<br />
1.0E+02 1 0E+02<br />
9.1 E+01 9.3E+01<br />
7.1 E+01 7.1 E+01<br />
6.9E+01 4.5E+02<br />
3.2E+01 4.7E+01<br />
2.6E+01 8.0E+01<br />
3.1 E+01 1.1E+02<br />
FORM Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/16/1998 9:25:00 AM<br />
LAB SAMPLE ID: 80327202 REPORT NBR: 4835 RECEIVED DATE: 3116/1998 12:15.00 PM<br />
CLIENT ID: BON693 ORDER NBR: B98-061 MATRIX: OTHER<br />
Number of Results: 17<br />
0<br />
0<br />
Comments:<br />
MDA<br />
REPORT<br />
UNIT YIELD RSTIMDA RST/CNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALQ<br />
UNIT<br />
DETECTOR<br />
ID<br />
6.21E+01 pCi/sam 95.10% 0.08 0.2 3/31/98 0.0238 SA LSC<br />
1.87E+00 pCi/sam 91.60% (3.) (1 4) 4/4/98 0.0247 SA ALPHA-SPEC<br />
2.00E-03 mg/L N/A (7.) N/A 3/16/98 100.0 ML SPECPHOTO<br />
2.63E+00 pCi/sam 6820% (12.7) (42) 4/4/98 0.0256 SA ALPHA-SPEC<br />
2.32E+00 pCi/sam 68.20% 015 0.38 4/4/98 0.0256 SA ALPHA-SPEC<br />
1.87E+00 pCi/sam 68.20% (10.4) (3.2) 4/4/98 0.0256 SA ALPHA-SPEC<br />
9.04E-01 pCi/sam 77.40% 0. N/A 4/3/98 0.0247 SA ALPHA-SPEC<br />
9.03E-01 pCi/sam 77.40% (11.5) (2.8) 4/3/98 0.0247 SA ALPHA-SPEC<br />
7.00E+01 pCi/sam N/A 0.38 0.71 3/27/98 0.0512 SA GAMMA<br />
NA pCi/sam N/A N/A (10.1) 3/27/98 00512 SA GAMMA<br />
1.69E+02 pCi/sam NIA 0.1 0.16 3/27/98 0.0512 SA GAMMA<br />
1.87E+02 pCi/sam N/A 0.84 (1.7) 3/27/98 0.0512 SA GAMMA<br />
1.17E+02 pCi/sam N/A 0.41 0.68 3/27/98 0.0512 SA GAMMA<br />
296E+01 pCi/sam 83.20% (45.3) (19.4) 4/2/98 0.0247 SA AB<br />
6.50E+01 pCi/sam 100.00% (1.9) (3.8) 4/2198 0.0238 SA LSC<br />
6.22E+01 pCi/sam 81.50% 0.13 0.31 4/5/98 0.0246 SA LSC<br />
7.32E+01 pCi/sam 72.40% 0.03 006 4/13/98 0.0228 SA LSC<br />
METHOD<br />
NUMBER<br />
RICHRC5078<br />
RICHRCS057<br />
EPA7196<br />
RICHRC5030<br />
RICHRC5030<br />
RICHRC5030<br />
RICHRC5010<br />
RICHRC5010<br />
RICHRCS017<br />
RICHRCS017<br />
RICHRC5017<br />
RICHRCS017<br />
RICHRC5017<br />
RICHRC5006<br />
RICHRC5022<br />
RICHRC5069<br />
RICHRCSO43
ISOTOPE RESULT<br />
TC-99 1.04E+01<br />
AM-241 3.42E+00<br />
HEXCHROME 2.00E-03<br />
U-234 4.54E+01<br />
U-235 9.73E-01<br />
U-238 4.12E+01<br />
PU-238 0.00E+00<br />
PU239/40 1.39E+00<br />
CO-60 4.71E+00<br />
CS-137DA 283E+02<br />
EU-152 -4.07E+01<br />
EU-154 1.48E+02<br />
EU-155 3.95E+01<br />
K-40 1.80E+03<br />
STRONTIUM 1.41E+02<br />
C-14 3.99E+01<br />
NI-63 7.75E+01<br />
C) SE-79 122E+01<br />
O<br />
)Yujnber of Results: 18<br />
C.1<br />
Comments:<br />
FORM Date: 4/16/1998<br />
SAMPLE RESULTS<br />
LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/16/1998 10:25:00 AM<br />
LAB SAMPLE ID: 80327203 REPORT NBR: 4835 RECEIVED DATE: 3/16/1998 12:15:00 PM<br />
CLIENT ID: BON694 ORDER NBR: B98-061 MATRIX: OTHER<br />
COUNTING TOTAL ERROR<br />
ERROR(2s) (2 s)<br />
2.7E+01 8.4E+01<br />
3 4E+00 3.5E+00<br />
0.0E+00 0.0E+00<br />
1.0E+01 1.3E+01<br />
1.6E+00 1.7E+00<br />
9.8E+00 1.2E+01<br />
0.0E+00 1.4E+00<br />
1.6E+00 1 6E+00<br />
3.7E+01 3.7E+01<br />
7.8E+01 8.3E+01<br />
9 0E+01 9.0E+01<br />
1.0E+02 1.0E+02<br />
9.0E+01 90E+01<br />
8.5E+02 8.7E+02<br />
2.4E+01 5.2E+01<br />
3.0E+01 4.6E+01<br />
2.8E+01 8.6E+01<br />
3.0E+01 1.1E+02<br />
MDA<br />
REPORT<br />
UNIT YIELD RST/MDA RST/CNTERR<br />
ANALYSIS<br />
DATE<br />
ALIQUOT<br />
SIZE<br />
ALQ<br />
UNIT<br />
DETECTOR<br />
ID<br />
6.27E+01 pCi/sam 95.10% 0.17 0.39 3/31/98 00236 SA LSC<br />
231E+00 pCi/sam 8250% (15) (1 ) 4/4/98 0.0224 SA ALPHA-SPEC<br />
2.00E-03 mg/L N/A 1. N/A 3/16/98 100.0 ML SPECPHOTO<br />
3.58E+00 pCi/sam 63.20% (12.7) (4.4) 4/4/98 00226 SA ALPHA-SPEC<br />
3.09E+00 pCi/sam 63.20% 0.31 0.59 4/4/98 00226 SA ALPHA-SPEC<br />
398E+00 pCi/sam 63.20% (10.4) (4.2) 414/98 0.0226 SA ALPHA-SPEC<br />
1.26E+00 pCi/sam 60.00% 0. N/A 4/3/98 0.0224 SA ALPHA-SPEC<br />
1.26E+00 pCi/sam 60.00% (1.1) 0.87 4/3/98 0.0224 SA ALPHA-SPEC<br />
6.49E+01 pCi/sam N/A 0.07 0.13 3/28/98 0.0524 SA GAMMA<br />
N/A pCi/sam N/A N/A (3.6) 3/28/98 00524 SA GAMMA<br />
1.49E+02 pCi/sam N/A -0.27 -0.45 3/28/98 0.0524 SA GAMMA<br />
197E+02 pCi/sam N/A 0.75 (1.5) 3/28198 0.0524 SA GAMMA<br />
1.53E+02 pCi/sam N/A 0.26 0.44 3/28/98 0.0524 SA GAMMA<br />
N/A pCi/sam N/A N/A (2.1) 3/28198 0.0524 SA GAMMA<br />
2.77E+01 pCi/sam 85.90% (51) (5.8) 4/2/98 0.0233 SA AB<br />
6.80E+01 pCi/sam 100.00% 0.59 (1.3) 412/98 0.0228 SA LSC<br />
6.22E+01 pCi/sam 89.90% (1.2) (2.7) 415/98 0.0222 SA LSC<br />
6.97E+01 pCi/sam 75.40% 0.17 041 4/13/98 0.023 SA LSC<br />
METHOD<br />
NUMBER<br />
RICHRC5078<br />
RICHRC5057<br />
EPA7196<br />
RICHRC5030<br />
RICHRCS030<br />
RICHRC5030<br />
RICHRC5010<br />
RICHRC5010<br />
RICHRC5017<br />
RICHRCS017<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRC5017<br />
RICHRC5006<br />
RICHRC5022<br />
RICHRC5069<br />
RICHRC5043
Quanterra Data Review C3eddist<br />
RADIOCHE.^IIISTRY<br />
^xorle G4ver -atnoer r:r. ^3 I L 1 ^' 3 ^ ^ 4 ^ 3 aC^ ^i322 L ^5 a^<br />
Ciem :D'<br />
No Datc —<br />
tau Saremie ^'umbcor SI7G: l.^ 22 7<br />
Method7m ?ammeters: YYl - 7• ti \<br />
_<br />
0<br />
Nam= C)'.a, r D e C en.. z„+<br />
Item I Ycs (.0 I aeN) I ?UA(J)<br />
A. Callbnsfon I<br />
1. Is the nh'bratim dmmtam[im alluded Wtete mp6obk? I I<br />
& Sample Analrus<br />
1. Am _he satt role yields iNut acstttaoc c mu? I J<br />
2 Wes.ul sample holdins tiara ma? I / J<br />
7. Is the sar..pic .Milumttm Detacib le .iennv < the C. Deeatm Limit? I I I<br />
C- QC Sampiea<br />
I. Is ute Siaric i.id wtb= ameounce airma I / I I<br />
Li st^ .e `.Iinu:am - OtIaC ble A=WY CQ the olank rtsW S Ibe C urnnn Deuaion I I I / ! `<br />
J. Is the aiank .quit < L: :he Cantraa Daman Imo?<br />
a. Is the aia > I;- the C.xtQae D • iirdt bee < C^ Dc m m Cinut? I ^_<br />
`. Isthe.iari'.3ult>the Camrt Dace:m i.:mis ba :be smile rtauit
Comments n any -No' response:<br />
First L :ei 3e•.iett<br />
Second Lecd Re•.ie•xv<br />
Form d LS-078.2i%.<br />
Qaaatcra Data Review Chedciist<br />
RIDIOCHENUSTRY<br />
Work Cyder number ( or. SL^31 ^_ y I(o! ,S^CI(o "`22Z 244 ^.3^^^--<br />
Cietn ID: R N r—<br />
Due oats: - G - 9<br />
Lab Sammie Number or SDG,i tr.!<br />
Method Test ?ammeter: f t a ut<br />
Z27^<br />
Munn- Q L L L. r'r<br />
Rnnevl I Ye (•/) I `loft) I &A(1) I'Lard<br />
Review lJl<br />
A. CaUbmtIon<br />
1. Is the nhbtwbb docwnevacm inchtded Wore app6ethle?<br />
I<br />
I /<br />
a Simple AtWpis<br />
I. Am the sample vielda wmitm atzsatatre anena7<br />
I /^<br />
Z W ere 311 sample holdms time nn^<br />
I I<br />
3. Is the s ie Mnimum Detectable A=nr y < the C^ Detattna Lent?<br />
C. QC Samples<br />
1. Is the blank •leld Wthm •=cs, siren.<br />
:. Is the Minunum Detectable A=vnY for the Blanc rout S the Caaae Daaston<br />
Litrut?<br />
3. Is the blank . ^ it < L: the Caneacc Detemon L _.?<br />
S, Is the alw3 > I,- the C.Yne9G Dawson L 1t tta < C.IICYS Dc,— Llmnl?<br />
!. Is the olaruc It> the ComnG Desec'on :nut hotthe sa>Rle nstt
First Lc. ei<br />
Second '_z% -I<br />
Form d 1-64 i96. Ret 1<br />
Quzu= a Data Review Checklist<br />
RADIOCHE KISTRY<br />
Work Oraerypnoer ,ak<br />
^3^ 4 8031 ^1 ^3ao6 ^^zzz 8^3^'r X27<br />
Cicm!D' .tJ N --j_<br />
Due Due: 4—<br />
Lab Sartmie ` umber or SOG:<br />
1lethod -M .'mntmurs: P •^ ^<br />
Muni.<br />
Renew Item ( Yea (J) I !7o (J) I WA(J) 11'Sssei<br />
;ess^ (.0<br />
A. Cailbrauoit<br />
1. Is the calrlumas doaunau ation included where applicable?<br />
a Sempie .iadrsie<br />
I /<br />
1. Arc the sample yields within •^^mane citniat<br />
Z Were all sample holding:imn me?<br />
I ^^<br />
7. Is :he zvrpie 11uumum De:stahle k=hN < the Cm Detection Limit^<br />
C QC Samples<br />
1, Is the biarA '•+eid wthin ae-eovncc ct.—t . a<br />
f.<br />
T?Ithe ^•t^.lf:3ml Der[Cadlt.i4'.IVIN:Cf :h the C,lntl<br />
Detection a^:?<br />
ctC4an . J l but the sampie rmlh
Qumzm a Data Review Cheddist<br />
RADIOCHEMISTRY<br />
war< over -umaer ^, t: i 31(o I 3 i v F^3 a•o 3 Z zZ 8C3 a 7<br />
Clem fn . $1+Z<br />
Due our. Lk- (O - k<br />
Cab Sammie Number ar SDG: (P ZZ 7<br />
Nethed 7= is tsnnes:<br />
u,avc C: ^_CeM^.,-t<br />
A. CGllbradon<br />
1. Is the ralibn = doevmerpasim aebsdeb w e s¢eahl ?<br />
se„ICV lt® I Ye(J) I No(J) I VA(J)<br />
& Semple Arraign I<br />
1. Ate the sample neids sec" tt= a^OUptx esteriat<br />
I<br />
II<br />
17niew (J)<br />
I /<br />
II II<br />
Z. W ere all ==It holdio3 time inn? I ^ I j ^ I i<br />
3. Is Ne sample \Ivsirss,m, Dens-^bk .ieJnry < yeGmn Deserswn Ijmit^ I I j l— ^ I<br />
C QC Sampies I<br />
1. Is the blamer •.field within aetrar>re =t .a<br />
Is :he `du= Detectable Aesn,v far l le Sara rink S the Cc Des ern I<br />
Lirmt7<br />
3. Is the dia r=un < l.= the Cra¢,a D^am tin?<br />
4. IS [he JINN > I,- the C.M?]C: DacJan i -1t II, < O,,,, a DQeGr41 LIIIYIT<br />
!. is the dark .a it > the Car, n L)d=on _:= hoebe samplensuh
Qaaatena Data Review Checklist<br />
RADIOCE9MMY<br />
Work Order„ambtlsk 8031 .3q T031G 03 0(0 8(3 D -a 3aNN o317^<br />
C.iaa ID: U ^//<br />
Due Datc.<br />
Lab Satmk Number m SDO:<br />
GG<br />
'to ^I<br />
w^ as -t S<br />
Mepmd Tea Pu® U<br />
^O<br />
M. Mx<br />
Rin wltm Ye(J) HON) VA(V) Tiled<br />
A. Cailbradoa<br />
1. Is the dbalmdoc mausum u tchwad- Im M*kz [a?<br />
IL Sample Analysis<br />
1. M the sa iple yidda with= ameouac= abeia? !/ 3 /<br />
2 Were all sample bolding tesee an? I I I -<br />
3. Is the saaWie Minnu m Deeaahle .Acm y < the Conta ct Deua an Unav<br />
^v<br />
Date y^^ %^J<br />
Date:<br />
` 3 `<br />
I 3<br />
C QC Sample<br />
1. Is the blank yield wigs acceptance ancris 3<br />
^tthe Mim nu n Dd=able Activity la the black ^ 5 the Ceetraa D etec tive (<br />
I I I _ i<br />
3. Is the blank teals < L_ the C.smaa Ddectta Lunt? I<br />
3<br />
3 I r<br />
`,<br />
S. Is the blank > It' the Contact Ddemm Lim but < Catract Detection Lao I ( 3 I -<br />
5. Is the blank result > the Contract Deeom Lank but the savle renh
Qutm=Ta Data Rcview CLeddiu<br />
RADIOCIM0 1LSMY<br />
Wok O mer,mtsea r,t $ 316 1 8011V43 9° a()6 3:) ;t<br />
Chen ID*<br />
Dim Dare lily<br />
Lab Sammie Nmobw er SDCr.<br />
.Method Tea Psnsrm<br />
41sms<br />
I<br />
>n. ^a a "7 5<br />
RZME Item Yam (J) 140(01 ) I WA(J ) 1^Ised<br />
Rs+isr•!Jl<br />
A. Ca llbradam<br />
1. Is the sal3num doemameam ioduded Mus a*kabia? ^.<br />
S Sampee Asuiris<br />
1. An the sarmle?itidt - anseuome avmia? !/<br />
1 Were all samplc bold* —m?<br />
3. Is the sur¢ie 4fakmem Daemhle Acuvdr < the Camas Datum t3mt? I I 3<br />
C. QC Samples<br />
1. Is the blank r cld wirhm scecomma m a 3 I I I<br />
2 Is the 4lutunum Daeamble Amvm (rr the blank rack S the Caara a Detetim<br />
[.unit?<br />
I<br />
3<br />
I /_<br />
3. V the blank trsua < I!- :he Caatna Docc uau Unlit? I<br />
3<br />
/<br />
s. Is the blank > Ir the Caeeraa Daaaeo 1= ba < C.srmaa Damask omit? I I ( 3 '<br />
3. Is the blank :mh> the Cauraaa Dettsesm Lino bm the sampie nmlt < the Cavaa<br />
Detaitan Lirtut^. I f 3<br />
6. Is the i.CS rook wuhm a¢sprafoe vuaa?<br />
7. Is the LCS neldvdth in aaxponre cmrna<br />
8. Is the LCS Mirm Detecahk Acttrn:/ 5 the Camaa Deenim Lam?<br />
9. 415%4tSD rauln aM peld nm •^ r++^+ mtau7<br />
10. Duplicate wnple tesuus and r dd am s¢epuoce av I<br />
D. Other<br />
1. Are all `iomm nfommsm vsmded and ased?<br />
Are ail required forms Ned oLaC<br />
3. Corm= acbodaioa used? I<br />
4. Traractpuen ducked.'<br />
S. Were all calculaiau ducked at a nar>nam fsogo ? ei<br />
6. Unats Checked'<br />
Comments on any -No' response:<br />
First Lwe! 3etdav: L% Li- `E^^{^t` Date:<br />
Second LL%--! Rrviewl Date:<br />
Form #: LS -038 .2 196. Rev 4<br />
3<br />
I I I j<br />
60 57
QUANTERRA LABORATORY NONCONFOR:N L-kNCE VIEmO (NCNI)<br />
PAGE 1 OF 2<br />
Project ID:<br />
Sample Numbers:<br />
r<br />
M<br />
NCM mriated by<br />
0 32 -7,202 D 03^7^a<br />
Tests: —f^o<br />
Matrix: y ^l u / D^ 7<br />
Analytical Area (cheek soorooriate area):<br />
LOG =: RD-98,<br />
• Sample control q GC Cl Wttchemistry l O-lData review<br />
• Organic preparation q HPLC q heals P'Rkadiochemistry<br />
• Inorganic p reparation q GC/MS q Reporting q Bioassay<br />
Nonconformance (check appropriate area):<br />
Holding Time rzolations (exceeded by days) QuAyAssurance/Quality Control<br />
Category 1. Laboratory Independent q 17. QC data repo rted outside of controls<br />
q I. Holding time expired in transit q 13. Incorrect procedure used<br />
q 2. Sample received > 48 hrs. or I/2 holding time has<br />
expired<br />
q 19. SOP intentionally modified tivith QA and Tech. approval<br />
q 3. Test added by client after expiration q 20. Imalid instrument calibration<br />
Category Il: Laborator y Dependent<br />
q 4. Instrument failure<br />
Cl 21- Insu ffi<br />
cient sample received for proper analysis<br />
Incomyror Incomplete Client Deliverable<br />
q 5. Analyst error q 2 Hardcopy deliverable error<br />
q 6. Login error q -13. Electronic deliverable error<br />
q 7. Miscommunication<br />
Reported detection limits eleti-ated due to:<br />
q 8. Other (complete description required) q 24. Sample matrix<br />
Category III: Analysis Reruns (OA, QC) q 2i. Insufficient sample volume<br />
q 9.<br />
IQ<br />
Surrogates<br />
Inte<br />
q 26- Other (complete description required)<br />
27. Other (specify): _<br />
ZL CGh- `C<br />
rn al Standards<br />
q 11. Spike Reco • eries<br />
q 1 2. Blank Contamination<br />
Category Il'. .anal.sis Rerms (Conf+nrtation)<br />
q 13. Second column<br />
q 1 4. Contamination check<br />
q 15. Confirmation of matrix effects<br />
q 16. Other (complete desc ription required)<br />
Noti fi cation ( check appropriate area):<br />
Com>¢nts/Espla^ination<br />
Client noti fied by (name and date): Client "s name and respon s e<br />
d<br />
VtSu ` do ^, f _<br />
GU! 71{7 ^E?L t /<br />
q jtf «Hung q by facsimile q process "as is" q re-_ t mple<br />
be telephone . Ap othe (explain) Z,2, I jo jli hold until q otSer (explain)<br />
Project Manager (signature and date): l f z<br />
0058
Corrective Action<br />
QUANTERRa LABORATORY NONCONFORMANCE MEMO (NCNI)<br />
PACE 2 OF 2<br />
Root Cause 1 nitkLI and date:<br />
LOGO: RD-93-<br />
1, hlrCC^ ^iiu^ s- ( n6o u)GnewPDtU^- ^r^¢>i^C -<br />
Corrective Action Initial and Date: (1q C<br />
Responsibility for performing CA assigned to:<br />
Actions to prevent recurrence Initial and Date:<br />
First Level Supenisor<br />
Responsible Manager: o /<br />
__Ouality Assurance Review<br />
Dy al/ omaly<br />
O Further action required:<br />
Assi gned to:<br />
QA signature:<br />
Corrective Action Ve rification<br />
11 Verified<br />
^' 4<br />
0 Cannot Verif} (specify reason): 1 ^ (` I<br />
Nonconformance demo Closure<br />
QA signature/date:<br />
Date:<br />
Date:<br />
Cl Deficienev O Rerun<br />
Date:<br />
/<br />
n<br />
CO5<br />
_
Quanterra Data Review Cbeddist<br />
RADIOCHEMISTRY<br />
'Cork Che er nvmtser r a,: 1 I Sn31e FSO a S-03 2 2 Z SO 71<br />
1<br />
C:imt!D'<br />
Due Date. -<br />
Lab Samvie `:timber or SM.<br />
method -,m?aametcs: C<br />
Manx:<br />
Z. Z7<br />
Ramme Item<br />
,L Calib ration<br />
t. Is the calibration daautsemaomf urluded Weee anpiicaW<br />
I<br />
IL Sample ..A W7sis I<br />
1. Are the sarfrole vichh vmmma aemtaoae attersa7<br />
:. Were ill Saafple holding tines met'<br />
3. Is the SN.:^ to Meruratem Dee imcle Acu"N< the Camae D eseeem Lann7 I<br />
I<br />
Yet (!) I `!o (!) I WA(!) I ^^IsW<br />
( f<br />
1l<br />
^_<br />
f<br />
I I ^^/I<br />
I C QC Sunpies<br />
1. Is she burn '•teld w thin ^.c asma j<br />
:. lathe .`,1__-urrz Detactable .ae_•nty for she Defe ction<br />
Litfsif^.<br />
3. Is the oianx Tuft < IG the Cancan Deecvan L:mei<br />
4. Is the ours > I,: the C.xeaaa De' .n i:sesf ba < Cman Dese c,, Limit? I I f_<br />
sr;e.11,<br />
!. 13 1he'JIarC :'31+I1 > Ltx C^- Dc %rC.IOn l:mn bm the s=%* l estdl < :he Ccnf<br />
Detection um.:'<br />
6. Is the i ZS cult wthm m=a' I I I i .<br />
7 . Is the :CS p,etd W then ]CL4N1C m1m.<br />
9. Is the LCS llmunum DCIL is 1 J"N < Lhc C as yh D et,,m LSLt?<br />
9, MS, MSD Buis and "sold ere: ac^[anc stem?<br />
10. DuPii^e sur.Ple real(: and ^seid mee. ac-Hang amsa? ^ I I ^ i<br />
D. Other<br />
I. .Are all Scnnr-ncrtnanoa indudd and noted?<br />
:. Are all ree_ud forma tiled out' I ^ I<br />
3. Curry me •_-odolog, used'<br />
a. Tat s ..p , cn cheekd'. I I I<br />
I<br />
7. Were ail n:alaneess aheeitd at a muumum fsequ , f 7<br />
6. Cn.0 cnccawd' I I /<br />
Commen: on on} "`o' resocnse: /U( A [ i-^, hk /u dr^S -/cr ^^L 1 _<br />
First Ln.i R_•.-te•.v"<br />
Date<br />
Second Le.e!Rr.7e•.v-<br />
Form d LS S. ; 96 Rcc<br />
Date:<br />
0000<br />
I
First Lie! R.ne.v Date<br />
Second Leve! 2etie•.r<br />
Form O LS -013? /96, l<br />
Quanterra Dan Review C3eekku<br />
v<br />
RADIOCHEEi LIMY<br />
Work Ordermunberrsh ^i31g^ ^.}I(,I ,^}J^b Oj^j^ S^'^i X 44 53 ^.3.)<br />
Client ID' f•f<br />
Due Datr. y — `i<br />
Lab Sumvie Vumbr or SDG:<br />
Method Tm paamens:<br />
Mama: I<br />
pas Item Yes (.0 *V) I WA(^/) 2^Iasd<br />
Rass!!1<br />
A CallbmClom<br />
1. Is the calibruim doounammm i tchded.Me appiimbler<br />
IL Semple AimiTsis<br />
1. Are the sample Melds wahm aaxpummorsona?<br />
` f<br />
I<br />
I /<br />
2. Were all sauvle holding tnm on? I I I<br />
I Is the satstple Minimum Desemab ie Aaeite < the C•amsa Daeomm Limb? I I '<br />
C QC Samples<br />
I. Is the blank Meld within a¢epaa: alum<br />
Z. Is the Misumum Daauble Aaivny for the Mani must S Ibe C.amact Detemon I<br />
Limit? I<br />
3. Is the blatu :sub < Ii= the Ceeffiaa Des>am L ou?<br />
a. I: the blank > 1 12 the Coma Daemon Lvb bu < Comma Deuam li®t?<br />
I ( /;<br />
I I I _<br />
I J I 1<br />
S. Is the blank result > the Co runa Dana Lines but :be sample tub
QuanaTm Data Review Chedd ist<br />
RADIOCHE1IISMY<br />
W ork Ot numurtat 8o31,e 'F5-03DOC 3222 ,3.-)4 FC3a _7.x_<br />
C' unt lD<br />
K ^,—<br />
Due Date: - la - Q Y<br />
Lib Samo!e Namur oe SDCr<br />
l.J q) 22 -7 S<br />
Nethad TeR ?atYRtei T TrtiP Sri<br />
Matnz 0<br />
A. Cillbnason<br />
'<br />
1. [s the olibatim dnaatmtatim ivrudd w.hee a, pwank?<br />
EL Sen<br />
AA&' sia<br />
Revmne It= I Yes (.0 I fb(J) I WA(^) I ~Ieved<br />
RMtN it l<br />
'°le the ' vi<br />
I I I i<br />
1. Are sample elds ndu, iteiat<br />
^.Wed all sple am haldig tea =?<br />
3. Is the San:pie Mitsomaa Deeraa!e Aa < the Camas Deeasv Sims^ I I<br />
C QC Sampies<br />
1. Is the b!anit '.ieid wIf= srntvtc =<br />
the M llllt'LmDctE le.A . N fO :he Aum.,. S:Sc CJIDIY['JC'i on<br />
". is<br />
3. Is the olank suit < l.= :be C. a Deeevon Ua 7<br />
I I I<br />
a. IS lh. 013 > I :he C.Imlf. Dneeaen L:ILI bn < C^ DecaiYO Lzma7 I ' I ^.^<br />
!. Is the o!arx X12 > the Ca .. Jeecott Z 1= bee ^hc sa npie resod
Qoanterra Dua R rinr Checklist<br />
RADIOCFI DUSTRY<br />
wnrk order-^,n^,.t ^'t^31 b I ^c3 i 8 4 FC3ao^C 5D3 a^ `6C3,P -7 )-<br />
Cientll)*<br />
Due Due--<br />
\_k<br />
- Cl 0<br />
Lab Surtnic Numhtr ar SDG: (,L Z2 -7 ^5<br />
Nahed —ea ?•^---T TO -r Q Sr<br />
.tune O<br />
Rene,. fleet I Yta(.0 I MoN) (<br />
1. ton =ii<br />
i<br />
I. Is the nlihruim docamtcvatton inducted Wiere^c7<br />
R Semple.arm17s6<br />
I. Are the sueic sidle.Wun acGeptante mreriat<br />
I<br />
- Were 111 simple bolding tuna met? I /<br />
3. Is the s . to Amarr+mt Dete=ble iGlnty < DeCaman Desecuao Limn?<br />
C. QC Sempies<br />
I. Is the Mara '.l cld Wtlml aLCplylCe ^1[er.1<br />
Is:he IIr==M J
Quantem Data Review CSedtEu<br />
RADIOCHMMISTRY<br />
W«konuok ^'31^t ^^i v 53o3a^^ 8^3aaa 8^3a - 7 a<br />
Cient ID-<br />
Due Dac.<br />
Lab Sammie *lumber or SDCr.<br />
A, J a a 7 S<br />
Method Tea parameters C - 1 Li<br />
\4atrim<br />
A. Callbrulos<br />
1. Is the calibration doammaom ecbadtd share appli able?<br />
S Semple Aasl7312<br />
1. Ara the sample viddis - acnnece anaria7<br />
times hem I Yea(.) No(1) I ;UA(.) 2-lavel<br />
Rsaieaal.\<br />
2. Were all sample hold ing mm meteI /<br />
3. Is the satpie Mkum ma Detectable .iron) < the Caaa t Deemm Li aise?<br />
C QC Sunple<br />
1. Is the blank held within acmaas am eria<br />
I /<br />
2. Is the Vint mire Detectable Ac m iv the blank nsuh S ibe Cm<br />
Limit?<br />
a Detection I I<br />
f<br />
' I _<br />
`<br />
i<br />
f<br />
3. Is the blank ;cult < lQ Ibe C.aueact Deueflon Lin? I I I I / i<br />
4. Is the blank > 1 R the Cacact Desom Lies bet < C vdria Detec oeu UnuL7 I I '<br />
3. Is the blank vault > the Canna De sera s limn his the sample ratk < the Cacao<br />
Detcuon Umtl?<br />
I<br />
I I ^-<br />
6. Is the LCS result within a¢cpunc Ivan? I/ I I '<br />
7. Is the LCS said within aonptm c ena<br />
B. Is the LCS M inimum Detectible Ass'm S the Carona Deuoos Lion? I I I<br />
9. MSi\fS r) .cults and y aid sheet acmuene cs ma? I I l<br />
10. Duplicate sample saints aid yi eld tots acceptance ancria?<br />
D. Other<br />
I. Ara all Noncoafimnanca ncludd aid acted?<br />
2. Are ail required Corms filed ate<br />
3. Cortex methodolo gy used?<br />
4. Transmpuan checked? I ^^<br />
S. Were all calcttlatons ch ecked a a ev®a® frequency? I f '<br />
6. Uni ts check ed?<br />
Comments on any -No' rspcnse:<br />
First L^:el Rabe% ^— Date:<br />
Second Ltvcf Review Date:<br />
Form ; LS-033,2!96.<br />
V14 r S<br />
006
Comm.it5 on am" No' resoc 0:<br />
First Lrrei Rr.ie:v:<br />
Second Letic! Actiie:r<br />
Form = LS-0 1 8.2 i96.<br />
Qunu=Ta Data Review Checklist<br />
RADIOCHL USTRY<br />
Wark Order-umta: Est O^'^^^7^ ^ 31 O ^^^lT-^O ^^Z2^ ^3a^L.<br />
cian:n N.^ C<br />
Due oast: L 1y -C !<br />
Cab Saenoie Number a SM t,J 2 Z 'T<br />
Method `a[ .'aaametom S 'e - -7<br />
A. Calibradon<br />
1. Is the elibmm dawmeaduian inchnded *wc ag6cahk?<br />
M Sample AaW7 312<br />
Rrne+lt® Yea (J) `*(J) WA LgVel<br />
icriw (J:<br />
I<br />
Dauc A _<br />
Dale<br />
I //<br />
1. Art the sample vields Imdun<br />
aarmaom entnar I I/<br />
2. Were all sample holding tim es mn?<br />
I I I I<br />
3. Is the satr•ie Minimeam Dc=:.xole A=v < ftC.ma s Desectsm Lmd?<br />
C. QC Samples<br />
1. Is the bunk •deld . dun .^-. :tsntcc a:tea<br />
0. Is the.`.linurum Cor des: blank a®u Sdse Catm'aa Detection<br />
L nit"<br />
3. Is the mask ^asuit < L: :he Canna aet,=a n L ma? I/<br />
4. Is the Manic > I,-- the Cantne D^on Lain bn< Ca mcn e Dcamomn Lamas? I<br />
'., fs Use blar3c ^3nll > Use Cantrac: Jenee:oo Lma he the sale nssl[
First Lz:,i Rv.ietc<br />
Second '_=^ e! R- iew-<br />
Form = LS-)',8.2/96.<br />
Qu=ern Data Review Check fist<br />
RADIOCHEaM 4-(;^ cr^ ,<br />
J. were all :al.-llsstaru :Pecked at a :wmr:S n rsc epumv?<br />
6. Units checkd?<br />
COmmen Ls on any'-`o' resccns:: i1,'• ,LDL<br />
'es It" L^(,^ G"X— Q<br />
Date -^fJ<br />
D= Y 6 ^^<br />
j<br />
6060
Qaaaterra Data Review C3eddist<br />
RADIOCHIJ. Y<br />
waeit order -umbe (It `a'A3 i Fs ^{ 8C3 i ^! `6C'3 ^ c^SG;S ^ .^. a ^rG3 ^ ^f N ^t 3 3 7<br />
cient :D: t k -7<br />
Due Date:<br />
L . Y<br />
4 -<br />
Lab Samote Vumbe or SDQ<br />
Method Tea ?a=nswer: 7—C - 9<br />
Natnrc G +h P<br />
-22-7,.5<br />
Renew ltea I Yes (.1 ) I No (,0 I VA(.t)<br />
A. CAUbmtlon I<br />
1. Is the alibtmm dootmemommon mc!uded -tax agfehlst<br />
I /^<br />
B. Sample Ameiyms<br />
1 . Are the sample yyields-was<br />
asreounm msaut<br />
:, Were all Sample holding—me?<br />
I<br />
I I /<br />
