6. OC2_L06Amine

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<strong>6.</strong>6 LABORATORY PREPARATIONS CH 3 Cl + CH 3 CH 2 NH 2 → CH 3 CH 2 NHCH 3 Fe/HCl OH - CH 3 CH 3 CH 2 CH 2 NO 2 ⎯⎯⎯→ ⎯⎯→ CH 3 CH 2 CH 2 NH 2 CH CH 3 NH 2 H 2 /Ni 3 CH 3 CH 2 COCH 3 ⎯⎯⎯→ ⎯⎯⎯→ CH 3 CH 2 CHNHCH 3 LiAlH 4 /Et 2 O H 3 O + PhCH 2 CN ⎯⎯⎯⎯⎯→ ⎯⎯⎯→ PhCH 2 CH 2 NH 2 (or H 2 /Ni/140 o C) CH 3 (CH 2 ) 4 CONH 2 + KOBr → CH 3 (CH 2 ) 4 NH 2
<strong>6.</strong>7 ANALYSIS OF AMINES -Water soluble amines → turn litmus blue -Water insoluble amines → soluble in dil. HCl -1 o , 2 o , 3 o Amines → classified by Hinsberg test -Nitrous test -aliphatic amines→ give unstable diazonium salts -aromatic amines → give stable diazonium salts
Page 1 and 2: 6 AMINES AND DERIVATIVES 6.1 STRUCT
Page 3 and 4: 6.3 PHYSICAL PROPERTIES -The only o
Page 5 and 6: -Reaction with Nitrous Acid C 6 H 5
Page 7: -Electrophilic Aromatic Substitutio
Page 11 and 12: Question 4. จงดุลสม

6. OC2_L06Amine

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