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Portamess 911 Oxy - Knick Elektronische Meßgeräte GmbH & Co.

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User Manual<br />

<strong>Portamess</strong>® <strong>911</strong> <strong>Oxy</strong><br />

SE 302 / SE 303


Warranty<br />

Defects occurring within 3 years from delivery date shall be remedied<br />

free of charge at our plant (carriage and insurance paid by sender).<br />

Sensors and accessories: 1 year.<br />

Subject to change without notice.<br />

Return of products<br />

Please contact our Service Team. Ship the cleaned device to the<br />

address you have been given.<br />

If the device has been in contact with process fluids, it must be<br />

decontaminated/disinfected before shipment. In that case,<br />

please attach a corresponding certificate, for the health and<br />

safety of our service personnel.<br />

Disposal<br />

Please observe the applicable local or national regulations<br />

concerning the disposal of “waste electrical and electronic<br />

equipment”.<br />

<strong>Knick</strong><br />

<strong>Elektronische</strong> Messgeräte<br />

<strong>GmbH</strong> & <strong>Co</strong>. KG<br />

Beuckestr. 22<br />

14163 Berlin, Germany<br />

Tel. +49-30-80191-0<br />

Fax +49-30-80191-200<br />

Internet: http://www.knick.de<br />

knick@knick.de


<strong>Co</strong>nventions Used in this Manual<br />

ITALICS are used for texts which appear in the<br />

<strong>Portamess</strong>® <strong>911</strong> <strong>Oxy</strong> display.<br />

Bold print is used to represent the texts of keys, e.g.<br />

cal.<br />

Display examples<br />

or<br />

keys whose functions are explained are frequently<br />

shown in the left-hand column.<br />

Note<br />

Notes provide important information which should<br />

always be observed when using the meter.<br />

Caution<br />

Caution means that the instructions given must<br />

always be followed to prevent malfunctions or<br />

damage to the device.<br />

Warning<br />

Warning means that the instructions given must<br />

always be followed for your own safety. Failure to<br />

follow these instructions may result in injuries.<br />

Information<br />

3


Safety Information<br />

Be sure to read and observe the following instructions!<br />

Whenever it is likely that the protection has been impaired, the meter shall<br />

be made inoperative and secured against unintended operation.<br />

The protection is likely to be impaired if, for example:<br />

• the meter shows visible damage<br />

• the meter fails to perform the intended measurements<br />

• after prolonged storage at temperatures above 70 °C<br />

• after severe transport stresses<br />

Before recommissioning the meter, a professional routine test in accordance<br />

with EN 61 010-1 must be performed. This test should be carried out by the<br />

manufacturer.<br />

Information<br />

4


EC Declaration of <strong>Co</strong>nformity<br />

Information<br />

5


Table of <strong>Co</strong>ntents<br />

<strong>Co</strong>nventions Used in this Manual................................................ 3<br />

Safety Information........................................................................ 4<br />

Be sure to read and observe the following instructions!................. 4<br />

EC Declaration of <strong>Co</strong>nformity...................................................... 5<br />

1 The Model <strong>911</strong> <strong>Oxy</strong> .................................................................... 9<br />

Package contents .......................................................................................... 9<br />

Intended use / Short description ............................................................ 9<br />

2 Operation ................................................................................. 11<br />

Meter design .................................................................................................11<br />

Display .............................................................................................................12<br />

Keypad .............................................................................................................13<br />

<strong>Co</strong>nnection and start-up ..........................................................................14<br />

How to handle meter and sensors ........................................................16<br />

<strong>Co</strong>nfiguration ................................................................................................17<br />

Calibration.......................................................................................................18<br />

3 Troubleshooting ...................................................................... 23<br />

Sensoface® .....................................................................................................23<br />

4 Maintenance ............................................................................ 25<br />

Changing the batteries .............................................................................25<br />

Cleaning the meter .....................................................................................26<br />

5 SE 302 / SE 303 Dissolved <strong>Oxy</strong>gen Sensors ........................... 27<br />

Safety precautions for sensor handling...............................................28<br />

<strong>Co</strong>mmissioning the SE 302 / SE 303 sensors......................................28<br />

Polarization.....................................................................................................29<br />

Sensor operation..........................................................................................29<br />

Sensor maintenance....................................................................................30<br />

Replacing the membrane and electrolyte..........................................30<br />

Sensor cleaning and servicing.................................................................31<br />

Storage of SE 302/SE 303...........................................................................32<br />

Sensor accessories: protection sleeve/immersion weight............32<br />

Table of <strong>Co</strong>ntents<br />

6


Appendix ..................................................................................... 33<br />

Product line and accessories....................................................................33<br />

Specifications for Model <strong>911</strong> <strong>Oxy</strong>...........................................................34<br />

