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Laboratory Methods of Organic Chemistry - Sciencemadness Dot Org

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90 EQUIPMENT REQUIRED BY THE BEGINNER<br />

EQUIPMENT REQUIRED BY THE BEGINNER<br />

I. APPARATUS<br />

Beakers, 100, 500, and 1000 c.c, one <strong>of</strong> each.<br />

Burette. 1<br />

Calcium chloride tubes, straight, 3.<br />

Cardboard for weighing (playing-cards).<br />

Condensers, Liebig type, one about 60 cm. long ; a shorter one,<br />

10-12 cm. long ; one <strong>of</strong> the Dimroth or coil type.<br />

Conical flasks, 50, 100, 250, 500 c.c, two <strong>of</strong> each.<br />

Copper wire for halogen test.<br />

Cork-borers.<br />

Corks, various sizes.<br />

Crystallising basins, glass, 3, 5, 7 cm., one <strong>of</strong> each.<br />

Distilling flasks, ordinary and Claisen types, 25, 50, 100 cc. one<br />

<strong>of</strong> each.<br />

Files, round and triangular, one <strong>of</strong> each.<br />

Filter flasks, 100, 500, 1000 c.c.<br />

Filter paper, a few sheets.<br />

Filter jars, 500 and 1000 c.c, one <strong>of</strong> each.<br />

Filter plates, porcelain, 1, 3, 5 cm.<br />

Filter tubes, long and short, 3 <strong>of</strong> each.<br />

Funnels, 2 <strong>of</strong> smallest size, one each <strong>of</strong> other sizes up to 12 cm.<br />

Cylindrical Buchner funnel, about 8 cm. Dropping funnel,<br />

25 c.c. capacity with short stem and 100 c.c. capacity with<br />

long stem.<br />

Glass buttons, for filtration, 2.<br />

Glass rods, 20 <strong>of</strong> various thicknesses and lengths, rounded at<br />

both ends but not thickened.<br />

Glass tubes, drawn out to form pipettes (dropping tube, p. 12).<br />

Glass tubing, straight and bent.<br />

Labels.<br />

Measuring cylinders, 10 c.c, 100 c.c.<br />

Melting-point tubes, thin (to be made by the student).<br />

Metal spatula.<br />

Mortar.<br />

1 The student should be able to carry out at once, at any time, the usual volumetric<br />

determinations. As a rale the readiness to carry out titrations in the<br />

organic laboratory is not so great as is urgently desirable.

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