M.Sc. Chemistry Syllabus Revised Implemented ... - Shivaji University

8.Coumarin Synthesis
9.Synthesis of Heterocyclic compounds.
10. Synthesis of Dyes
B)Estimations:
1.Estimation of unsaturation.
2.Estimation of formalin.
3.Colorimetric Estimation of Dyes
4.Estimation of Amino acids
(Any suitable Expt. may be added.)
REFERENCE BOOKS
1.A text book of practical organic chemistry- A. I. Vogel.
2.Practical organic chemistry- Mann and Saunders.
3.A handbook of quantitative and qualitative analysis- H. T. Clarke.
4.Organic Synthesis Collective Volumes by Blat.
M.Sc I – Semester I
Physical Chemistry Practicals
Students are expected to perform 15-20 experiments of three and half hours
duration.
Experiments are to be set up in the following techniques.
1. Potentiometry:
Determination of solubility and solubility product of silver halides, determination
of binary mixture of weak and strong acid etc.
2. Conductometry :
Determination of mixture of acids and relative strength of weak acids.
3 Refractometry :
Determination of molecular radius of molecule of organic compound.
4 Polarimetry :
Kinetics of inversion of cane sugar in presence of strong acid.
5 Chemical Kinetics :
Kinetics of reaction between bromate and iodide.
6 Partial Molar Volume :
Determination of PMV by intercept method, density measurements etc.
( New experiments may also be added )
Books recommended for Practicals :
1 Findlay’s Practical Chemistry – Revised by J.A. Kitchner (Vedition)
2 Text Book of Quantitative inorganic analysis : A.I. Vogel.
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