Specifications for SE 302 / 303 sensors................................................36<br />

Glossary....................................................................................... 37<br />

Index ............................................................................................ 38<br />

Table of <strong>Co</strong>ntents<br />

7


1 The Model <strong>911</strong> <strong>Oxy</strong><br />

Package contents<br />

Please check the completeness of the shipment after<br />

unpacking.<br />

The package should include:<br />

• Model <strong>911</strong> <strong>Oxy</strong> incl. batteries and sensor quiver<br />

• Carrying strap<br />

• User manual<br />

Intended use / Short description<br />

• The Model <strong>911</strong> <strong>Oxy</strong> serves for simultaneous measurement<br />

of temperature and dissolved oxygen in water<br />

taking account of the barometric pressure.<br />

• Temperature compensation is automatic using an<br />

NTC 22 kΩ.<br />

• The meter complies with the European EMC<br />

regulations.<br />

• The meter is IP 66 protected to EN 60 529 (jet water<br />

from all directions).<br />

• Only three alkaline AA (LR6) batteries are required for<br />

uninterrupted operation for approx. 1000 hours.<br />

• Sensor connection via SixPlug.<br />

• Automatic calibration in air can be performed directly<br />

in the sensor quiver.<br />

• Thanks to the continuous polarization of the<br />

connected sensor, it is always ready to use.<br />

The Model <strong>911</strong> <strong>Oxy</strong><br />

9


• To prolong battery life, the meter switches off automatically<br />

when it is inactive for either one hour or twelve<br />

hours.<br />

The Model <strong>911</strong> <strong>Oxy</strong><br />

10


2 Operation<br />

Meter design<br />

1 <strong>Co</strong>nnector for dissolved oxygen sensor<br />

2, 3 Not used<br />

4 Not used<br />

5 Sensor quiver, removable<br />

Operation<br />

11


Display<br />

1 Sensor data very good (Sensoface®, page 23)<br />

Sensor data still acceptable<br />

Sensor must be checked<br />

2 Replace battery<br />

3 Press cal key<br />

4 Wait<br />

5 Measurement units (main display)<br />

6 Measurement units (secondary display)<br />

7 Main display<br />

8 Secondary display<br />

9 Error message<br />

10 Slope and zero point<br />

Operation<br />

12


Keypad<br />

▲<br />

▼<br />

Switches the meter on or off. After power-on, the meter<br />

automatically performs a self-test.<br />

Returns the meter to the measuring mode from any<br />

function. The meas key can also be used to switch the<br />

meter on.<br />

Select and change parameters (or modes).<br />

Starts calibration.<br />

Note<br />

+<br />

Opens the configuration menu. Meter must be<br />

switched off. Keep the cal key depressed and then<br />

press the on/off key.<br />

When pressing down two keys simultaneously, make<br />

sure that the left key of the illustration is pressed first.<br />

Operation<br />

13


<strong>Co</strong>nnection and start-up<br />

Sensor connection<br />

SE 302<br />

SE 303<br />

ZU 0554<br />

ZU 0555<br />

Note<br />

The meter can be combined with the following dissolved<br />

oxygen sensors from our range of accessories.<br />

Dissolved oxygen sensor with integrated NTC temperature<br />

detector (1.5-m cable / SixPlug)<br />

Immersion sensor with integrated NTC temperature<br />

detector (5-m cable / SixPlug)<br />

An adapter cable allows connection of various<br />

commercial dissolved oxygen sensors:<br />

For connection of process sensors with 4-pole cap<br />

For connection of process sensors with VP cap<br />

When using commercial sensors, please contact <strong>Knick</strong><br />

<strong>Elektronische</strong> Messgeräte <strong>GmbH</strong> & <strong>Co</strong>. KG to ensure<br />

compatibility between sensor and Model <strong>911</strong>.<br />

How to connect the sensor via SixPlug<br />

Notch<br />

Plug<br />

Tab<br />

Socket<br />

• Slightly insert the plug into the socket and turn it<br />

until the tab in the socket seats in the plug notch.<br />

• The plug will then slip deeper into the socket.<br />

• To tighten the assembly, shift the knurled nut over<br />

the plug and turn it clockwise until the stop.<br />

Caution<br />

Safe electrical contact is only made when the knurled<br />

nut is screwed on until the stop.<br />

Operation<br />

14


Terminal assignments<br />

<strong>Co</strong>nnection.................................................Socket<br />

<strong>Co</strong>nnector for dissolved oxygen sensor..................... 1<br />

n. c........................................................................................2, 3<br />

n. c............................................................................................ 4<br />