3. Is the sampic Minimum Dcw=ble iC.tnN n Detmsm Limis^. I ,'}<br />
C QC Semple,<br />
Y^<br />
I ge LAvd l<br />
-CT ^ I^ ^<br />
L is the hi= 1eid wtthta as = atma I I I<br />
L is t he Micur..um Da --r •. .iCtnty :or the blank arta<br />
S th Ca Damson<br />
I I -<br />
3. is the Mark ^11 < L- :he Can== _-aecvon Irma? I /sue I _<br />
a. Is the oiu > I,: Itta Camas ',?ct¢:ton L .Vt but < C. Doccum Lunt?<br />
3. IS the D[wk : It > the Cams.-. C
Richland Laborato ry<br />
Quanterra Data Review Check List<br />
Work Order Number(sl: 9'U3<br />
Lab Sample Numbers or SDG: ^Z / 7<br />
Method/TestiParameter. e^f^<br />
A. Initial Calibration<br />
METALS<br />
vyZ ^^<br />
Review Item<br />
1. Performed at required frequency wih required number of levels?<br />
2. Correlation coefficient within QC limits?<br />
3. Initial calibration ve rification (ICV) analyzed immediately after calibration<br />
and results within QC limits? V<br />
4. Initial calibration blank(ICB) analyzed immediately after ICV and<br />
concentrations of all paramete rs < reporting limit?<br />
B. Continuing Calibration<br />
1. CC V analyzed at required frequency and all parameters within QC lirnits?<br />
2. CCB analyzed at required frequen cy and all results < reporting limit?<br />
C. Sample Analysis<br />
1. Were any samples with concentrations above the linear range for any parameter<br />
diluted and reanalyzed?<br />
Yes<br />
V)<br />
No<br />
(V)<br />
N/A 2nd Level<br />
Review ( 3 ^<br />
2. Were all sample holding times met? i<br />
D. QC Samples<br />
1. All results for the preparation blank below limits?<br />
2. MS or MS/NISI) recove ries within QC limits and n/aRPD (forMSD) acceptable ^C<br />
3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable?<br />
4. Analytical spikes within QC li<br />
mits where applicable?<br />
S. ICP only: One se rial dilution performed per SDG?<br />
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy ?<br />
7. ICP only: Interference check samples GCSA, ICSAB) and FECAL analyzed at the<br />
re uired fre uencies and within 9C limits?<br />
page 1 of 2<br />
606
E. Other<br />
1. Are all nonconformances included and noted?<br />
2. Is the cormct date and time of analysis shown?<br />
Review Item ( Yes<br />
( ^)<br />
3. Did the analyst sign and date the frmt page of the analytical tmm?<br />
4. Correct methodology used?<br />
5. Transcrip tions chocked?<br />
No<br />
(V)<br />
N/A 20 Level<br />
Review (^)<br />
6. Calculations checked at minimum frequenc y? 3 ^/<br />
7. Units checked?<br />
Comments on any "No" response:<br />
Analyst: Kw Lz e 7 ^ ^O n ^ Date:<br />
Second-Level Review: 12 Ie Date: 3/4/"<br />
Form No. CG-191. Rev. 2,1/97<br />
page 2 of 2 Go b<br />
i
Richland Laborato ry<br />
Qanter a Data Review Check List<br />
METALS<br />
Work Order Numberts): 31ffzl S7 3)11<br />
Lab Sample Num bers or SDG: u/ .^275 4J 0<br />
Method/Test/Parameter. U+lo ur?L L Tl?-47f<br />
A. Initial Calibration<br />
1. Performed at required frequency wih required number of levels?<br />
2. Correlation coefficient within QC li<br />
mits?<br />
Yes No N/A 2"d Level<br />
Review Item Review (^)<br />
3. Initial calibration ve rification (ICV) analyzed immediately after calibration<br />
and results within QC limits? L/ j<br />
4. Initial calibration blank(ICB) analyzed immediately a fter ICV and J<br />
concentrations of all parameters < repor ti ng limit?<br />
B. Continuing Calibration<br />
L CC V analyzed at required frequency and all parameters within QC limits?<br />
2. CCB analyzed at required frequency and all results < repot ting limit?<br />
C. Sample Analysis<br />
1. Were any samples with concentrations above the linear range for any p arameter<br />
diluted and reanalyzed? v i'<br />
2. Were all sample holding times met?<br />
D. QC Samples i<br />
1. All results for the prepara ti on blank below limits?<br />
2. MS or MS/NiSD recove ries within QC limits and °/aRPD (for MSD) acceptable ^F<br />
3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable?<br />
4. Analy tical spikes within QC limits where applicable?<br />
5. ICP only: One se rial dilu tion performed per SDG?<br />
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy ?<br />
7. ICP only: Interference check samples (ICSA, ICSAB) an d MCAL analyzed at the<br />
required frequencies and within limits?<br />
—I<br />
page 1 of 2 GUI U
E. Other<br />
1. Are all nonconformance included and noted?<br />
2. Is the correct date and time of analysis shown)<br />
3. Did the analyst sign and date the front page of the analytical run?<br />
4. Correct methodology used?<br />
5. Transcriptions checked?<br />
6. Calculations checked at minimum frequency?<br />
7. Units checked?<br />
Comments on any "No" rssponsc:<br />
Analyst: -^?C, Lg_ '7^) ^G<br />
^ ^<br />
^)<br />
Second-Level Review: 1/7?^^34/j/^<br />
Form No. CG-191. Rev. 7, 1/97<br />
Review Item Yes No N/A 22° Level<br />
Review (/)<br />
Date: 3//l /9e<br />
Date: 31191?^<br />
page 2 of 2 [ ^! 1
Richland Laboratory<br />
Quanterra Data Review Check List<br />
METALS<br />
Work Order Numher(s): Q a2 ] 9 7<br />
Lab Sample Numbers or SDG: /V 2 2-7 S t &-)C2291<br />
Method/Test/Parameter: Qk*t, L - rr<br />
A. Ini tial Calibration<br />
Yes No N/A 2°d Level<br />
Review Item (1) Review (V)<br />
1. Performed at required frequency wih requited number of levels? 3 /<br />
2. Correlation coefficient within QC limits?<br />
3. Initial calibration ve rification (ICV) analyzed immediately after calibration<br />
and results within QC limits?<br />
4. Initial calibration blank(ICB) analyzed immediately after ICV and<br />
concentrations of all paramete rs < repor ti<br />
ng limit? / _I<br />
B. Continuing Ca lib<br />
ration<br />
1. CCV analyzed at required frequency and all parameters within QC limits?<br />
2. CCB analyzed at required frequency and all results < reporting limit?<br />
C. Sample Analysis<br />
1. Were any samples with concentra tions above the linear range for any parameter<br />
diluted and reanalyzed?<br />
2. Were all sample holding times met?<br />
D. QC Samples<br />
1. All results for the prepara tion blank below limits? j<br />
2. MS or MS/NiSD recove ries within QC limits and °/aRPD (for MSD) acceptable?^^^<br />
3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable?<br />
4. Analytical spikes within QC limits where applicable?<br />
5. ICP only: One serial dilu tion performed per SDG?<br />
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency?<br />
7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the<br />
required frequencies and vvithin C limits?<br />
page 1 of 2<br />
8 4<br />
60"tZ
E. Other<br />
1. Are a ll nonconformances included and noted?<br />
2. Is the correct date and time of analysis shown?<br />
3. Did the analyst sign and date the from page of the analy tical run?<br />
4. Correct methodology used?<br />
5. Transc riptions chocked?<br />
Rem Item Yes No N/A 224 Level<br />
Review (V)<br />
6. Calculations checked at minimum 5squmcy?<br />
7. Units checked? j<br />
Comments on any "No" m6ponse:<br />
Analyst: ^Q7^P ` 41<br />
d 3<br />
Second-Level Review: ^al^f p<br />
Form No. CG-191. Rev. 2, 1/97<br />
Date: 3 z/ fzpz<br />
Date: 31145<br />
page 2 of 2 6 0 7 3<br />
I
Richland Laborato ry<br />
Quarteim Data Review Check List<br />
METALS<br />
_^b!_31 i srLf ^_<br />
Work Order Num ber(sl: ZbL gp<br />
Lab Sample Numbers or SDG: ^^ W O<br />
Method/Test/Parameter:<br />
A. Initial Calibration<br />
1. Performed at required frequency wih requited number of levels?<br />
2. Correlation coefficient within QC limits?<br />
Yes No N/A 2°a Level<br />
Review Item (`) Review (v)<br />
3. Initial calibration ve ri fication (ICV) analyzed immediately after calibration<br />
and results within QC limits?<br />
4. Initial calibration blank( ICB) analyzed immediately after ICV and<br />
concentrations of all parameters < reporting limit?<br />
B. Continuing Calibration<br />
1. CCV analyzed at required frequen cy and all parameters within QC limits?<br />
2. CCB analyzed at required frequency and all results < repor ting limit?<br />
C. Sample Analysis<br />
L Were any samples with con centrations above the linear range for any p arameter<br />
diluted and reanalyzed? v<br />
2. Were all sample holding ti<br />
mes met?<br />
D. QC Samples<br />
L All results for the prepara tion blank below limits?<br />
2. MS or MS/MSD recove ries within QC limits and °/d2PD (for MSD) acceptable? py<br />
3. LCS percent recove ry within QC limits and %RPD (for LCSD) acceptable?<br />
4. Analytical spikes within QC limits where applicable?<br />
5. ICP only: One se rial dilu tion performed per SDG?<br />
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency ?<br />
7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the<br />
re aired fre uencies and within C limits? `/<br />
I<br />
3<br />
i ^^<br />
page 1 of 2 60! 4<br />
—i<br />
_r<br />
P,
E. Other<br />
1. Are all nonconfonnances included and noted?<br />
Review Item Yes<br />
( ^)<br />
2. Is the correct date and time of analysis shown? 3<br />
3. Did the analyst sign and date the front page of the analytical rm?<br />
4. Correa methodology used?<br />
No<br />
(^)<br />
NIA<br />
(^)<br />
221 Level<br />
Review ( 3 )<br />
5. Transcriptions checked? 3 j<br />
6. Calculations checked at minimum frequency? 4<br />
7. Units checked? C7<br />
Comments on any "No" response:<br />
Analyst: y O'XC e- ^o^ 0 Date: 3/ ( 8/ p k<br />
Second-Level Review: ^^1. ^
Richland Laboratory<br />
Quanterra Data Review Check List<br />
N =ALS<br />
Work Order Numbedsl: 8C 3<br />
Lab Sample Numbers or SDG: &. b :-^ a O<br />
Method/Test/Parameter. y)<br />
A. Initial Calibration<br />
1. Performed at required frequency wih required number of Levels?<br />
2. Correlation coefficient within QC limits?<br />
Yes No N/A 2"d Level<br />
Review Iten (V) Review (^)<br />
3. Initial calibration veri fication (ICV) analyzed immediately after calibration<br />
and results within QC limi ts?<br />
4. Initial calibration blaak(ICB) analyzed immediately after ICV and i<br />
concentrations of all paramete rs < reporting limit?<br />
3<br />
I<br />
B. Continuing Calibration<br />
L CCV analyzed at required frequency and all parameters within QC limits? / 3<br />
2. CCB analyzed at required fn quen cy and all results < reporting limit? 3 —^<br />
C. Sample Analysis<br />
1. Were any samples with concentrations above the linear range for any parameter<br />
diluted and reanalyzed?<br />
2. Were all sample holding times met?<br />
D. QC Samples —i<br />
L All results for the preparation blank below limits? t/ v<br />
2. MS or MS/MSD recove ries within QC limits and %RPD (for MSD) acceptable4 ov v<br />
3. LCS percent recove ry within QC li<br />
mits and %RPD (for LCSD) acceptable?<br />
4. Analy tical spikes within QC limits where applicable?<br />
5. ICP only: One serial dilution perfo rmed per SDG?<br />
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy?<br />
7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the j<br />
required frequencies and within QC limits? 3<br />
3<br />
3<br />
—<br />
3 i<br />
page 1 of 2 / U
E. Other<br />
Review Item Yes<br />
(3)<br />
1. Are all nonconformances included and noted? 3 j<br />
2. Is the correct date and time of analysis shown?<br />
3. Did the analyst sign and date the front page of the analytical run?<br />
4. Correct methodology used?<br />
5. Transc riptions checked? i<br />
6 Calculations checked at minimum frequency?<br />
7. Units checked?<br />
Comments on any "No" response:<br />
Analyst: Date: ,311 p k<br />
Second-Level Review: /),^ Date: 3 . 1-191y F<br />
Form No. CG-191. Rev. 2. 1/97<br />
No<br />
(-01)<br />
N/A<br />
(3)<br />
2=d Level<br />
Review ( 3 )<br />
page 2 of 2 li 0 i i
Richland Laborato ry<br />
^w° ` alters Data Review Check List<br />
METALS<br />
Work Order Num ber{s): Yo y y<br />
Lab Sample Numbers or SDG: 14,0 ,,?Q75<br />
Method/Test/Parameter. C & ^j Q<br />
A. Initial Calibra tion<br />
Review Item<br />
1. Performed at required frequency wih required num ber of levels?<br />
2. Correlation coefficient within QC limits?<br />
3. Initial calibration verification (ICV) analyzed immediately after calibration<br />
and results within QC limits? j<br />
4. Initial calibration blank(ICB) analyzed immediately after ICV and<br />
concentrations of all parameters < reporting limit?<br />
B. Continuing Calibration<br />
L CCV analyzed at required frequency and all parameters within QC limits? t,-'<br />
2. CCB analyzed at required frequency and all results < repor ting limit?<br />
C. Sample Analysis<br />
1. Were any samples with concen trations above the linear range for an y parameter<br />
diluted and reanalyzed?<br />
2. Were all sample holding times met?<br />
D. QC Samples<br />
L All results for the prepara tion blank below limits?<br />
2. MS or MS/NISD recoveries within QC limits and %RPD (for MSD) acceptable?; p'k<br />
3. LCS percent recove ry within QC limits and %RPD (for LCSD) acceptable?<br />
4. Analytical spikes within QC limits where applicable?<br />
Yes No N/A 2°a Level<br />
Review (^)<br />
5. ICP only: One serial dilu tion performed per SDG? ^1<br />
3<br />
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency?<br />
7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the<br />
required frequencies and within 2C limits?<br />
page 1 of 2 Go! u<br />
i
E. Other<br />
1. Are all nonconformances included and noted?<br />
2. Is the correct date and time of analysis shown?<br />
Review Item Yes<br />
( ^)<br />
3. Did the analyst sign and date the fiont page of the analy tical tun?<br />
4. Correct methodology used?<br />
5. Transcrip tions checked? 3<br />
No<br />
(^)<br />
N/A<br />
(^)<br />
2—d Level<br />
Review (V)<br />
6. Calculations checked at minimum frequency? 3 i"<br />
7. Units checked?<br />
Comments on any "No" response:<br />
Analyst: `,(^ X Le j1/^12a1^<br />
Second-Level Review:<br />
Form No. CG-191. Rev. 2. 1/97<br />
page 2 of 2<br />
Date: 3 //L ^rfR<br />
Date: 3//E<br />
Go -, J
Richland Laboratory<br />
Quante"a Data Review Check List<br />
METALS<br />
Work Order Number(sl: X '.<br />
lab Sample Numbers or SDG: U) L2275<br />
Method/Test/Parameter: '<br />
A. Ini tial Calibration<br />
1. Performed at required frequency wih required num ber of levels?<br />
2. Correlation coefficient within QC limits?<br />
Yes No N/A 2°d Level<br />
Review Item Review ( 3 )<br />
3. Initial calibration ve rification (ICV) analyzed immediately after calibration<br />
and results within QC limits?<br />
4. Initial calibration blank(ICB) analyzed immediately after ICV and<br />
concentrations of all parameters < reporting limit? 3<br />
B. Continuing Calibration<br />
1. CCV analyzed at required frequency and all parameters within QC limits?<br />
2. CCB analyzed at required frequency and all results < repor ting limit?<br />
C. Sample Analysis<br />
I. Were any samples with concen tra ti<br />
ons above the linear range for any parameter<br />
diluted and reanalyzed?<br />
t/ 3<br />
2. Were all sample holding ti mes met? j<br />
D. QC Samples lj<br />
1. All results for the prepara ti<br />
on blank below limits?<br />
2. MS or MSQvISD recove ries within QC li<br />
mits and °/dtPD (for MSD) acceptable?!! 1 F<br />
3. LCS percent recovery within QC limits and °/gRPD (for LCSD) acceptable? I I —^<br />
4. Analytical spikes within QC limits where applicable? 3<br />
5. ICP only: One serial dilu tion performed per SDG? 3 j _<br />
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy?<br />
7. ICP only: Interference check samples (ICSA, ICSAB) an d MCAL analyzed at the Lj<br />
re uired fre uencies and within C limits?<br />
page 1 of 2<br />
^.<br />
_I<br />
G 0 j 0
E. Other<br />
1. Are all nonconformances included and noted?<br />
2. Is the correct date and time of analysis shown?<br />
Review Item Yes<br />
(^)<br />
3. Did the analyst sign and date the front page of the analytical run?<br />
4. Correct methodology used?<br />
5. Transcriptions checked?<br />
6. Calculations checked at minimum frequency?<br />
7. Units checked?<br />
Comments on any "No" response:<br />
Analyst: 41 z i_e_ `7 ^0.^1<br />
^<br />
^^ ""<br />
Second-Level Review: r pt A&d<br />
Form No. CG-191. Rev. 2, 1/97<br />
page 2 of 2<br />
Date:<br />
3<br />
No<br />
V)<br />
Dater IZ P%<br />
NIA 29° Level<br />
Review V)<br />
/<br />
V0$t
CHAIN OF<br />
CUSTODY FORMS
C_<br />
C<br />
or<br />
v<br />
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -01 Page 1 of !<br />
Collector Company Contact Telephone No. Project Coordinator Data Turnaround<br />
R. Fahlberg Steve Ma rske 373 4 316 WEISS, RI.<br />
21<br />
Project Designation Slorpling Location SAF No. Days<br />
105-C Phase I & Phase If -Concrete Samples 100 Area B98-061<br />
Ice Chest No. Field Logbook No. Method of Shipment<br />
_^ - - C, — Iland deliver<br />
Shipped 'I (I<br />
Quanterra Incorporated<br />
Olfsite Perty rop No. Bill of Lading/Air Bill No.<br />
POSSIBLE SAMPLE IIAZARDS/REMARKS<br />
Radw.,m, c<br />
Sproul llandling and/or Sloragc<br />
SATIPLE ANALYSIS<br />
^^ Preservation<br />
rv^ae<br />
Type of Container p<br />
No. of Cnnlainer ( s) -<br />
Volume \'<br />
(^/^ Sa i¢m 111 In<br />
^ J 'L<br />
SPed.l<br />
Imwnio^s<br />
Ci ^^^^J<br />
w<br />
11-<br />
Sample No Matrls• Sample Date Santple'fime s"'td v ^. qti` a5„tY [:'••^:, jg .r'n'3!^* , sl'^.rlt'°,:. 'f.^s '^a i aa q^%',`:-<br />
C,<br />
L<br />
BON680 CI Other Solid<br />
S<br />
SPEI LAI. INS 11 4 IRONS Matrix<br />
111 %IN III I'IOSSI..SSIOV Sign/Print Nawr.<br />
III I( -I' hlc0a6- 60 ttA lSupal0accl l eudl, Mcauq - 9421 - (CV ) , C6rumnmin llt, " 7146,<br />
s<br />
sk<br />
_<br />
-<br />
s,,d<br />
sa.linan<br />
I(LIlP1 .Lcdlly (I - Y•/- D1 Iuuc Rua dIII<br />
-2 O<br />
U I..... Pill, 8080,iAi 1<br />
I 0 . I I54, I. 0 I<br />
1 ill.tia 0a S,,,,ou..ulY (e 0137,<br />
1551"A a .. 0 24I I 0 ryi. I Wlu 0wn<br />
bait6(11<br />
I mpie Il y a<br />
Vi t 152<br />
n . SO,<br />
sU<br />
si.<br />
-<br />
sWi4<br />
61,dae<br />
of na1 + 0 0lcluu^ 14c uJlq<br />
^^<br />
10e1f5111uu<br />
- ^^(^ } C` `j 9<br />
. Mi LrCI<br />
r a ,j^0.1<br />
L3 Sr- 90 EDIT l Sr<br />
1, ¢^t s<br />
A<br />
" V , Can<br />
141w 1 uuLed 11 1Ito, nue wl scd it, I>.em' Inn e v q<br />
I(c<br />
^^<br />
.<br />
a<br />
i<br />
m<br />
UI<br />
I<br />
-<br />
nil<br />
a s " I m<br />
ho-<br />
III - 111pe<br />
hall uyw.Lcl I10 U.uc l un. I(cco.cd II Ill.nc l llv. I I w ^<br />
11111110A 111111 It nr.l Ito Iltic Uam^l lnm<br />
St( IOUs<br />
FIN'AI SVAII'Lf. 14 1.Iki'll 111.1 .0111, Ilalc/I inm<br />
I IISI'IISI I IfIN
C<br />
cc:<br />
li.-<br />
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -02 Page I of<br />
-'olleclor Company Contact Telephone No. Project Coordinator Data Turnaround<br />
R. Fahlherg Steve Marske 373 -4316 WEISS, RL<br />
21 Days<br />
Project Designation Sampling Location SAF No.<br />
103-C Phase 1 & Phase II -Concrete Samples 100 Area B98-061<br />
Ice Chest No. Fie ld Logbook No. Method of Shipment<br />
Hand deliver<br />
'hipped To Mile Properly Bill of Ladin Air Bill No.<br />
Quanterra Incorporated<br />
POSSIBLE SAMPLE IIAZARDS/11EAIARKS<br />
Radioaclim<br />
S pecial Ilandling and/or Storage<br />
SANIPLE ANALYSIS<br />
Prese valion<br />
None<br />
Type of Container P<br />
No. of Container(s) Z<br />
Volume<br />
IL<br />
sw acm t 11 In<br />
speci al<br />
m,wnrnns<br />
Sample No Mali:y • Sample Date Sample Time }-^ _, ` `.I z, =,gyp' = • s -:t(do. -<br />
BON681 j, -^ Other Solid — 3 ' ^," Z<br />
I SPF.CIA I. INSIRI C"II ONS Matrix<br />
HAIN OF PO SSE SSION<br />
ItcLw uuhcJ e" Dnm"Imo<br />
Sign/Print Names<br />
Re
Environmental<br />
Contractor<br />
Contractor<br />
Visa<br />
Team<br />
Interoffice Memorandum<br />
M.<br />
'.nrna!<br />
D. A. St. John r.0-19<br />
See Below<br />
°"M 1'ebruary 27.1999<br />
rtiaa S. L. Winslow<br />
RadCun Engineering<br />
X3-41/531-0700<br />
susurcr: CURIF ESTIMATE FOR S111PP1NGCON[:RETF. CORE SAMPLES<br />
CotQatration (obi/e)<br />
2.55 pCilg<br />
1.2F3 pCi/g<br />
4.95 pCi/g<br />
7.5E-1 pCi/g<br />
2.550 pCifg<br />
7.5E-2 pCi/g<br />
1.5 1<br />
1.46L'3 pCi/g<br />
CCN: 055088<br />
Job No. 22192<br />
Wnm•A.av Ap<br />
Div w•<br />
a, ion<br />
nn v<br />
c•n wn<br />
Swwn Cob Im<br />
The 1i111uwing calculations show that core sample: with a direct reading of equal to or Icss than<br />
400.000 dpm/1Merin' will be below the definitionorrulivactive material as defined in 49 CFR 173.403<br />
of 70 Bq/g (2F.3 pCi/g). Each sample will consist of contxete material from four, two inch core<br />
samples and enough water to arike a slurry consismacy. 'the distribution of radionuclides is hued on<br />
previous concrete samples rakcn from the below gtadie Fuel Storage Basin that would also he<br />
representative of these concrcec samples.<br />
(jiven:<br />
Cyiinder Volumc = itA Radius of concrete core (r) = I inch<br />
Concrete Density = 2.35 g/em' Height of cam sample taken (h) - 0.25 inches<br />
27 pCi = Dq Maximum 5rn:1 reading on core = 400,000 dpna/ I OOcm'<br />
2.'_2 dpm = pCi<br />
Calculations:<br />
V — (3.14) (1 in.)'(0 25in) = 0.78 in' (16.4 ciOin-' (4 con: samples) = 51.2 cm'<br />
(400,000 dpm/51.2 cm) (cm'/2.35 g) = 3.32E3 dpVg<br />
3.321:3 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g<br />
SI.W:dld<br />
°Co<br />
Percent Distribution(`7)<br />
0.17<br />
"'cs<br />
432<br />
EU<br />
82<br />
0.33<br />
1"Eu 0.05<br />
90Sr 17<br />
7Ai Ain 0.005<br />
239'rx'Pu<br />
0.1<br />
TU rAr-:<br />
('epics:<br />
S. 0. Marske X5-53<br />
P. A. Newman X3141<br />
RadCun Engineering file/LB XO-23<br />
<strong>Document</strong> and Into Services 010-09<br />
'0<br />
0085
Environmental<br />
Restoration ERC Team<br />
Contractor<br />
Interoffice Memorandum<br />
TO' D. A. St. John I.0-19 LATE: l-ebruary 27. 1998<br />
"O''' F'` ' See 13clow<br />
FROM:<br />
* Av<br />
S. L. Winslow<br />
RadCon Enginuing<br />
X3-41/531-0706<br />
suwECT: CURIE ESTIMATE FOR SHIPPING CONCRETE CORE SAMPLES<br />
Concentration_(^Ci/;><br />
2.55 pCi/g<br />
I.2F.3 pCi/g<br />
4.95 pCi/g<br />
7.5E-1 pCi/g<br />
2.55E2 pCi/g<br />
7.5F.-2 pCi/g<br />
1.5 2C.Ug<br />
1.46E3 pCiig<br />
Job No. 22172<br />
wnan 0.epmrRpu.N .nU<br />
P+Ow w^<br />
I 1 V w/,<br />
W n l0,<br />
CCN: 055081;<br />
s^+l..,cw. !Fw<br />
The ibllowing calculations show that core samples with a direct reading of equal to or less than<br />
400,000 dpm/100cm' will be below the definition of radioactive mate rial as defined in 49 CFR 173.40±<br />
of 70 Bq/g (2F3 pCi/g). Lach sample will consist of concrete materi al from [our. two inch core<br />
samples and enough water to make a slurry consistency. 'fhe dislrihution cdmdionuclides is based on<br />
previous concrete samples taken front the below grade Fuel Stora ge Bas in that would also be<br />
representative of these com:rctc samples.<br />
'ven:<br />
Cylinder Volume = nr'h Radius of concrete core (r) = I inch<br />
Concrete Density = 2 3 5 ylem' Ileight of care sample taken (h) - 0.25 inches<br />
27 pCi = Bq Maximum direct reading on :ore = 400.00 0 dpnl/lUUcn1`<br />
