ASTM Standards

Method 5599ASTMMemberOxygenates Using O-FIDEPA O-FID Oxygenate Petrochemical StandardsAccuStandard has formulated this second oxygenate version to meet the specific analyte requirements set forth in the EPA methodology.ASTMASTM D-5599EPA Gasoline Refinery Oxygenates Calibration CurvesEPA O-FID Quantitative Calibration Mixes (without Internal Standard)M-GRO-CAL-EPA-SET-10ML$ 350 / set of 5 x 10 mL5 comps.Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5Calibr. range Wt. % Wt. % Wt. % Wt. % Wt. %Methanol 0.30 - 12.00 6.00 12.00 3.00 0.30 9.00Ethanol 0.30 - 12.00 0.30 3.00 6.00 9.00 12.00t-Butanol 0.30 - 12.00 0.30 6.00 9.00 12.00 3.00MtBE 0.30 - 15.00 15.00 7.50 11.25 3.75 0.30RFA Gasoline 78.40 71.50 70.75 74.95 75.70Originally designed forD-5599-95For our complete line ofOrganic Standards,request a copy of ourCatalog.EPA O-FID Quantitative Calibration Mixes (with Internal Standard)M-GRO-CAL-IS/EPA-SET$ 175 / set of 5 x 1 mL6 comps.Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5Calibr. range Wt. % Wt. % Wt. % Wt. % Wt. %Methanol 0.29 - 11.40 5.70 11.40 2.85 0.29 8.55Ethanol 0.29 - 11.40 0.29 2.85 5.70 8.55 11.40t-Butanol 0.29 - 11.40 0.29 5.70 8.55 11.40 2.85MtBE 0.29 - 14.29 14.25 7.13 10.69 3.56 0.291,2-Dimethoxyethane (ISTD) 5.00 5.00 5.00 5.00 5.00RFA Gasoline 74.48 67.93 67.31 71.20 71.92EPA O-FID Quantitative CalibrationCheck Standard(without Internal Standard)M-GRO-EPA-CC-10ML$ 50 / 1 x 10 mLM-GRO-EPA-CC-10ML-PAKSAVE 20% $ 200 / 5 x 10 mL5 comps.Wt./Wt. %Methanol 4.0Ethanol 8.0tert-Butanol 5.0Wt./Wt. %Methyl tert-butyl ether 12.0RFA gasoline 71.0EPA O-FID Spiking SolutionM-GRO-EPA-SP-5MLM-GRO-EPA-SP-5ML-PAKWt./Wt. %Methanol 14.3Ethanol 28.6$ 50 / 1 x 5 mLSAVE 20% $ 200 / 5 x 5 mL4 comps.Wt./Wt. %tert-Butanol 14.3Methyl tert-butyl ether 42.8EPA O-FID Quantitative CalibrationCheck Standard(with Internal Standard)M-GRO-EPA-CC/IS-5ML$ 35 / 1 x 5 mLM-GRO-EPA-CC/IS-5MLPAK SAVE 20% $ 150 / 5 x 5 mL6 comps.Wt./Wt. %Methanol 3.80Ethanol 7.60tert-Butanol 4.75Wt./Wt. %Methyl tert-butyl ether 11.40RFA gasoline 67.45DME (internal standard) 5.0Oxygenate Free Gasoline RefineryBlankM-GRO-BLNK-10MLM-GRO-BLNK-10ML-PAKRFA Gasoline (neat)$ 10 / 1 x 10 mLSAVE 20% $ 40 / 5 x 10 mLTechnical NoteAdditional Oxygenate calibration,check standards, and independentreference standards can be found inASTM method D-4815 (page 24) orD-5622 (page 37). The requiredQA/QC procedures in EPA methodsstipulate a calibration checkstandard be used once peranalytical batch or per 10 sampleset. AccuStandard has bulkpackaged check standards to meetthis increased usage.Internal StandardM-GRO-IS-5MLM-GRO-IS-5ML-PAK$ 10 / 1 x 10 mLSAVE 20% $ 40 / 5 x 10 mL1,2-Dimethoxyethane (ISTD)Cross Reference TableASTM IP ISO DIN JIS AFNOR sorted byASTM Method see beginning of Catalog36 Quality System is Certified to comply with the International ISO 9001 Quality Standard