March 3 - 5,1999, Karlsruhe, Germany - FZK

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B.E.S.T. Ventil+Fitting GmbH Heinrich-Hertz-Str. 5a 76694 Forst Tel.: 07251 /9722-0 Fax: 07251/9722-50 e-mail: swagelok@best-ka.de Zwei-Klemmringverschraubung Absperr- und Regulierventile Nadelventile Kugel- und Kükenhähne Hochdruckbauteile Rückschlag- und Überströmventile Filter und Filterelemente 1 Manometeradapter Gewindeadapter Vakuum-Produkte
Pilotanlagen - mit Rohrreaktoren (Festbett) - nach dem Schleifenprinzip - Mikroreaktoranlagen Ernst Haoge Apparatebau GmbH & Co KG, KG: Sitz Mülheim a. d. Ruhr, Amisgericht Mülheim a. d. Ruhr, HRA 451. Persönlich haftende Gesellschafterin: Ernst Haage Apparatebau Verwallungs GmbH, Sitz Mülheim a. d. Ruhr, Amtsgericht Mülheim a. d. Ruhr, HRB 2240. Geschäftsführer: Karin Hesselmann, Alfred Hesselmann, Dipl. Kfm. Thomas Hesselmann ERNST HAAGE [Hg Apparatebau GmbH & Co KG PRODUKTPROGRAMM - Laborautoklaven Inhalt 0,15-7,5 Itr. Betriebsdruck bis 350 bar Betriebstemperatur bis 500 °C - Mikroautoklav Inhalt 50 ml Betriebsdruck 350 bar Betriebstemperatur 350 °C - Sonderausführungen Inhalt bis 5.000 Itr. Betriebsdruck bis 2.000 bar Betriebstemperatur bis 800 °C - Hochdruckarmaturen Ernst Haage Apparatebau GmbH & Co KG Hauskampstraße 58 • D-45476 Mülheim an der Ruhr Telefon 0208/40302-0 Telefax 0208/40302-77
Page 1: Forschungszentrum Karlsruhe Technik
Page 4 and 5: Als Manuskript gedruckt Für diesen
Page 6 and 7: Tagungsband der internationalen GVC
Page 8 and 9: Table of Contents Polymers Key Lect
Page 10 and 11: High-pressure apparatus for phase e
Page 14: Polymers 3
Page 17 and 18: ) Precipitation thresholds or polym
Page 19 and 20: solubility of the polymer in the fl
Page 21 and 22: Cationic polymerizations are normal
Page 23 and 24: which is then polymerized. Phase mo
Page 25 and 26: 16. M. Super, E. Berluche, C. Coste
Page 27 and 28: 1-hexene 97 wt% Acros vinyl acetate
Page 29 and 30: acetate / ethylene / nitrogen decre
Page 31 and 32: optical high-pressure cell monomer
Page 33 and 34: 9.5 7,5 '—>—•—I—>—I—>
Page 35 and 36: use of homogeneous catalysts in scC
Page 37 and 38: [9] Yakoumis, I.V., Vlachos, K., Ko
Page 39 and 40: directly related with the nucleatio
Page 41 and 42: MMA), and stabilizer (5.0358 g). Th
Page 43 and 44: kg/mol. Table 2 gives the pseudocom
Page 46 and 47: GVC-Fachausschuß „High Pressure
Page 48 and 49: adequately described by using the s
Page 50 and 51: GVC GVC-Fachausschuß „High Press
Page 52: criterion of successful modificatio
Page 55 and 56: Silica used for supercritical fluid
Page 57 and 58: from experiment B21 with the base -
Page 59 and 60: in different separators. The unit w
Page 61 and 62: Conclusions The reported results sh
Page 63 and 64:
pressures a part of the solvent eva
Page 66 and 67:
GVC GVC-Fachausschuß,.High Pressur
Page 68 and 69:
Using the SWP EOS one can calculate
Page 70 and 71:
GVC-Fachausschuß,Jügh Pressure Ch
Page 72:
Results are shown in Figure 3. It c
Page 75 and 76:
Taking into account the fluid mecha
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66 1
Page 79 and 80:
Experimental The complete set-up is
Page 81 and 82:
70 i
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72 !
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GVC-Fachausschuß „High Pressure
Page 88 and 89:
Pressure M e d i u m Firstly, we re
Page 90:
Extractor 226 Itrs, ID 400, 350 bar
Page 94 and 95:
GVC-Fachausschuß ,Jügh Pressure C
Page 96 and 97:
Tab. 4: Results with industrial was
Page 98 and 99:
Another challenge connected with de
Page 100 and 101:
GVC-Fachausschuß„High Pressure C
Page 102 and 103:
GVC-Fachausschuß „High Pressure
Page 104 and 105:
eflects the supercritical behavior,
Page 106:
6. Davies, IT.; Chem. Eng. Sei.; 19
Page 109 and 110:
-1.5 T 1 P j—1 1 p 1 1— 1 3 5 !
