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Metals and Ceramics Division - Oak Ridge National Laboratory

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Cermet Composites for Wear Applications<br />

R. J. Stafford<br />

Cummins Inc.<br />

Objective/Scope<br />

TiC/Ni3Al is a composite of TiC powder in a Ni3Al matrix which was developed in collaboration<br />

with <strong>Oak</strong> <strong>Ridge</strong> <strong>National</strong> <strong>Laboratory</strong> (ORNL) <strong>and</strong> CoorsTek. Its composition was established to<br />

match the unique properties required for Cummins Fuel Systems applications. CoorsTek <strong>and</strong><br />

ORNL have developed the processing methods to make the material, while Cummins has been<br />

responsible to finding an application for it <strong>and</strong> testing the material as fuel system components<br />

<strong>and</strong> evaluating their performance versus other materials. The objectives of this work are to<br />

characterize the material <strong>and</strong> optimize the composition <strong>and</strong> processing. Specific objectives are:<br />

• Optimize injection molding binder composition <strong>and</strong> sintering cycles to achieve 99+%<br />

density. This will include the determination of the shrink rate during sintering for<br />

prototype tool construction <strong>and</strong> demonstration.<br />

• Determine production viable sources for all raw components in the composition.<br />

• Test prototype components in intended application on Cummins’ fuel system test rigs to<br />

show viability of material in an application.<br />

Approach<br />

• A prototype injection-molding tool of a proposed Cummins Fuel Systems component will<br />

be made <strong>and</strong> test pieces of the TiC/Ni3Al cermet will be produced to near-net shape for<br />

evaluation of shrinkage, microstructure uniformity, <strong>and</strong> density.<br />

• Prototypes machined from isostatically pressed rods of the TiC/Ni3Al cermet will be<br />

tested on abuse tests at Cummins Fuel Systems.<br />

• Production source for NiAl powder will be identified <strong>and</strong> processing parameters for the<br />

new powder determined to ensure the properties of the final composition do not vary<br />

from the properties of the composition using the original NiAl powder.<br />

Technical Highlights<br />

Ni3Al/TiC Composite<br />

Testing <strong>and</strong> pending approval of a new source of the critical NiAl raw material from Accumet is<br />

underway. ORNL (Tiegs) has sintered test parts from first prototype design successfully to the<br />

same density as the previous material (from X-Form, now out of business). A test lot of powder<br />

has been processed through milling at ORNL, compounded into feedstock, molded <strong>and</strong> debound<br />

at CoorsTek, it is waiting for a new sintering trial at Colorado School of Mines (CSM). Some<br />

initial parts sintered at CSM were 97.7% dense; whereas, the parts sintered at ORNL were 98.8%<br />

dense.<br />

From these tests, we will measure a final shrinkage to create the mold for the revised prototype<br />

part. The part was redesigned to add stock for fixturing during the finish grinding operations at<br />

Cummins.<br />

.

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