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<strong>Design</strong> <strong>of</strong> <strong>High</strong> <strong>Frequency</strong> <strong>Ultrasound</strong> <strong>Transducers</strong> <strong>using</strong><br />

Micromachining<br />

Tung Manh, Anh Tuan. T. Nguyen, Lars H<strong>of</strong>f and Tonni F.Johansen<br />

Abstract— We present a new design <strong>of</strong> high frequency<br />

ultrasound transducers <strong>using</strong> thick-film PZT on Silicon for<br />

medical application. Air is used as backing material for the<br />

PZT film, and the ultrasound pulses are transmitted through<br />

the silicon substrate. The silicon substrate is micromachined to<br />

build acoustic matching layers to optimize the acoustic coupling<br />

between the active PZT layer and the tissue, and achieve a<br />

large bandwidth. The number <strong>of</strong> matching layers in the design<br />

could be either two or three, depending on the fabrication<br />

methods to make the PZT thick-film, i.e. tape casting or screen<br />

printing. A prototype <strong>of</strong> two matching layers for a 10MHz<br />

transducer has been made. 1D analytical calculations and FEM<br />

simulations show that the proposed design will have a 3 dB<br />

bandwidth ranging from 7.5 MHz to 13 MHz, or 55%<br />

bandwidth at center frequency <strong>of</strong> 10 MHz. Acoustic<br />

measurement is ongoing.<br />

I. INTRODUCTION<br />

H IGH frequency ultrasound transducers are wanted in<br />

medical imaging applications where high resolution is<br />

needed [1]-[2]. Most <strong>of</strong> today’s medical ultrasound<br />

transducers are based on an active ceramic layer <strong>of</strong> lead<br />

zirconate titanate (PZT) vibrating in thickness mode. To<br />

achieve frequencies in the range 10 to 100 MHz, the<br />

thickness <strong>of</strong> the active ceramic layer must be between 20<br />

and 200µm. Such a thin layer is difficult to lap down to a<br />

correct thickness, whereas too thick to build up by thin film<br />

techniques. In this paper, we propose <strong>using</strong> thick-film<br />

technology and silicon micromachining as fabrication<br />

technologies to bridge this gap.<br />

Previous work in this field includes Zang et al. [1], who<br />

fabricated a high frequency ultrasound transducer <strong>using</strong> PZT<br />

thick-film on a Silicon (Si) substrate, which can be annealed<br />

to a temperature <strong>of</strong> 750 0 C without reaction between the PZT<br />

film and the Si substrate. This improved the film properties<br />

compared to the previous work by Lukacs et al. [2], who<br />

used Aluminum (Al) substrate. In both <strong>of</strong> these works, the<br />

Manuscript received April 01, 2010. This work is funded by the<br />

Research Council <strong>of</strong> Norway under Grant No. 176540.<br />

Tung Manh, Anh Tuan T. Nguyen and Lars H<strong>of</strong>f are with the Faculty <strong>of</strong><br />

Science and Engineering, Vestfold University College, P.O. Box 2243, N-<br />

3103 Tønsberg, Norway (e-mail: tung.manh@ hive.no).<br />

Tonni Franke Johansen is with the Department <strong>of</strong> Circulation and<br />

Medical Imaging, University <strong>of</strong> Science and Technology, Trondheim,<br />

Norway.<br />

substrates served as temporary layers, and were etched <strong>of</strong>f to<br />

form epoxy backed transducers. This enhanced the<br />

bandwidth <strong>of</strong> the transducers, but reduced the sensitivity.<br />

We present a new design for an ultrasound transducer<br />

where substrate is kept. Using Silicon micromachining<br />

technology, the substrate is machined to form layers with<br />

descending characteristic acoustic impedance from the PZT<br />

film to the load material. These layers function as acoustic<br />

matching between the thick-film and the load. The back side<br />

<strong>of</strong> the thick-film is air, serving as the transducer backing.<br />