Page 111 and 112:
100
Page 113 and 114:
The temperature of the reactor mate
Page 115 and 116:
Both process streams, the organic p
Page 117 and 118:
cated slightly above those of the f
Page 119 and 120:
au v + c-b (v + c)(v + c + b) with
Page 121 and 122:
the real ones [24], but the more ad
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Fig. 2: Picture of the tumbling rea
Page 125 and 126:
Table 1: Batch experiments Reactant
Page 127 and 128:
116
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118
Page 131 and 132:
Results and Discussion By changing
Page 133 and 134:
122
Page 135 and 136:
Figure 2. Scheme of experimental ap
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glucose yields are in a narrow rang
Page 139 and 140:
CO Ö O 'S ! o d o O Gas eq Liquid
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mol/gcataiysh, we have achieved rea
Page 143 and 144:
selectivity for mono-alkylation and
Page 145 and 146:
Table 1. Oxide aerogels designation
Page 147 and 148:
hydrogenation of soybean oil. Their
Page 149 and 150:
«2 1X3 1 Stmpti t>
Page 151 and 152:
PYROLYSIS T(C) —•— 0,5 MPa H2
Page 153 and 154:
142
Page 155 and 156:
144
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X hyd=X s(T,p)-XlHT,p t) (5) where
Page 159 and 160:
expansion is obtained. By comparing
Page 161 and 162:
the thermodynamic cycle (Figure 1)
Page 163 and 164:
FIGURE 2: Scheme of the apparatus (
Page 165 and 166:
three phase equilibrium. fi(T,p,y 1
Page 167 and 168:
from a thermostated bath. The screw
Page 169 and 170:
200 100 O 313.1 K + 323.1K • 333.
Page 171 and 172:
summarize briefly, the anthraquinon
Page 173 and 174:
atio vs. time is about constant, th
Page 175 and 176:
0 0 0 ^ ^ Header Cooler P2 Ni Ff# i
Page 177 and 178:
800 S 600 200 300 Pressure [bar] Fi
Page 179 and 180:
Figure 1. A: Buffer Volume B: Press
Page 181 and 182:
40. Figure 6. Experimental (• thi
Page 183 and 184:
available PSRK / UNIFAC parameters
Page 185 and 186:
Results and Discussion Some typical
Page 187 and 188:
lower temperatures to a much strong
Page 189 and 190:
Detennination of solubility For det
Page 191 and 192:
The same phase behaviour show for e
Page 193 and 194:
182
Page 195 and 196:
184
Page 197 and 198:
14 0 2 4 6 8 10 12 14 gC02/g solid
Page 199 and 200:
ed carotenoids (capsanthin and caps
Page 201 and 202:
flowing from top to bottom. The out
Page 203 and 204:
Extraction of Lemon oil O 0 u Men t
Page 205 and 206:
Experimental Methods The high-press
Page 207 and 208:
The size of the phase surface area
Page 209 and 210:
Extraction experiments were carried
Page 211 and 212:
1 1 1 1 1 1 1 1 1 1 1 1 1 r— 0,5
Page 213 and 214:
solid material and therefore also b
Page 215 and 216:
these two substances in the extract
Page 217 and 218:
are mentioned in Table 1. The valve
Page 219 and 220:
Figure A.Mentha M A % area trans-sa
Page 221 and 222:
albumin (purity > 98 %, fatty acid
Page 223 and 224:
& Isobutanol & Acetone & EtOH & MEO
Page 225 and 226:
214
Page 227 and 228:
about 278 K. The 99,9 % carbon diox
Page 229 and 230:
At constant temperature the solubil
Page 231 and 232:
220
Page 233 and 234:
222
Page 235 and 236:
224
Page 237 and 238:
In a pressure vessel, the substance
Page 239 and 240:
mixing process. In fig. 6 a thermog
Page 241 and 242:
A complete release of active ingred
Page 243 and 244:
system. The phase transition pressu
Page 245 and 246:
4 Figure 7. SEM photography of micr
Page 247 and 248:
The primary solution was fed with a
Page 249 and 250:
16 0 1 , , , ~ , 1 40 50 60 70 80 9
Page 251 and 252:
Model In order to elucidate the rol
Page 253 and 254:
1200 1000 £ 800 I eoo I
Page 255 and 256:
the particles by Scanning Electron
Page 257 and 258:
where v is the molecular volume of
Page 259 and 260:
dissolution power of the fluid. Thi
Page 261 and 262:
up to 4 pm. The particles are agglo
Page 263 and 264:
process starts and continues for se
Page 265 and 266:
11. York, P.; Hanna, M. Salmeterol
Page 267 and 268:
256
Page 269 and 270:
258
Page 271 and 272:
The non-ideality of the fluid phase
Page 273 and 274:
262
Page 275 and 276:
11.3 vol%. This low raffinate conce
Page 277 and 278:
temperature lowers the ethanol conc
Page 279 and 280:
hydrodynamic behaviour of packed co
Page 281 and 282:
detected at a pressure of 16.4 MPa,
Page 283 and 284:
) Diketones Zinc chloride (21.6 g,
Page 285 and 286:
alcane N° type Feed (mg.) At (1 >
Page 287 and 288:
• Micell Technologies Corp., Rale
Page 289 and 290:
Under higher pressure the polarity
Page 291 and 292:
Fluid compression Two possible flui
Page 293 and 294:
QU Mass flowmeter -A- Manual valve
Page 295 and 296:
•HxH c=>-tX Modifier Compressed a
Page 297 and 298:
operating point FA. A A. A A . A A
Page 299 and 300:
Kohlensäurewerke Deutschland. Labo
Page 301 and 302:
Fig. 3 shows the liquid hold-up and
Page 303 and 304:
292
Page 305 and 306:
Results Patent view of selected bra
Page 307 and 308:
- chemistry with polymers and react
Page 309 and 310:
asket upper section. At that moment
Page 311 and 312:
Influence of the amount of oil to e
Page 313 and 314:
covers a wide range of metal workin
Page 315 and 316:
[1] J. Schön, N. Dahmen, H. Schmie
Page 317 and 318:
Other chemical-physical processes f
Page 319 and 320:
308
Page 321:
Lüdemann, H.-D. 173 Luft, G. 15, 4
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March 3 - 5,1999, Karlsruhe, Germany - FZK

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