Methods for the determination of 3-MCPD-fatty acid esters

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Conclusions of Second Collaborative Study Results of the Method Validation and the Proficiency Test 1. „BfR Method 9“ delivered reproducible results, which are comparable with the results of all applied „in-house“ methods acidic hydrolysis „BfR Method 8“ HFBA derivatization „BfR Method 10“ 2. more than 90% of the laboratories reached a z-score < |2| for all five samples Angelika Preiß-Weigert 18 May 2010 3rd Meeting AOCS Expert Panel on Process Contaminants page 16
Third Collaborative Study in fat containing foods Schedule Types of Food Infant formula Margarine Hazelnut or Chocolate Spread The work for preparing the study - like method development and homogeneity studies - is still ongoing Shipment of samples October 2010 Report of results December 2010 Finalization of evaluation March 2011 You are kindly invited to participate in this study. Angelika Preiß-Weigert 18 May 2010 3rd Meeting AOCS Expert Panel on Process Contaminants page 17
Page 1 and 2: FEDERAL INSTITUTE FOR RISK ASSESSME
Page 3 and 4: First BfR Collaborative Study (2008
Page 5 and 6: Strategy for the Development of BfR
Page 7 and 8: Characteristics of the methods Hydr
Page 9 and 10: Sample materials Second Collaborati
Page 11 and 12: 3-MCPD-fatty acid esters [mg/kg] in
Page 13 and 14: Second Collaborative Study (2009) M
Page 15: z-Score Results Second Collaborativ
Page 19 and 20: Second Collaborative Study - Profic
Page 21 and 22: Methode „BfR 9“ Umesterung im A

Methods for the determination of 3-MCPD-fatty acid esters

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