Gentamicin Sulfate Assay by HPLC with Charged Aerosol ... - Dionex
Gentamicin Sulfate Assay by HPLC with Charged Aerosol ... - Dionex
Gentamicin Sulfate Assay by HPLC with Charged Aerosol ... - Dionex
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6Table 2. Results for one day of replicate sample analysisSampleMeasured<strong>Gentamicin</strong>Concentration(mg/mL)Precision(RSD) n = 3Label Claim(% <strong>Gentamicin</strong> Base)DeterminedSample Amount(% <strong>Gentamicin</strong> Base)AmountSpiked(mg/mL)Ointment (rep. 1) 0.12 0.81 0.1 0.1 0.080 103Ointment (rep. 2) 0.14 4.86 0.1 0.1 0.080 111Ointment (rep. 3) 0.13 2.63 0.1 0.1 0.080 113Recovery(%)Ophthalmic Ointment(rep. 1)0.13 2.12 0.3 0.3 0.080 111Ophthalmic Ointment(rep. 2)0.13 0.77 0.3 0.3 0.080 92Ophthalmic Ointment(rep. 3)0.13 1.09 0.3 0.3 0.080 80Cream (rep. 1) 0.087 1.87 0.1 0.1 0.010 101Cream (rep. 2) 0.087 1.12 0.1 0.1 0.010 98Cream (rep. 3) 0.073 1.79 0.1 0.1 0.010 98Ophthalmic Solution(rep.1)0.051 1.64 0.3 0.3 0.034 112Ophthalmic Solution(rep.2)0.052 3.02 0.3 0.3 0.034 91Ophthalmic Solution(rep.3)0.055 1.27 0.3 0.3 0.034 93
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