Cathode<br />

Anode<br />

NTC 22 kΩ<br />

Note<br />

All calibration and configuration data remain permanently<br />

stored even if the meter is switched off or the batteries are<br />

removed (battery replacement).<br />

Operation<br />

15


Note<br />

Pressing on/off switches the meter to measuring mode.<br />

At power-on, the meter performs a self-test:<br />

• Simultaneous lighting-up of all display segments<br />

• Display of model designation <strong>911</strong><br />

• Display of software version<br />

The meter can also be switched on with the meas key.<br />

In that case only a short check is performed.<br />

How to handle meter and sensors<br />

Caution<br />

The sensor quiver<br />

The sensor can be kept permanently in the sensor quiver<br />

of the meter. A moisturized fleece in the quiver prevents<br />

the sensor from drying out.<br />

How to store the sensor in the quiver:<br />

• Take the fleece out of the empty quiver, moisten it and<br />

put it back into the quiver.<br />

• Remove the protection cap from the sensor.<br />

• Insert sensor into the quiver.<br />

Be sure to keep the fleece in the quiver moist.<br />

• Switch the Model <strong>911</strong> <strong>Oxy</strong> on. If required, polarize the<br />

sensor for 6 hours (see page 29).<br />

Operation<br />

16


<strong>Co</strong>nfiguration<br />

+<br />

Activate configuration:<br />

Keep the cal key depressed and then press the on/off<br />

key.<br />

The meter acknowledges activation of configuration<br />

mode.<br />

Press cal to proceed.<br />

Salinity.<br />

Adjust using arrow keys: 0 - 45<br />

Press cal to confirm.<br />

Selection of concentration (mg/l) / saturation (%)<br />

Display formats: xx.xx mg/l / xx.x mg/l / xxx.x % / xxx %<br />

(Select using arrow keys.) Press cal to confirm.<br />

Calibration interval.<br />

Adjust using arrow keys: 0 - 14 (days)<br />

Press cal to confirm.<br />

Auto switch-off (Display off when meter not active).<br />

Select using arrow keys: 1 / 12 (hours)<br />

Press cal to confirm.<br />

Select measurement unit for temperature display.<br />

Select using arrow keys: °C/°F<br />

Press cal to confirm.<br />

Operation<br />

17


Calibration<br />

Regular calibration of the sensor slope is required to<br />

obtain precise measurement results.<br />

The SE 302/303 sensors have a very low zero point current.<br />

A zero calibration is therefore not required (see page 36).<br />

If other dissolved oxygen sensors with different offset<br />

characteristics are connected via adapter, a zero<br />

calibration is possible.<br />

Caution<br />

Caution<br />

Prior to initial start-up or after the sensor has been disconnected<br />

from the meter for more than 5 minutes, the sensor<br />

must be polarized before calibration or measurement<br />

(see page 29).<br />

Without calibration every dissolved oxygen meter delivers<br />

an imprecise measured value! Especially after replacing<br />

the DO sensor, the electrolyte, or the sensor membrane,<br />

you must perform a calibration!<br />

For 2-point calibration, perform zero calibration first.<br />

Operation<br />

18


Calibration – Slope<br />

Place sensor in water-saturated air, e.g.:<br />

Moisten the fleece in the sensor quiver of the meter and<br />

place sensor in the quiver. Wait for stable temperature<br />

and humidity conditions, i.e. until the measurement<br />

display has stabilized.<br />

To activate calibration: Press cal.<br />

Select slope calibration using arrow keys.<br />

(Select: AirCAL)<br />

<strong>Co</strong>nfirm by pressing cal (or cancel with meas).<br />

The calibration procedure is started. (Hourglass flashes)<br />

Sensor current (compensated) is displayed.<br />

End of calibration: PRESS cal flashes.<br />

<strong>Co</strong>ncentration/saturation and sensor current are<br />

displayed.<br />

Press cal to save new slope (or cancel with meas).<br />

Possible error messages during calibration<br />

ERROR and t.out are flashing.<br />

Maximum calibration time exceeded.<br />

Press meas to cancel calibration.<br />

Wait for stable temperature and humidity conditions if<br />

required and repeat calibration.<br />

ERROR and Slope are flashing.<br />

Slope out of range.<br />

Press meas to cancel calibration or<br />

press cal to start a new slope calibration.<br />

Operation<br />

19


Calibration – Zero point<br />

Place sensor in oxygen-free medium and wait for a stable<br />

measured value:<br />

To activate calibration: Press cal.<br />

Select zero calibration using arrow keys<br />

(Select: 0Point)<br />

<strong>Co</strong>nfirm by pressing cal (or cancel with meas).<br />

The calibration procedure is started. (Hourglass flashes)<br />

Sensor current is displayed.<br />