2.22 dpm = pCi<br />
Calculations:<br />
V - (3.14) (1 in.) 2( 0.25in) = 0.78 in' (16.4 can `/in) (4 cure samples) = 51.2 cm'<br />
(400.000 dpm/51.2 cm) (cm'2.35 g) = 3.32E3 dpm/g<br />
3.3213 dpnn'g (pCi/2.2 dpm) = 1.5E3 pC'i/g or 55.4 Bq/g<br />
SI VAld<br />
Percent Distribution( 7o )<br />
'"Co 0.17<br />
"'Cs 82<br />
1 1 Lu 0.33<br />
"°Eu 0.05<br />
"°Sr 17<br />
'°' Arn 0.005<br />
"°'="'Pu 0.1<br />
TOTAL<br />
Copies:<br />
S. 6. Marske X5-53<br />
P. A. Newman X3-41<br />
RadCun Enginee ri ng File/LB XO-23<br />
<strong>Document</strong> and Info Se rvices 110-09<br />
V^^O
F%jwI 1<br />
SAMPLE CNECX-IN LIST<br />
CaterTime Received: . ^ 151 SG*<br />
wcnc Order Number L' ? i ( ^' ^(GI Say 1R- C^^ ^I<br />
Shipping Container IDk l SJ^ Chin dCustody;<br />
RFSHSOw-93-0003 -<br />
Revision<br />
^1<br />
(1 ^^' l<br />
1. Custody Sealsaod*Ong , I i ktar Yes IC II<br />
2 Custody Seals d*d and signed? Yes K,40 No I 1<br />
3. Chain-of-Custody recatd presenO<br />
GC<br />
Yes I 1<br />
4. Caalet temperaftae<br />
5. Vennici telpad* materials is Wet ( ; 3rY ( l<br />
6.<br />
Number of samples in shipping corainer<br />
7. Sample holding Imes exceeded? Yes [ ; No I 1<br />
8. Sammhave<br />
tape hazard Labels<br />
seats appropriate sample labels<br />
9. samples are_<br />
_SLm good wnd ition lealdng<br />
broken _ have air bubbles<br />
10. Where any anomalies identified in sample receipt?<br />
11. Cescsiption of mana lies (nude sample numbers)_<br />
Sample Custcdianllabaatorl '^ Date_<br />
Yes I 1 No I<br />
Telephoned To: Ongy<br />
IA<br />
60S;
Frlrr 1<br />
SAMPLE CHECK-IN UST<br />
DateMme Received: SG#:<br />
^^c ^ sc ar-^--aoo_ -<br />
4" Sion<br />
Work Crder Number. l'^ ^^ SAF #:-<br />
Shipping Container ID: U d chair of Custody # I ^ (J - ^^ ^^<br />
1. Custody Seals an shipping contain ritW. Yes I I<br />
2 Custody Seals dated and signed? Yes ( No [<br />
3. Chain-of-Custody record present? Yes
Client Sample Screening Results<br />
I D-Mar-98<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
BII ON14CI 3/9/19981:42:00 P7)2 1A 3/10/199811:23:38 BOM4CI<br />
(QUID 1HI+kg,<br />
3/10/1998 ^ :51 ANI BKG<br />
An]D t /10/1998 ' ,Alq: 5.00E-01 01 (Dpm/ 5.49E-01 (uCl/ 1.24E-0j<br />
,-Ppt mg:2.1 Unita: L Bet; ): 5.42E+01 So);--J.hE-0 3<br />
DI11 130 1,14C2 3/9/19981:42:00 PM QUAD2 1 B 3/101 19981123:38AN1 BON14C2<br />
LIQUID Bkg: 3/10/1998 8:43:51 A BKG<br />
A nI Dgt : 3/10 ToI Sr, AIy: 5.00E-0^ OE+01 Alp; (Dp V 738 -0 (uCU 8.07E-06<br />
/Pptmg: 2.6 Inks: /L m Bet( ,-^q): I.IIE+01 2.51E-04.<br />
30 16 9.49333333 841 27.233333<br />
i<br />
100 4 0.04 0 0.8<br />
2.47E+01 ± 2.3E+01 CAT OE+00 1.<br />
LIg )i 1'44+03 3 8.7E+01 I 2A ^^^L`^<br />
w 6<br />
0.03<br />
(p 1.6 01 ± 2.4E<br />
Llg): 5.01E+02 .3E<br />
202 833333 -<br />
95 "-^ 0.95<br />
4T E+00 Lob<br />
I Alq<br />
11111 BON680S 3/9/1998 1:42:00 PM QU kD24D 3/1 0/'199811:23:51 AN1 BON680S<br />
30 1130 37.6066667 124390 4145.4333<br />
90G 100 6 0.06<br />
0.9<br />
I SOLID Bkg: 3/10/19988:43:55AN1 BKG<br />
AN Dote: 3/10/1998 Tot Sa,Alq: 1.63E+02 9.81E+01 Alp; (Dpm/ -1.71E+01 (uCU 4.27E-02 (pCV .7.83E+01 ±9.4E+00 CAT 1.6E+02 Lab<br />
Ppt mg: 98.1 / UNta:g mg Bel; Alq): 9.19E+03 So): 6.86E+00 Ljg): 4.22E+04 ± 1.2E+02<br />
III<br />
2.4E-03<br />
14c I-IC<br />
DIII BON681P 3/9/19983:15:OOPM QUAD2IA 3/10/199811:54:54AN1 DON68IP 30 5 0.12666667 96 2 4<br />
G a LIQUID Bkg: 3/10/1998 8:43:51 AN1 BKG 100 4 0.04 80 0.8<br />
An] Dote: 3/10/1998 Tot So, Alq: 1.80E+00 100E+01 Alp; ( )pm/ 3.23E-0 1 (uCU 2.62E-05 (pCU 1.45E+01 ± 2.4E+01 CAT 1.7E+00 lab<br />
I-pt mg: 69 Units: 1. / ml Bel; Alq): 4.79E+00 So): 3.88E-04 Ljg): 2.16E+02 ± 3.1E+01 I 2.3E-0t<br />
Alq<br />
BIII BON681S 3/9/19983:15:00 PM QUAD21B 3/101199811:54:54 AM BON681S 30 13 0.40333333 234 6.85<br />
GSOLID Bkg: 3/10/19988:43:51 ANt BKG 100 3 0.03 95 0.95<br />
AN Date: 3/10/1998 3'ot Sa,A1q: 1.90E+02 1.1511+02 Alp; (Dpnt/ 2.58E+00 (uCU 1.93E-03 (pCU 1.02E+01 ±5.5E+00 CAT 4.9E+00 lab<br />
Ppt mg: 114.5 Unite: g / mg Bet; Alq): 1.55E+01 So): 1.16E-02 Llg): 6.09E+01 + 4.6E+00 I , 1.6E+00<br />
DIII 13ON6801 : 3P)/19981:42.001'M QUAD24C 3/10/199811:23:51 AN1 11ON680P 30 43 1.39333333 3426 11339<br />
LIQUID llkg: 3/10119988:43:55 AM BKG 100 4 0.04 81 0.81<br />
AnlDate: 3/10/1998 'Pot Sa,Alq: 1.80E+00 LOOLWI Alp; (Dpntl 4.48E-0 1 (uCU 3.64E- 0 5 (pCU 2.02E+01 +2.2E+01 CAT 1.2E+00 tab<br />
Pp( mg; )A /^ Unite: I. nJ IRq Alq): 2.141:+02 So): 1.74E-02 Leg): 9.66E+03 + 1.7E+02 1 5.2E-03<br />
r<br />
^<br />
'^I i^ 1) 9. Y , '17 1, I cA^4<br />
O 0-.4/nr-9N QDanterra Environment Se rvices, SCP V2.03<br />
CO )<br />
Alq<br />
Ids<br />
I'll:
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-o61-03 vase ! '/ !<br />
ullectur Company Contact Telephone No. Project Coordinator Data Turnaround<br />
R. Iahlhcr,<br />
Project Pro Designation<br />
I Des i ,<br />
Steve Niarske<br />
Sampling Location<br />
373 -4316 WEISS, RL<br />
SAF No.<br />
21 Days<br />
105 C Vhax 18' Phase II -Conercre Samples 1(111 Area 898-061<br />
Ice Chest Nu. Meld I. ,ghouh No. Method of Shipment<br />
L- L J r _ Hand deliver<br />
Shipprd IF, 011silr 1'roperty No. Bill of fading/Air Bill Nu.<br />
I luanwira lncorpofFacd n IF<br />
POSSIBLI. SAN11'LL IJAZAlt DS/REMARKS<br />
RaJioaa i.c<br />
Special Ilandlln8 and/or Sturaye<br />
Presen'atiun<br />
I)pe of Container<br />
No. of ('ontalner ( s)<br />
\'olmne<br />
(^^^ 'y^ ^''^<br />
111<br />
S:ANIP1.F 0%<br />
CIJLk>« -7,<br />
031 g ^a C^ c h i X0-5<br />
Sample No Nlalric Sample Dare Sample 'I 11 11 c<br />
BON682 Other Solid<br />
P<br />
IL<br />
sec uem (p m<br />
saeoal<br />
SPE('LU. INS IRE 'CI'IONS<br />
N1mriy<br />
I OI: POSNI.SSION ,'Ign/Prini Name,<br />
( 111( I N1n.d.-bnI''%'s .niF") ll aaJ l, Ntocl- w 74 71- I C V). C hmm moi l l° -119e,<br />
s<br />
SI.<br />
- soil<br />
- seammu<br />
1 cl Iqm ch
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -04 page 1 of !<br />
Collector Company Conlact Telephone No. Project Coordinator Rata -turnaround<br />
R. Fahlberg Steve Marske 373-0316 WEISS, RI,<br />
Project Resignation Sampling Location SAF No. 21 Days<br />
105-C Phase I & Phase II - Concrete Samples 100 Area B98-061<br />
Ice Chest No. Field Logbook No. Melbod of Shipment<br />
L.°L — l 3 C ) r — 2<br />
Hand deliver<br />
Shipped 1'.<br />
Quanerre Incorporated<br />
POSSIBLE SAMPLE IIAZARRS/REMARKS<br />
OBske Property No., .<br />
AL-11-4<br />
r+aa.<br />
Bill of Lading/Air Bill No.<br />
A'<br />
Radioacl,e<br />
Preservation<br />
'pecial handling and/or Storage<br />
SA MPLF. ANALYSIS<br />
'Iype of Container<br />
No. of Container(s) -<br />
Volume<br />
P<br />
IL.<br />
5.^ m01in<br />
SaCn1<br />
10'^^.°1O°`<br />
03193 Chi g0318^ Pao(-<br />
Sample No Matrix Sample Date Sample Time ^ni 1111, ^`-E .-+p ;, ^. M ,+ '#„n c fr v ' ,. S+}<br />
BON683 O^ Other Solid /lJ S D ^l r'j7 X '^ 9 _ t<br />
11 UN<br />
01 PO.SSI SSION<br />
It i.... ..aJ l^i /^^ ^^Ii^9 un<br />
^^^ o ^ 3<br />
11eWignnh d ll/<br />
SPF('L I. INS TI1VC110 11 S Mumix'<br />
Sign/Print Nwura S<br />
(I11(l'M
C<br />
l<br />
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-05 Page 1 of i<br />
Collector<br />
R. Fahlberg<br />
Company Contact<br />
Steve Marske<br />
Telephone No.<br />
373 -0316<br />
Project Coordinator<br />
WEISS, RL<br />
Data Turnaround<br />
Project Designation Sampling Location SAF No.<br />
21 Days<br />
105-C Phase I & Phase 11 - Concrete Samples 100 Area B98-061<br />
Ice Chest No. Field Logbook No. Method of Shipment<br />
4- L — / 3 2 [land deliver<br />
'hipped "I o Offske Property No. Bill of Lading/Air Bill No.<br />
Quanterra Incorporated<br />
POSSIBLE SAMPLE IIAZARDS/REMARKS<br />
Radioactive<br />
S pecial Handling and/or Storage<br />
SAMPLE ANALYSIS<br />
Preservation<br />
Type of Container<br />
No. of Container(s)<br />
Volume<br />
r+o^e<br />
p<br />
IL<br />
See Item ( 1) in<br />
Speaal<br />
Io:nom"'^`<br />
803183 ^^ gc^31^'4 ^^d<br />
Sample No Mavis Sample Date Sample Iime n^ 1L .E--;t' ry aii v`; ;/!<br />
BON684 3 Other Solid S/`/ `.r ^, `. '^ V<br />
CHAIN OF POSSESSIO N<br />
RJulgnuhnl n1 h,,, s^ U lc 5<br />
./^0< P<br />
RcLm mha fy IJeLL`I ic<br />
Rcllnqul>heJ 11 1 Dale Tmm<br />
Sign/<br />
i<br />
J Recce Ily<br />
Lcl.edIt,<br />
Remi.eJ Hp<br />
int Names<br />
/<br />
1lalel1lnm<br />
amfllme<br />
v Dm,Tlnle<br />
ti<br />
SPECIAL INSTRUCTIONS Ma tr ix<br />
s<br />
I R 1 1 Nlo, is b010A (Super ace) ILead); Mercup - 7471 -(CV), Chromuun flea -7196, SG<br />
IV II, 8080 ( All i 1211 1lice, t SI t sc P) (Ce'ium 1 V C ,bah-60, Europium I S'_. SO<br />
L uy'w -U.L 1'.......n-139;. Ai w ......n-24 1 Isotopic P wo iiu . Isuwpic t)mnu m. Sell SI<br />
-1 G N'<br />
"lPn (f(Is'1 - 19 N^ ^/-6^ Sr-^^ -/o- - u^ / Sr, U<br />
Teoh 17q (^ bon 14, , 46 71/( 'ly Sean 1)<br />
or<br />
I
Environmental<br />
Restorati on<br />
Contracto ERC Team<br />
Interoffice Memorandum<br />
zO D. A. St. John r.0-19 b"rz0 February<br />
27. 1999<br />
1"Y1• '` See Below<br />
l<br />
ncoa: S. L. Winslow<br />
RadCun EngUla:ring<br />
S1. W:dld<br />
to Co<br />
137 CS<br />
Percent Distribution(r/o)<br />
0.17<br />
82<br />
132EU<br />
ueEu<br />
0.33<br />
0.05<br />
"Sr 17<br />
741 Ain<br />
209/zwpu<br />
0.005<br />
0.1<br />
TOTAL:<br />
X.1 -41 1531-0700<br />
suuecr: CURIE. ESTIMATE FOR SHIPPING CONCRETF. CORE SAMPLES<br />
Job '49. 22192<br />
wwvwll^Mwsrw '10<br />
D,DW NA<br />
il ♦ www<br />
a' Vole<br />
R11<br />
caw vw<br />
CCN: 055082t<br />
The lirllowing calculations show that con; sampicswith a diner reading of equal to or less than<br />
400.000 dpm/IOOcm z will be below the definition of radioactive material as defined in 49 CFR 173.40:<br />
e<br />
of 70 Bq/g (2F3 pCi/g). Lath sample will consist of concret inaterial from four. two inch core<br />
samples and enough water to make a slung consistency. 'Ile distribution of radionuclides is haled on<br />
previous concrete samples taken from the below grade Fuel Storage Basin that would also be<br />
representative of these concrete samples.<br />
(jivgn::<br />
Cylinder Vulurm = nr'h Radius of camrlete corer) = I inch<br />
Concrete Density = 2.35 g/cm' Height of c:cee samplc talcen (h) - U.25 inches<br />
27 pCi = Bq Maximum dimt reading on core = 400,000 dpm/IUOcmz<br />
222 dpm = pCi<br />
Calculations:<br />
V-(3.14)(1 in.)-(025in) = 0.78in'(16.4cm'/irrj(4 core samples)=512 cm'<br />
(400.000 dpm/51.2 cm) (cm' 12.35 g) = 3.32E3 dp Wg<br />
3.321:3 dpm'g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 841g<br />
Conics:<br />
S. 0. Marske X5-53<br />
P. A. Newman X3 -4 1<br />
RadCon Engineering File/LB XO-23<br />
<strong>Document</strong> and Into Services 110-09<br />
Cotltsatration (tom/0<br />
2.55 pCifg<br />
1.2F3 pCi/g<br />
4.95 pCilg<br />
7.513 -1 pCi/g<br />
2.55E2 pCi/g<br />
7.5F.-2 pCi/g<br />
1.5 VQr<br />
1.461'3 PCi/g<br />
X090
Figure 1<br />
SAMPLE CHECK-IN LIST<br />
DateTme Received: 3C//11'0 ICES 14 t /^ SG#:_ ^ 2 ^^^^<br />
Work Order Number. 0 t ^^`T SAF #-<br />
Shipping Container 10: ^ C ^ h h6^ Chain of Custody # L - (L<br />
1. Custody Seals on shipping container intact?<br />
2. Custody Seals dated and signed?<br />
3. Chain•of-Custody record present?<br />
4. Cooler temperature<br />
5.<br />
Vermiculite/packing materials is<br />
6. Number of samples in shipping container.<br />
7. Sample holding times exceeded?<br />
8. Samples have:<br />
J tape hazard labels<br />
_custody seals app ro priate sample labels<br />
9. Samples are:<br />
V .n good condition leaking<br />
broken have air bubbles<br />
10. Where any anomalies identified in sample receipt? Yes f 1 No [ -,/<br />
11. Description of anomalies (include sample numbers):<br />
Sample Date:<br />
Telephoned To: On gy<br />
N,<br />
PFSH-SOW-93-0003<br />
Revision 5<br />
Yes [+40 11<br />
Yes ( `el^4o (1<br />
Yes ( No [ 1<br />
Wet [ 1 C ry tTr G-( ,<br />
Yes (I No (I<br />
LU9`
Client Sample Screening Results 3 l0<br />
10-Mar-98<br />
CLIENTCODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCPMB<br />
bhi BON682F 3/10/19981:05:00 PM QUAD2IA 3/10/19983:01:18PM BON682F 30 Is 0.56 69 1.5<br />
1<br />
/ I LIQUID Bkt: 3/10 1 1998 8:43:51 AM BKG 100 4 0.04 80 01<br />
A nt Date: 3/10/1998 Tut Sa, Alq: 1.80E 4 00 , LOOE+01 Alp; (Dpm/ 1.89E+00 (uCV 1.53E-04 (pCV 8.51E+01 ± 3.1E+01 CAT 2.9E-0 1 Lab<br />
_<br />
Ppl mt: 1 L5 Unite: L 3' , ml Bet; Alq): 2.79E+00 So): 2.26E-04 Lit): 1.26E+02 + 2.6E+01<br />
I I^<br />
4.0E-0f<br />
Alq<br />
ut<br />
Ant De / 0/1998 Tot a, Al 2.000<br />
pt m!;: j Un 13;/L<br />
1.00E+0 AI (DpM 0 L^+00 ( 'V O.00E (pCV .00E+00i* Num! CAT 3A)E+00 Lab<br />
I<br />
ml 1A; q): O.00Et00 )3^0.00E+00 LIlU :OOE00 ± qNu ! -^ 2.OE00<br />
1.<br />
Bill -BBN68'2S 3/10/19981:05:00 I'M QUAD2 1 B 31 10/19983:01:18PM DON682S 30 937 31.2033333 87485 2913.2167<br />
^O(o$3 5<br />
SOLID Bkp 3/10/19988:43:31 AM BKO 100 3 O.OI 93 0.95<br />
AM Date: 3/10/1998 ToISa,Alq: 2.00E+02 9.15E+01 Alp; (Dpn3 2.39E+00 (uCl/ 2.35E-03 (pC9/ 1.18E+01 +6.3E+00 CAT 4.3Et00 Lab<br />
Ppt nq: 91.5 1 1,11 13: g / m8 net; Alq): 6 49E43 Se); 6.39E100 LIt): 3.I9E 4 04 ± 1.1!102<br />
111<br />
'v_ 3.1 F.-03 Alq<br />
LIt<br />
Bill BON683F 3/10/19981:05:00PM QUAD2 1 C 3/10/19983: 01 :ISPM BON693F 30 127 4.13333333 9212 306.17667<br />
M LIQUID Bkg: 3/10/1998 8:43:51 AM BKG 100 10 0.1 89 0.89<br />
An] Date: 3/10/1998 Tot Sa, Alq; 1. 11 0E+00 1.00E+01 Alpi (Dpm/ 3.34E+00 (4C7/ 2.71E-04 (pCY/ 1.lIEw2 f3.4Ew 1 CAT 1.7E-0 1 4b<br />
Pptmt: 7 3 Units: 1, 3 ml Bet; Alq): 6.06E+02 So): 4.91E-02 Lit); 2.73E+04 ±2.8E+02 I (/LBE-0 7<br />
^C<br />
Bill BON683S 3/10/19981:05:00 PA1 QUAD2 11) 3/10/19983:01.18 PM LION683S 30 5 0.02666667 75 1.68<br />
g0^68as SOLID Bkt: 3/10/19988:43:51 AM BKG 100 14 0.14 82 0.82<br />
' 1 1 D Anl Datc 3/10/1998 Tut Se, Alq: 2.00E+02 J/<br />
8.53E+01 AI p; (DpM 6.13E-0 2 (uCY/ 6.30E-05 (pCY/ 3.23E-0 1 ± 3.3E+00 CAT 1.2E+02 Lob<br />
'll<br />
Pptmt: 85.3<br />
Units: g mg Bet; Alq): 3. 72E+00 Se): 3.93E-03 LIt): 1.96E+01 ±3.6E+00 I L S.IE+00 AIq<br />
I-It<br />
LI<br />
1 U-.1 far-98 Quanterra Environment Se rvices, SCP V2.83 I
(7--<br />
C)<br />
Client Sample Screening Results<br />
11-Mar-98<br />
®x)11 I^<br />
CLIENT CODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
Bill BON684 3/11/1998 QUAD2 1 A 3/ 11 /19989:5104AM BON684 30 9 0.23333333 109 27716667<br />
C -' LIQUID Bkg: 3/11/19992:34:24 AM BKO 600 40 0.06666667 517 0.8616667<br />
Anl Date: 3/11/1998 Tot So, Alit : 2.00E+00 1.00E+00 Alp; (Dpm/ 1.04E+00 (uCB 9.38E-04 (pCl/ 4.69E+02 ± 3.9E+02 CAT 5.3E-02 Lab<br />
Ppt sing: 49,7 Units: L ml Bet; Alq): 5.94E +00 Sa): 5 . 35E-03 LI8): 2.67E +03 ±3.4E+02 11.9E-02<br />
BHI BON783 3/11/1998 QUAD21H 3/11/19989:51:34AM BON783 30 6 0.14333333 35 0.2383333<br />
LIQUID Bkg: 3/11/19982:34:24 AM BKG 600 34 0.05666667 557 0.9283333<br />
Ant Date: 3/11/1998 Tot Sa, Alq: 1.00E+01 1.00E+01 Alp; (Dpm/ 4.39E-0 1 (uCt/ 1.98E-04 (pCl/1.98E+01 ±2.IE+01 CAT 1 .3E 400 Lab<br />
Pptme: 0 Units: L , ml Bet; Alq): 3.72E-01 Ss): 1.68E-04 LI8): 1.68E+01 ± 1.7E+01 I 3 .0E+00 LIC<br />
C) 11-Mar-98 Quanterra Environment Se rvices, SCP V2.03 1<br />
'Iq
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST 698-061-06<br />
Collec Compan) Contact Telephone No. Project Coordinator Data Turnaround<br />
It Pahlbcrg ^(,(<br />
Steve N1a rske 373-4316 WEISS. RI_<br />
Project Designation trampling Location 'AF No.<br />
105-C Phase I k Phase II - Concrete Samplcs 100 Area B98-061<br />
Ice If No. Field Logbook No. Method of Shipment<br />
— Z<br />
hand de li ver<br />
Shippcd'IL ll,kc Property No. Bill of La t in /Air Bill Nu.<br />
Quanlerru h 1 c0rpnmlad<br />
POS9BLL SAMPLE IL\ZARDSBEM:A RKS<br />
Itadluaclne<br />
Jpecial Han dling and/or Storage<br />
Presen'alion<br />
Iypc of Container<br />
rA<br />
rv o,l=<br />
No. of ('ontaincr(s) -<br />
'plu m e<br />
^^ /,<br />
5.\MI'Lh: :V^.^ \\:\11515<br />
Sample No Slamy ' Sample D at e Sample Mime<br />
BON685 C)' Other Solid ^.- /_ 3<br />
P<br />
I1.<br />
Sae uanlll nl<br />
Inwua arm<br />
SPI'.('L\1. INS I fit l (' IONS<br />
21 Days<br />
Pare 1 !<br />
( \IN OI POS.SI'.SSION Sigel/1 1 1'1111 Names SS, II<br />
III II1'M.lal,,-o 110%ISI I Il IL cl l l.. ,id i. Nkc -7471- 1( V) . C hromlun, l 1c\-7106. SI SuIJO 11.<br />
a= I't It enXO ,AI a .tut 1 Sp 'I ascot ( ]. C (6,11-60 I_ p v m sal u<br />
L. 1.111
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-07 Page ! or !<br />
( 'effector<br />
R. Fahlhcrg rLJ(<br />
Company Contact Telephone Nu. Project Coordinator Data Turnaround<br />
Steve hlarske 373-4316 WEISS, RL<br />
Project Designat en 'ampling Location SAF No.<br />
105-C Phase 13 Phase II - Concrete Samples 100 Area B98-061<br />
Ice Chest \'o.^l y^ p ^/1 r— / Field Logbook No. 3<br />
Method of Shipment<br />
J M "9` 10 _ ^L (land deliver<br />
Shipped to<br />
Quante ira IncogwraleJ<br />
POSSIBLE SAMPLE IIA%ARDS/REI11ARKS<br />
RaJiaaaivc<br />
)ffske Property No<br />
Prne rvat on<br />
N..<br />
Bill of Lading/Air Bill No.<br />
N<br />
"type of Container<br />
P<br />
Special Handling and/or Storage<br />
SA NIPIL .-ANA L}'SIS<br />
No. of Cunlalner ( a) -<br />
Volume<br />
IL<br />
S ec aan (I I ,n<br />
Spc ,xl<br />
loroou,nos<br />
21 Days<br />
X03, ^C^ m<br />
SanlpleNo. Matrix • SampleDale Sample Tinic rn, - S s - m R:j^ k>i d 9'p Fik'^,4?+.+i„^';}i• r ,'lfl r^'{t I+tom,,,(.`-^„t<br />
SON686 N Other Solid - )^_ f/<br />
^d 0 (]<br />
SPECIAL INSTRUCTIONS Matrix<br />
AIN 0 F POSSESSION<br />
1, y shcJ N^<br />
//]^<br />
^S l ^^ V „^a<br />
Sign/Print Names __<br />
(1) ICI'Maa6- 6010A (S upen,acu)if eadl, Mercup-7471-(CV), Clo.on flex-)196,<br />
key a - Ihre^unc 1'Ui^ 5080 1 1 SJ " (Ian aSlx -211, 1 Ce' 137 C bah 60 L ru( um 15 1 -<br />
^^h.......,*1 1 : - I"s; - A" iv c,nn?JIla l,nc lhu r S.Iv<br />
^^ i (<br />
S<br />
SE<br />
S1<br />
,I<br />
-<br />
-<br />
-<br />
So,i<br />
SNuncn,<br />
SoI,J<br />
ucLmgm.L.J B. Inec lw^^<br />
.^<br />
" I " nqI.11wu„n<br />
I
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -08 Page I f<br />
'olleetur Company Contact Telephone No. Project Coordinator Data Turnaround<br />
R. Fahlberg I Steve Marske 373-4316 WEISS, RL<br />
Project Designation Sampling Location SAF No.<br />
105-C Phase I k Phase II - ('o 11 crete Samples 100<br />
Area LL — 1 3 B98-061<br />
Ice Chest No. Field Logbook No.<br />
L L - _ Z<br />
Shipped 10<br />
Quantcrra Incorporated<br />
POSSIBLE SAMPLE IIALARDS/RE\L\RKS<br />
xodioaclive<br />
Special Handling and/or Storagc<br />
p<br />
^/p<br />
S\1111'1,L AN, 1,%SIS<br />
Method of Shipment<br />
Hand deliver<br />
Offske Property No Bill of Lad in /Air Bill No.<br />
Preservalion<br />
rvon.<br />
'I ype of Container P<br />
Nn. of Container(s)<br />
V'nlu me<br />
I f.<br />
Sec i te m 10 in<br />
Specul<br />
Innmaiuns<br />
"/`loll / c-^^<br />
Sample Na Matrix Sample Dale Sample'I'ime ?'>'^Y'S^D:"itP, ,hst°eft';a ,M. Li<br />
BON687 Other Solid S - - ^Y .^ U S ^Z C a<br />
21<br />
DAYS<br />
A^,^<br />
'.9nuv{c,,+pT'f'.`<br />
SPECIA1. INSTRI1CI IONS Matrix<br />
11 %1'% 01 POSSESSION Sign Print Names<br />
fl) I(I'Alna6-eu II^A ltiupul^accl ll.eaul, Meaup- "TJTI-(CVj. Chroinmm lle^-T196,<br />
s<br />
9i<br />
- S'11<br />
- S
Environmental<br />
Restoration FJ^C Contractor Team<br />
D- mow+ A<br />
Interoffice Memorandum a'<br />
911 V<br />
TO ' 1:). A. St. John r.0-19 DA TE ' hebruary 27.1999<br />
n,•n:s'<br />
See Below raOW S. L. Winslow<br />
R ulCun Engineering<br />
X'+-4 1 /531 -0 706<br />
WJUECT: CURIE. FSTiMATE FOR SUPP1NC CONCRETE CORE SAMPLES<br />
CCN: 05508lt<br />
W° A 2Z'n<br />
awl e0^ orb<br />
The following calculations show that cur sunplawith a direct reading of equal to ur icss than<br />
400.000 dpm/10(km' will be below the definition of radioactive mate rial as de fi ned in 49 CFR 173.40;<br />
of 70 Bq/g (2F.3 pCi/g). Lach sample will consist of concrete material form four, two inch con<br />
samples and enough water to make a slutr • consissncy. The diianhution of radionuclides is biped un<br />
previous concrete samples taken front the below grade Fuel Storage Basin that would also he<br />
representative of these concrete samples.<br />
Given<br />
Cylinder Volume = arh Radius ofco=cte core (r) = I inch<br />
Concrete Density = 2.35 g/cm' Height of core sample taken (h) — 0.25 inches<br />
27 pCi = Bq Maximum tEmt reading on core = 400.000 dpm/100cat"<br />
2. 22 dpin = pCi<br />
Calculations:<br />
V — ( 3.14) (1 in.) `( 0.25ia) = 0.79 in' (16.4 cm 'in') (4 Lure satuplcs) = 512 cm'<br />
(400.000 dpni/5 L2 cm) (em'/2.35 g) = 3.32E3 d;mlg<br />
3.3213 dpm/g (pCi/2.2 dpm) = 1.5E3 pC'ilg or 55.4 Bq/g<br />
ti1.W:dld<br />
Percent Distrihution(`l) Concentration ( L Cih)<br />
°Co 0.17 2.55 pCi/g<br />
"'Cs 82 1.2F3 pCi/g<br />
"lieu 0.33 4.95 pCUg<br />
"'Eu 0.05 7.5E-1 pCi/g<br />
°0Sr 17 2.55 112 pCi/g<br />
"Ann 0.005 7.5E-2 pCi/g<br />
139124111<br />
Pu 0.1 L5- C<br />
Civics:<br />
S. Ci. Nlarske X5-53<br />
P. A. Newman X1-41<br />
RadC'on Enginee ring File.!LB XO-23<br />
<strong>Document</strong> and Intb Services 110-09<br />
TOTAL: 1.4613 pCi/g<br />
Gido
Environmintil<br />
Contractor<br />
Contractor ERC Team<br />
Interoffice Memorandum<br />
TO' I). A. St John LO-19 DATE:<br />
Sec 13clow<br />
Corr=ration (pCi/0<br />
2.55 pCi/g<br />
1.2E3 pCi/g<br />
4.95 pCi/g<br />
7.5E-1 pCi/g<br />
2.55E2 pCi/g<br />
7.5F-2 pCi/g<br />
1 5 OCUM<br />
1.4613 pCi/g<br />
373 °"79 F"-02<br />
1^ebruary 27. 1999<br />
At<br />
nto+t: S. L. Winslow<br />
RadCun Engineering<br />
X34 1/531-0706<br />
SU BJECT. C'URIF ESTIMATE FOR SJUPP1NGCONCRF.TE CORE SAMPLES<br />
Job No. 22171<br />
.^wY..YY.... b<br />
D\.0 . -A<br />
Ol e for<br />
n v<br />
CCN: 055088<br />
.Su^w\Cob !I!0<br />
The hollowing calculations Show that con: 5amplawith a direct reading of equal to or less than<br />
400.000 dpm/l0(km' will be below the definition of radivactive material as defined in 49 CFR 173.403<br />
of 70 Ay/g (2F.3 pCi/g). Lach sample will cunsistof concrete material itu n four - two inch co re<br />
samples and enough water to make a slurry consL*ncy. 'Fhe distribution of radionuc lides is based on<br />
previous concrete samples uJten front below grade Fuel Storage Basin that would also he<br />
representative of these concrete samples.<br />
(jiver:<br />
Cylinder Volume = n r'h Radius of concrete core (r) = I inch<br />
Concrete Density = 2.35 g/em `Height of com sumple taken (h) - 0.25 inches<br />
27 pCi = Dq Maximum Jima reading on core = 400.000 dprn/IUOcaY<br />
2.22 dprn = pCi<br />
('alUUldlions:<br />
V - ( 3.14) (1 in.)'(U 25in) = 0.79 in' (16.4 car/i n -')(4 cure simplcs) = 512 cm'<br />
(400.000 dpnr/51.2 cm') (cm' 12.35 g) = 3.32E3 dpn/g<br />
332L3 dpm/g (pCi/2. 2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g<br />
ti1.W:dld<br />
°Co<br />
"'Cs 82<br />
02 E<br />
Percent Distribution(%)<br />
0.17<br />
0.33<br />
'"Eu 0.05<br />
"'Sr<br />
17<br />
W ,.iun<br />
taoawPu<br />
0.U05<br />
0.1<br />
TU'fAL<br />
('ones•<br />
S. (i. Marske X5-53<br />
P. A. Newman X3 -4 1<br />
RadCun Enginee ring File/LB XO-23<br />
<strong>Document</strong> and Into Services 110-09<br />
6 16.4.
