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Laboratory Methods of Organic Chemistry - Sciencemadness Dot Org

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EXTKACTION APPAEATUS 35<br />

The extraction apparatus is used chiefly for dissolving out<br />

sparingly soluble constituents from mixtures, and for isolating<br />

natural products from (dry) vegetable or animal material. Occasionally<br />

it is very useful for " recrystallising " sparingly soluble<br />

substances from the extraction thimble by means <strong>of</strong> an appropriate<br />

solvent (especially ether). As a rule, crystals <strong>of</strong> the dissolved<br />

material separate already from the solution in the flask during the<br />

process <strong>of</strong> extraction. This solution soon becomes supersaturated<br />

even while hot.<br />

L<br />

FIG. 25 FIG. 26 FIG. 27<br />

When solvents <strong>of</strong> high boiling point are used the extraction<br />

thimble is directly suspended by a thin wire in the round-botomed<br />

flask, but should not dip into the liquid.<br />

WORKING WITH COMPRESSED GASES<br />

Nowadays every university laboratory is doubtless supplied with<br />

steel cylinders in which the most important gases in common use are<br />

stored in the compresed state.<br />

These gases are :<br />

(1) Oxygen, hydrogen, nitrogen.<br />

(2) Carbon dioxide, chlorine, ammonia, sulphur dioxide.

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