End of calibration: PRESS cal flashes.<br />

Press cal to save new zero point.<br />

Possible error messages during calibration<br />

ERROR and t.out are flashing.<br />

Timeout.<br />

Press meas to cancel calibration.<br />

Wait for stable conditions if required<br />

and repeat calibration.<br />

ERROR and 0Point are flashing.<br />

Zero current out of range.<br />

Press meas to cancel calibration or<br />

press cal to start a new zero calibration.<br />

Operation<br />

20


Measurement<br />

Pressing meas accesses the measuring mode from all<br />

functions. In the measuring mode, the main display<br />

indicates the measured variable and the secondary<br />

display shows the temperature:<br />

Fig. 1: Display during salinity measurement<br />

Caution<br />

Device self-test<br />

When the meter is switched on using the on/off key, an<br />

automatic self-test is performed. When the self-test has<br />

been passed, PASS appears in the secondary display.<br />

The meter then switches to measuring mode.<br />

If FAIL is displayed, you must switch the meter off and<br />

return it to the manufacturer.<br />

Auto switch-off<br />

To prolong battery life, the display switches off automatically<br />

when it is inactive for a period longer than specified.<br />

You can choose between switch-off after one or after<br />

twelve hours.<br />

Sensor polarization voltage is not switched off.<br />

Operation<br />

21


AutoRead<br />

The AutoRead function minimizes errors caused by<br />

measurement cycles which are too short. During<br />

measurement of dissolved oxygen, the same criteria are<br />

applied as for calibration (waiting time, stability).<br />

To take an AutoRead measurement:<br />

Press the meas key for at least 2 seconds.<br />

Only one measurement is taken. Measurement is<br />

indicated by a flashing A on the display:<br />

Fig. 2: Display during AutoRead measurement.<br />

Only when the measured value has stabilized, flashing<br />

will stop and the display will be frozen.<br />

Pressing meas starts a new measurement.<br />

To exit AutoRead mode, hold down the meas key for at<br />

least 2 seconds.<br />

Operation<br />

22


3 Troubleshooting<br />

Sensoface®<br />

The little smiley in the display (Sensoface®) alerts for sensor<br />

problems (defective cable, maintenance request). The permitted<br />

calibration ranges and the conditions for a friendly,<br />

neutral, or sad Sensoface® are summarized in the following<br />

chart:<br />

Permissible<br />

range<br />

Slope Zero point Response<br />

time<br />

25 to 130 nA -2 to +2 nA max. 720 s<br />

Calibration<br />

timer *<br />

> 35 to < 90 nA > -0.3 to < +0.3 nA ≤ 300 s ≤ 80 % expired<br />

> 30 to 35 nA<br />

or<br />

90 to 600 s**<br />

Clock icon on<br />

80 to ≤ 100 %<br />

expired<br />

expired<br />

* The cal timer is set during configuration (switched off with 0000).<br />

** (>720 s: calibration aborted)<br />

Note<br />

Disregarding the Sensoface® display, the meter continues<br />

measuring the process variable.<br />

Troubleshooting<br />

23


Err Meaning Cause Display Remedy<br />

01 Measurement<br />

range exceeded<br />

03 Temperature<br />

range exceeded<br />

04 Zero cannot be<br />

calibrated<br />

05 Slope cannot be<br />

calibrated<br />

07 (AutoRead only)<br />

Sensor signal<br />

not stable<br />

11 (AutoRead only)<br />

Sensor signal<br />

not stable<br />

18 <strong>Co</strong>nfiguration or<br />

calibration data<br />

defective<br />

• Overflow<br />

• Sensor defective<br />

• Temp detector<br />

defective<br />

• Short circuit<br />

• Electrolyte used<br />

up<br />

• Sensor defective<br />

• Electrolyte used<br />

up<br />

• Sensor defective<br />

19 Factory settings, System failure<br />

system memory<br />

defective<br />

Measured value and<br />

Error 01 flashing<br />

Temperature display<br />

and Error 03 flashing<br />

Smiley “sad” and<br />

Error 04 flashing<br />

Smiley “sad” and<br />

Error 05 flashing<br />

Measured value and<br />

Error 07 flashing<br />

Error 11 flashing<br />

Error 18 flashing<br />

Error 19 flashing.<br />

Display reads FAIL<br />

Check sensor,<br />

calibrate if required<br />

Check sensor<br />

Check sensor,<br />

calibrate if required<br />

Check sensor,<br />

calibrate if required<br />

Check opening for<br />

pressure sensor<br />

(1 mm dia. breakthrough<br />

at enclosure<br />

rear)<br />

Clean sensor<br />

<strong>Co</strong>mpletely reconfigure<br />

and calibrate<br />

the meter<br />

The meter must<br />

be repaired and<br />

recalibrated at the<br />

factory.<br />

Note<br />

The Model <strong>911</strong> <strong>Oxy</strong> simultaneously measures temperature and<br />

