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Mycotoxin E book 3 A5 size 04

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MYCOTOXINS<br />

Sampling: Critical Point<br />

Ÿ<br />

Quantifying <strong>Mycotoxin</strong> concentration of a maize lot based on<br />

1 sample will give high uncertainty in results<br />

-9<br />

<strong>Mycotoxin</strong>s are measured in nanogram (10 g) of ycotoxin<br />

per gram of RM/Feed (parts per billion or ppb)<br />

In a test procedure conducted by Whitaker et al shows<br />

- Sampling variance of 5 kg sample of shelled<br />

peanuts is 521.4<br />

- Sample preparation variance is 59.2<br />

- Analytical (TLC) variance is 50.1<br />

The Variance in results can be reduced by obtaining a<br />

representative sample correctly and using more sensitive<br />

analytic methods<br />

Obtaining a representative sample of feed or grains<br />

Collect from different points from<br />

- Moving stream of feed/grains<br />

- From silos<br />

- From truck<br />

Ÿ M<br />

Ÿ<br />

Ÿ<br />

Ÿ<br />

Ÿ<br />

1 ppb is equal to 1 second in 32 years or 1 drop of water<br />

in Olympic <strong>size</strong> swimming pool!<br />

Thomas. B. Whitaker, Raymond. D. Coker<br />

42 43

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