This structure increases sensitivity and avoids problems with<br />

reverberations in the backing material.<br />

The paper contains a description <strong>of</strong> the design transducers<br />

with details <strong>of</strong> the fabrication process to form matching<br />

layers. Details <strong>of</strong> fabrication steps to build the entire<br />

transducer can be found elsewhere [3]. The performance <strong>of</strong><br />

the designs is described analytically <strong>using</strong> the Mason stack<br />

model [4]. Finite Element Method (FEM) simulations are<br />

included to improve and verify the analytical 1D calculation.<br />

II. DESCRIPTION OF THE TRANSDUCER<br />

Fig. 1 (a) – (b) Cross sections <strong>of</strong> the transducers with two/ three matching<br />

layers. Top view <strong>of</strong> (c) 1-3 composite and (d) 2-2 composite.<br />

Cross sections <strong>of</strong> our transducer designs are shown in Fig.<br />

1(a-b). The structure includes a PZT plate operating near its<br />

half-wavelength resonance, covered by front and back<br />

electrodes. The front is covered by two or three acoustic<br />

matching layers, each having thickness λ/4; where λ is the<br />

wavelength <strong>of</strong> the longitudinal bulk wave normal to the


layer, at the centre frequency <strong>of</strong> the transducer. For two<br />

matching layers design [Fig. 1(a)], these two layers are: 1) a<br />

layer consisting <strong>of</strong> a composite between Si and a polymer,<br />

and 2) a layer <strong>of</strong> polymer. For three matching layers design<br />

[Fig. 1(b)], the three layers are: 1) a substrate layer <strong>of</strong> Si, 2)<br />

a composite layer between polymer and Silicon and 3) a<br />

polymer layer. Since tape-casting method gives the<br />

properties <strong>of</strong> PZT plate similar to bulk ceramic [5], the three<br />

matching layers approach should be used. In contrast, the<br />

screen printing method with sol-gel mixture provides a film<br />

with acoustic impedance approximately equal to that <strong>of</strong><br />

Silicon, two matching layers must be used.<br />

The composite layer is made as either 1-3 connectivity<br />

[Fig. 1(c)] or 2-2 connectivity type [Fig. 1(d)] <strong>using</strong><br />

micromachining techniques [6]. The 1-3 type is preferred for<br />

high frequencies (>20MHz) due to the fact <strong>of</strong><br />

manufacturing. The two electrodes function as the electric<br />

port to connect the transducer to the electronics. They<br />

should be made sufficiently thin so that their influence on<br />

the acoustic performance <strong>of</strong> the transducer is small.<br />

However, the electrodes must also be adequately thick and<br />

dense to block the diffusion between Si substrate and the<br />

thick-film [7]. An appropriate thickness is less than λ/10,<br />

where λ is the wavelength <strong>of</strong> the longitudinal bulk wave in<br />

the PZT plate.<br />

The transducer is constructed as either a single circular<br />

element or an annular array with ring elements for foc<strong>using</strong>.<br />

Scanning for image formation will be done mechanically by<br />

rotation and/or translation.<br />

III. ANALYTICAL AND FEM SIMULATIONS<br />

A. Analytical simulation<br />

The performance <strong>of</strong> the designs was modelled analytically<br />

<strong>using</strong> the Mason equivalent circuit model. In this model,<br />

PZT ceramic <strong>of</strong> type pz27 is used as the active layer, the<br />

substrate is -oriented Si, the electrodes are <strong>of</strong> Pt and<br />

the polymer is epoxy resin. A water-like medium with<br />

acoustic impedance 1.6 Mrayl is used as load. The material<br />

parameters used in the modelling are listed in TABLE I.<br />

As demonstration, only simulation corresponding to the<br />

design with two matching layer transducer at the centre<br />

frequency <strong>of</strong> 10MHz <strong>using</strong> 2-2 composite type as matching<br />

layer is performed. Fabrication <strong>of</strong> such a layer is given in<br />