dissolved oxygen taking account of the barometric pressure. If<br />

the process pressure deviates from the barometric pressure, a<br />

corresponding error is produced for saturation measurement.<br />

<strong>Co</strong>ncentration is still indicated correctly.<br />

Troubleshooting and Maintenance<br />

24


4 Maintenance<br />

Changing the batteries<br />

When the battery symbol appears in the display, the batteries<br />

need replacement. However, the meter can still be<br />

used for a few days. When the battery voltage continues<br />

to drop, the meter will switch itself off.<br />

To replace the batteries, you need 3 alkaline AA cells (or<br />

LR 6) and a screwdriver (either straight-blade or Phillips).<br />

Make sure that the meter is carefully closed again and the<br />

protective cover is properly mounted on the meter after<br />

changing the batteries.<br />

• Close the protective cover and remove the sensor<br />

quiver.<br />

• Lift the hook, unscrew the four screws on the back of<br />

the meter and remove the lid.<br />

• Remove the old batteries from the battery holder.<br />

• Insert the new batteries in the specified direction.<br />

• Make sure the protective cover is in the notches provided<br />

and the rubber seal is correctly seated, especially<br />

near the sensor socket.<br />

• Remount the lid and secure it with the screws.<br />

Be sure to tighten the screws thoroughly.<br />

• Remount the sensor quiver.<br />

Note<br />

When changing the batteries, all calibration and configuration<br />

data are retained. The time and date must be reset.<br />

Maintenance<br />

25


Caution<br />

If you want to store the meter for a longer period of time,<br />

the batteries must always be removed beforehand.<br />

Leaky batteries may damage the meter.<br />

If the meter was disconnected from a power source for a<br />

longer time, e.g. because the batteries were empty or had<br />

been removed, the sensor must be polarized (see page 29).<br />

Cleaning the meter<br />

To remove dust and dirt, the external surfaces of the meter<br />

may be cleaned with water and a mild household cleaner,<br />

if necessary.<br />

Maintenance<br />

26


5 SE 302 / SE 303 Dissolved <strong>Oxy</strong>gen Sensors<br />

Intended use / Short description<br />

The Models SE 302 / SE 303 are low-maintenance sensors<br />

for measurement of dissolved oxygen and temperature in<br />

water. They require no flow and provide highly accurate<br />

values.<br />

The sensors are intended for operation with <strong>Knick</strong> Model<br />

913/913 OXY portable meters.<br />

They are connected to the meter via a cable with SixPlug<br />

connector.<br />

The Model SE 303 is intended for application with the<br />

ZU 0605 immersion weight.<br />

Build-up of the sensors<br />

1 Cable connection<br />

2 Thread for fastening the immersion weight<br />

3 <strong>Co</strong>ne for fixing the sensor in the quiver<br />

Plastic body with<br />

4 anode<br />

5 cathode<br />

6 Membrane module filled with electrolyte (replaceable)<br />

7 Cap sleeve with protective bars<br />

8 Plastic protection cap<br />

Sensors<br />

27


Safety precautions for sensor handling<br />

Warning<br />

When the sensor is damaged or otherwise manipulated,<br />

alkaline (caustic) electrolyte may escape. With a pH<br />

value of 13, the electrolyte is strongly alkaline. Always<br />

avoid contact with skin, particularly eyes and mucous<br />

membranes.<br />

In case of a contamination immediately flush the affected<br />

parts with plenty of water.<br />

If you don’t feel well, immediately consult a doctor.<br />

When replacing the electrolyte and the membrane module,<br />

it is inevitable that electrolyte comes into contact with<br />

your fingers. Therefore be sure to wear protective gloves.<br />

Observe the technical specifications (see page 36)!<br />

<strong>Co</strong>mmissioning the SE 302 / SE 303 sensors<br />

Prior to initial<br />

start-up<br />

<strong>Co</strong>nnection<br />

Caution<br />

• It is recommended to replace the electrolyte as<br />

described on page 30 to compensate for electrolyte loss /<br />

consumption during storage.<br />

• Visually check the membrane for cracks or notches<br />

(When the membrane is damaged, the membrane<br />

module must be replaced, see page 30).<br />

• <strong>Co</strong>nnect the sensor to the meter observing the corresponding<br />

instructions (see page 14).<br />

Prior to initial start-up or after the sensor has been disconnected<br />

from the meter for more than 5 minutes, the sensor<br />

must be polarized before calibration or measurement.<br />

Sensors<br />

28


Polarization<br />

Sensor operation<br />

• <strong>Co</strong>nnect the sensor to the Model <strong>911</strong> OXY.<br />