Oate/7me Received:<br />
Figure 1<br />
SAMPLE CHECK4N LIST<br />
~ ! ^^ I S Ll SGS Li ln Z^7S<br />
(j<br />
Work Order Number. ^1 ^^^^^L'^^^ SAF<br />
RFSH-SOW-93-0003 -<br />
Revision 5<br />
Shipping Container 1 0: 51)1 90 Chain ofCustody # ^ 7^^ ^ – ^L ^ ^^^o ^ L ^<br />
1. Custody Seals on shipping container intact? Yes [ ] No ( ^<br />
2. Custody Seals dated and signed? Yes [ ] No [ 11^<br />
3. Chain-of-Custody record present? Yes W N or( ]<br />
4. Cooler temperature l<br />
L)<br />
S. Vermiculite/packing mate rials is Wet [ ] t ry (I<br />
6.<br />
Number of samples in shipping container.<br />
7. Sample holding times exceeded? Yes [I No (I<br />
8. Samples have:<br />
tape hazardlabe<br />
astcdy seals _appropriate sample labels<br />
9. Samples are:<br />
o good condition le akn9<br />
broken have air bubbles<br />
10. Where any anomalies identified in sample receipt? Yes [J'No [ ]<br />
11. Description of anomalies (include sample numbe#<br />
Sample CustodianlLaboratc ry: — L^_ ( a te: ^,<br />
Telephoned To: On gy<br />
I 'l
RFSH-SO W-93 -0003<br />
Revision 5<br />
Figure 1 _<br />
SAMPLE CHECK-IN LIST<br />
OateMme Received: nn `^ SG#:<br />
b /^; ^nns^^<br />
Work Order Number. 5^ ^ w tk i.^ tJLE'<br />
Shipping Container 10: Chain of Custody -616<br />
1. Custody Seals on shipping container irdact? Yes t /No (1<br />
2. Custody Seals dated and signed? Yes l7 No (1<br />
3. Chain-of-Custody record present? C Yes "b ( I<br />
4. Cooler temperature<br />
5. Vermiculite/packing mate ri als is Wet I! D ry ( -r'<br />
6. Number of samples in shipping container:<br />
7. Sample holding times exceeded? Yes ( ] Vo [ }<br />
6.<br />
10.<br />
Sam s have:<br />
tae hazard labels<br />
^tody<br />
seals _appropriate sample labels<br />
9. Samples are:<br />
in good condi tion leaking<br />
broken _have air bubbles<br />
Where any anomalies iden tifi ed in sample receipt? Yes (] No [,<br />
11. Desc ription of aromalies (include sample num bers):<br />
Sample Custodian/Laborato ry: ^jL 3/y1 ^J(Jjr`Z,/,/e:<br />
Telephoned<br />
IA<br />
pp<br />
C-1 03
n<br />
Q 0 3 X05 Cy r,-) D 3-)6& - Zed<br />
Client Sample Screening Results<br />
11-Afar-98<br />
/0 — rye ^^ 1<br />
CLIENTCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSR NETCPMB<br />
Bill BON685 3/11/199812:00:00 PM QUAD23A 3/11/19981:02:54 PM BON685 30 3 0.025 44 0.525<br />
V I<br />
LIQUID Bkg: 3/11/1998234:41 AM BKO 600 45 0.075 565 0.9416667<br />
An] Dale: 3/11/1998 Tot Sa,Alq: LOOE 4 00 LOOI;f OO Alp; (Dpm/ 6.25E-0 2 (uCU 2.81 E-05 (pCl/ 2.81E+01 + 1.9Ei02 CAI' 8.9E-01 Lots<br />
Ppl mg: 2.9 / Units: L ml Bet; Alq): 9.83E-0 1 So): 4.43E-04 Ljg): 4.43E+02<br />
+2.OE+02<br />
Bill BON686 3/11/1998 12:00:00 PM QUAD23B 3/11/19981:02:54 PM BON696 30 1712 57 127510 4249.4083<br />
V LIQUID Bkg t3/11/1998 2:34:41 AM BKO 600 40 0.06666667 555 0.925<br />
Ant Dow 3/11 1 1998 To1Sa,Algi LOOEt00 1.00E+00 Alp; (Dpm/ 1.50E+02 (uCU 6.77E-02 (pC7/ 6.77E+04 t2.3E+03 CAT 3.7E-04 Lab<br />
Ppt mg: 95.5 UNb: L ml Bel; AI 9.32E+03 So): 4.20E+00 L 4.20E+06 + 1.2E+04<br />
111<br />
1.2E-06 Alg<br />
F—^ l-hinr- vN 011 BnlerrB Envlrunmcnl Se rvices, SCP V2.03<br />
G<br />
I<br />
I.IE-01<br />
Alit<br />
LI[
Client Sample Screening Results<br />
12-Afar-98<br />
CLIENT CODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
BBI BON687 3/12/1998<br />
V<br />
LIQUID 3<br />
And Date: 3/12/1998 Tot St, Alq: 1.00E+00 3<br />
Ppt m8: 49.6Units: L<br />
/<br />
QUAD21A<br />
Bke:<br />
1.00E+00<br />
nil<br />
3/12/199811 :01:02AM BON687<br />
3/12/1998 12:01:04 AM BKG<br />
Alp; (Dp W 8.39E-0 1 (uCl/ 3.78E-04<br />
Be(; AIql^ 3.27E+00 Sal: ) 1.48E-03<br />
30 7 0.18 74 1.54<br />
600 32 0.05333333 556 0.9266667<br />
(pC7/ 3 .78E+02 + 3.9E+02 CAT 3 6.6E-02 Lab<br />
L le)^ 1.48E+03 + 2.8E+02 I 3.4E-02<br />
Ci<br />
H<br />
C ( 12-Afar-98 Quanterra Environment Se rvices, SCP V2.03 I<br />
Alit<br />
Ide
^J<br />
J<br />
J<br />
-T<br />
Bechtel <strong>Hanford</strong> Inc CHAIN OF CUSTODY/SAMPLE ANALI'SIS REQUEST B98- 661 -09 pare ! ^( !<br />
Collector<br />
R. I'allbere<br />
^y^<br />
DD (A<br />
Company' Contact<br />
Steve Nlarskc<br />
"I"elephone No.<br />
373-4316<br />
Plotter( Coordinator<br />
WIiISS, BI"<br />
Project Designation Sampling Location SAF No.<br />
10?-C Phase I k Phase II - Cuncrcle Sanlplce 100 Area B98-061<br />
Ice Chest No. Field Loghonk No.<br />
_ — I '^ C3<br />
Nlethod of Shipment<br />
Hard deliver<br />
Shipped In Offshe Propero No. Bill of I.Ad inll/Air Dill No.<br />
Quanmrru Incorpo rated ^/<br />
POSSIBLE SA NIPLE 11.1LA RDS/RF,NIARGS<br />
Nadioaclir.<br />
Special Handling and/or Storage<br />
1. NN IA SIS<br />
L) I Cam ^C'3 -) r' ^<br />
Preservation<br />
I ype of ( retainer<br />
No. of ( onlatner(s)<br />
\'olumc<br />
_ 'U^^1.^ 5«mm Ulm<br />
Symi.l<br />
Lou„^o„„<br />
w(<br />
Sample NU. Nfalm Sample Dale smilplc I III1C<br />
11_<br />
Daw Turnaround<br />
BON68B Other Solid ti' _ _ = (.i / _,:C .^ t J^- ^•' la C<br />
C11kIN OF POSSESSION<br />
^I<br />
^< "I .1.111 ”L.<br />
Sign/frill Names<br />
LA<br />
14ur. ^,I IIJ __ ^(,^ ( "1 _^<br />
21<br />
Days<br />
SPE( I I I I, INS VIIC 1IONS Nlulri,<br />
11) ICI' Rlela6 - I , ,iv, i v, Uu mieeccl II eud Nlacul 1411 Chnnmu^I Ile. - 1196<br />
KVI.<br />
111i.1.m , rXel 6:3 SC S4 ! /o - IS/<br />
JJJ<br />
^eC^nef^uyv^ -9^l C^rLbv^ -(¢<br />
NeI )1,.dIt. Ueielwr, Necrncdill U.ue lum / i ^Vl<br />
R .... yim...A H 'U,Ilc I Ka.anid lli Uem luu`<br />
L.\I1111
Bechtel Hanforfl Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -10 Page i nr<br />
Collector Company Contact 7 elephone No. Project Coordinator Data Turnaround<br />
R. Fahlberg Steve Marske 3734316 WEISS, RL<br />
Project Designation Sampling Location 'AF No.<br />
105-C Phase I & Phase II -Concrete Samples 100 Area B98-061<br />
Ice Chest No. Field Logbook No. 7<br />
Method of Shipment<br />
/ 7 / —/3 (D _ Z Iland deliver<br />
'hipped lo Offsite Property No.. Bill of Lading/Air Bill No.<br />
Quanterra Incorporated<br />
POSSIBLE SAMPLE IIALARDS/RENIARKS<br />
Radioactive<br />
Special Handling and/or Storage<br />
Preservation<br />
'type of Container<br />
No, of Container(s)<br />
Volume<br />
SANII'LE AN.U.\'SIS I^<br />
Sa ucm fIl n<br />
Speual<br />
Innmciinns<br />
3<br />
r<br />
II.<br />
a^<br />
21 Days<br />
0 L, ''- G2<br />
Sample Nn. Matrix ' Sample Date Sample Time ° ;, i u a ,, d; • '.J: ,.:. t'd. ."f .'^rtA`. `Ht :.Sr yB lkl . , :`° C' ' . + y rr_ ' . :' '..<br />
BON689 V Other Solid -12 - 131S<br />
SPECIAL INSTRUCTIONS Ma trix'<br />
CIIAIN OF POSSESSION Sign/1' it][ Names S - s,,,1<br />
(1) CPMemis- 6010A ISupnoxcl lLcedlMcraoy-/4/1-(CV), Chraniwn lien-/196. S[ - 5
Environmental<br />
Restoration ERC ream<br />
Contractor<br />
Interoffice Memorandum<br />
TO'' D. A. St. John LO-19 arc<br />
nrua'<br />
5).W:dld<br />
Set; Below Fa"`<br />
Percent DistrihutionM<br />
°Co 0.17<br />
(IT C." 82<br />
132 E 0.33<br />
'"Eu 0.05<br />
A7Sr 17<br />
'"'Ain 0.005<br />
'''"'"'Pu 0.1<br />
TDTAL:<br />
T_ -^7n<br />
l-ebruary 27.1998<br />
S. L. Winslow<br />
RadCun Engiw:cring<br />
X341/531-0706<br />
sualacr: CVRIK FSTIMATE FOR Stl1PP1N000NCUTF. CORE SAMPLES<br />
Job No. 22172<br />
v..,. J. A....r w<br />
P.D. wA<br />
CCN- 055088<br />
ov IO.0<br />
nn v.<br />
tae w.<br />
L..a. CeM 'rV<br />
The IbIlowing calculations show that con; sampltswith a direct reading of equal to or less than<br />
400.000 dpm/100cm' will be below the definition of riftwctive material as defined in 49 CFR 173.40-,<br />
of 70 By/g (2F3 901g). Lach sample will consist ofcoacrctc material from four. two inch co re<br />
samples and enough water to make a slurry consisxncy. '11w distribution of radionuclides is based on<br />
previous concrete samples taken front the below Vade Fuel Sloragc Basin that would also he<br />
representative of these cuncretc samples.<br />
(jiven:<br />
Cylinder Volume = nrh Radius of concrete core (r) = I inch<br />
Concrete Density = 2.35 gJcm' height of core sample taken (h) - 0.25 inches<br />
27 pCi = Bq Maximum &vet reading on con = 400,000 dpm/lUucalt<br />
2.22 dpm = pCi<br />
Calculations:<br />
V-(3.14)(1 in.) `(025in) = 0.78 in' (16.4cm `/inj(4 van: samples) = 512 Lm'<br />
(400.000 dpm/5 L2 cm) (cm/2.35 g) = 3.32E3 dpm/g<br />
3.321:3 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 kg<br />
C(Mics:<br />
S. (. Marskc X5-53<br />
P. A. Newman X3-41<br />
RadCun Engineering He!LB XO-23<br />
<strong>Document</strong> and info Services 130-09<br />
Cona mtration (uC:V0<br />
2.55 pCiig<br />
1.2F3 pCi/g<br />
4.95 pCiig<br />
7.5E-1 pCilg<br />
2.55E2 pCi/g<br />
7.5F.-Z pCi/g<br />
1.5 OCUZ<br />
1.460 pCi/g<br />
nl<br />
0103
Environmental<br />
Job No. 22172<br />
Restoration<br />
Contractor a,.n,. w,<br />
Interoffice Memorandum"` w•~ a' iolt<br />
n w<br />
S WA<br />
S~ Cod. !m<br />
Concentration (pCi/")<br />
2.55 pCi/,v<br />
1.2F.3 pCi/g<br />
4.95 pCi/g<br />
7.5E-1 pCi/g<br />
2.55E2 pCi/g<br />
7.5F.-2 pCi/g<br />
1 5 nCi/g<br />
1.46L'3 pCiig<br />
CCN: 055081,<br />
r ERC Team -^- A ^°<br />
TO; I). A. St. John 1.0-19 °ATL` hebtuary 27. 1999<br />
' OM1'" Scc Below FROM: S. L. Winslow<br />
RadCua Engineering<br />
?634 1/531-0706<br />
suuecT. Cl:R1F: FSTfMATE FOR SHIPP1NCCONCRETE CORE SAMPLES<br />
The following calculations shnw that core s arnplcs widi a direct reading of equal trl or less than<br />
400,000 dpm/ 1 00em' will be below the de fi nitionofradioactive material as defined in 49 CFR 173.403<br />
of 70 Bq/g (2F3 pCi/g). Gach sample will consist of concrete mate rial from four, two inch co re<br />
samples and enough water to make a slurry coruiSrncy. 'I-he distribution of radionuclides is based on<br />
previous concrete samples taken front the below grade Fuel Storage Basin that would also he<br />
rcprescntative of these concrete sunples.<br />
Given:<br />
Cylinder Volutuc = nrh Radius of caucrcte core (r) = I inch<br />
Concrete Density = 2.35 elem' height of con: sample taken (h) — 0.25 inches<br />
27 pCi = Dq Maximn m liwt reading on core = 400.000 dpnt/1 Wcar<br />
2.22 dpm = pCi<br />
Calculations:<br />
V — (3.14) (1 in.) `(0 25in) = 0.79 in' (16.4 cm'/iii) (4 core samples) = 512 cm'<br />
(400.000 dpm/5 L2 cm) (cm'/2.35 g) = 3 3 2E3 dtm/g<br />
3.32L3 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g<br />
51.W:dld<br />
mCu<br />
117<br />
C.<br />
Percent DistributionO<br />
0.17<br />
82<br />
"`flu 0.33<br />
1"Eu 0.05<br />
1'Sr 17<br />
'°'Ain<br />
11 91'4U<br />
Pu<br />
0-UU5<br />
0.1<br />
TO rAi<br />
Cn ies:<br />
S. (J. Marske X5-53<br />
P. A. Newman X3111<br />
RadCun Engineering file. !LB X0-23<br />
<strong>Document</strong> and into Services 110-09<br />
0109
Figure 1<br />
^I<br />
Date/Time Received: `l<br />
^.Z-<br />
Q<br />
^%1 ^v SGS.,<br />
RFSH-SOW-93 -0003<br />
Revision 5<br />
SAMPLE CHECX-W UST _ v<br />
Work Order Number.<br />
SAF S ^(j CzQ3 ^j ^j–(,^¢ 1 -<br />
Shipping Container ID: "K-R .<br />
//}}<br />
chain o(Qstody S ^g 3 Dot ^1 -09<br />
^1rAq?,<br />
1. Custody Seals on shipping contairx intact? Yes [q/No ( I<br />
2. Custody Seals dated and signed? Yes B-INo (1<br />
3. Chain-of-Custody record present? Yes ( No (1<br />
4. Cooler temperature l<br />
o<br />
5. VerrnicufdeJpacking mate ri<br />
als is Wet [ Dry k/l )—<br />
in<br />
6. Number of samples shipping cadainer.<br />
7. Sample holding times exceeded? 2« Yes No [<br />
8. Samples have:<br />
tape `hazard libels<br />
_____custody seals _approprieie sample labels<br />
9. Sam les are:<br />
in good condition Ong<br />
broken Inge air bubbles<br />
10. Where any anomalies iden tified in sample receipt? Yes (j No<br />
11. Descrip ti<br />
on of anomalies (include sample numbers:<br />
Telephoned To: On gy<br />
C,li^
Figu re 1<br />
RFSH-SOW-93-0003<br />
Revision 5<br />
SAMPLE CHECK-IN LIST<br />
S<br />
Date^me Received: , ^I ^ l^^l / SG# l l^ ^l ^— 7<br />
1<br />
Work Order Number. SAF #: f5 1 — -<br />
Shipping Container ID: Chain of Custody if<br />
1. Custody Seals on shipping contakw intact? Yes [ 1,140' [ 1<br />
2. Custody Seals dated and signed? Yes [I No ( ]<br />
3. Chain-of-C ustody record preserd? Yes _ ,] No ( ]<br />
4. Cooler temperature<br />
5.<br />
/` e<br />
"7<br />
VermicuWpacicing mate ri<br />
als is Wet [ [ C ry (^<br />
6. Number of samples in shipping cmtainer. c<br />
7. Sample holding ti<br />
mes exceeded? Yes [ ] No [ ]<br />
8. Sa les have:<br />
Pe<br />
/ custody seals<br />
hazard labels<br />
_appropriate sample labels<br />
9. —8mptes are:<br />
in good condition leaking<br />
broken have air bubbles<br />
10. Where any anomalies identified in sample receipt? Yes [ ] No<br />
11. Desc ri ption of anomalies (include sample numbe rs):<br />
Sample Custodian/Laborato ry:<br />
Telephoned To: On.<br />
14<br />
C11i
(7)<br />
^ 96 . D3 1 C'-.n, 3<br />
Client Sample Screening Results<br />
13-Mar-98<br />
( J<br />
CLIENTCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NET CPMB<br />
Dill BON698 3/13/1998 QUAD2IA 3/13/199810:21:17 AM BON699 30 9 0.24142857 57 0.96<br />
O I LIQUID Bkg: 3/13/1998 1 :30:18 AM BKG 700 41 0.05857143 658 0.94<br />
An! Date: 3/13/1998 Tot Se, Algl 1.00E+00 , 1.00E+00 Alp; (DpM 1. 21E+00 (uCV 5.45E-04 (pCV 5.45E+02 t 4.1E+02 CAT 4.6E-0 2 Lab<br />
Ppt mg: 51.3 1^ Units: 1 1 ml Bet; Alq): 1.98E+00 Sa): 8.94E-04 Llg): 8.94E+02 ± 2.5E+02 I / 5.6E-0 2 Ni<br />
Bill 130N689 3/13/1998 QUAD2113 3/13/199810:21:17 AM I1ON689 30 661 21.9790476 47335 1576.8733<br />
OLIQUID Bkg: 3/13/1998 1:30:18 AM BKG 700 38 0.05428571 672 0.96<br />
And Date: 3/13/1998 Tot Sa, Alq: 1.00E+00 1.00E+00 Alp; (DpM 2.19E+01 (uCB 9.84E-03 (pCV 9.84E+03 + 8.5E+02 CAT 2.5E-03 Lab<br />
Ppt mg: 50 / Units: L / , ml Bet; Alq): 3JOE+03 Sa): 1.49E+00 Ljg): 1.49E+06 + 6.8E+03<br />
IIt<br />
/ 7.4E-05<br />
MLIL<br />
13 111 IION753 3/13/1998 QUAD2 1 C 31]3/199810:21:17 AM BON753 30 0 -0.0571429 84 1.9057143<br />
SOLID Bkg: 3/13/19981:30: 1 8 AAt BKO 700 40 0.05714286 626 0.8942857<br />
An] Date: 3/13/1998 Tot Sa, Alq: 2.50E+02 9.77E+01 Alp; (DpM -5.47E-0 1 (uC i/ -6.30E-04 (pCU -2.52E+00 ± 4.8E+00 CAT 2.5E+02 Lab<br />
Ppt mg: 97.7 Units: g<br />
/<br />
/ mg Bet; Al Alq); 4.30E+00 Sa ) : 4.96E-03 L c)^ 1.98E+01 ± 3.2E+00 I / 5.0E+00<br />
Bill BON734 3/13/1998 QUAD2 113 3/ 13/199810:21:17AAI BON754 30 8 0.20666667 77 1.4709524<br />
SOLID Bkg: 3/13/1998 1:30:18 AM BKG 700 42 0.06 767 1.0957143<br />
And D ate: 3/13/1998 Tot Sa. Alq: 2.50E- +02/9.60E + 01 Alp; (DpM 1 .31E+00 (uCit 1.54E-03 (pCV 6.16E+00 ±5 .6E+00 CAT HAE+00 tab<br />
Ppt mp 96 Units: g mg Bel; Alq): 3.19E+00 Sa): 3.74E -03 Leg): IA9E +0 1 ± 3 . 1E+00 I / 6 . 7E+00<br />
BIII BON755 3/13/1998 QUAD22A 3/13/1998 10:21:21 AA1 BON755 30 3 0.05571429 70 1.4004762<br />
SOLID Bkg: 3/13/19981:30:26 AN] BKG 700 31 0.04428571 653 0.9328571<br />
Ant Dale: 3/13/1998 Tut Sa,Alq: 2.50E+02 9.61E+01 Alp; (DpM 2.80E-0 1 (uCl/ 3.28E-0 4 (pCi/ 1.31Et00 +4.5E+00 CAT 3.8E+0I Lab<br />
Ppt mg: 96.1 Units: g mg Bel; Alq): 2.98E+00 Sa): 3.50E-03 Ljg): 1.40E+01 ± 2.8 E+ 00<br />
/<br />
I l<br />
Alq<br />
Ll g<br />
Llg<br />
7.2E+00 Alq<br />
LI g<br />
13111 11ON756 3/ 13 /1998 QUAD22B 3/13/1998 10:21:21 Mt 130N756 30 8 0.20952381 66 1.2314286<br />
SOLID nkg: 3/13/1998 1:30:26 AM BKG 700 40 0.05714286 678 0.9685714<br />
AN Hate: 3/13/1998 Tot Sa, Alq: 2.50E+02 9.73E+01 Alp; (DpM 1.32E+00 (uCI1 I.53E-03 (p(7/ 6.12E+00 ±S.OE+00 CAT 8.2Et00 Lab<br />
Ppt mg: 97.3 / Unitr. g / , mg Bet; Alq): 2.57E+00 Sa): 2.97E-03 LIg): 1.19E 4 01 + 2.5E+00 I / SAE+00<br />
Alq<br />
Llg<br />
1^-s<br />
^e<br />
ra<br />
13-h/ar-98<br />
Quanterra. Environment Se rvices, SCP V2.O3
G_<br />
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-o61-I I Parc ! of I<br />
Collector<br />
n<br />
J !-.. "'aIF=> ^ y qh+ / RQ - A<br />
Project Designation<br />
105-C Phase 1 A Phase II - Concrete Samples<br />
ornpany Contact Telephone Nu.<br />
Steve Marske 373-4316<br />
Sampling Location 1_<br />
10O Area (os -c IMP twvc 3<br />
Project Coordinator<br />
WEISS, RI,<br />
F No.<br />
098-061<br />
Ice Chest No. Field Logbook No.<br />
I<br />
r L_ '3 UC1<br />
Alethod of Shipment<br />
Iland deliver<br />
Shipped 'I u<br />
Quanterra Incorporated<br />
Bill of Lach/Air Bill No.<br />
POSSIBLE SAMPLE IIAZARIIS/REMARKS<br />
Radioaco,,,<br />
Special Handling and/or Storage<br />
SAMPLE ANALYSIS<br />
Olfsitc Property No.<br />
NA<br />
Preservation<br />
'I ype of Container<br />
Nn, of ('oriminer(s)<br />
/Vll/l"/<br />
Volume<br />
/ J<br />
Nose<br />
I I.<br />
See imm I I)ir<br />
Special<br />
Insimcram<br />
N<br />
Data Turnaround<br />
2<br />
^ Days<br />
-Ckk ivA 9 6-^)a425-<br />
Sample No - >j /<br />
rH 0<br />
mric • Sample Dole Sample Mime - ..... ! }'t gr ,. .2<br />
,,^, ..:<br />
BON690 G I Other Solid (3 MA (Z^l t'^ fJ Li I c<br />
SPECIAL INSTRIC I IONS<br />
t'ILMN OF POSSESSION Sign/Print Names<br />
.<br />
(1) KTMndls- 6010A(Sop,rlrace) I Lead), Mercwy-7471-(CV); C'hrumlum Ilea -7196,<br />
1t6 00p uhe li' lot 12541; Damns Spectroscopy Dam.Tu, Re ei B' Ddie,' n ICBs 6080 lA¢n D<br />
IC smm-U7 Cobal"O,Eur pion-152,<br />
^p<br />
oop, n 191. 1. , u n-1551, A e,c un-241 I I , ¢ Ismoprt 1r000000 s.1c<br />
^i NqR rCJLI^.^ 5 C<br />
p %//<br />
P c mq^^^.hcd lb _._ li ci cl n, 1
c)<br />
H<br />
1Q<br />
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 - 12 Paee !<br />
Cullectur<br />
`1<br />
pp<br />
+tam -per & l i) -r / ^a IN I<br />
Project Designation<br />
10 -C Those I k Phase II - conciew Sulllples<br />
Company Contact<br />
Steen hla rs ke<br />
Sampling Location<br />
10O Arca — I OS f- p Ilea ( +0 3<br />
Ice Chest Nu. Field Logbook No.<br />
EL -I IUA -6 L<br />
Shipped 7L<br />
Offs to Property No.<br />
Ouanicrra Incorpurmcd<br />
POSSIBLE SAi\IPLE IUZ\RDS/BENIARFS<br />
Badioaciice<br />
Special Ilandthig and/or Smreac<br />
BON691<br />
^03^G CAM<br />
Simple No I I I )<br />
O.^<br />
S:k1I 1 1.1;<br />
AN%11SIS<br />
h1A<br />
Prnscrcaliun<br />
Telephone No.<br />
373 -4316<br />
Project Coordinator<br />
WEISS. RL<br />
SAF No.<br />
B98-061<br />
Method of Shipment<br />
Iland del I%er<br />
Bill of Lading/Air Bill No.<br />
w^<br />
Data Turnaround<br />
we -_--<br />
2 nays<br />
'1'1'pe of Container i 1<br />
Nu. W 1loth... r'I'1^1 I _.<br />
\'plume<br />
IL<br />
see ueni lu in<br />
sn=.ml<br />
^03r^ 4^ - i^^(n( Ll-<br />
Iri% a .tialllple Pate Sample I II11C<br />
Other Solid 13 M RR ^/ Q ^(J ^^ —?<br />
--<br />
_ -<br />
L<br />
- -1<br />
l I<br />
l f<br />
SPLCUL INSIRI I - IONS Main<br />
( HAIN OF POSSESSION Sign/Print Nit s s,,,i<br />
1111CI'MUa6-onl uq lS,ipuvecq lead;. Al t..... 74al- IC VL C6mauum lien-7190_ g. Spa<br />
Ita-1 ^,,,<br />
,d i, n,<br />
Nd nq ,I .J<br />
n Jp le4 1 UaI, Imm Re Dmclm,. I('0 - 8080 Ioi I I4 l ,G.iiiiin,i Stearn,- pp 1- in-13 7, C pbah60_f I n-15?- do s..i<br />
P 1 in-I,I P -hit A u_}i I. I. P . I I I ue I.ul, pl. li I i. Sale V r..<br />
^CQ,eC/L<br />
13H92<br />
yg b3^ ^- .C- /3 )<br />
- -- u.l- I ^„e p^ 'd - ,, .Ie 1,^^e I UC/cp-Y^., SelPn.If CM -7^1^ N^^jEe/-103; Sr-^FJ, ^I ,I ^<br />
90 7 15<br />
Te ^^lef L(^ ^q ' L'arbon -l¢<br />
ff<br />
III, I- 1 m, ken nl P7 Ualc I me "ic v<br />
Hehn.pu,h ed ii, )a” lime Itacmled It, I)mo 1111,<br />
/ ^ ^ / /N ^^ nl I<br />
J3 I lu<br />
1—k \I (11(1 ft li. Inl. Dmc'l iiim<br />
Sf f l ION<br />
--<br />
F IN \L 5 \\II'L f;<br />
UNI I ISI I If IM1<br />
U,pu..d nl.n,.,.l -. -.. - - - - b,p„^ I ^^ - -<br />
-<br />
-<br />
Uaie I ne<br />
,u o q<br />
i- ^x<br />
of<br />
i y...a..
