ASTM Standards

LUFT/LUST StandardsOil, Grease & TPHMethod 1664413 & 4188440Method 1664Oil, Grease & Total Petroleum Hydrocarbon DeterminationPrecision and Recovery (PAR) Spiking SolutionM-1664-5ML$ 15 / 1 x 5 mLM-1664-5ML-PAKSAVE 20% $ 60 / 5 x 5 mL4.0 mg/mL each in Acetone 2 comps.M-1664-20ML$ 25 / 1 x 20 mLM-1664-20ML-PAKSAVE 20% $ 100 / 5 x 20 mL4.0 mg/mL each in Acetone 2 comps.HexadecaneStearic acidTechnical NoteAccuStandard's Precison and Recovery (PAR) Spiking Solution wasdeveloped for the new Method 1664. This performance based method wasdeveloped to replace previous gravimetric procedures which incorporatedFreon-113 as the extraction solvent for the determination of Oil and Greaseand Total Petroleum Hydrocarbons. Each standard is packaged in a flamesealed ampule conveniently sized for quality control of the analytical batch.Method 413.2 & 418.1Oil, Grease & Petroleum HydrocarbonConcentrates MixChlorobenzene (25.0)Isooctane (37.5)Total Petroleum Hydrocarbon Analysis by IRM-418-CON$ 35 / 1 x 1 mL% by volume 3 comps.Hexadecane (37.5)Oil, Grease and PetroleumHydrocarbon Total Recoverable (IR Method)M-418 $ 30 / 1 x 1 mLM-418-PAKSAVE 20% $ 120 / 5 x 1 mLTotal 4.15 mg/mL in Freon 113, (Parts by volume)3 comps.Chlorobenzene (10.0)n-Hexadecane (15.0)Isooctane (15.0)Method 8440Total Petroleum Hydrocarbon AnalysisTotal Recoverable Petroleum Hydrocarbon MixM-8440 $ 20 / 1 x 1 mLM-8440-PAKSAVE 20% $ 80 / 5 x 1 mLAt stated conc. in Tetrachloroethene3 comps.Chlorobenzene (0.10 w/w %)n-Hexadecane (0.15 w/w %)Isooctane (0.15 w/w %)Total Petroleum Hydrocarbon Concentrate MixM-8440-CONM-8440-CON-PAKChlorobenzene (25.0 vol %)n-Hexadecane (37.5 vol %)$ 30 / 1 x 1 mLSAVE 20% $ 120 / 5 x 1 mL3 comps.Isooctane (37.5 vol %)Silica Gel Cleanup Calibration SolutionM-8440-SGC$ 10 / 1 x 1 mLM-8440-SGC-PAKSAVE 20% $ 40 / 5 x 1 mL10.0 mg/mL in TetrachloroetheneCorn OilLeaking Underground Storage TankRetention Time StandardThis product can be used to screen a sample todetermine what type of petroleum spill that may havecaused the contamination.Retention Time StandardDRH-010S$ 20 / 1 x 1 mLDRH-010S-PAKSAVE 20% $ 80 / 5 x 1 mL25 µg/mL each in CH 2 Cl 2 7 comps.n-Hexanen-Decanen-Dodecanen-Tetracosanen-OctacosaneTechnical Noten-Triacontanen-TetracontaneNEWA sample showing peaks in the C6-C10 range generallyindicates a gasoline spill. Samples with the peaks in the C24-C12 range are indicative of a diesel spill while samples withthe higher carbon numbers above C24 are typically oils orlubricants. Once the initial screen is complete, more detailedwork can be done to further identify the contaminant.Total Petroleum HydrocarbonPattern Recognition StandardsThis book contains chromatography for thevarious petroleum products typically foundduring LUFT/LUST site investigations. Thechromatography shows each fuel pattern in a25 minute analytical run for early elutingpetroleum products like gasoline to lateeluting products like motor oil. In addition,an n-alkane standard (DRH-008S) analyzedunder identical conditions has been overlaidon each petroleum product chromatogram.Use of the book will assist the chemist’sidentification of the fuel for patternrecognition.The n-alkane standard (DRH-008S) overlay provides n-alkane referencepoints between the standard and the unknown sample. These beginning andending n-alkane reference points can be used to establish gross hydrocarbonconcentrations. By comparing the specific n-alkane range of the closestidentified petroleum standard to that of the unknown sample a reproduciblegross hydrocarbon number can be achieved. To Order, BOOK-TPH $ 35LUFT/LUSTFax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com97