The sensor will be polarized after 6 hours (also with the<br />

meter switched off).<br />

Duration of polarization when the sensor has been<br />

disconnected for ...<br />

• more than approx. 10 minutes:<br />

<strong>Co</strong>mplete polarization for 6 hours<br />

• less than approx. 10 minutes:<br />

Polarization for 45 minutes.<br />

• less than approx. 5 minutes:<br />

Polarization for 10 minutes.<br />

• If the sensor has not been connected sufficiently long to<br />

the Model <strong>911</strong> <strong>Oxy</strong>, it must be polarized (see above).<br />

• Switch the meter on.<br />

If required, polarize the sensor for 6 hours.<br />

• Remove protection cap (8). Keep sensor in air with the<br />

membrane (6) pointing downwards.<br />

• Start calibration at the meter (see page 18).<br />

• Measurement: Keep the membrane module (6) pointing<br />

downwards!<br />

• Store sensor in the meter quiver after each use.<br />

Moisten the fleece.<br />

• SE 303 only: With the immersion weight at the cable, the<br />

sensor can be lowered, e.g. into a basin. This must take<br />

place very slowly.<br />

Note<br />

It is recommended to keep the sensor connected to the<br />

meter. This ensures that the sensor membrane is permanently<br />

polarized – also with the meter switched off – and<br />

the sensor is always ready to use.<br />

Sensors<br />

29


Sensor maintenance<br />

When used in water only, the sensors are of low maintenance.<br />

• Calibrate regularly (see page 18)<br />

• Visually check the membrane for cracks or notches.<br />

When the membrane is damaged or the sensor response<br />

times become too long, the membrane and electrolyte<br />

should be replaced.<br />

Replacing the membrane and electrolyte<br />

Note<br />

Be sure to proceed as described in the following.<br />

• Loosen the SixPlug connection.<br />

• Screw off the cap sleeve from the sensor body and carefully<br />

pull it off.<br />

• Pull off membrane module from inner body. If it is<br />

jammed, you should push it out using the flat side of<br />

your fingertip.<br />

• Before replacing the electrolyte, the membrane module<br />

must be removed from the cap sleeve.<br />

• Clean the inner body using a soft paper tissue.<br />

• Fill the membrane module with O 2<br />

electrolyte until it<br />

is half full. Be sure that there are no air bubbles in the<br />

membrane module. Air bubbles can be removed by<br />

carefully knocking against the membrane module.<br />

• Push the membrane module in vertical position over the<br />

inner body. Excess electrolyte is pushed out and must be<br />

soaked up with a paper tissue.<br />

• Carefully push the cap sleeve over the mounted<br />

membrane module and screw it on. Be sure that the cap<br />

sleeve is dry and clean.<br />

• After every replacement of electrolyte or membrane<br />

module the sensor must be polarized for 6 hours.<br />

• Then a calibration must be performed (see page 18).<br />

Sensors<br />

30


Sensor cleaning and servicing<br />

• You can carefully clean the sensor with soapy water (or<br />

with chemically non-aggressive agents) and then rinse<br />

it thoroughly.<br />

• Visually check the membrane for cracks or notches.<br />

When the membrane is damaged, the membrane and<br />

electrolyte should be replaced.<br />

Sensors<br />

31


Storage of SE 302/SE 303<br />

Clean the sensor and membrane before storing them (see<br />

page 16).<br />

Filled with electrolyte and closed with the protection<br />

cap or kept in the quiver at the meter, the sensors can be<br />

stored for several months.<br />

Sensor accessories: protection sleeve/immersion weight<br />

ZU 0605<br />

The protection sleeve/immersion weight for SE 303<br />