Environmental<br />
Restoration ERC Team<br />
Contractor 1>.D. WA<br />
CCN: 055088<br />
fob Vo.2zt72<br />
W^^A^ a<br />
Interoffice Memorandum a' ^'' w° iWA w^ ran ^<br />
S C<br />
SMw•CoA 11!0<br />
TO: D. A. St. John LO-19 °ATE: I ebnwy 27. 1999<br />
Scc Bclow MO.% S. L. Winsl ow<br />
RadCuu Engine ering<br />
X3-41/531-0706<br />
suuecT: CURIF. ESTIMATE FOR SJUPPINCCONCRETFE, CORE SAMPLES<br />
The following calculation simw that core sampleswith a direct reading of equal to or less IlLin<br />
400.000 dpm/1 00cm'will be below the definition ofradivactive material as de fi ned in 49 CFR 173.40;<br />
of 70 Bq/g (2F3 pCl/g). Lach sample will consistofeoncrete mate rial from flour, two inch core<br />
samples and enough water to make a slurry consisrncy. 'fhe distrihutiun of radionuclides is hased ern<br />
previous concrete samples taken front the below gmdt! Fuel Storage Basin that would also be<br />
represcniative of these cunercic samples.<br />
'iven:<br />
Cylinder Volume = nih Radius of co acte core (r) = I inch<br />
Concrete Density = 1 35 g/cm' height of care sample taken (h) - 0.25 inches<br />
27 pC; i =13q Maximum Jana reading on core = 400,000 dprni i UUcni'<br />
2?2 dpm = pCi<br />
Calculations<br />
V — (3.14) (I in.)'(U._5in) = 0.78 in' (16.4 ctrl'/in^ (4 care santplcs) = 51? cm<br />
(400.000 dpni/5 L2 cm') (cm'2.35 g) = 3.32E3 dim/g<br />
3.32L3 dpin"l; (pCi2 2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g<br />
SINAld<br />
Percent Distribution(%) Conceatration (VOW,<br />
nCo 0.17 2.55 pCi/g<br />
"'Cs 82 1.2F.3 pCilg<br />
'''lEu 0.33 4.95 pCi/g<br />
"'Eu 0.05 7.5E-1 pC ilg<br />
°"Sr 1 7 2.55E2 pCi/g<br />
SA'Atn 0.005 7.5E-Z pCi/g<br />
'39n 'Pu 0.1 1 5 nCU<br />
Co ics:<br />
S. G. lvlarske X5-53<br />
P. A. Newnlatt X:>-4 1<br />
RadCon Enginee ri ng FildlLB X0-23<br />
<strong>Document</strong> and Into Services 110- 0 1)<br />
TU'fAL_ 1.46U3 pCi/g<br />
61 115
Figu re 1<br />
SAMPLE CHECK-IN LIST<br />
DateTme Received: d 3 51 Sc'k W uOb/^2 S<br />
Work Order Number.<br />
0^<br />
Shipping Container ID: '^ ^ Chain of Custody #<br />
SAF # 13 I JGG-QP<br />
RFSH-SOW-93-0003<br />
Revision 5<br />
1. Custody Seals on shipping container inta ct? Yes ( q-,K o<br />
2. Custody Seals dated and signed? Yes (q- o<br />
3. Chain-of-Custody record present?^ Yes ( o ( ]<br />
4. Cooler temperature<br />
5. Vermicurde/packing mate ri<br />
als is Wet (] D ry<br />
6. Number of samples in shipping container.<br />
7. Sample holding times exceeded? Yes [I No 14--'<br />
8. Samp have:<br />
tape _hazard labels<br />
custody seals !approp riate sample labels<br />
9. Samp are:<br />
ii^n good condition leaking<br />
broken have air bubbles<br />
10. Where any anomalies identified in sample re ceipt? Yes [ I No [q--^<br />
11. Descrip tion of anomalies (in cl<br />
ude sample numbers):<br />
Sample ate: 6<br />
Telephoned<br />
?4<br />
G.
H<br />
Client Sample Screening Results<br />
13-Mar-98<br />
l3-Afar-98<br />
03^^3 LIB i^ 03,E 40 ".<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
Blil BON690 3/13/1998 QUA 1324B 3/13/1998 1:15:37 PM BON690 30 7 0.17619048 71 1.3838095<br />
D' LIQUID Ilkg: 3/13/1998 1:30:14 AA1 BKG 700 40 0.05714286 688 0.9828571<br />
Anl Dale: 3/13/1998 Tot So, Alq: 1.00E+00 1.00E+00 Alp; (Dpi/ 5.84E-0 1 (uCB 2.63E-04 (pCl/ 2.63E+02 ± 2.6E+02 CAT 9.5E-02 Lab<br />
Ppt me: 1 1 5 Unib: L MI Bet; Alq): 2.64E+00 So): 1.19E-0 3 LI8): 1.19E+03 ± 2.5E +02 I / 4.2E-02 Alq<br />
LIE<br />
Bill 13ON691 3/13/1998 QUAD24C 3/13/19981:15:37PM BON691 30 2 0.00666667 30 -0.002857<br />
dZ- LIQUID Bkg: 3/13/19981:30:14 AM BKG 700 42 0.06 702 1.0028571<br />
AM Dote: 3/1 3/1998 Tot So, Alq: I.00E+00 LOOE+00 Alp; (Dpm/ 2.02E-02 (uCV 9.12E-06 (pCU 9.12E+00 + 2.0E+02 CAT 2.7E+00 Lab<br />
PplmB: 1.5 / UNin: L / , ml Be(; Alq): -9.36E-03 So): -4.21E-06 LI8): 4.21E+00 + 1.6E+02 I I.OE+00 Mq<br />
LIE<br />
Quanterra Environment Se rvices, SCP V2. 0 3<br />
p
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES T B98-061 -I6 PaRe<br />
Collector/ /<br />
a/t r4 J1 RAld<br />
Project Dealgnation<br />
105 -C Phase 1 R Phase II - Concrete Samples<br />
Conlini ('unlact 7 elepbonr No.<br />
Steve Maroc J7J-4716<br />
ampling Location<br />
I OO Atea<br />
Project Cnordinalnr<br />
W11S. S, lit.<br />
AF No.<br />
1198-061<br />
I" Cheat Na Field Logbook No. .Method of Shipment<br />
Mpped To<br />
Quanterra Incorporate)<br />
POSSIBLE SAMPLE IIAZARDS/REMARKS<br />
Radloaetiv<<br />
peclal Handling and/or Storage<br />
{land deliver<br />
Offsiie Properly No. hill of LadinR/Air hill No.<br />
Prese rvation<br />
T) or of Container<br />
"°^°<br />
No. of Cnnldner( s ) 7<br />
Volume<br />
s^^^ Ce)Da^7S<br />
SAMPLE ANALYSIS<br />
^03a ^'•I m g03X7,)- PC,4<br />
Sample No. Matrix • Sample Date Sample lime<br />
1. O Z Other Solid 3 —/6^ f U<br />
CHAIN OF POSSESSION Sign/Print Names<br />
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-14 Page 1 of !<br />
Collector company Contact Telephone No. Project Coordinator Data 'turnaround<br />
to o+Mhrr 3 A!11 /1 Steve Marske 3734316 WEISS. RI.<br />
4 I<br />
Project Designation /'\,<br />
Sampling Location SAF No.<br />
105-0 Phase 1 & Phase 11 - Concrete Samples 100 Area B98-061<br />
Ice Chest No. Field Logbook No. Method of Shipment<br />
Hand deliver<br />
- hipped To Offske Property No. Bill of Lading/Air Bill No.<br />
Quanterm Incorporated<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
Radioactive<br />
S pecial Handling and/or Storage<br />
S.-vNIPLE AN'AIA SIS<br />
Preservation<br />
Nape<br />
T) pe of Container P<br />
No. of Container(s1<br />
A'olume<br />
u.<br />
sec eem al i ^^<br />
Special<br />
Inswnlo^.<br />
Sample No. Matrix Sample Date Sample How .. .»r a __ .., ^<br />
BON693 02 Other Solid ._ 6 p<br />
21 Days<br />
CII N OF P SS.FSS ON<br />
R<br />
^ery^^ pl<br />
y D<br />
^ ^<br />
I?/ C<br />
Sign/Print Names<br />
A ^<br />
h^<br />
IJate'I c<br />
2<br />
/<br />
?/<br />
//'<br />
/_<br />
SPECL%L INST] tIONS<br />
fll lU'Meia6-bU1041Jupenrao 1, 1.cad;-Memw.-74-1- ICVL Chronmunlie'- 71 96.<br />
PCBs roscopv Q,smm-137_ Cobalt-60, Lawtalim-152.<br />
Furop um I ^1 Cumpwm I n Ai enaum-?GI Imtopie Plwmuum. Isotopic lJrann lm_ Sale<br />
^ /<br />
/^<br />
(Aj"V( — /^/3^ 9<br />
s<br />
St<br />
s0<br />
Si<br />
Matrix<br />
Snit S.Emc^<br />
-- Solid<br />
= Sluay.^<br />
6v Relinquished By Ua le71lnc Rece . ced B1 ^ryVL'^<br />
lI..CC.. t_<br />
)ale.Time l<br />
^^—^ ^^— ^^_ ^r -<br />
1)<br />
t<br />
- N'a^a<br />
- Olt<br />
Reli ted BS hale I mx Rewncd Bc Dale-lime<br />
echne-h'urv^ - `I q<br />
J<br />
r, 4
Bechtel <strong>Hanford</strong> Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-15 F! ,f 1<br />
Collector /^^ 7<br />
ISr1`fq .v+<br />
^,y {^ (<br />
Project Designation Sampling Location<br />
1051' Phase I & Phase II -Concrete Samplcs<br />
100 Area<br />
Compa nN Contact Telephone No.<br />
Steve Marske 373-4316<br />
Project Coordinator<br />
WFISS. RL<br />
'AF No.<br />
B98-061<br />
Ice Chest No. Field Logbook No. Method of Shipment<br />
Hand deliver<br />
Shipped I o<br />
Quanterra Incorporated<br />
POSSIBLE S,\htI'Lf: 11:\Z.\RDS/Kt:\I:\1265<br />
Radioacinc<br />
)(life Propert N .N o. Bill of Lading/Air Bill Nn.<br />
I'rescn'alion<br />
Tcpe of Container<br />
No. of Cunlainer(s)<br />
pecial Ilandling and/or Storage \. 1 rent<br />
nonr --<br />
II.<br />
s.e urin U i ^<br />
spe^al<br />
SA M P[ E ANA 1.1 S IS °51N°°°`<br />
^03^? X11 Cl^ rti1 ^D^^^^^ ^^(<br />
Sample No Matrix " Sample (late Sample Time J- .. --<br />
BON694 03 Other Solid<br />
l)<br />
S G<br />
N<br />
Data I urnaround<br />
S / }L<br />
21 Days<br />
SPECI:A1, IN'STRt'CI IONSNtaulx<br />
CI P IN OF 'OSSESSION Sign/Prins Names<br />
F / _ IulclNt 1 i. e 1 A.NI, ", - I I( I a rr,.<br />
s. ,.a,,.<br />
Sel ui' ^<br />
I<br />
N.^^,^J<br />
qq pp )a l e linen kece b, Ual is I'( 11 41 80 1io i 1 Cin AI CCrtrs op C Is'. t b h 60 ( uuopiiiiii I'' so s.^<br />
I.i ,hr .............^.:, ni..ic ._'41. I. n.pJlrno 6nopicLen n<br />
N-CLLL /b ^p'lyC^ lZ/5 C<br />
SJ< SI ,i1ue<br />
^7 q<br />
keLnquahed lac __-- Uom llmc aca-n u113.Deie'Iim^<br />
--7,7.<br />
^^<br />
l/lM<br />
rl f "^ {<br />
CC..^^ I<br />
clinqunacd I{, iLeo Ilwa kecur cJ b, Uam linen °`'r r { l//ti-e b^r / -<br />
ehnyuuhN U. Unir lnr,^ Remir ad I4 hntc lnn^<br />
S1. C [ ION<br />
FIN.AI. tiA AII'Lt_ U I d Ata h o a<br />
DISPOSII ION<br />
_<br />
1—all-<br />
/ A G^ 3 , cJ//.^<br />
_ Unl .cJ B Uuc I unc<br />
Ua In.
Res Environmental<br />
Hestoratlon<br />
Contractor<br />
^^^ Team<br />
Interoffice Memorandum<br />
M D. A. ^4. John 1.0-19<br />
t 0M.N.<br />
See Below<br />
t'"TE:<br />
IRON:<br />
373 c'.17g<br />
1^cbruary 27. 1999<br />
S. L. Winslow AV<br />
RadCun Engineering<br />
X3-41/531-0706<br />
SUBJECT. CURIF ESTIMATE FOR SHIPPING CONCKETE CORE SAMPLES<br />
Job No. 22172<br />
D. D. »-A<br />
OC 10.c<br />
q w<br />
suww. cod. IM<br />
C C N: 055OHN<br />
The following Calculations show that core !iampleswith a direct reading of equal to or less than<br />
400.000 dpm/l 00cm'will be below the definition ofradivactive material as defined in 49 CFR 173.40;<br />
of 70 Bq/g (2F.3 pCi/g). Lerch sample will consist of concrete material Bonn four, two inch core<br />
samples and enough water to make a slurry consistency. 'Fhe dist ri bution al radionuclides is based on<br />
previous concrete samples taken from the below grade Fuel Storage Basin that would also be<br />
representative of these concrete samples.<br />
"vet :<br />
Cylinder Volume _ nr'h Radius of concrete core (r) = I inch<br />
Concrete Density = 2.35 g/Cm' Height of core sample taken (h) - 0.25 inches<br />
27 pCi = Bq Maximum tfrrect reading on core = 400.000 dpm/ 100cm1<br />
2.21 2 dpm = pCi<br />
Calculations:<br />
V - (3.14) (1 in.) 4(U.25in) = 0.78 in' (16.4 cot'/irrj (4 care samples) = 51.7-1 cm'<br />
(400.000 dpnl/5 1. 2 cm) (cm'/2.35 g) = 3.32EI dtm/g<br />
3.320 dpm/g (pCi/2.2 dpm) = 1.5E3 pCUg or 55.4 Bq/g<br />
SI . W Ald<br />
Percent Distribution(%) Cortcentration (VCi/g)<br />
"Co 0.17 2.55 pCi/g<br />
137<br />
Cs 82 1.2E3 pCi/g<br />
02Eu 0.33 4.95 pCi/g<br />
`Eu 0.05 7.5E-1 pCi/g<br />
"'Sr 17 2.55E2 pCi/g<br />
Z41<br />
Ain 0.005 7.5F.-2 pCi/g<br />
2J'U2 4U<br />
Pu 0.1 L5 .i/<br />
Co ies:<br />
S. G. Marske X5-53<br />
P. A. Newman X3-41<br />
RadCun Enginee ring File/LB XO-23<br />
<strong>Document</strong> and Into Services 110- 09<br />
TD'fAL: 1.4683 pCUg<br />
G1^1
Figure 1<br />
SAMPLE CCK-IN LIST<br />
Date/TlmeReceived: ^^ ^^^^^ SG#:<br />
Work Order Number. 0 ^3 7<br />
r<br />
RFS H-SOW-93-0003<br />
Revision 5<br />
^ ^^0^ SAF #: oU^i -<br />
Shipping Container lD: O) Chain of Custody # /^0 "(',&/-<br />
1. Custody Seals on shipping container intact? Yes eNo<br />
2. Custody Seals dated and signed? Yes KNo [ ]<br />
3. Chain-of-Custody record present? Yes [>r No [ ]<br />
O<br />
4. Cooler temperature<br />
5. Vermiculite/packing mate rials is Wet [I Dn/^^<br />
6. Number of samples in shipping container.<br />
7. Sample holding ti<br />
mes exceeded? Yes [ ] No [4---<br />
8. Samples have:<br />
_ Llape<br />
custody seals<br />
hazard labels<br />
appropriate sample labels<br />
9. Samp s are:<br />
n good condition leaking<br />
broken have air bubbles<br />
10. Where any anomalies identified in sample receipt? Yes [ ] No<br />
11. Desc ription of anomalies (include sample numbers):<br />
Sample Custodian/Labor/ UL ^^ Llj4<br />
Telephoned To: On C/<br />
I
Client Sample Screening Results<br />
17-Mar-98<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
Bill B0HJI0 3/17/1998 QUAD21B 3/17/19989:38:04AA1 BOH1I0 30 11 0.32 107 2.6266667<br />
SOLID Bkg: 3/17/199812:19:30 A61 BKG 600 28 0.04666667 564 0.94<br />
Ant Date: 3/17/1998 Tot Sa, Alq: 5.00E+02 1.02E+02 Alp; (DpM 2.10E+00 (uC7/ 4.66E-03 (pCU 9.33E+00 ±5.3E+00 CAT 5.4E+00 Lab<br />
Ppt mg: 101.6 / );nits: G mg Bet; Alq): 5.73E+00 Sal: 1.27E-02 LIg): 2.54E+01 ± 3.4E+00 I 3.9E00 Alit<br />
Dill 13011/11 3/17/19')8 QIJAD21C 3/17/I9989:38:04AM 8011111 30 13 0.37333333 308 9.2816667<br />
SOLID Bkg: 3117/1998 12:19:30 A11 BKG 600 36 0.06 591 0.985<br />
An] Date: 3/17/1998 Tot Sa, Alq: 5.00E+02 9.95E+01 Alp; (Dpm/ 1.90E+00 (uCV 4.31E-03 (pCU 8.62E+00 ± 5.4E+00 CAT 5.8E+00 Lab<br />
Ppt mg: 99.5 Units: g mg Bet; Alq): 2.06E+01 Sa): 4.66E-02 Llg): 9.32E+01 +5.9E+00 I , LIE+00 Alq<br />
"It<br />
BHI BOHJI2 3/17/1998 QUAD21D 3/17/19989:38:04Abi BOHJI2 30 12 0.34666667 212 6.1383333<br />
SOLID Bkg: 3117/1998 12:19:30 A.\I BKG 600 32 0.05333333 557 0.9283333<br />
And Date: 3;17/1998 Tot Sa, Alq: 5.00E+02 9.91E+01 Alp; (DpM 1.98E+00 (uCU 4.50E-03 (pCU 8.99E+00 ±5.4E+00 CAT 5.6E+00 Lab<br />
Ppt me: 99.1 Units: g mg Bet; Alq): 1.36E+01 Sa): 3.10E-02 Llg): 6.20E+01 +4.9E+00 I ,- 1.6E+OU Alq<br />
LIg<br />
Bill BOHJ13 3/17/1998 QUAD22A 3/17/19989:38:08 AM BOH113 30 1 -0.0183333 346 10.638333<br />
SOLID Bkg: 3/17/1998 12:19:41 AM BKG 600 31 0.05166667 537 0.895<br />
Ant Date: 3/17/1998 Tot Sa, Alq: 5.00E+02 9.87E+01 Alp; (Dpm/ -7.95E-01 (uCU -1.81E-03 (PC[/ -3.63E+00 ±4.6E+00 CAT 5.0E+02 Lab<br />
Ppt me: 98.7 Units: g mg Bet; Alq): 2.30E+01 Sa): 5.25E-02 LIg): 1.05E+02 +6.IE+00 I 9.5E-01 Alq<br />
LIg<br />
Bill BOHJ 14 3/17/1998 QUAD22B 3/17/19989: 38: 08 AM BOHJ14 30 20 0.59666667 670 21.385<br />
SOLID Bkg: 3/17/1998 12:19:41 AM BKG 600 42 0.07 569 0.9483333<br />
And Date: 3/17/1998 'rot Sa, Alq: 5.00E+02 LOSE+02 ,Up; (DpM 2.83E+00 (uCi/ 5.91E-03 (pCU 1.18E+01 +S.IE+00 CAT 4.2E+00 Lab<br />
Ppt mg: 107.8 ))nits: g m g Bet; AI9h 4.74E+01 Se ) : 9.90E-02 L e): 1.98E•+02 ± 8.0E+00<br />
I<br />
S.IE-01<br />
LIC<br />
LIg<br />
Bill BON692 3/17/1998 QUAD22C 3/17/19989:3808AId BON692 30 7 0.19166667 310 9375<br />
LIQUID Bkg: 3/17/1998 12:19:41 AM BKG 600 25 0.04166667 575 0.9583333<br />
AN Date: 3'17'1998 Tot Sa, Alq: 100E+00 1.00E+00 Alp; (Dpn,/ 2.40E-01 (uCV 1.08E-04 (pCU 1.08E+02 + 1.9E+02 CAT 2.3E-01 Lab<br />
Ppt mg: 04 Units: I, ml Bet; Alq): 1.73E+0i Sa): 7.81E-03 LIg): 7.81E+03 +4.9E+02 1 64E-03 Alq<br />
LIg<br />
CI<br />
F-+<br />
T 17-Afar-98 Quanterra Environment Services, SCP V2.03<br />
C.7
L^<br />
T J<br />
CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B<br />
BHI BON693 3/17/1998 QUAD22D 3/17/19989:38:08 AM BON693 30 7 0.16166667 117 2.96<br />
LIQUID Bkg: 3/17/1998 12:19:41 AM BKG 600 43 0.07166667 564 0.94<br />
Ant Date: 3/17/1998 Tot Su, Alq: 1.00E+00 1.00E+00 Alp; (Dpm/ 6.55E-0 1 (uCl/ 2.95E-04 (pCi/ 2.95E+02 ±3.7E+02 CAT 8.5E-02 Lab<br />
Ppt mg: 512 / URNS: L -! ml Bet; Atq): 6.09E+00 So): 2.74E-03 Llg): 2.74E+03 ± 3.4E+02 I LSE-02<br />
BID BON694 3/17/1998 QUAD23A 3/17/19989:38:12 AM BON694 30 6 0.11166667 57 0.8816667<br />
G 3LIQUID Bkg: 3/17/1998 12:19:48 AM BKG 600 53 0.08833333 611 1.0183333<br />
An] Date: 3/17/1998 Tot So, Alq: 1.00E+00 1.00E+00 Alp; (Dpm/ 5.45E-0 1 (uCV 2.45E-04 (pCl/ 2.45E+02 +3.8E+02 CAT 1.0E-0 1 Lab<br />
Ppt mg: 5$. 1 UNta: L / ml deh, Alq): 1.78E+00 Sa): 8.02E-04 Lg): 8.02E+02 ± 2.4E+02<br />
1<br />
6.2E-02<br />
LIIg<br />
BHl B0N8616 3/17/1998 QUAD23B 3/17/19989: 38: 12 AM BON8M6 30 119 3.92 5799 192.32333<br />
LIQUID Bkg: 3/17/199812:19:48 AM BKG 600 28 0.04666667 586 0.9766667<br />
And Date: 3/17/1998 Tot Sa, Atq: 6.00E+00 1.00E+01 Alp; (Dpm/ 7.45E+00 (uCU 2.01E-03 (pCl/ 3.35E+02 +4.OE+01 CAT 7.5E-02 Lab<br />
Ppt mg: 3.5 ,/ UNb: L ml Bet; Alq): 3.66E+02 So): 9.88E-02 Llg): 1.65E+04 ± 2.2E+02 1 , 3.0E-03<br />
BHI BON8Af7 3/17/1998 QUAD23C 3/17/1998938- 1 2ANI BON8M7 30 23 0.71833333 107 2.6683333<br />
LIQUID Bkg: 3 1 17/1998 12:19:48 AM BKG 600 29 0.04833333 539 0.8983333<br />
And Date:<br />
Ppt mg:<br />
3/17/1998<br />
5.9 !<br />
Tot Sa, Alq: 6.00E+00 /<br />
UNb: L<br />
1.00 E+01<br />
ml<br />
Alp;<br />
Bet;<br />
(Dpm/ 2.18E+00<br />
Alq): 4.79E+00<br />
(uCl/ 5.89E-04<br />
So): 1.29E-03<br />
(pCl/<br />
Llg):<br />
9.81E+01<br />
2.16E+02<br />
±2.7E+01<br />
+ 3.0E+01<br />
CAT<br />
I<br />
2.5E-0 1 Lab<br />
^-<br />
2.3E-01<br />
Alq<br />
LIg<br />
BHI BON8M8 3/17/1998 QUAD23D 3/17/199893812Abf BON 10,1 8 30 36 1.13666667 114 2.89<br />
LIQUID Bkg: 3/17/1998 12:19:48 AM BKG 600 38 0.06333333 546 0.91<br />
And Date: 3/17/1998 Tot So, Alq: 6.00E+00 1.00E+01 Alp; (Dpm/ 3.46E+00 (uCl/ 9.36E-04 (pCl/ 1.56E+02 + 3.0E+01 CAT 1.6E-0 1 Lab<br />
Ppt mg: 3.5 / Un1b: I. / ml Bet; Alq): 4.83E+00 Sa): 1.31E-0 3 Lg): 2.18E+02 +2.9E+01<br />
I /<br />
2.3E-0 1<br />
AI<br />
Llg<br />
17-,Liar-98 Quanterra Envi ronment Se rvices, SCP V2.03<br />
!'^,71 i<br />
LIg<br />
LIg
1(`uanterra<br />
Soria<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
ANALYSIS A^ _MATRIX 0 TYW'R DUE DATE y -6 -`t<br />
I^ R`t C-T--rnENr<br />
WORK ORDER SEQUENCE # CLENT COMhom<br />
J 03161 -1B<br />
QCBATMFEACrENTMANK<br />
6^+1<br />
J N a. -ix QC BATCBMAIM BI ANK<br />
J o b t b l -iM oQ<br />
(circle)<br />
J 2M or 2S<br />
(fie)<br />
D o3tbt -O^<br />
!Sb3l6to\ J 1 `^<br />
gu3 J$gO2<br />
803 Zo(o O Z.<br />
03 222.02<br />
$03 Z'7 2_O1<br />
Batched and QC updated bye on 3 •Z5-^<br />
QC BATCHMAMUXREAC0;r<br />
SPOM<br />
QC BATC HMAIRDVREAGENT SPUKE<br />
Duplicate ofSamo # $0 3 t b 1 01<br />
Rec'd in Prep Lab by on Z" _W Sop# tLtF RCSot Rn'- 0 _<br />
Rec'd in Sep Lab by v a/ on— Sop# Rn i<br />
Rec'd in Sep lab by on Sop# Rte=<br />
EDY ^P by<br />
on `I - 3 - C<br />
Sop# i^ i C h ,l C 5 U 0<br />
^^ 11nn<br />
rr %<br />
by l an Sop# 6 ^Cl QQQ ^- Rid 6<br />
Rec'd in C.R j 3 'T<br />
Da ta Reviewed byon^ Sop# 6 Cr/ (sF?1^7. M-4 Z^<br />
O riginal batch sheet complete akvl u n file to be filed with the FIRST listed work order number.<br />
FORM NO.: RC-52.1/98. Rev. 8 2Faceo n^,G c<br />
CRT<br />
RPT u .TS = ^C^^S^ S(^ ^2u^ o s o^ O e yccw^ -^ nor rc 1 sA<br />
CT<br />
= \c0<br />
GI^,,<br />
c,T- =N 5 T = A-s p ^ ^ —
\^ ^c CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 10-Mar-1998<br />
Page 1<br />
' CUSTOMER: BHI SAMPLE DELIVERY GROUP<br />
^p<br />
11ATRIX OTHER ^ BATCH NUMBER<br />
CUSTOMER<br />
LIES ID DUP ACCOUNT ID COMMENTS<br />
5A, A^<br />
Ser)_<br />
__°_______=====ESJA625 ---------- ==<br />
To3^b1\S IQO129 )<br />
1 ) 80316101 ESJA626 II BON680 O.000S6 8-<br />
Pr.11/2 4 /91 91,11/29.98<br />
2 ) sea t 6t62 6H f s vriooi<br />
— '7t p?^16101<br />
ESJA627 p.oco3' 73<br />
J^AjCQTIONS (Initial !. Date)<br />
9<br />
1) INITIATED l ^ l !D 5) COUNTINC/MEASUREMENT LAB<br />
SOPS) #<br />
SOP (5) #<br />
2) PREP LAB RECEIVED l9scY o.L 6) DATA REVIC:WED AND<br />
ANALYTICAL_ PREP STORED<br />
SOP(.`' .-) ;# {iy Np^So3 0<br />
3) SAMPLE REMAINDER STORED 3-2S-7,y<br />
SOP (s) I) , xo-<br />
4) SEPARATION 1-AD RECEIVED<br />
`iiiP i S) ,^<br />
SOPS) #<br />
_<br />
--<br />
UIZu
lV<br />
V i<br />
l ` ^Ulx CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 11-Mar-1998<br />
1^I V Page 1<br />
^Y •<br />
CUSTOMER: DHI<br />
SAMPLE DELIVERY GROUP (,^oaa-7.^<br />
W0<br />
j<br />
MATRIX OTHER V -W/ HATCH NUMBER 03<br />
1 )<br />
2 )<br />
3 )<br />
CUS 1'OMER<br />
OES ID DUP ACCOUNT ID COMMENTS<br />
5 A, M*L<br />
CS r^<br />
80318402 E SJA628I BOP4's 3 0.00 0355<br />
Pt.11 /24 / 91 81-11/24.98<br />
863r "^' -I3PI^ 89)1684<br />
ACTIONS (Initial & Date)<br />
1) INITIATED<br />
Wu-<br />
^^<br />
a) SCP(Si #<br />
5) COUN T INWM-A- ,_RE', FNT . La<br />
EDP (5) # _--<br />
2) PREP LAD °E'`lVFD 6) 0-A-A R;-:'J(1- ED AND<br />
- ---- ANfiLYT7CiiL FP,EP STORED<br />
SCF(S) ff (^ H(mac SO 3^<br />
Off,(• -<br />
3) L E R E l , tA'_NDER S--0RE0 3.26siP - Qws<br />
4) SEPAR?iTION LAC RE:_:=i`.'I)<br />
