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Research and development for industry: Advanced ... - CSIR

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TOWARDS A NEW TITANIUM SECTORPiloting atitanium metalproductionprocessTitanium powder produced with a <strong>CSIR</strong> process. Examples of products madewith the powder are also displayed: The part in the very front through additivemanufacturing <strong>and</strong> the other two through powder metallurgy processes.advantage to the envisaged localtitanium metal <strong>industry</strong>. Thisprocess is being developed by the<strong>CSIR</strong> in a stage-wise manner tomanage the inherent scale-uprisks, <strong>and</strong> it has now reachedthe stage where the design,construction <strong>and</strong> operation ofa small pilot plant have beenapproved by the DST <strong>and</strong> the <strong>CSIR</strong>.The pilot plant has a nominaldesign capacity of producing2 kg/h of titanium powdercontinuously. Construction <strong>and</strong>commissioning of the plant are tobe completed by 31 March 2013.Test campaigns to gain scaleupin<strong>for</strong>mation regarding theprocess, <strong>and</strong> to produce sufficientproduct <strong>for</strong> evaluation by potentialcustomers, are planned followingsuccessful commissioningof the plant.Similar to the <strong>CSIR</strong>, a numberof organisations worldwideare busy scaling up theirown variations of processesto produce titanium metalpowder. Problems with theprocess include the veryhigh heat of reaction, thevery fast rate of reaction, theaggressive <strong>and</strong> hazardousnature of the chemicalsinvolved, <strong>and</strong> the tendency ofthe titanium product to <strong>for</strong>mlumps that block the reactorinlets <strong>and</strong> outlets.In the <strong>CSIR</strong>’s process, therate of TiCl 4reaction isslowed down by executingthe process in a molten saltmedium that allows bettercontrol of the titaniumparticle morphology thanother process variations.In parallel to the technical work, acommercialisation task team withrepresentation from industrial<strong>and</strong> financial concerns has been<strong>for</strong>med to plan <strong>and</strong> manage workto ultimately realise commercialimplementation of the strategy.South Africa’s entire titaniumbeneficiation strategy dependslargely on the success of thispilot plant <strong>and</strong> its furthercommercialisation. Being ableto produce titanium powder ata much lower cost than presentimports will make this light metalan economically viable option,from which many industries canbe created <strong>and</strong> sustained.– Dawie van VuurenEnquiries:Dr Dawie van Vuurendvvuuren@csir.co.zaDr Dawie van Vuuren heads up the <strong>CSIR</strong>’spiloting of titanium metal production.To date, no organisation in the world has been able to produce titanium powder directly in a continuous manneron a commercial scale from titanium tetrachloride (TiCl 4– the usual precursor used <strong>for</strong> titanium metal production).The <strong>CSIR</strong> has developed a process that can do just this, <strong>and</strong> will be setting up a pilot plant in the near future.| 28|Following Australia,South Africa is endowed withthe second largest (about 16%)of titanium-bearing reservesin the world. In South Africa,the mineral is mined <strong>and</strong> thenconcentrated to <strong>for</strong>m slag.This is exported as a relativelylow-value commodity, meetingabout 20% of the world’scurrent raw material dem<strong>and</strong> <strong>for</strong>titanium dioxide pigment, <strong>and</strong>titanium metal production.“The national benefits thatwould arise from a worldscale,low-cost titanium metalplant are considerable.”The potential to add more valueto the raw material throughthe establishment of titaniumpigment <strong>and</strong>/or metal industrieshad been identified in a numberof South African governmentstudies (dating back more than15 years) <strong>and</strong> featured in anumber of national strategies.Why SA needs a titaniummetal producing plantThe national benefits thatwould arise from a world-scale(20 000 tons per annum), lowcost(about US$20/kg milledproducts at 50% of the currentprice) titanium metal plant areconsiderable, with the mostimportant being:• Revenue of about US$400million per annum from themilled product plant alone canbe <strong>for</strong>ecast. Revenue couldincrease to almost US$1 000million per annum once adownstream <strong>industry</strong> <strong>for</strong> theproduction of semi-finishedproducts has been fullydeveloped.• Establishing an <strong>industry</strong> willlead to many downstreammanufacturing enterprises thatwould not be possible withoutsuch a local <strong>industry</strong>.• There is potential <strong>for</strong> the creationof about 1 500 permanent jobsonce the downstream <strong>industry</strong>has been developed to a pointwhere semi-finished productsare produced. This numbercould increase with more finalproducts.• These industries wouldpotentially create opportunities<strong>for</strong> the establishment of small<strong>and</strong> medium enterprises <strong>and</strong>complement Black EconomicEmpowerment.• Support industries could bedeveloped that will further assistwith the expansion of the SouthAfrican economy through jobcreation <strong>and</strong> revenue generation.• A large part of South Africa’sannual importation of about800 tons of titanium invarious <strong>for</strong>ms (sponge, scrap,ferrotitanium, etc.) can bereplaced, saving aboutUS$5 million per annumin <strong>for</strong>eign exchange.In order to realise the opportunityto establish a titanium metal<strong>industry</strong> in South Africa, a focusedprogramme to achieve such anobjective was <strong>for</strong>mulated in 2007by the Department of Science <strong>and</strong>Technology (DST) together withthe <strong>CSIR</strong> <strong>and</strong> the research <strong>and</strong><strong>development</strong> community.A novel process to producetitanium metal powderA key element of the programmeis the <strong>development</strong> of a novelprocess to produce titanium metalpowder that will give a competitive| 29 |

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