serves to hold the sensor down and increase mechanical<br />

protection.<br />

For sensor specifications, see page 36.<br />

Sensors<br />

32


Appendix<br />

Product line and accessories<br />

Ref. No.<br />

Sensors Dissolved oxygen sensor with 1.5-m cable SE 302<br />

Dissolved oxygen sensor for immersion<br />

measurements, with 5-m cable<br />

(without immersion weight)<br />

SE 303<br />

Accessories<br />

<strong>Oxy</strong> Set A for lab and field measurements,<br />

consisting of: SE 302 oxygen sensor with<br />

1.5-m cable, rugged field case, replacement<br />

quiver and fleece (5 units)<br />

ZU 0602<br />

<strong>Oxy</strong> Set B for immersion measurements, ZU 0603<br />

consisting of: SE 303 dissolved oxygen sensor,<br />

with 5-m cable, protection sleeve/immersion<br />

weight, rugged field case, replacement quiver<br />

and fleece (5 units)<br />

Protection sleeve/immersion weight for<br />

SE 303 immersion sensor<br />

ZU 0605<br />

Moisturizing fleece (8 units) ZU 0571<br />

Membrane kit (4 membrane modules T96,<br />

individually packed, 25 ml electrolyte)<br />

Sensor quiver / calibration chamber and<br />

moisturizing fleece (5 units)<br />

<strong>Co</strong>nnecting cable for connection of process<br />

sensors with 4-pole cap, 3 m<br />

<strong>Co</strong>nnecting cable for connection of process<br />

sensors with VP cap, 3 m<br />

Flow-through fitting for SE 302 sensor, glass,<br />

with hose connections<br />

ZU 0604<br />

ZU 0331<br />

ZU 0554<br />

ZU 0555<br />

ZU 0284<br />

Appendix<br />

33


Specifications for Model <strong>911</strong> <strong>Oxy</strong><br />

DO input<br />

Input for SE 302 / SE 303 dissolved oxygen sensors,<br />

various process sensors with 4-pole or VP cap<br />

Saturation 0 to 600 % (0 °C to 55 °C) 1)<br />

configurable to 0.0 to 199.9 % in the range 0 to 200 %<br />

Meas. range<br />

Measuring current 0 to 600 nA<br />

Meas. error 2,3,4) 0.5 % meas.val. + 0.2 %<br />

<strong>Co</strong>ncentration<br />

Meas. error 2,3,4)<br />

Barometric pressure<br />

Salt correction<br />

Calibration<br />

cal<br />

0.00 to 60.0 mg/l (0°C to 55°C)<br />

configurable to 0.00 to 19.99 mg/l in the range 0.0 to 20.0 mg/l<br />

0.5% meas.val. + 0.05mg/l<br />

700 to 1080 hPa<br />

<strong>Co</strong>nfigurable to 0.00 to 45.00 g/kg<br />

Solubility function to EN 25814<br />

0 = switched off, SA icon inactive<br />

Automatic with water-saturated air in quiver,<br />

Zero calibration possible<br />

Calibration range Zero point ±2 nA<br />

Polarization voltage<br />

Slope<br />

675 mV<br />

25 to 130 nA<br />

Cal timer 0 to 14 days default setting 6 days<br />

Pressure correction<br />

Temperature input<br />

Automatic using integrated pressure sensor<br />

NTC 22 kΩ integrated in DO sensor<br />

Meas. range -5.0 to +55.0 °C / 23 to +131 °F<br />

Resolution 0.1 °C / 1 °F<br />

Meas. error 2,3,4)<br />

Temperature<br />

compensation<br />

< 0.5 K<br />

Automatic with NTC<br />

Appendix<br />

34


Display<br />

Measuring cycle<br />

Self-test<br />

Power supply<br />

LC display 67 x 35 mm, 7-segment<br />

Measurement display: mg/l; %, °C, °F<br />

3 Sensoface® indicators,<br />

8 icons or symbols<br />

10 years<br />

(EEPROM)<br />

Emitted interference:<br />

EN 61 326 Class B<br />

Immunity to interference:<br />

EN 61 326<br />

Operation: –10 to +55 °C<br />

Transport and storage: –20 to +70 °C<br />

PA enclosure with integrated sensor quiver<br />

<strong>Co</strong>lor Pigeon blue RAL 5014<br />

Dimensions<br />

Ingress protection IP 66<br />

H 160 mm, W 130 mm, D 35 mm<br />

1) 600 % only possible for slope values < 90 nA, normal pressure and 25 °C.<br />

