Synthesis, Structure and Catalytic Activity of ... - Jacobs University

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Ch.1 Introduction _____________________________________________________________ 2003 41,42, 24 monomer di As2W19Ti2 2007 43 15 25 L d monomer mono (MeO)TiW5O18 1996 44 10 a: Keggin ion b: one host-two guests system meaning two metal cations in one vacant site c: Wells-Dawson ion d: Lindqvist ion *: structures based on IR and NMR (no XRD data) #: Cp is cyclopentadiene Fig. 1.7 Polyhedral representation of “PW11Ti” Fig. 1.8 Polyhedral representation of “PW10Ti2” 17
Ch.1 Introduction _____________________________________________________________ Fig. 1.9 Polyhedral representation of “P2W15(TiO2)3(OH)3” Despite of what is mentioned above; monomeric Ti-substituted polyoxoanions still exist in literature, such as the monosubstituted monomeric Keggin [PW11TiO40] 5- (entry 1) first reported in 1983 by Domaille and Knoth 25 and the monolacunary Lindqvist functionalized by a methoxy titanium group (entry 25) (Fig. 1.10). Fig. 1.10 Polyhedral representation of the Linqvist structure [(MeO)TiW5O18] 3- 18
Page 1 and 2: Synthesis, Structure and Catalytic
Page 3 and 4: Abstract __________________________
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Page 7 and 8: Chapter III Synthetic Results 3.1 G
Page 9 and 10: 4.2.3 Catalytic experiments 121 4.2
Page 11 and 12: Fig. 1.16 Polyhedral representation
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Page 15 and 16: Codes of Compounds Compound K8[Ti4O
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Ch.3 Synthetic Results ____________
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Ch.4 Catalytic Results ____________
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p-xylene conversion (mole %) Ch.4 C
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TEACHING Teaching assistantships in
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Appendix 1. Cyclic Ti9 Keggin Trime
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Synthesis, Structure and Catalytic Activity of ... - Jacobs University

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