soli (^) 's ..rte<br />
iiUri 5; ii<br />
V ti
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1995<br />
Page I<br />
;j CUSTOMER: BHI SAMPLE DELIVERY GROUP 03 0,^<br />
O<br />
-a^/^/^-<br />
MATRIX : OTHER ^ U -Ov I BATCH NUMBER 03 'a^<br />
CUSTOMER<br />
QES ID DUP ACCOUNT ID COMMENTS<br />
SPrrwM<br />
1 ) 0a296Q! — -BFII 900160w<br />
2 ) 80320602 ESJAG29<br />
Pr.11124/9' E%.11124.98<br />
I BON636 0 .00083b<br />
3 ) 80220 699 BI IT B6P 16E3<br />
ACTIOj4S (Initial °. Date)<br />
1) INITIATED ^A ^5) COUNTING/PIEASUREPIENT LAD _<br />
nnj^<br />
SOP (S) it /\j—) SOPS) #<br />
2) PREP LAD RECEIVED 3-11^_ rl k a,< 6) DATA REVIEWED AND<br />
ANALYTiCP,I. PREP STORED<br />
SOP (S) 9t ?JSagC5o 'S--o<br />
3) SAMPLE REMAINDER STORC{D -3 (,AP' °C<br />
4) SEPARATION; LAO PECEIP -D<br />
SO(' i S) It ... 4..<br />
SOP (8) !1<br />
SOP(S) #<br />
Gl^^i
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G<br />
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CUSTOMER: BHI<br />
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998<br />
Page 1<br />
SAMPLE DELIVERY GROUP<br />
^(<br />
MATRIX OTHER (^' BATCH NUMBER 03 o<br />
CUSTOMER<br />
QES ID DUP ACCOUNT ID COMMENTS<br />
S ^ Aug<br />
1 80322201<br />
3 •^<br />
2 ) 80322202 I BON689 0.000GS5<br />
------------- --------- ------------ ----- - -- ------------- --<br />
ACTIONS (Initial `z Date)<br />
^^.)l/<br />
1) INITIATED zo V1 ;51g9 5) C'UNTINC/MEA5UREi •1ENT LA3<br />
SOP(S) # SDP(S) #<br />
2) PREP LAB RECEIVED 3-L9- '^t 1' orc 6) DATA REVIEWED AND<br />
ANALYTICAL PREP STORED<br />
SOf (s) ;ir^ttg:cam<br />
SOP(<br />
3) SAMPLE REMAINDER STORED 3-_zb-Q Fos<br />
4) SEPARATION 1- A0 RECEIVED<br />
SOP(s) 4 J^<br />
SOP(S? It<br />
)n<br />
6121
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^1 -,CIlO<br />
USTOMER: BHI<br />
MATR D: : OTHER<br />
- AMFL.E CELIVER' : .-R - 1 -11'<br />
B A T:H NUM'-R<br />
93<br />
CUSTOMF_R<br />
OES ID OUP ACCOUNT ID COMMEN-"5<br />
Sl:- A JJ,4^<br />
1 ) 80327201 D ' , - I 00116 172 C.000(o ^- 7<br />
3 4 SQQQ' " a4 •arc n 01.i(-aa<br />
--------<br />
irtitiaL '< Dc'.:e<br />
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1INITIATED Jo<br />
"' S) C .^.^INTi": /;1-ASURE"iF_NT -`.3 —<br />
EOP (5) # ^SOf (S `'.<br />
2) FR=P LAB RECEIVED 1)-TA REVD: *WED AND<br />
ANALYT'CiAl- PREP STORED<br />
3) S-,^IPL.E R7- )T r•d nF--F c-I it L-<br />
4) -cr ARri 1. i^fJ i_."' LV:_LJ<br />
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BATCH SUMMARY/CHAIN OF CUSTODY<br />
ANALYSISA--z-yr mmix dMINF-L DUE DATE -b- ct8<br />
S w RRy<br />
_ WORICORDER SEQUENM0 CLIENT coheAwn<br />
J cJ-sI Fr 9 -IB QC BATCH REAG'FNT WAka<br />
J N 14 ix QCBATCHMATRi 3-e&<br />
I O 31&4 -IMot©<br />
(ank)<br />
j -2M or 2S<br />
D O3 Zoe<br />
(aide)<br />
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QCBATCHMATRIX/R C NT<br />
SPUM<br />
^S 0:s t^401 03 zsR<br />
^b -5 16102 1'4<br />
$03 zo6ol b3 2 S^<br />
^t7322201 -^' 1"<br />
^O TJ 2'-1`l 01 bZ<br />
$03 2 r ? bz<br />
03<br />
Batched and QC updated by ^ on 5-is -'JY<br />
Rec'd in Prep Lab by -.p a on 3-t5 4<br />
Rec'd in Sep Lab by > on-]?<br />
Rec'd in Sep lab on<br />
ED/^PP^y ^^ on Y- 3 -^^ S<br />
^/ J<br />
QC BATCH MATRDMMACENT SPHO<br />
Duplicate of L ple #_3T3 zo 603<br />
Sop# 1Z^cs1QCSr) Re47_<br />
n,<br />
Sop# ^1C^^C S^ Rn'^<br />
Rev3<br />
Sopy fZ i C N TIC JO^2 Retii<br />
Rec'd in C.R. by on Sop# Red<br />
Data Reviewed by on Sop#<br />
L2Rna<br />
^7y<br />
Original batch shee and complete calculation file lobe Wed with the FIRST fisted work order number-<br />
FORM NO.: RC-52,1/98, Rev. 8<br />
IZ^ utj.T-s S PF 5^ ^^ 3/^UG^ C^<br />
CT Tw nE = too Mw ^^G^ ^l _ p i /.<br />
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sp^ "A4-<br />
ESJA623 O.C)?-Lk-7<br />
Pr. 11/24/97 91.11124.98<br />
ESJA624 0 - P- Z-14<br />
Pr.11/24/97 81 .11/24.9 8<br />
jo<br />
2 5 --cL<br />
G I I-)
C%ivanterra<br />
Emimnmlmd<br />
Senxu<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
ANALYSIS Peso MATRIX o ihF--e- DUE DATE q-C `t8<br />
s^^ RRy<br />
WORK ORDER SEQUENCE CLIENT COMMENTS<br />
J oil Sr y -1B<br />
bbl<br />
QC BATCH REAGENT BLANK<br />
1 f-i (4 -1X QC BATCH MATRIX BLANK<br />
J t m l" -IM oQ<br />
(Ckk)<br />
J lq -2M or 2S<br />
(cycle)<br />
D 0 3 Z.ob ' 03<br />
QC BATCH MATRDUREAGENT<br />
SPIKE<br />
So^1^401 03 zs A,<br />
^b3l6toz<br />
a la<br />
$ p 3 z.obol 03 5 4<br />
^IJTa?-Z2ol<br />
N la<br />
Fr 0 ,6 02<br />
$03?rl?4b'z-<br />
03<br />
Batched and QC updated by w - on 3- 2. s-4X<br />
Rec'd in Prep Lab by :]^ aL on-3 t°r 4d<br />
Rec'd in Sep Lab by---O on ^' )<br />
Rec'd in Sep lab by on<br />
(E^/CPPT by Its on 3 C g<br />
QC BATCH MATRM REAGENT SPIKE<br />
Duplicate of Sample # %' 03 7. 06o3<br />
S 0134 RICS-1QCSOV3 Rev#_<br />
Sop#.0 ^r,^ ^'S 7<br />
Sop#<br />
Rev#<br />
^/ 3/ ^t ( Rev#<br />
Sop# _ !C ( (^ U 3 1 Rev#<br />
Recd in C.R. by on^'^/9^ Sop#a1 C1711eDL,)X 9 Rev# J<br />
Da ta Reviewed by on I I T Soo_ ^'C 2p-2— Rev#<br />
Original batch sheet and omplete calculation fi le to be filed with the FIRST fisted work order number.<br />
FORM NO.: RC-52,1/98, Rev. 8<br />
Rf ^ urn= ^e_^(5r«<br />
Lr T^ V-+^ = 2.00<br />
C- T- =n 5T =<br />
f-- L<br />
G I J 8
-<br />
3b3 fr`11B ESJA613<br />
_ 3oswAIS I2HI225 1<br />
ESJA614 p.pZio<br />
Pr.11/24191 91.11/24.90<br />
-Doc<br />
"-° -<br />
ESJA615 - _ -- --<br />
Pr.11124191 6%.:1124.90<br />
3-1q 1t F ova<br />
^ \-ce+acSo%3-'Z:5<br />
3•zs 1t^ o t<br />
r^<br />
p.ozi9<br />
G1i9
v't_J<br />
ESJA616<br />
___Pcll/24/918%.11/24.98<br />
25 -`L<br />
5R- RNAL<br />
`Irjr-19' , U<br />
C1•t0
f308 -CIO<br />
-- - - ESJA617 - -- -p.OZd'1<br />
Pr. 11/24/97 81.11/24.98<br />
.---<br />
_ - .5 zs ax<br />
ESJA618<br />
Pr.11/24197 81.11/24,98<br />
-- - ESJA619<br />
D032o603 Pr.11/24/97 81.11124.98<br />
3 lg 'Uv-<br />
c^^ ^H2cSOCs ^o<br />
3^ZS-42r o^<br />
N^<br />
0 •oZ`1S<br />
- -----<br />
U14.i
SISS^i -SS^^--<br />
-- ESJA620<br />
Pt,11/24/91 U.11/24.98<br />
h I) S<br />
R ^c uri c so ^S -o<br />
J-zS `iFs^<br />
O.O ZSS<br />
Ll^^
-- -<br />
_ ESJA621 O.OZ3`F<br />
Pr.11/24/91 Br nne as<br />
- -------- -. ESJA622<br />
Pr.11/24/91 IX.11/24.98<br />
R^ceF2c5a,3-^<br />
3-2-5-tir o„ cl<br />
N<br />
Y ^
Olb /<br />
3 -Zs 'Y<br />
ESJA623 - --<br />
Pr.11124197 3%.11/24.98<br />
ESJA624<br />
Pr.11124 191 31.11/24.98<br />
R^^2cso^3^<br />
3-25-`i e- out<br />
5H- Avtm<br />
Q' OZ^ 1<br />
x_02 zV<br />
6l ti
N.rmanterm<br />
se.^<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
ANALYSIS Pu00 MATRIX 0 TtW±j DUE DATE y-6-cLk<br />
tip"( CS m wr<br />
WORK CRDER SEQUA a # amir COmmem<br />
J o 5 l b l -1B QC BATCH REA(EN M ANK<br />
J N 1n. -ix QCBATCHMAMUSAW<br />
J o 3 L 61 -imam<br />
(dale)<br />
J N 2M or 2S<br />
(drde)<br />
D o3ibt -Qt<br />
p^Tj 16101 ^' 1"<br />
go3 t8`{o2<br />
8o3 Zob oZ<br />
p3 22.Z02<br />
$03 Z'7 L0^<br />
Batched and QC updated by-^i ec on 3 Z5-%<br />
3•<br />
QC BATCH MATRDOMAGENT<br />
SPIIKE<br />
QC 13ATCH MA2RDORFAGENT SPM<br />
Duplicate of Sample # $A 3 -IN lb<br />
Rec'din Prep Lab by ^ on 3_ 19_4 Sop#RtCt Q-So13 Re,4 0<br />
? C<br />
Recd in Sep Lab by on 76 Sop# L' ^' C c yCJ<br />
7 !^^IZ ^7 =e<br />
/,'C S7v<br />
Recd in Sep lab by on Sop# Rn:<br />
PPTby<br />
v<br />
on-3 Sop# Zict^ t• 39 Rn= 1<br />
Recd in C.R by on 31 3>1 14 Sop# r hi poa7 r R ^^<br />
jptq-1- i--K<br />
Data Reviewed by on 11' Sop#__ SC yam- JL,^i J<br />
L<br />
O riginal batch sheet complete calculation file to be filed with the FIRST Lsted work order number.<br />
FORM NO.: RC-52, M8, Rev. 8<br />
2^ w = e a-Z I SA<br />
Gr S.v9 7 = i`kect<br />
— { —<br />
StH ^QAC ^, v.. ,S o^DRy cew.e...Tj ^o .— to Tel S-`/^^.^<br />
6145
I<br />
^3^^^<br />
CHAIN-OF-CUSTODY B4TC1-i ANAL`(`.ilS RECORD 10-Mar-1998<br />
D9Page 1<br />
CUSTOMER: BHI E;At1P!_E DELIVEPY GROUP<br />
MATRIX : OTHER ^ ^ BATCH NUMBER O^'Jbl<br />
CUSTOMER<br />
OES ID DUP ACCOUNT ID COMMENTS<br />
.5,4 AuAI<br />
( ^s"<br />
__====3b3i6^=a ESJA625 _______-______-----=<br />
So3i6l Ls14HI326 l<br />
1 ) 80316101ESJA626 I BON6(30 p-0Ob36<br />
ouStsio( ESJA627<br />
2 ) F^p Pr.11/24/91 EI.11/24.98<br />
3 •u<br />
------------- ------ - ------------- --<br />
ACTIONS (Initial & Date)<br />
1) INITIATED^ 5) COUNTING/MEASUREMENT LAD _<br />
SOP(S) # _ SOP(S) # —<br />
2) PREP LAB RECEIVED 3 -09 4Y WI, 6) DATA REVIEWED AND<br />
ANALYTICAL. PREP STORED<br />
SOP(S) # ^icc+-¢cSO^b=o<br />
SOPS) #<br />
-3) SAMPLE REMAINDER STORED 3 -zc^r pn<br />
4) SEPARATION LAD RECEIVED<br />
90 p ( 01) f ^'^<br />
S u p (F) 3<br />
0146
)CUSTOMER- BHI<br />
MATRIX : OTPER<br />
OES TD<br />
PUI;,O#<br />
CHf;IN-OF-C'_! STODY SWCH ANALYSIS RECI ]RD 11-Mar-1998<br />
^<br />
q<br />
SAMPLE DELIVERY GROUP<br />
ID[ BATCH NUMBER<br />
CUSTOMER<br />
DUP ACCOUNT ID<br />
S h Awe<br />
1 ) BB8iB4i1 8i-ITr^OC BA^!E}-:^<br />
^ .L 6 4Y<br />
2 ) 80318402 ESJA628 I 1301,4 683 0.0003155<br />
Pr.11/24/9 1 91.11/24.98<br />
3 ) 8A8184HS 43itI3 ,-, --"-'3d<br />
JJ^^^^//'^^<br />
4it^ ^?S<br />
Page 1<br />
OL^Ts7F—<br />
COMMENTS<br />
RC TIONS (Initial !, Date)<br />
Q<br />
1) INITIATED ^^^ 5? c; UNTI'i^/MEASURE:`?ENT LAD<br />
SOPS) # SOP (S) #<br />
2) FREP LAB RE(,E T_ V F.) T S- k9 Y orL_-<br />
SUP (`:) , ._ R^trf^4So ^3 o<br />
3) 5=MPLE REi4Fl 17 ii'^:!* ST,-RF_O 3!Lb•^Y^ 4<br />
4) SEPARATION t.:=,C RF.0=IV.0<br />
,'tNALYTIC:'I_ PRE? STORED<br />
SOPS) #<br />
Ci^i
0 /qg<br />
CUSTOMER: BHI<br />
MATRIX : OTHER<br />
1 )<br />
QES ID<br />
*41 PUISO 4-"<br />
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1999<br />
Page 1<br />
^/^ SAMPLE DELIVERY GROUP<br />
1319-v" ) BATCH NUMBER<br />
booms<br />
03 -xi.10<br />
CUSTOMER<br />
DUP ACCOUNT ID COMMENTS<br />
SA- AWAi<br />
------------------------<br />
3-Lb<br />
2 ) E303206O2 ESJA629 I BON6360.0O0£eb6<br />
Pr.11/24191 8.11124.98<br />
3 ) "QO32 B er6 5 514 r-^nTeaa^<br />
3,Zy<br />
------ ----------------------------------<br />
A(^ TIGHS (Initial Datc)<br />
1) INITIATED<br />
l<br />
1^l^D `a) COUNTINO/MEASUREMENT LAB<br />
SOPS) 4k '/U1/V S7i'(S? m<br />
2) PREP LAB RECE' !)ED 75-t- p yvc 6) DATA P.EVI.vJEE AND<br />
ANALYTICAL_ PREP STORED<br />
3) SAI•iPLE REiMAIitD'i--F ST'JR' r) S,Z6-9S<br />
4) SEFARATION LAP RECEP.: L`<br />
SOP (3) #<br />
6:.40-
(^ ^Q<br />
*#* PUISO*#<br />
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998<br />
Page I<br />
CUSTOMER: BHI<br />
SAMPLE DELIVERY GROUP<br />
MATRIX<br />
Q /p<br />
OTHER Koo<br />
/ BATCH NUMBER 03'(29,;?<br />
1 ) s2ee<br />
CUSTOMER<br />
GES ID DUP ACCOUNT ID COMMENTS<br />
SR A+A,l<br />
3-x6 ,W<br />
2 ) 80322202 I BON6E90.00o655<br />
- -- ------- ------------------- - ----- ---------------- --<br />
ACTIONS (Initial '< Date)<br />
3<br />
1) INITIATED "1^^ 5? t:'UPITINr/M,=AStRci iENT - 8 __<br />
SOPS) if SOPS' it -<br />
2) PREP LAB RECEIVED _3- (gkY o^ h) DATA REVIEWED AND<br />
ANALYTICAL ?REP STORED<br />
90F(S) is _1Z cH?cS^^3a<br />
SOPS; #<br />
3) SAMPLE REMAINDER STORFD 3 -26 -2 P c-t^<br />
4) SEPARAT I ON _1;B PFi;= :`Jta;<br />
9 0P(S) it ^A<br />
SOP (3) ;i<br />
6149
^ CHAIN- O=-CUST77-`'( B?TCI- ANAL''P'iS RECORD 17-Mar-1995<br />
i l<br />
Page 1<br />
CUSTOMER: BHI SAMPLE DELIVERY GROUP<br />
/I)/^ ^f<br />
W(/^/<br />
MATRIX OTHER kJ `s - Ob / BATCH NUMBER Oc/ -az l OS<br />
CVSTOm<br />
GES ID DUP ACCOUNT ID<br />
5A. ANA-,<br />
COMMENTS<br />
(D rr><br />
1 ) 60327201 J " I BON692 0 •ooa^ 7<br />
2 ) 80'12720 2 BI iI 3 uAYBON69a<br />
3 )^B09272 39 BH; °"` 80W.694<br />
'ur<br />
6'4<br />
3•zc<br />
------ -------------------------------<br />
ACTiO 0IS (Initial & Date)<br />
1) INITIATEDO 5) C UN-I".=%i9EASURE''EMT Lr;3<br />
SOPS) # __.J>!^ SOP(-) #<br />
2) PREP LAB RECEIVED 3-( 9t -iY - 71^^ .<br />
SOPSS) i) ^tc^+ac5y3 ^<br />
3) SAMPLE REi"RI !')EP °.TOR-n<br />
4) SEPARATION L.-'<br />
:;C AP i ::^) nJ ^<br />
r_ rc":; )<br />
f,) 0,T„ REV r -_JED nMD<br />
Ai'iALY-iCAI- PREP STORED<br />
50f iS) #<br />
Gl;,o
RPj<br />
R 1'. ,'uanterra<br />
s^<br />
BATCH SUMMARYICHAIN OF CUSTODY<br />
ANALYSIS o-o MATRIX 0M %V*, DUE DATE 4A-b-aS<br />
S t-v RRy<br />
WORK ORDER SEQUMgCE 0 C[ma COMMe (g<br />
J-:3-S1&`4 4B3<br />
O ^l I<br />
QCBATCHREAGe rffiAW<br />
J N 14 -I% QC BATCH MATRM SAM<br />
1 031Fsy -1M ot©<br />
(dide)<br />
QC BATCHMATRUVRFACENr<br />
SPIIM<br />
J 2M or 2S QC BATCH MATRDORFAGENr win<br />
D O 32'1 z..<br />
Z Duplicate of Sample# $032'^ Zo z<br />
80 TS 1t4o1 03 zsR<br />
Fo3lbloZ<br />
a la<br />
$03 zo601 03 2 SA<br />
^032Z201<br />
.^ la<br />
Fr0b z yy ol oZ<br />
^03 Z'12bZ<br />
03<br />
Batched and QC updated by -DVc on 5-is-qY<br />
Recd in Prep Lab bY- oc- on 3 -ter 4d<br />
Sop#- '-uC C -U<br />
Rev# Q_<br />
Rec'd in Sep Lab by ^ .^ one^ - 36 SF Sop# &i &kf ,S 6 3 6 R--v# C`<br />
Recd in Sep lab by<br />
/CPPT by<br />
pp<br />
on<br />
^<br />
Sop#<br />
Sop#<br />
Rev#<br />
i 3) Rev#<br />
Rec'd in C.R. by f j ' a0 an Vw ^t Sop# a0»> r Rev# o<br />
^n<br />
Data Reviewed by i^ on' (^ GI gyp#<br />
O ri ginal batch sheet an complete calculation file to be filed with the FIRST fisted work order number.<br />
FORM NO.: RC-52,1/98, Rev. 8 S^<br />
t ^x^ra c ^^ 2 ti c-Ait1C ^u3<br />
= po- L /S ic^<br />
LT S tV 5T = At5 PEC-<br />
0151
_<br />
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_-_-__ESI27495 --<br />
X31 y`<br />
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s_o y9<br />
EQIE316<br />
\<br />
---__ So3 y _os<br />
^fr`1_ 0.03^34ode,<br />
lS .._... . _..,..,, fs a 1 -__ _ _-----_----- 5.ov^<br />
—<br />
ESI27496Ci•ozv3<br />
_ ,. _<br />
Pr. 73113/97 8x.:'_!13/9A 5.0 op 8<br />
s ss•t<br />
- ESI27497 6.0?z6 5 ^-7 1 ^ —<br />
P [.1?! 13 / 91 3x,'.2!' 3'9B<br />
2^c \+ec5^ \3 ^<br />
r ^-<br />
_<br />
-<br />
_-<br />
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ESI27498<br />
9r.12/13197 31.12 /13/9 2<br />
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e+C<br />
'-QUO 1<br />
-vU •. JF;^ ^^ lrC _—__<br />
5 A An Al<br />
SPe<br />
S-061-7<br />
-<br />
FE<br />
c153
AN+_'.,1 PECCPD—filar-194(3<br />
5 P, P ~ AIL<br />
ESI27499 -- — o.ozS7<br />
Pr,"/:: /97 ?a./:3133<br />
S-ZA4r<br />
ESI27500 - -- — -<br />
_ O .o^4Z<br />
l9 -4k<br />
V^^c rFecSo i3-o<br />
3-L6 ALP<br />
61-34
^1 v F7- 1 ,f -<br />
^cl C^<br />
5{f A.AI<br />
ESI27501 O•oab l -<br />
Pr.12/ 11 '3,1<br />
--- --- -<br />
1 3a:12/13/98<br />
..<br />
S- 0 5 9 So<br />
OdC-<br />
- - - - - - - - ---<br />
•xL'E1'<br />
nl^^<br />
- - - 3-Zl-q-a'<br />
{ZlCµ2CSo^3^ ---- -- -<br />
tiw<br />
C 15
- _ ESI27502 0.0ZS1<br />
Pr,12/13/97 Ba,12!13/93<br />
ES I27503 G<br />
Pr.;J'3/97 s"a 12/13/?8<br />
3 -4t c^^<br />
`tZ is t+^CCSa rS-o<br />
_ —_ _ 3-^b 2k art<br />
N ^'<br />
S o(o 17<br />
s 91 ^^<br />
-.<br />
_..---- -<br />
6156
---------- ESI27504<br />
..___L7o32'r ZO2 ESI27505<br />
_<br />
ESI27506<br />
1-2b-4Y o«<br />
^v<br />
$ k "At<br />
------ --- —<br />
p.oz a6
BATCH SUMMARY/CHAIN OF CUSTODY<br />
4 0 A A31s ut y0 MATPJX on-WA DUE DATE 9-6-9<br />
T5R`( Cam WT-<br />
_ F9 )P% CstDER<br />
1 Va __._ _ _- —<br />
l0 3 t 6 t -1M oQ<br />
SEQUFNM# QgNf COMMENTS<br />
-1B QC BATH REAGENT BLANK<br />
-IX QC BATCHMATRIX BLANK<br />
(arcle)<br />
I -2M or 2S<br />
(ar de)<br />
Do3tbt -fit<br />
^S17 -516 1 01 "' t °<br />
gu3 1$`^oZ<br />
8o3 Zob oz-<br />
-6 2ZZOz<br />
$03 Z'TZO\<br />
Batched and QC updated by^cz_ on 3 -25-alr/<br />
Rec'd in Prep Lab by on<br />
Rec'd in Sep Lab by<br />
74<br />
Rec'd in Sep lab by on<br />
3-<br />
_ onoa -a C -9 F<br />
Re<br />
(EL)/CPPT by /b on q /3'q g<br />
QC BATCH MATRDUREAGFNP<br />
SPDM<br />
QC BATCH MATRUMA(ENI SPUM<br />
Duplicate ofsample #X03 t b t o l<br />
Sop#RK-t''RCSot^ ReO Q<br />
Sop^^IC,.^P[' .sago R^?Q<br />
sops >2i CL-ec 57 3q Rcn'-<br />
Rec'd in C.R by on Sops Rte=<br />
Data Reviewed by / ' ^C^ ' p ^^<br />
Cl k y Sops -1 L I ^^ C E ^c Z R-<br />
Original batch sheet and mplm ration file to be filed with the FIRST' rioted work order number.<br />
FORM NO.: RC-52. 1/98. Rev. 8 1 ^— Qxtr 2^- ., ,^<br />
i<br />
4 z w 5 R,CNQ^_ °3•.<br />
5ET fRA^-no.J iS OF PRy ^c.w,a-..^^ n^oT 0^" l^rn{ SR.5-L6-`LS^<br />
C^T^-J i2a D.ru.o c0`3"- -<br />
R.PT llwtn = FCi-`spt CTTtw.Ec200 = IBS L G158
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 10-Mar-1998<br />
Page 1<br />
CUSTOMER: BHI SAMPLE DELIVERY GROUP<br />
MATRIX OTHER<br />
N-1611<br />
BATCH NUMBER (/'<br />
CUSTOMER<br />
GES ID DUP ACCOUNT ID COMMENTS<br />
SA-AuAL<br />
SI 7507<br />
^3 \61^^ ` ._<br />
_______=_______-___________________________<br />
i S.oS fG<br />
503161LS EQIE317 ^S_p3S'o•^26797 l 1 .5.03^"J.<br />
1 ) 80316101 ESI27508 Pr.1211?191 37.1211i/9P<br />
I BON680 C^-oOV376<br />
S_ 0 S ]lp<br />
2 RWI 89N68}<br />
ESI27509<br />
_____ O03t6101_?r..2113/97_°1.:2i'.'.r 19_____________<br />
ACTIONS (Initial & Date)<br />
1) INITIATED III 5) COUNTING/MEASUREMENT LAB<br />
SOPS) # SOP (s) #<br />
2) PREP LAB RECEIVED 3 _l q a k oc r- 6) DATA REVIEWED AND<br />
ANALYTICAL PREP STORED<br />
SOPS) #6 ^^t42LSo^3^<br />
SOP (9) #<br />
3) SAMPLE REMAINDER STORED<br />
]UI ' 1 ^J ) iI N<br />
4) SEPARATION LAD RECEIY[-D<br />
^)O('iS? tt<br />
6150
^CUSTOMER:<br />
CHAIN-DP-CUSTODY BATCH ANALYSTS RECORD 11-Mar-1998<br />
Page 1<br />
BHI^^//<br />
SAMPLE DELIVERY GROUP ^Oa375<br />
MATRIX : OTHER 8q S-aj I BATCH NUMBER<br />
CUSTOMER<br />
GES ID DUP ACCOUNT ID COMMENTS<br />
SA- A+.JkIL-<br />
-------------- ------- -- ----------====^sr^^===___-----------------____<br />
1 ) A01 8401SHI -- bo'^<br />
2 ) 80316402 ESI27510 I BON603 0 -000 -6-70<br />
3 )<br />
Pr,1211 3 '7 7 38.11!11/P2,<br />
3 ;4tY<br />
S_ 05 7(p<br />
---- - - ------ ----- - ------------------------<br />
ACTIONS (Initial '< Date)<br />
1) LNITIATED<br />
SOPS) #t<br />
3^^i I<br />
^O<br />
io— Y l<br />
5) (;DtJNTIN>;'i1EAStJREPii_NT LaB<br />
COPS) #<br />
2) PREP LAB RECEIVED h) DATA RE4'I`. WED AND<br />
AtdAL'f 1 lC A(_ PREP STORED<br />
SOP (S) is 50k3--p<br />
so? (5) #<br />
3) SAMPLE REMAINDER STOR-D 3.2k_ -q^tPlk,<br />
SOP (3) ii<br />
4) SEPARATION LAB RECEIVED<br />
FjOF' (3 ) ;i<br />
^it;lJ
CUSTOMER BHI<br />
MATRIX OTHER eq -G(; J<br />
CHAIN—OF—CUSTODY BATCH ANALYSIS RECORD 12—Mar-1998<br />
Page 1<br />
SAMPLE DELIVERY GROUP -75<br />
QES ID CUP ACCOUNT<br />
1 ) sum<br />
2 ) S0330602 ES I27511 I BON-5,96 0 -000 1r 'S9<br />
raft<br />
BATCH NUMBER O3 ^ T^ r<br />
CUSTOMER<br />
ID COMMENTS<br />
so, ai m-<br />
======<br />
61- 71-01-45 (init=_a1 & Cate) -------- —<br />
1) INITIATEC ^_^^^[^^ S) CCUNTI'dG%P! cA URE`IEiiT L:1L+<br />
SOP(S) ii ^l/^ScP(5;<br />
2) PREP LAD RECEI`.'ED, 6) PATH REVI:..iE_, AND<br />
3) SAMIPLE iENl ii!DFR STORCn<br />
`iOP(^ ) 4S I\ -<br />
4) SEPARATION L A'_1 REi- El')' L)<br />
u-,P(°!<br />
G161
^ 3 CH A IN-OF-C'.JST^=^DY BATCH AN ALYSIS RECORD 13-i1ar-199 8<br />
' `^<br />
Page 1<br />
` CUSTOMER: BHI<br />
SAMPLE DELIVERY GROUP ^-Z5<br />
MATR I X : OTHER<br />
QQ ^n<br />
l u w BATCH NUMBER<br />
1 )<br />
CUSTOMER<br />
DES ID DUP ACCOUNT ED COMMENTS<br />
32,i,R^'<br />
2 ) 803?2202 ESI27512 I BQi•46og 0•0006(-2<br />
v., 2i?' :1. 121 :3/ca<br />
S,o3^a<br />
— ---- — —ACTiDidB (Inii;iai '< Date) ------------ —<br />
1) INITIATED h"_/ 5? C UNTi' ;MEAS)REi1ENT LAB<br />
SOP(S) g 11^^ ^SGT ;Si k<br />
2) PREP LAB RECEIVED 7 _' 1'1-1Y_16) UAia 'EviF:' E7 FiN_<br />
Ai.IN^'r'T; ^AL °JE? STCRD __..__._<br />
3) SAMPLE REMr^ T.N i )ER STORCO<br />
4) SEPARA T: I,;N !. RCEI ij_i)<br />
SOPS) #A —^'-<br />
5CJl(cl. ^<br />
50F'iSi sk ___<br />
G16C.
