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Structural, Spectral, Biological and Electrochemical Studies Of Some ...

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Chapter3. 40<br />

SPECTRAL, ELECTROCHEMICAL AND BIOLOGICAL STUDIES OF<br />

COPPER(II) COMPLEXES WITH N-N-S DONOR LIGANDS<br />

3.1 Introduction 40<br />

3.2 Experimental 43<br />

3.2.1 Materials<br />

3.2.2 Syntheses ofcomplexes<br />

3.2.3 Measurements<br />

3.3 Results <strong>and</strong> discussion 46<br />

3.3.1 Magnetic susceptibility<br />

3.3.2 Vibrational spectra<br />

3.3.3 Electronic spectra<br />

3.3.4. EPR spectral investigations<br />

3.4 <strong>Electrochemical</strong> studies 70<br />

3.5 Antimicrobial activity 75<br />

3.5.1 Test organisms<br />

3.5.2 Sample preparation<br />

3.5.3. Procedure<br />

3.6 Concluding remarks 81<br />

References 82

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