M.Sc. Chemistry Syllabus Revised Implemented ... - Shivaji University

Rinehart and Winston Inc )
M. Sc. Part – I (Semester - II)
CH – 201: Inorganic Chemistry Practical Course
(Practical no. 211 and 212)
1. Ore analysis – ‘2’ ores
2. Alloy analysis – ‘2’ (Two and three components)
3. Inorganic Preparations and purity – ‘4’
References:
1) A text book of Quantitative Inorganic Analysis – A. I. Vogel
2) Experimental Inorganic Chemistry - W. G. Palmer
3) The analysis of minerals and ores of the rarer elements – W. R. Schoeller
and A. R. Powell, Charles, Griffin and Company Limited
SEM-II
ORGANIC CHEMISTRY PRACTICLES
1.Qualitative analysis:
Separation and identification of the two component mixtures using
Chemical and physical methods.
2.Thin layer chromatography (TLC).
3.Column chromatography and steam distillation techniques.
4.Determination of percentage of Keto-enol form.
5.Estimation of pesticides
(Any other suitable experiments may be added).
REFERENCE BOOKS
1.A text book of practical organic chemistry- A. I. Vogel.
2.Practical organic chemistry- Mann and Saunders.
3.A handbook of quantitative and qualitative analysis- H. T. Clarke.
4.Organic Synthesis Collective Volumes by Blat.
M.Sc I – Semester II
Physical Chemistry Practicals
Students are expected to perform 15-20 experiments of three and half-hours
duration.
Experiments are to be set up in the following techniques.
1 Potentiometery:
Determination formal redox potential of system, determination of binary mixture
of halides.
2. Conductometry :
Titration of ternary acid mixture of acids, Verification of Onsagar Equation for
1:1 type strong electrolyte.
3 Refractometry :
Determination of atomic refractions of H, C and Cl atoms.
4 Cryoscopy:
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