II<br />
CHr+I N -OF-C':JSTODY BaT(;H AN-CYSTS RECORD 17-Mar-199£;<br />
Pa a 1<br />
CUSTOMER: BHI SAMPLE DELIVERY GROUP W 0020<br />
MATRIX OTHER( v" I BATCH NUMBER Da ^^<br />
CUSTOMER<br />
GES ID DUP ACCOUNT ID COMMENTS<br />
SA• PNni<br />
1 ) 80327201 ESI27513 I SON692 0-00066<br />
2 )<br />
3 Roaa7292 Bill--SON", ^4<br />
-- - --<br />
/r<br />
03 i<br />
ACTIONS (Initial & Date) -- --------- -<br />
1) I NITIATED ^ ^. :' _ „'i1 ---<br />
SOP(S) # 4 --<br />
2) PREP LAB P,ECEIYED 3:x`1 F h) OAT= PEYI WED AND<br />
ANALY 7 ICA1_ PREP STORED<br />
SOP (S) R Ott 2C 13^<br />
SOP (S) #<br />
3) SAMPLE PENAINDEFR S?OR D __Zb_^LY OTC<br />
4) SEPAR I) TION LAP, RECF-:IVF-0<br />
GOYO i; ^<br />
i70P (t ) i!<br />
ciss
uanflerra<br />
J o3I bt<br />
S riaa<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
AC ALYSIS MATRIX OTrWA DUE DATE y-6-9--<br />
-r!,2Y CS=m Ekm<br />
WORK OMM SEQUE NCE # CUENr COM1mm<br />
QCBATCHREAGENTHIAMC<br />
Afl, IX<br />
EAC3- 26 -4 1<br />
J N %x -1X QCBATCHMAIRIXEILM<br />
1 o b t 61 -1M oQ<br />
(fie)<br />
on<br />
I}<br />
QCBATCHMATRDURFAGWr<br />
2IM 844 C-oo 1<br />
J N tA. -2M or2S QC BATCH MATRDURF GWr SPUM<br />
Do3tbt _Ot<br />
DSO -St6lo1 "' 1 a<br />
gv3 L$`ao2<br />
803 Zo(o pZ<br />
03 2-2.?-Oz<br />
$O3 z-7Z.0 \<br />
Batched and QC updated by- - ^Dvt on 3 -Z5-ul<br />
Rec'd in Prep Lab by -err— on 3 -w<br />
Rec'd in Sep Lab<br />
Dapii eate of Sample #g0 3 t 61 01<br />
R tC+eCs0t-7 1<br />
W-' R tc-t 5() Rn'--^_<br />
Rec'd in Sep lab on Sop# Rey;<br />
ED/CPPT by on Sop# Rn:<br />
Rec'd in C.R- by / oa 3 2G Q Sop#<br />
Data Reviewed by<br />
Rev-,-<br />
RIC /f 7 Reo O<br />
n<br />
r/ Sop#_f'(ZC Low) ^ ^<br />
C-<br />
O riginal batch sheet and mplete calculation fi le to be filed with the FIRST rived work order number.<br />
FORM NO.: RC-52- IM, Rev. 8 C 00 nT -r k yr E = 4500jo u n., =m S:r= C ^ 2<br />
JP, ^ tarn trs = ^CC / SA G-Lc Z5<br />
CR'1<br />
SR k pRy ^^ ^..- X02 ^, „o- ^^ s^<br />
G1G^
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 10-Mar-1998<br />
Page 1<br />
Li CUSTOMER: BHI SAMPLE DELIVERY GROUP<br />
MATRIX OTHER BATCH NUMBER<br />
QES ID<br />
06% Ix<br />
1 ) 80316101<br />
2 )<br />
ACCTIONS (Initial & Data)<br />
1) INITIATED p^'I ' l 5) COUNTING/MEASUREMENT LAD<br />
SOP(s) 0 IJ SOP(3) #<br />
2) PREP LAD RECEIVED 6) DATA REVIEWED AND<br />
RK rrR^SO^?'1 ANALYTICAL PREP STORED<br />
SOP(s) # R \cHtccSo 13-0<br />
SOP (S) #<br />
3) SAMPLE REMAINDER STORED 3- 2-S-4Y o.^,<br />
SOP(s) if r<br />
4) SEPARATION LAB RECEIVED<br />
L<br />
DUP ACCOUNT<br />
CUSTOMER<br />
ID COMMENTS<br />
SA oncE..+,y' (S i})<br />
iw ====o..ems====e—=itai==o------s^^==o^<br />
K FahE O rMr+h<br />
SOP( cl ) 4<br />
CO r\r Tiw f- _ 5 ) , I e-O =ZS) PC, /S^<br />
1030<br />
NfG cool 0-1 w.*. 91 %L" LSt (^N L6/y1fjP Q^^91D<br />
BHI BON680 o4vruMtYY 103,0 C,z355 /-G zeoe "e<br />
G. 16
Q^^- q' ^<br />
CUSTOMER: BHI<br />
MATRIX : OTHER<br />
1 )<br />
OES ID<br />
CHAIN-OF-CUSTODY BAT -, F l ANALYSIS RECORD 11-Mar-1998<br />
Page 1<br />
^<br />
j<br />
SAMPLE DELIVERY GROUP<br />
II BATCH NUMBER Vt/<br />
CUS I'OMER<br />
DUP ACCOUNT ID Sq COMMENTS<br />
s A A. AA. aRTc<br />
2 ) 80310402 BHI B01•4683 0.2z4utomacggottSG L( ^09^1<br />
3 ) -86^^946aS•s5-tc OUTPn i n<br />
1 , 14<br />
i ON5 (I 1 1 i t i a l '. Date)<br />
1) INITIATED _^/ 0 5) C7UNTIN,/MEASUREMENT LAB<br />
SOP (5) # Xa E A SOPS) #<br />
2) PREP LAD RECEIVED 3_IQ--4-K off_ 6) DATA REVIEWED AND<br />
ANALYTICAL PREP STORED<br />
SOPS) R __R>^+44 0 -^<br />
3) SAMPLE REMAINDER STORE;U 3_25-4Y oaf<br />
SOP ( S ) SI<br />
4) SEPARriTIOfd LAB RE;; ['':) --<br />
(,OVv7T T/ 01 e = 5U)<br />
b, eo = 2s ) P G^S^<br />
SOi'(^) #<br />
6166
I J<br />
CHAIN-OF-CUSTOD`' BAI --,- ANAL' . ' 'l i S RECORD 12-Mar-1998<br />
Page 1<br />
/ CUSTOMER: BHI Elid'IPI_E :DELIVE` : Y GROUP<br />
MATRIX : OTHER p'(i(1 BATCH NUMBER d3-^<br />
C US'r OMER<br />
GES ID DUP ACCOUNT ID SA<br />
1 ) X93=^ r_nt c 3.2.SA' NW; $HHthF3^<br />
sR<br />
COMMENTS<br />
2 ) 80320602 BHI BON6061 (M' X 1wo o•'k 107 G3 Z6rh,^R9 g I /03<br />
3 ) 89829 92 yHf E) E)<br />
ACT! DO , ' ( Initial & 0.3t2)<br />
J 7'<br />
1) INITIATED ^^((^^ / ^^U 5) COUNTINOiMEASUREMENT LAD _<br />
SOP(S) 4 _ND S^F'(5) #<br />
2) PREP LAB RECEIVED 3_L^_Q o_rL_ 6) DATA REVI WED AND<br />
2^rtac So Z-I ANALYTICAL PREP STORED<br />
SOP (S) # _ i^kr^?CSo^3 0<br />
SOP(°„ #<br />
3) SAMPLE REP1ATMrEP STDPI-') ^^zs 4t__os^<br />
4) SEPARATION LAD RECL-l ki: D<br />
c16
CHAIN-OF-CUSTODY B%T." ANAL'ii S RECORD 13-Mar-1998<br />
Page 1<br />
/ ^^^<br />
I V t CUSTOMER BHI SAMPLE OELIVEFiV GROUP L(J(<br />
27s-<br />
MATRIX : OTHER BATCH NUMBER 03 d^<br />
OES ID DUP ACCOUNT<br />
CUSTOMER<br />
ID<br />
SA-<br />
i ) '^922e^^.=`^'}^e^s•z $fIF $9HiS8B<br />
s P. rw^C<br />
2 ) 80322202 BHI BON689t2'^"* l3`S O.vzco<br />
ACTIONS (Initial & Date)<br />
COMMENTS<br />
1) INITIATED `// "/^ Gl 5) C,OUNTIN9/MEASL'REt1ENT LAB<br />
SOPS) # IJ 117v^ SOPS) ;!<br />
2) PREP LAD RECEIVED _
AUSTOMER<br />
MATRIX<br />
BHI<br />
rAi".'A -x :^<br />
CHAIN-OF-CL B,4TC1' ANAL' `.aIS RECORD 17-Mar-1998<br />
OTHER j-/ &W<br />
SAMPLE:'JELIVER`/ GROUP<br />
BATCH NUMBER<br />
Page I<br />
D^^ S<br />
o ^5-;rZa<br />
CUSTOMER<br />
OES ID DUP ACCOUNT ID COMMENTS<br />
SA SR- n^n^<br />
---------------------------------------- ^^ _____ `SIN- )<br />
1 ) 803E720t CHi EOi964211oh'+HR. o83a O.4oyS(^ ^<br />
G )<br />
3 ) —eose-7,R<br />
oar - Z -c<br />
HT 1391v69q<br />
1) INITIATED - 1 -' F 'NT LAG<br />
2) PREP L.rQ "c: is iE T'dED 3 -49 AY - 9v5 h) OATA RE`.-'IF:'AED AN'_)<br />
F2.c rt 2a5o 1-7-1 AN-?LY-iC at_ = RE= ST )R=D<br />
3) =, 7 NFI_E i;Eit.f Ir;:,. .r S' I?+.) _3 -25 Y<br />
/<br />
Co^^^ ^rrc r = soy G^^ - zs c, ^^ C,^ se<br />
2,/4141P9^<br />
^_<br />
6161
^!s'aanf-errs<br />
F nimnn<br />
S nim<br />
BATCH SUMMARYICHAIN OF CUSTODY<br />
AtIALYSIS n .' MATRIXo=_DUE DATE<br />
Sw RRy<br />
PORK ORDER SEQUENM # Q1EN7 cch owlem<br />
1 oil& y -IB<br />
6<br />
QC BATMREAGENrN AW<br />
1 N Iq -IX QC BATCBMATRIXB[Aw<br />
1 031&H , -1moom<br />
( cirde)<br />
1 t4 -2M or 2S<br />
(drdc)<br />
QC BATCBMATRDUREAGENr<br />
SPUM<br />
QC BATCBMATRDQREAGENr SPIKE<br />
D 03 bolo "Ol -<br />
Dupli=cofSample # go3zo601<br />
Ff 03 I LA 01 03 Z SR<br />
$b31blOZ<br />
a la<br />
$Ozo6ol b3 2 s^<br />
$0322201<br />
FfOb 2'-1`i 0\<br />
$03 Zr12bZ<br />
la<br />
p'Z<br />
03<br />
Batched and QC updated by Atli` on -5-aS-4Y<br />
- 3• 5-4d'<br />
12\LC{-RCSo ^7 \<br />
Rec'd in Prep Lab by a or.- on 3 -1°r 2 Sop#3 tCN --X Reo C)<br />
Rec'd in Sep Lab on Sop# Re+<br />
Rec'd in Sep lab on Re%-J<br />
ED/CPPT byon Sop# R e%-J<br />
Rec'd in C. R. by<br />
on-— Sop#-KCN200 )O Z ReO^_<br />
Data Reviewed by on ^/ ? lip# ^C^^12^7 Rn^^<br />
O riginal batch sheet<br />
lT-'T^' `77-^^^ y -U^<br />
complete calculation file to be tSlMed \vrth th j<br />
e FIRST fisted work order number.<br />
FORM NO.: RC-52,1/98, Rey.$<br />
/ ^Q (^ 7 ( n /<br />
(Coo<br />
(T^ o = too<br />
c r s ,j s-F =GAR<br />
UUl<br />
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SA<br />
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25Ntk22045 1 --^j.^ 7- /77R ^ 7^0^<br />
Sob1FSN15 QCAG387 o9FEBgK?zap 1 (ZL McvgY oil<<br />
..... - ..; lO rrN^t41f eg35 0.0537<br />
3-lq<br />
Co^Nt ^^"'^ '600)<br />
a-asac<br />
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VKiZ^ci4AC<br />
Su^Z-I -<br />
R^.HatcSoil-O<br />
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3/ 26 ^1 5f<br />
17MAR 4 8' /C6<br />
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__—_DOSZobol __wp _ _ .__ _ o,os¢T 67 _27^^ R98 16^3^<br />
_--._ _ __<br />
7Z ^c cr,;zc Sv « -I<br />
2 ^^rt-ttc S o t3 ^<br />
- I<br />
3-25-`c^ i^crt<br />
Gov^^ ^«r - ^oo^ 6c^ _ g oo A-7 Pc, /sue<br />
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1<br />
r<br />
6173
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--VOL S- Lot Dw- -<br />
4Y 2i r.rwF Otti'r<br />
{Zkc tN-zc SoV3-^ — - - —<br />
= 3 LS-4d oat<br />
G C) U ,l t- ^;^ e = 600, feu = / Oo-. c, P c,/sue<br />
J N(.<br />
G17^^
ti\ ^<br />
- -.. 3 - iS -`L8ij<br />
jute ^ So ^T -I<br />
R.c^+ltc Sc^3-O<br />
3 -25 -`-r Ddt<br />
r- ^A<br />
600, c- t71,)-ie- z 6c)O 6e-a _ / OJ ' -'-)<br />
SA oRT[ CS^^<br />
Gli5
f^-1^ Ole I U^ ^<br />
SA St3 RvFl^<br />
or3s^ C1 ft) -<br />
- 16Yri4^Cg3'o42S OoStZ - -^^^^t^-.+a ozzY<br />
l6mnagX loz5 o-oSLy - C -3 .2817ygF^1E' /^3 /<br />
-1/ -7<br />
eo a,^ Scu - -<br />
3-ig-2k oR<br />
Ric n Q^Sp^"1 -^<br />
2.c-eKCgo.3 ^<br />
3-ZS-^6" art<br />
N Vi<br />
I<br />
6c ^o J (^^O _ IOd^,L^ PC//SGT<br />
_<br />
L1ly
l ''4'uanferra<br />
S erica<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
ANALYSIS^ MATRIX DUE DATE 444-8<br />
S LV RRy<br />
_ WORK ORDER SEQUIIAM / CLIENT combaRm<br />
I v3l&y -1B<br />
6 H-t<br />
QC BATCH REAGENT MAW<br />
J ^1 -ix QC BATCH MATME AM<br />
I Oil& i -1M<br />
(crcle)<br />
J „ l4 -2M or 2S<br />
D 032Kg<br />
(drde)<br />
of<br />
^50 1 €y ol 03 zsR<br />
^b3 16102<br />
a IA.<br />
$03 i? 0601 b3 2 SA<br />
201<br />
Ala<br />
Fs03R 14'1 oZ<br />
^0 T.7 Z'12bZ<br />
O-^<br />
Batched and QC updated by yt on 3-t s -Q<br />
QC BATCHMATRDURFAWIT<br />
ED/CPPT by on SOP# 15-4<br />
Recd inR C. by on N GfJ Sop#_f.'1^N2^ Rn3 C^<br />
Da ta Reviewed by ! on 7 3-if Cnml 11^<br />
9 CIFAAZ<br />
sY-' J q I. l y 3 ^.<br />
QC BATCH MATRDJRFAGeTr SPIIM<br />
Duplicate of Sample # %702 Lt uc t<br />
Recd in Prep Lab by at on 3-tit Qd Sop# -IS: ZO-- RM 0_<br />
Rec'd in Sep Lab by<br />
Op<br />
7.T n 1 on Sop# i t ti R c 00 E<br />
RL,-4<br />
Rec'd in Sep lab by on Sop# ReS i<br />
O riginal batch sheetAnd complete calculation file to be fi led with the FIRST rested work order numb,<br />
FORM NO.: RC-52. 1/98, Rev, 8<br />
X: PrnQ- dI A PR '^. 1 3: U<br />
G1lt<br />
n
--<br />
- ---'^p3lfr4ti3-ESF14249<br />
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! STOP i ER<br />
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y S Y O. of 3'} bc. OT^P^ ^^-Z7$75T'<br />
///J<br />
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2 57 ^1 ? o, uZ3a 6D OZR ^Y_pf£1s 0/<br />
ES£14 258<br />
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p^ ^^c a i•.ica<br />
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- - '^'^q -4Y ors<br />
2^ct+¢t5a^3a<br />
_<br />
GIs- .J
Gluanterra<br />
.s w.<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
ANALYSIS -7-sr MATRIX DUE DATE y-6-4.R-<br />
T1tN !'fenEntr<br />
WORKORDER SEQUENCE# MINT CODS<br />
1 161 -1B<br />
^t+1<br />
QC BATC HREAGEN T W A M<br />
J nj1A -1X QC BATCH MAMIX ff-ea<br />
J - 0 3161 -1M aim<br />
(°=IC )<br />
J 2M or 2S<br />
(aide)<br />
D o3tb1 -01<br />
QC BATCH MATRDC/RF.AGENI'<br />
SPUM EQGp;(, 9 'ec-193f 1.1ti349^^<br />
QC BATCH MATRM71AGENP SPUM<br />
Duplicate of Sample #S0 3 1 b 10 1<br />
x'0316 1 01 "' 1 °' _<br />
gv3 l$`{02<br />
803 i;o^ oZ<br />
a3 2zZ.oz<br />
X03 ^'7 ZO1<br />
Batched and QC updated by^vt on 3 -Z5-%K<br />
Rec'd in Prep Lab by ^ on -3 -n -w SVOJR ^^ t* Q-S O t Red n<br />
Rec'd in Sep Lab by - 12on ;1 1 $^¢ , S c }L ^^'[' Rn -Z<br />
Recd in Sep lab by on Sop3 r " / F R^<br />
ED/CPPT by<br />
.4<br />
1 on<br />
sopit_—L-_ R<br />
Recd in C.R. by / on Sopd^iC f^/^L^^n ^ -4 ,<br />
Data Reviewed by a3-Y^ $opi frJ^C^" AZ- Re,'^<br />
O riginal batch sh and complete calculation file to be filed with the FIRST listed work order number.<br />
17MM NO.: RC-51 1/98, Rev. 8<br />
SA fRM-na ^ ^S off' aRy C.evre.^Z^ No: of TOM1 SA Ij yJ h (•^<br />
3/ 3i^4 Y<br />
5 R s^9<br />
x;18
^ vtp/<br />
rx* -C)-A '--Cq ***<br />
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 10-Mar-1998<br />
Page 1<br />
CVSTOMER: BHI SAMP1- DELIVERY GROUP ( D f^J^^^<br />
MATRIX OTHER n r BATCH NUMBER 111<br />
^/Ixv CUSTOMER<br />
GES ID DUP ACCOUNT ID<br />
PVT „n Sft a„^<br />
COMMENTS<br />
]0316\^$ ESF?4_51 =__----___________-------<br />
G^.C, (<br />
____(ofCIA<br />
IOAgg )/Z3<br />
So3lbttS EQGF264<br />
1 ) 80316101 ESF '_ 42,' 2 I BON680 q-).D bL<br />
-Do3l6\ol ESF14253 QS.! n.000366 (ip<br />
ACTIONS (Initial & Date)<br />
1) INITIATED ^^ 5) COUNTING/MEASUFEF'ENT LAD<br />
SOP(S) # 40 SOPS) #<br />
2) PREP LAB RECEIVED 6) DATA REVIEWED AND<br />
ANALYTICAL PREP STORED<br />
SOP (S) # Q^L+-2^ 50 ^^-7<br />
SOP (S) #<br />
3) SAMPLE REMAINDER STORED 3_Zb^Lt^<br />
4) SEPARATION LAD RECEIVED<br />
SOP (S) 4 - \°<br />
SOP(5) 4<br />
G<br />
1<br />
C18J
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 11-Mar-1998<br />
1 Page 1<br />
11,<br />
CUSTOMER: BHI<br />
J SAMPLE DELIVERY GROUP<br />
MATRIX : OTHER<br />
^^((<br />
U-^t BATCH NUMBER O j<br />
1 )<br />
CUSTOMER<br />
GES ID DUP ACCOUNT ID COMMENTS<br />
P P'r w'f- s R ^<br />
S•u<br />
2 ) 80318402ESF142^4 II BON633 G^.^ o -oou3V9 (.¢ 1,410R4^1 /lli<br />
3<br />
iq<br />
AC<br />
3u^<br />
IONS ( 1:111: a1 0: T)-1<br />
------ ---<br />
T<br />
1) INITIATED 5) COUNTiNC/NEASURENENT LAB<br />
SOP(S) 0 jVnD SOPS) #<br />
2) PREP LAB RF_CEIVED 3 •19_TY_ wet b) DATA REVIEWED AND<br />
ANALYT?CAI_ PREP STORED<br />
3) SAMPLE REi`1A'NDER STOR 1) -z6-LR Ot<br />
4) SEPARATION L 4 3 RECEIV(I)<br />
SOP (5) #<br />
GIS5
CHAIN-OF-CUSTODY BATCH AID.-,LYS;IS RECORD 12-Mar-1998<br />
I tq)<br />
Page 1<br />
fvfL CUSTOMER: BHI<br />
/I)<br />
SAMPLE DFLIVERY GROUP IND ]^7<br />
MATRIX<br />
n^<br />
OTHER ^ /^ lJ1 BATCH NUMBER 0^ r<br />
CUSTOMER<br />
0ES ID DUP ACCOUNT ID P T.,c Sar ^^ COMMENTS<br />
1 j—ffB3Re6ei A(+1 5 B6WbE35<br />
2 ) 80320602 ES-14265<br />
v. ^o • , ..<br />
I<br />
,:a<br />
BON686 ZF j.j O coOF5 7 0bg 8' / Zz-<br />
3) L-893@ B 60 3 BI I I O1^ B II 'J^<br />
AC-IONS (T t i d a l '< Date) ------ -------<br />
I<br />
1) INITIATED LAB<br />
2) PREP LAB RECEIVED 3_,l9_•9P.^^ 6) DATA REVD=tiED AND<br />
`ur(S) 4S Fjv_-*,^C J\3^<br />
3) SAMPLE REN(kiN i)E:R ST P Pt=D _ -2b-z% oJ^<br />
4) SEFARATION L.AE Ri:CEiV>.D<br />
SOP (S) if _-------<br />
Ocf' (0) iF<br />
ANALYTIC I_ PREP STORED<br />
SOP(Si
-$*t _-AL-SR c44<br />
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998<br />
l) Page 1<br />
1 2CUSTOMER: BHI<br />
SAMPLE DELIVERY GROUP<br />
MATRIX : OTHER<br />
_/)/p v^-^' I BATCH NUMBER D3'a3^<br />
GES ID DUP ACCOUNT<br />
CUSTOMER<br />
ID<br />
wZ' SA- ANA^<br />
APT<br />
COMMENTS<br />
1 ) 80322201 ---81i^ `"--a te B^eH6c65<br />
2 ) 80322202 °SF14_5o lI BON639 Gy.Z 0. 000"6 6C. i ApR 1zz^<br />
------------ --------- ------ - ------ --<br />
ACTIONS CTIOi JS (Initial & Date) -----------<br />
1) INITIATED < 3 5) COUNTING/MEASUREMENT LAL+<br />
2) PREP LAB RECEIVED aL-t9-9g _ 5) DATA FEVIE-WED AND<br />
A.NALYTI;P.I_ PRE° STDRED<br />
3) SAMPLE REMAINDER STOR. D 3_Z6=4T _p^<br />
4) SEFARATiOi: LAP RECEI'-TGh<br />
SOp(G) R<br />
Gigs
3 l / CUSTOMER<br />
MATRIX<br />
-** TOTAL-SR # -I*<br />
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 17-Mar-1998<br />
9 e<br />
EHI SAMPLE DELIVERY GROUP<br />
OTHER rl -LV I BATCH NUMBER<br />
CUSTOMER<br />
OES ID DUP ACCOUNT ID COMMENTS<br />
r ^r<br />
Lh.r.^ CsA^ -------<br />
1 ) 80327201 BHI BON692 Q3.1 O-0006&T^ 6D //}iie4$ 12.Zl<br />
2<br />
3 )<br />
f ------ - -ACTIG10S (Initial & Date) - ------- --<br />
1) INITIATED 1) GOUPJTiPJG/hIEASUREi`f:-NT LAP<br />
SOP(S) 4 SOP (5) t --<br />
2) PREP LAB RECEIVED 6) DATA PEV1EWED AND<br />
r`.NALYTICAL PREP STCRED<br />
501 1 (S) # $_^^±^2c So i3^<br />
SuP(5) #<br />
3) SAMPLE RENAI-'NDER STCRPn 3 Lb-4g out<br />
4) SEPARATION! LAD P.ECEIV'_D<br />
-<br />
cis, j
%uanterra<br />
.Sb.iCV<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
ANALYSIS C-1 q MATRIXo+DUE DATE y -6-9k<br />
t!^R`( r-rr-mEnlr<br />
WORK ORDER SEQUENCE a amir CONAENIS<br />
J- 03161 -10 Wj,;AJ QCBATC$REAGEM'BIAW<br />
J . ^U. D^ I (ro iX QC BATCHMAMUX IS AIS<br />
J o 316 t IM oQ<br />
J-<br />
D o31b1<br />
(dtde)<br />
2M or 2S<br />
(dude)<br />
01<br />
^'p3161o1 '^ 1 "<br />
gn3 LB^oZ<br />
g03 F-06 pZ<br />
b3 Z? 02<br />
$03 z-2z0^<br />
Batched and QC updated by-^i e^ on 3 -2<br />
3•<br />
QC BATCH MATRDUREAt3Nr<br />
SPUM<br />
QC BATCHMATRUMEAG NT SPUCE<br />
Dupticade of Sample H 8`0 3 t 61 01<br />
Rec'd in Prep Lab by on 3- H -w S0 05L1C- C-So 1 i Rn,= 0<br />
Rec'd in Sep Lab by uM , on #-G fe Sop#12(_ e-- SG,2.) Rni /<br />
Rec'd in Sep lab by on 41 SOP# _ RnLj—<br />
ED/CPPT on Sop# Rni<br />
Rec'd in C.R by on yl, l+r So p(__,<br />
Data Reviewed by - ^`^ l^ Sop# e- ^4 Z<br />
O riginal batch sheet an complete calculation file to be filed with the FIRST Esttd work order number.<br />
FORM NO.: RC-52. I/98. Rev 8<br />
S4 FRAc c10<br />
i s 0-^ O R y 5 0 L- o, Nor o^ 1 S;<br />
&L-L- s 02 1 = Gi9i1<br />
Rn
CHAIN-OF-CUSTODY BATCH ANALY;l S RECORD 10-Mar-1998<br />
Page 1<br />
'J<br />
CUSTOMER: BHI<br />
SAMPLE DELIVERY GROUP I/ ^^<br />
MATRIX<br />
Q<br />
OTHER ^ ^ u -D0 l<br />
/`^)<br />
BATCH NUMBER ll -0I<br />
CUSTOMER<br />
OES ID DUP ACCOUNT ID COMMENTS<br />
sa aaa^<br />
---------------- ----------------------------<br />
1 ) 803161010.000 1040 BHI SON660<br />
2 ) 80216192 Biii 130H681<br />
^..3•i6<br />
1) INITIATED<br />
D031b 4o l 0_•000blg<br />
it<br />
3<br />
ACTIONS (Initial & Date)<br />
^ 5) COUNT IN /MEASUREi•4ENT LA3 ___<br />
SOPS) # SOP(S) i4<br />
2) PREP LAB RECEIVED 3_-v =L -ci^j^.^ Ei) 4)jT;n REVIh.WED ANO<br />
,04l%LY I i L FRS? STGRcD<br />
SOP ( ) ) if R -<br />
SOP (S) #<br />
3) EA'NPLE REf!AINiiER SIOR I=D s-2S-qY _o L<br />
4) SEPAROTION LAB RECEIVED<br />
SOH (5 i 4<br />
L191
CHAIN-OF-CUSTODY BATCH ANAL`SIS RECORD 11-Mar-1998<br />
1 3 ^1 Page 1<br />
CUSTOMER: BHI SAMPLE DELIVERY GROUP ^<br />
Q<br />
MATRIX : OTHER f ^ lam' i BATCH NUMBER o3'IS<br />
CUSTOMER<br />
GES ID DUP ACCOUNT ID COMMENTS<br />
gp dal<br />
1 ) 603E 8481 7" ac 3-zs<br />
I?I13 $9PF6^^<br />
2 ) 80010402 0.0006\ 7 DHI BON6 33<br />
3 ) ^ BE)S I BR6S T'°` 3 ' Fill! BER16 j4<br />
----------------------------------------nr<br />
I%i') ri<br />
1) INITIATED `) CCUNTI'?G!i IcA5UREi`lEi T L.AB<br />
SCP ( S ) 4 SOP (S) ##<br />
2) PREP LAD ^.__ :." - 5-t5 9^ S___ b) hATA REVIEWED AND<br />
t^.iINALYTICAI_ PREP STORED<br />
SOt' (5 i ;E Ri^H RC S9 ^3 -o —<br />
GOP (7)<br />
3) SAMPLE RE?A 7 ^'0^° '-TSJ,;" h 3_z5- ciY O(t --<br />
4) E /?i i,l IiJIli L.'?L' FL t.t I'i -11<br />
--<br />
619
1 / 1<br />
CHAIN—OF—CUSTODY BATCH ANAL"S IS RECORD 12—Mar-1998<br />
Page 1<br />
I/ CUSTOMER: BHI SAMPLE DELIVERY GROUP<br />
MATRIX : OTHER HAW BATCH NUMBER<br />
(,^<br />
CUSTOMER<br />
OES ID DUP ACCOUNT ID COMMENTS<br />
SR AUkI<br />
%A<br />
2 ) 60320602 0 .00 1 1 4c BHI BON686<br />
3 ) (36226692 _<br />
i-u ^Lr _R 41 uQW687 -<br />
- -- ------- -------- -- ---- ------------------------------- ----<br />
IJACTIONS (Initial ?< Date)<br />
ff<br />
1) INITIATED ^ t _ vC 5) COUNTiW,/M=ASURE;'lENT LAI3<br />