2) to IEC 746 Part 1, at nominal operating conditions<br />

3) ± 1 count<br />

4) plus sensor error<br />

Appendix<br />

35


Specifications for SE 302 / 303 sensors<br />

Function principle<br />

Dimensions:<br />

Body length<br />

Body diameter<br />

Cable length<br />

Materials:<br />

Membrane<br />

Body<br />

O-rings<br />

<strong>Co</strong>nnection<br />

Temp detector<br />

Membrane-covered, amperometric sensor<br />

120 mm<br />

12 mm<br />

SE 302: 1.5 m<br />

SE 303: 5 m<br />

T-96: Teflon/silicone/Teflon<br />

(reinforced with steel mesh)<br />

PPS<br />

Viton®, silicone<br />

Cable with SixPlug connector<br />

NTC 22 kΩ<br />

Temperature range 0 to 60 °C<br />

Ambient conditions<br />

Air humidity 0 to 100 %<br />

Sensor signal<br />

in room air:<br />

in oxygen-free<br />

medium<br />

50 to 110 nA at 25 °C<br />

< 0.3 % of signal in room air<br />

Range 0.01 to 60 mg/l at 25 °C<br />

Detection limit<br />

Response time t 98%<br />

Accuracy<br />

< 0.3 % of signal in room air, max 30 ppb<br />

< 90 s at 25 °C, from air to nitrogen<br />

±1 % of signal, max ±30 ppb<br />

Dependency on flow < 5%, 1% at 0.3 m/s<br />

Polarization voltage<br />

Polarization time<br />

-675 mV<br />

< 6 h<br />

Regeneration Electrolyte and membrane module replaceable, see page 30<br />

Submersibility<br />

5 m<br />

Appendix<br />

36


Glossary<br />

Automatic<br />

switch-off<br />

(AutOFF)<br />

AutoRead<br />

function<br />

cal<br />

Calibration<br />

<strong>Co</strong>ncentration<br />

GLP<br />

meas<br />

Percent<br />

saturation<br />

Response time<br />

Salinity<br />

Slope<br />

Zero point<br />

To prolong battery life, the meter switches off automatically<br />

when it is not operated for a period longer than<br />

specified. Switch-off can take place after one or after<br />

twelve hours.<br />

Only stable values are displayed as measurement result.<br />

This minimizes errors resulting from measuring cycles<br />

which are too short.<br />

Key for activating calibration.<br />

Adjustment of dissolved oxygen meter to sensor<br />

parameters (slope, zero)<br />

The amount of dissolved oxygen per volume (e.g. in<br />

mg/l). Calculated by the meter from the oxygen partial<br />

pressure and the solubility function.<br />

Good Laboratory Practice: Guidelines for performance<br />

and documentation of measurements in the laboratory<br />

This key allows return to measuring mode from all other<br />

levels.<br />

Ratio (in percent) of the measured quantity of O 2<br />

to the<br />

highest possible quantity (saturation)<br />

Time from the start of a calibration step to the stabilization<br />

of the measured values.<br />

The salinity indicates the salt content of sea waters, for<br />

example.<br />

Transfer characteristic of the sensor:<br />

Sensor current / oxygen partial pressure<br />

Sensor signal which is output when measuring in an<br />

oxygen-free medium such as pure nitrogen.<br />

Glossary<br />

37


Index<br />

23<br />

°C / °F, configuration 17<br />

A<br />

Accessories 33<br />

Automatic self-test 21<br />

AutoRead function 22<br />

Auto switch-off, configuration 17<br />

Auto switch-off, description 21<br />

B<br />

Battery replacement 25<br />

C<br />

Calibrating the slope 19<br />

Calibrating the zero point 20<br />

Calibration, general 18<br />

Calibration interval, configuration<br />

17<br />

Changing the batteries 25<br />

Cleaning the meter 26<br />

Cleaning the sensor 31<br />

<strong>Co</strong>mmissioning the sensors 28<br />

<strong>Co</strong>ncentration measurement 17<br />

<strong>Co</strong>nfiguration 17<br />

<strong>Co</strong>nnecting the sensors 14<br />

<strong>Co</strong>nnections, overview 11<br />

D<br />

Declaration of <strong>Co</strong>nformity 5<br />

Diagnostics, Sensoface 23<br />

Display format 17<br />

Display icons 12<br />

Disposal 2<br />

Dissolved oxygen sensors 27<br />

E<br />

EC Declaration of <strong>Co</strong>nformity 5<br />

Electrolyte replacement 30<br />

Error messages, overview 24<br />

Error messages, slope calibration 19<br />

Error messages, zero calibration 20<br />

G<br />

Glossary 37<br />

I<br />

Intended use 9<br />

Intended use, sensors 27<br />

K<br />

Keypad 13<br />

M<br />

Maintenance 25<br />

Measuring mode 21<br />

Membrane replacement 30<br />

O<br />

Operation 11<br />

Order information 33<br />

<strong>Oxy</strong>gen sensors 27<br />

P<br />

Package contents 9<br />

Polarization 29<br />

Product line 33<br />

Protection sleeve/immersion weight 32<br />

R<br />

Replacing the membrane and<br />

electrolyte 30<br />

Index<br />

38


S<br />

Safety precautions 4<br />

Safety precautions for sensor<br />

handling 28<br />

Salinity, configuration 17<br />

Saturation measurement 17<br />

SE 302 / SE 303 dissolved oxygen<br />

sensors 27<br />

Self-test 21<br />

Sensoface 23<br />

Sensor accessories 32<br />

Sensor care 16<br />

Sensor connection 14<br />

Sensor maintenance 30<br />

Sensor operation 29<br />

Sensor polarization 29<br />

Sensor quiver 16<br />

Sensor specifications 36<br />

Short description 9<br />

SixPlug connector 14<br />

Slope calibration 19<br />

Socket assignment 15<br />

Specifications, portable meter 34<br />

Specifications, sensors 36<br />

Start-up 14<br />

Storing the meter 26<br />

Storing the sensor 16<br />

T<br />

Technical data 34<br />

Technical terms 37<br />

Temperature display °C / °F 17<br />

Terminal assignments 15<br />

Troubleshooting 23<br />

W<br />

Warranty 2<br />

Z<br />

Zero calibration 20<br />

Index<br />

39


084071<br />

TA-193.402-KNE03 20120904<br />

Software version: 1.x

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