SOP(S) 4 SOP(S) #<br />
2) PRE? LAD REC E IVED 3=1.^^K. D^^ 6) DATA RE'J[t_WED AND<br />
IgALYTIC `)L PREP STORED<br />
SOP (5) t# ^t^So ^3<br />
3) SAr.PLE REMAINDER STOR^_0<br />
4) SEPAR A TION L=° 9E-,-E`4's_,)<br />
SC P 13) 4 wW.<br />
F)<br />
(JigJ
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998<br />
Page 1<br />
31 / CUSTOMER: BHI SAMPLE DELI`,lERY GROUP WQ^^^^<br />
MATRIX : OTHER M8-bul BATCH NUMBER<br />
1 )<br />
CUSTOMER<br />
QES ID DUP ACCOUNT ID COMMENTS<br />
5 A Au A^<br />
zs<br />
2 ) 80322202 0. 00 t O 2S l BHI BON639<br />
------------- ----------- --------------- — --<br />
ACTIONS (Initial & Date)<br />
1) INITIATED(-1 U) COUNTING/MEASUREMEidT LA3<br />
2) PREP LAB RECEIVED -j°1-gH_°nc S) DATA REVIEWED AND<br />
ANALYTICAL PREP STORED<br />
SOPS) H Rjct"<br />
SOP (3) n<br />
3) SAMPLE REMAINDER STORED 3_ zS '^K Oaf<br />
4) SEFARATION LAD RECEP;`;i)<br />
SUP (5 ) ;' _ _ —^W----<br />
SCP (^:) It<br />
61,9,1
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 17-Mar-1998<br />
Page 1<br />
/ CUSTOMER: BHI WIPLE DELIVERY GROUP<br />
MATRIX OTHER -oCQ, BATCH NUMBER<br />
CUSTOMER<br />
QES ID DUI' ACCOUNT ID COMMENTS<br />
-SA AmPrc_<br />
1 ) 80327201 (0 .00lozz DHI BON692<br />
2 ) , 20=7202 VY^-3 . 2 5 tL1( 8 1693<br />
3 ) —Be -327E 3 ° L4 -Hi BON694<br />
719g<br />
1-a'<br />
`^J ^<br />
1) INITIATED _ 3 > CuUid^ ;'=Ci IG1SU°EPIE^JT Ld7<br />
2) PREP LAD RECEIVED 3-l^L-RY_D _ > DATA REV IE!:ED AND<br />
Arl.ALYTICAI_ FRET STCt?HD<br />
3) SAMPLE R i''.,a;i;L'=R ".: i_'I
i..T":}1M1frt::l<br />
Sen+:rx<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
ANALYSIS 5F.-77 MATRIX C) T^ DUE DATE_a -6 -Ur<br />
^R`( CS=m Etvr<br />
WORK ORDER MQMCE s CENT Comme T$<br />
J 03161 - 113 QC BATCiREAGUITBtANK<br />
J ^ tw -1X QC BATCH MAT= BLANK<br />
J o 3 t 61<br />
J N In<br />
- 1m aim<br />
(code)<br />
-2M or 2S<br />
(mde)<br />
QC BATCH MAIMMAGENT<br />
SPUCE<br />
QC BATCH MATRDUREACENT SPLICE<br />
Do-6tb1 -01 -_<br />
Dt>Q lirate of Saittple B g0 3 l 61 01<br />
FSb3l6 l o1 '^ 1 `^<br />
gub l$ 1oZ<br />
8o3 zob oZ<br />
03 2ZZ02<br />
$03<br />
Hatched and QC updated by-^dt on 3 LS-LJ<br />
Rec'd in Prep Lab by ean 3 A _ Sopiig tL g-SO t 3 Re%-<br />
Recd in Sep Lab by l A on ^^ ^^ Sop3 C^ ^^ L ` R n^<br />
Rec'd in Sep lab by on Sop# Rcv<br />
ED/CPPT by on SopB p Rn<br />
Recd in C.R. by !^ on 3 31 SOP# 7^ Ic- ^G l R^ ^^<br />
3,70-,-<br />
Da ta Reviewed by on Sop! ^^^' Cc [ R^<br />
O riginal batch sheet add complete calculation file to be filed with the FIRST Eved work order number.<br />
FORM NO.: RC-52.1/98. Rev. 8<br />
50. tS of 1 {Lj CS-,: WN ') tvoT of- set<br />
CWT 1^^ -. Rab^•F ^ a.LQ.<br />
Li^U
I<br />
CHAIN-OF-CUSTODY B,4TCFi ANAL Y 51S RECORD 10-Mar-1998<br />
Page 9 1<br />
CUSTOMER: BHI ^/'y SAMPLE DELIVERY GROUP W D ^^<br />
MATRIX : OTHER I3 ^ (/ {may I BATCH NUMBER<br />
CUSTOMER<br />
0ES ID DUP ACCOUNT ID COMMENTS<br />
S(} Auk<br />
1 ) 80316101 ° _ _ = ' )' _JN680 o-oco3 ra<br />
2 ) 863t6ie _ _ I e<br />
1) INITIATED<br />
13^ti6a<br />
ACTIONS (Initial & Date)<br />
^ ^5) CSUNTIN•f,/MEASURE-,KENT LAB<br />
SOPS) # 410- i^ SUP(S) ?k _<br />
2) PREP LAB RECEIVED 6) DATA REVIEWED AND<br />
ANALYTIC ;)_ PREP STnRED<br />
SOP (S) Sk ^^tE2C5 o^T»<br />
SOP(S) u<br />
3) SAMPLE REMAINDER STDREO 3-Z6 0.8 q^<br />
SOF'(S) i; V-<br />
4)<br />
n<br />
SEPARATION LAB RECEivi -0 ^^^(^^!^ ^^^^\\<br />
SOP3,^^IT^4^<br />
^^19,
!<br />
**^^ SE-79 ***<br />
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 11-Mar-1998<br />
CUSTOMER BHI<br />
Page 1<br />
SAMPLE DELIVERY GROUP (,voa07<br />
MATRIX OTHER I BATCH NUMBER 03-1<br />
CUSTOMER<br />
GE3 ID DUP ACCOUNT ID COMMENTS<br />
5{} A"4tz-<br />
1 ) 3,Lb<br />
3<br />
80318402 I BON633 O •oeo357<br />
----Y<br />
5<br />
-- ------ ^ ^ir T I OI •aS (I n i t i a 1 `. D.^ ^: a) ------------<br />
1) INITIATED / ` )^ :) COUNTI`JG/i`IaASUREi`IENT LAB<br />
SOPS) # SOP (s) #<br />
2) PREP LAB RECEIVED 3-g-9^0^_ 6) DATA nEVIEWED AND<br />
3) SAMPLE REMAINDER STORED _3-26 `^k_OyC<br />
4) SEPARATION LAB RECEI'V,<br />
n^<br />
ANALYTICAL PREP STORED<br />
SOP(S) #<br />
G L J ,j
*n 5F-79#r<br />
I,^<br />
^<br />
V<br />
q li^<br />
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1998<br />
Page 1<br />
CUSTOMER: BHI<br />
V hf'<br />
MATR IX OTHER /y . 1<br />
I'\ l<br />
SAMPLE DELIVERY GROUP OQQ7.S<br />
BATCH NUMBER O3 -°Cy<br />
CUSTOMER<br />
GES ID DUP ACCOUNT ID COMMENTS<br />
S!! AwA -<br />
1 ) 805Efto s'f c5<br />
2 ) 80320602 -- I B 0N61360. 000 rs50<br />
3) eeszewe Bi )l3 "^- BE)H687<br />
- -- ----------------- -------<br />
ACTION-- (Iuitiai & Date)<br />
1) INITIATED _ ^(^?7D^ 5) COUNT iNC!t1EAS'.JRE'tENT LAB<br />
SOP(S) # S010 (S) t#<br />
2) PREP LAB REC_eVEG 3 _lg _fig ,_ 6) DATA REVD - WED AND<br />
FiN.^- Y i.AL =RE P STOR E71)<br />
SOPS) 4 F^^Cti C50^3 0<br />
Soe (s) #<br />
3) SAMPLE REMAIfdDER ST07v:D 3.26-`^rr<br />
4) S EE cAR.fTI^CN<br />
Sr)^ c :^) ,i ,^^<br />
l<br />
^l l n i^
^CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998<br />
Page 1<br />
CUSTOMER: BHI SAMPLE DELIVERY GROUP<br />
MATRIX : OTHER ^(^ ^ BATCH NUMBER 0v _Z/92<br />
CUSTOMER<br />
QES ID DUP ACCOUNT ID COMMENTS<br />
S tOr AN A k-<br />
---------------------------- -----<br />
1 ) C $<br />
3.7bRTf<br />
2 ) 80322202 - - : II BON 639 0.000657<br />
1 CTIOi.3S (Initial Data)<br />
1) INITIATED / ^1 `) CCUNT?NC;/ IN IEASUREPIC 'i\iT LAD<br />
2) P R EP L AB R EI` iEC 3.1^g$ b) I IATA ,EVI; WED AID<br />
SOP (S) # R'CH-Re5013-0<br />
3) SAMPLE REMAIPIDER STOR'1) 3_- 26 "2'? r--A.<br />
4) SEPARATIuP"! LAL<br />
AiNALYTICAI.. P R EP °_.T04Ei<br />
^Pc<br />
G; 3 0
W A^<br />
CUSTOMER<br />
MATRIX<br />
EHI<br />
OTHER ^U cb I<br />
h^^ SE:-!9<br />
^^n<br />
CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 17-Mar-1998<br />
SAMPLE DELIVERY GROUP<br />
BATCH NUMBER<br />
^^(^ ^7 Page 1<br />
I.W^ I<br />
o3-a7a<br />
CUSTOMER<br />
QES ID DUP ACCOUNT ID COMMENTS<br />
5^4 ANR^<br />
1 ) 80327201 ' " eC= ` ' I BON692 O-0006°tb<br />
3.26'45 "<br />
3 ) ^69327^ P+f 13—^^tl^`^Q ^'.At'^,5^4<br />
------ -- - --- ---- ---- -- - ---------------------------<br />
'^CTI0PJ:3 (Inibxal ', Dace:<br />
1) INITIATED 5) COVivT-NS/MEASUREMENT LAD<br />
SOP(S) J^'3 5i7P(5) R<br />
2) PREP LAB RE Ei•1 D 3-)5_= jy^ 6) DATA REV!'-W;ED AND<br />
(`,N1LY7-,-j`j PREP STORED<br />
Sop 1. 3 i K R%L'wfC 4501 3 -i7<br />
SOP ( 0 )<br />
3) SAMPLE Ri_i', i' i;GP STOP! D 'b -26-43 V+<br />
4) EEPARAT10iI LA-r `?=r'EIY,-D<br />
G^G^
(j..%"uanterra<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
ANALYSIS TL . Q MATRIX O TlifA DUE DATE L -6 `Lk<br />
r,a`4 rV-rn FIUT<br />
WORK ORDER SEQUENCE # CLINT<br />
J-. 0316 1 -1B QC BATCHREAGE"NP BLANK<br />
J - N ^ k -ix QCBATCHMATMBLANK<br />
1 0 3161 -1M 0(a)<br />
(circle)<br />
1 -ZM or 2S<br />
(aide)<br />
Do3tbt -fit<br />
^Sb-Sl6lo1 "' 1 °'<br />
QC BATCHMA<br />
SPDM<br />
p GEgr<br />
QC BAT CHMATROGRFAGENT SPIKE<br />
Duplicate of Sample # $0 3161 01<br />
gv3 tB^lOz I -<br />
g03 i_06 02<br />
go3 2zZO2<br />
$-03 Z: '7Z0\<br />
Hatched and QC updated by^_ on 3 -2 5-%^<br />
Rec'd in Prep Lab by -- vr.- on 3 -H -W Sop>9RtCttRCSoI^ M-2 C)_<br />
Rec'd in Sep Lab by 6TL1)<br />
on 312- 411 Y<br />
Rec'd in Sep lab by /L( — on SOP# Rte:<br />
ED/CPPT on SOP# R.t -<br />
Rec'd in C . R_ by---4- on 'f I i k r SOpag _ tZ r tilts, 7 ,o t Rn-4 o<br />
Da ta Reviewed by on<br />
sop# t^<br />
^F`T^ ^Re1d<br />
O riginal batch sh t and complete calculation file to be filed with the FIRST Gsted work order num be r.<br />
FORM NO.: R -52. 1/98_ Rev 8<br />
SCE ^--RA
J r<br />
CHAIN-OF-CUSTODY HATCH ANALYSIS RECORD 10-Mar-1998<br />
ql/1 Page 1<br />
1) INITIATED<br />
SOP (S) #<br />
"Do3 16) b 1 O-00038Z<br />
ACTIONS (Initial & Date)<br />
oaa^7<br />
CUSTOMER: BHI SAMPLE DELIVERY GROUP<br />
MATRIX OTHER VuI BATCH NUMBER<br />
/,<br />
_1(^I<br />
CUSTOMER<br />
QES ID DUP ACCOUNT ID COMMENTS<br />
SA, Afjn^<br />
1 ) 80316101 0.000yrt BHI BON680<br />
2 ) R0314410:2 LZtc 5-25 9d I I BON 681<br />
5) COUNTING/MEASUREi`1ENT LAB<br />
SOP (5) #<br />
2) PREP LAB RECEIVEll 3-i9 - CC _ 6) DATA REVIEWED AND<br />
ANALYTICAL PREP STORED<br />
SOP (S) # ^R-L4A^\J^:^)<br />
SOP (s) #<br />
3) SAMPLE REMAINDER STORED•z51t<br />
4) SEPARATION LAB RECEIVED<br />
SOPS) B J w<br />
SOP' (S) !k<br />
vL,.^J
n/ ^j\x CHAIN-OF-CUST011`r' BAICFi ANAL`iTiIS RECORD 11-Mar-1998<br />
UU ,J` U<br />
Page 1<br />
, I TOMER: BHI<br />
-j<br />
501PLL DELIVERY GROUP W6422 /<br />
llV// MATRIX OTHER g- BATCH NUMBER LCJ<br />
1 )<br />
CUSTOMER<br />
OES ID SDAU pACCOUNT (D COMMENTS<br />
2 ) 60318402 0-00034Z BHI BONE03<br />
3 ) sea^a4e^ 0at3•z54k -IT<br />
1) INITIATED<br />
/<br />
tiC<br />
01dS (Tuitial I< Date)<br />
-1<br />
U 5) COUNTING/MEASURE4IENT L D<br />
SOPS) # r-! SOPS) 4<br />
2) PREP LAD RECEIVED 3-Ict-4^^SL 6) DATA =.EVCEWFID AND<br />
ANALYTICAL PREP STORED<br />
SOP (s) 4 R1ctFScL^i^^-o<br />
3) SAMPLE REMAINI)ER STOR`--r )<br />
C^ ^^ (J i If rJ<br />
4) ===;RATIO;•! L B RE.C==VC0<br />
o^(s a<br />
L20el
:r Tr-99<br />
CHAIN--OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1998<br />
` Page 1<br />
l•<br />
/ CUSTOMER: BHI<br />
SAMPLE DELIVERY GROUP<br />
MATRIX<br />
^Q<br />
OTHER ^^ D` BATCH NUMBER LEA OWE<br />
^-st<br />
CUSTOMER<br />
OES ID DUP ACCOUNT ID COMMENTS<br />
5A AQ At<br />
1 ) 9a-3:0601 --Z)0C -s•u Ski; BGW609<br />
2 ) 60320602 0-00°6a6 BHI BON636<br />
3 ) QQ-2ncn- 1 -pe 3 • 2,5 am;<br />
_ ^l_Ap:T C1=5<br />
13 ,90CA97<br />
1) INITIATED _) t^b COUNTING !NEISUP,Ei'IEhIT LAB<br />
SOPS) 4 oWG SOI'iS? T<br />
2) PREP LAD RECEIVED ^_-1q-^^^` 6) DATA RE"'IcWEL' AND<br />
ANALYTICAL PREP STDRED<br />
90F`-) 4 R^t}iZC v\3 ^<br />
SC i'' Ie/ '^<br />
3) SAMPLE REMAIi`OEF ST7RL 1)<br />
4) SEPARATION LAD RECEIV:T)<br />
I 1 _`) 'It<br />
LL-VJ
GvJ ^)<br />
^<br />
II<br />
VIA//<br />
CUSTOMER<br />
MATRIX<br />
BHI<br />
CHAIN--OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998<br />
Page 1<br />
SAMPLE DELIVERY GROUP IJDo^^7S<br />
OTHER IO^(/(^ I BATCH NUMBER<br />
CUSTOMER<br />
QES I 1) DUP ACCOUNT ID COMMENTS<br />
'S4 quq^<br />
1 ) 89a2229 } B)a4 BQW;$38<br />
2 ) 80322202 0-00°6 77 BHI 13 01.4609<br />
ACTIONS (ILtitial & Date)<br />
^j<br />
1) INITIATED 5) CUNTING/MEASUREMENT LAB<br />
SOP(S) # SOP (S) #<br />
2) PREP LAB RECE.'.VED ?Zlc]. ^<br />
SOf' S) i5 _F<br />
Ur TA di:b!ED %)i;-:<br />
!i'1-'LYT.Gt\L PREP S 7 0R="D<br />
c+ Q _ i3 -Q)<br />
3) SAMPLE PENAI`CER STORi=O 3_ZS ^^^uL<br />
G20G
C`IAIN-OP-CUSTODY BATCH ANALYSIS RECORD 17-Mar-1996<br />
Page 1<br />
1 i<br />
CUSTOMER: BHI SAMPLE DELIVERY GROUP<br />
MATRIX OTHER ^ BATCH NUMBER<br />
OES Ill DUP ACCOUNT<br />
CUSTOMER<br />
ID COMMENTS<br />
S y A+jf4fr<br />
------------------ - --------------______________________________________<br />
I ) 80327'-101 0_00ob !o BHI BON692<br />
2 ) BHi<br />
----------- -- -- -- ----- - --- - -------------- - -<br />
lACCjTICNS (I) itiai D-i-)<br />
1) INITIATED +)^ i ;_.H?_?I !NI \SURE`:1F.NT LAR<br />
6OP(S) #_^ L ^! SO? (S)<br />
21 PREP LAB :R c.(;=iVED I ` -`Z$ DDS b) i) ATA REV ( f:WFD AND<br />
AidALV'_:AI_ of^cp ST'^ftED -__<br />
3) SAMPLE F'EV-J ;Ii : i?E? S T OR :D 3.25-4^_f^t^<br />
4) ScP:ARr1Ti:=?; _-- YD:C= ' .t:+:<br />
SCf' (B i ;;<br />
)!)<br />
U2 o
' l i uani'erra<br />
E _l,st8<br />
S Tiv<br />
BATCH SUMMARY/CHAIN OF CUSTODY<br />
AVALYSIS TC -9 MATRIX DUE DATE LI -b-`c8<br />
st_%j R-&y<br />
19 ORK ORDER SEQUENM # QdENi' C lzg mm<br />
1 oil&`V -1B<br />
cs t+i<br />
QCBATCHREAGENI'BLANK<br />
J ata. _Ix QCBATCHMATRDMHIAMC<br />
J O31 h-4 _IM 099)<br />
J N<br />
(dsde)<br />
lq 2M or 2S<br />
(drde)<br />
D 03 iky -Ol<br />
QC BATCH MATRI)WEACENT<br />
SPUM<br />
QC BATCH MAIRDUREAGENT SPIIM<br />
Duplicate of San* #i $703 1840 1<br />
^SO^I&4ol 03<br />
-a la<br />
Wn 227<br />
^b3 1b102<br />
$0b2.o6o1 b3 2- 5A<br />
$03a22o1<br />
S-0 -5 P- bZ<br />
^ro3 Z 12b2<br />
,., l a _.<br />
OTC<br />
Batched and QC updated by 'wL on 5-2--s-1Y<br />
Rec'd in Prep Lab by -7z> eL on 3 -t°t Aqv<br />
Rec'd in Sep Lab by_ 1Wl on >> 2 9 Si<br />
Rec'd in Sep lab by on<br />
ED/CPPT by on<br />
Sop# a CtA 2CSbv3 RCO 0<br />
Sop# A^ C I7 R C 1 6615 Rev*<br />
{,<br />
^ Rev#<br />
Rec'd in C.R- by it on 3Sop# f` /c ,Q y^ryyl ) Rev<br />
Data Reviewed by on ^- Z' Sop# f ` L W ( Ma 2Rn-4__ _ L<br />
Original batch sheet and I<br />
complete calculation file to be filed with the FIRST fisted work order number.<br />
FORM NO.: RC-52,1/98, Rev 8<br />
Revd<br />
6 206
cclaq<br />
w^'M t+s
_<br />
SF^ Aa A^<br />
Jll,! ''CUTS<br />
G^1C
^!^ n"mil 12^^ 1 ?5<br />
P, ^LrKZC S o i3 ^<br />
5 25 -Z<br />
^l
Get
SAr A-&) A^<br />
621 J
jS A-<br />
V-D<br />
621=
CLIENT:<br />
PROJECT ID:<br />
BHI_45<br />
SAP B98-061<br />
Cr+6 CHAIN OF CUSTODY<br />
MATRIX: OTHER DUE DATE: 03/31/98<br />
SDG W02275 BATCH: 03-184<br />
SAMPLE # CLIENT ID COMMENTS<br />
W803184 01A BON682<br />
W803184 02A BON683<br />
W803184 03A BON684<br />
Comments:<br />
q QC REQUIRED<br />
INITIALS DATE ^ SOP#<br />
COC INITIATED L^ 7 , N/A<br />
SAMPLE PREPARATION 3/1 1 gz RICHWC5003 Rev 2<br />
SAMPLE ANALYSIS 3 ^ RICHWC5003 Rev 2<br />
DATA REVIEW RICHWC5003 Rev 2<br />
L^-1J
CLIENT:<br />
PROJECT ID:<br />
CS+6 CHAIN OF CUSTODY<br />
BHI_15 MATRIX: OTHER DUE DATE:<br />
SAP B98-063 SDG W02261 BATCH:<br />
SAMPLE # CLIENT ID COMMENTS<br />
W803216 01A BON894 (^, ^j b8,5)<br />
W803216 02A BON895 (^Gy 3)<br />
W803216 03A BON896 C' JG ,kj ypl<br />
Comments:<br />
El QC REQUIRED<br />
04/01/98<br />
03-216<br />
INITIALS DATE SOP#<br />
COC INITIATED ^j(C^ N/A<br />
SAMPLE PREPARATION RICHWC5003 Rev 2<br />
SAMPLE ANALYSIS RICHWC5003 Rev 2<br />
DATA REVIEW<br />
3 !^ Cyy RICHWC5003 Rev 2<br />
C^lU
CLIENT:<br />
PROJECT ID:<br />
BHI_45<br />
SAY B98-063<br />
Cr+6 CHAIN OF CUSTODY<br />
q QC REQUIRED<br />
MATRIX: WATER DUE DATE: 03/31/98<br />
SDG W02261 BATCH: 03-186<br />
SAMPLE # CLIENT ID COMMENTS<br />
W803186 01A BON783<br />
Comments:<br />
INITIALS DATE SOP#<br />
COC INITIATE D N/A<br />
SAMPLE PREPARATION<br />
^<br />
RICHWC5003 Rev 2<br />
li<br />
SAMPLE ANALYSIS RICHWC5003 Rev 2<br />
DATA REVIEW 3 Q RICEWC5003 Rev 2<br />
G
CLIENT:<br />
PROJECT ID:<br />
BHI_45<br />
SAF B98-061<br />
Ci+6 CHAIN OF CUSTODY<br />
MATRIX: OTHER DUE DATE:<br />
SDG W02275 BATCH:<br />
SAMPLE # CLIENT ID COMMENTS<br />
W803272 OIA BON692<br />
El QC REQUIRED<br />
04/06/98<br />
03-272<br />
W803272 02A BON693 ?o32,790/<br />
W803272 03A BON694<br />
Comments*<br />
COC INITIATED<br />
INITIALS DATE SOP#<br />
'31 -7 /9 9<br />
SAMPLE PREPARATION 36l RICHWC5003 Rev 22<br />
SAMPLE ANALYSIS<br />
a !6<br />
N/A<br />
RICHWC5003 Rev 2<br />
DATA REVIEW RICHWC5003 Rev<br />
G^:1^<br />
it<br />
it
CLIENT:<br />
PROJECT ID:<br />
Ci+6 CHAIN OF CUST0DY<br />
BHI_45 MATRIX: OTHER DUE DATE:<br />
SAF B98-063 8DG W02281 BATCH:<br />
SAMPLE # I CLIENT ID ( COMMENTS<br />
W803279 01A BON898 C ^0Y0 ><br />
Comments:<br />
COC INITIATED y _<br />
El QC REQUIRED<br />
04/06/98<br />
03-279<br />
INITIALS DATE SOP#<br />
r/, `/ b<br />
SAMPLE PREPARATION RICHWC5003 Rev 2<br />
SAMPLE ANALYSIS RICHWC5003 Rev 2<br />
DATA REVIEW RICKWC5003 Rev 2<br />
N/A<br />
^"^.j
CLIENT:<br />
PROJECT ID:<br />
Cr+6 CHAIN OF CUSTODY<br />
BHI_45 MATRIX: OTHER DUE DATE:<br />
SAY B98-061 SDG W02275 BATCH:<br />
SAMPLE # CLIENT ID ( COMMENTS<br />
W803206 01A BON685<br />
04/01/98<br />
03-206<br />
QC REQUIRED<br />
W803206 02A BON686<br />
a-LD ^i41eL ,- 1ficGI uulwl-luL-( r3r) L<br />
W803206 03A BON687 grj32^ld^^<br />
Comments:<br />
INITIALS DATE SOP#<br />
COC INITIATED 7^= N/A<br />
SAMPLE PREPARATION RICHWC5003 Rev 2<br />
SAMPLE ANALYSIS RICHWC5003 Rev 2<br />
DATA REVIEW RICEWC5003 Rev 2<br />
G4.
CLIENT:<br />
PROJECT ID:<br />
Ci+6 CHAIN OF CUSTODY<br />
BHI_15 MATRIX: OTHER DUE DATE:<br />
SAP B98-063 SDG W02261 BATCH:<br />
SAMPLE # CLIENT ID I COMMENTS<br />
W803216 01A I BON894 C r3 .Qb8& l<br />
W803216 02A BON895<br />
(pO<br />
W803216 03A BON896 C'JG/ l ^^^<br />
Comments:<br />
3 )<br />
q QC REQUIRED<br />
04/01/98<br />
03-216<br />
INITIALS DATE SOP#<br />
COC INITIATED ^^ ^7 N/A<br />
SAMPLE PREPARATION<br />
SAMPLE ANALYSIS<br />
3 ^z^ ^C<br />
3/1<br />
RICHWC5003 Rev 2<br />
RICHWC5003 Rev 2<br />
DATA REVIEW 3 / 4 Y RICHWC5003 Rev 2-<br />
nn^<br />
^^1
CLIENT:<br />
PROJECT ID:<br />
BHI_45<br />
SAF B98-061<br />
Cr+6 CHAIN OF CUSTODY QC REQUIRED<br />
MATRIX: OTHER DUE DATE: 04/02/98<br />
SDG W02275 BATCH: 03-222<br />
SAMPLE # CLIENT ID I COMMENTS<br />
W803222 01A I BON688<br />
W803222 02A BON689<br />
Comments:<br />
80 A)<br />
INITIALS DATE SOP#<br />
COC INITIATED ^- __^( N/A<br />
SAMPLE PREPARATION<br />
3 13 1q - RICHWC5003 Rev 2<br />
SAMPLE ANALYSIS Tfo 3 13 4 RICHWC5003 Rev 2<br />
DATA REVIEW RICHWC5003 Rev 2<br />
7 .^ r
CLIENT:<br />
PROJECT ID:<br />
Ci+6 CHAIN OF CUSTODY<br />
BHI_45 MATRIX: OTHER DUE DATE:<br />
SAF B98-063 SDG W02281 BATCH:<br />
SAMPLE # CLIENT ID COMMENTS<br />
W803242 01A I BON897<br />
Comments:<br />
QC REQUIRED<br />
04/03/98<br />
03-242<br />
INITIALS DATE SOP#<br />
COC INITIATED / N/A<br />
SAMPLE PREPARATION RICHWC5003 Rev 2<br />
SAMPLE ANALYSIS<br />
DATA REVIEW<br />
3/Na<br />
RICHWC5003 Rev 2<br />
M 3 9 1 ,^, IRICHWC5003 Rev 2 1
CLIENT:<br />
PROJECT ID:<br />
BHI_45<br />
SAF B98-061<br />
Cr+6 CHAIN OF CUSTODY QC REQUIRED<br />
MATRIX: OTHER DUE DATE: 04/03/98<br />
SDG W02275 BATCH: 03-244<br />
SAMPLE # CLIENT ID I COMMENTS<br />
W803244 01A BON690<br />
W803244 02A BON691<br />
Comments:<br />
I IALS DATE SOP#<br />
COC INITIATED ^' /,^ N/A<br />
SAMPLE PREPARATION RICHWC5003 Rev 2<br />
SAMPLE ANALYSIS 3r/9 RICKWC5003 Rev 2<br />
DATA REVIEW 7j lb<br />
^^ RICHWC5003 Rev 2<br />
i
CLIENT:<br />
PROJECT ID:<br />
BHI_45<br />
SAF B98-061<br />
Cr+6 CHAIN OF CUSTODY<br />
0 QC REQUIRED<br />
MATRIX: OTHER DUE DATE: 03/30/98<br />
SDG W02275 BATCH: 03-161<br />
SAMPLE # CLIENT ID COMMENTS<br />
W803161 01A BON680<br />
W803161 02A BON681<br />
Comments:<br />
INITIALS DATE SOP#<br />
COC INITIATED ^^ N/A<br />
SAMPLE PREPARATION 3/Old RICHWC5003 Rev 2<br />
SAMPLE ANALYSIS RICHWC5003 Rev 2<br />
DATA REVIEW 34497 RICHWC5003 Rev 2
CLIENT:<br />
PROJECT ID:<br />
Ci+6 CHAIN OF CUSTODY<br />
BHI_15 MATRIX: OTHER DUE DATE:<br />
SAF B98 - 063 BDG W02261 BATCH:<br />
SAMPLE # CLIENT ID I COMMENTS<br />
W803216 01A BON894 l rJG/-) (a^GJ<br />
W803216 02A BON895 ( J30 ^,-/ by3 )<br />
W803216 03A BON896<br />
Comments:<br />
El QC REQUIRED<br />
04/01/98<br />
03-216<br />
INITIALS DATE SOP#<br />
COC INITIATED 7 N/A<br />
SAMPLE PREPARATION 3/^^/ 8 RICHWC5003 Rev 2 II<br />
SAMPLE ANALYSIS<br />
31&<br />
—<br />
RICHWC5003 Rev 2<br />
DATA REVIEW RICHWC5003 Rev 2<br />
G^t_v<br />
I