IV. The second design can be found in [3].<br />

In the 10MHz transducer design, the thickness <strong>of</strong> the PZT<br />

plate is 177 µm, corresponding to λ/2 at frequency 11MHz,<br />

covered by two Pt electrodes with thickness <strong>of</strong> 3.0 µm and<br />

acoustic impedance <strong>of</strong> 84.7 Mrayls. The first matching layer<br />

is composite <strong>of</strong> Si and epoxy with thickness <strong>of</strong> 152µm and<br />

acoustic impedance <strong>of</strong> 8.9 Mrayls, whereas the last matching<br />

layer is 63µm thick epoxy with acoustic impedance <strong>of</strong><br />

2.85Mrayl [Ep<strong>of</strong>ix (Struers, Solilull, UK)]. This epoxy has<br />

acoustic impedance higher than the optimal value <strong>of</strong><br />

2.3Mrayl but was chosen due to its availability in our lab.<br />

The effective elastic parameters <strong>of</strong> the composite<br />

Si/Epoxy matching layer can be calculated <strong>using</strong> the<br />

theoretical model developed by Smith et al. [8], with some<br />

modifications. The resulting parameters are<br />

2<br />

⎡ p S<br />

2(<br />

c12 −c<br />

) ⎤<br />

S 13<br />

p<br />

c33 = v⎢c11 −( 1− v) ⎥+<br />

( 1−v)<br />

c11<br />

(a)<br />

S S p p<br />

⎢ ( 1−<br />

v)( c11 + c12 ) + v( c11+ c12)<br />

⎥<br />

⎣ ⎦<br />

p S<br />

2<br />

⎡ ( c12 −c13<br />

) ⎤<br />

S p<br />

c33 = v⎢c11−( 1− v) ⎥+<br />

( 1−v<br />

S p ) c11<br />

(b)<br />

⎢ ( 1−<br />

vc ) 11 + vc⎥<br />

11<br />

⎣ ⎦<br />

S p<br />

ρ = vρ + ( 1−v)<br />

ρ<br />

Z = c ρ<br />

c33<br />

V =<br />

ρ<br />

where the overbars ( x ) refer to effective parameters <strong>of</strong> the<br />

composite, superscript p refer to parameters <strong>of</strong> the polymer,<br />

and superscript S to parameters <strong>of</strong> the silicon substrate.<br />

cij are the elastic coefficients, ρ is the density, v is the<br />

volume fraction <strong>of</strong> Si in the composite; Z , V are the<br />

effective acoustic impedance and longitudinal wave speed in<br />

the thickness direction <strong>of</strong> the composite, respectively. (a) is<br />

the equation used for 1-3 composite whereas (b) is for 2-2<br />

type. The others are for both.<br />

The electro-acoustic transfer function, i.e. the transfer<br />

function from the voltage over the electrodes to the pressure<br />

at the transducer surface, is calculated for a 10MHz design<br />

and plotted in Fig. 2. The upper graph shows the frequency<br />

response, while the lower shows the impulse response, in the<br />

time domain. These results give an effective 3-dB bandwidth<br />

from 7.5 MHz to 13 MHz with centre frequency 10 MHz,<br />

i.e. 55% relative bandwidth.<br />

B. FEM simulation<br />

Analytical model, based on the Mason equivalent circuit,<br />

is well established in transducer modelling for describing<br />

thickness mode vibrations. However, it is limited by being a<br />

1D model. Hence, the composite layer must be described as<br />

one material with a set <strong>of</strong> calculated effective parameters,<br />

the anisotropic nature <strong>of</strong> Si is not handled, and lateral modes<br />

as well as effects <strong>of</strong> a finite width are not included.<br />

Fig. 2 Electro-acoustic transfer function and output waveform <strong>of</strong> 10MHz<br />

transducer<br />

33


Fig. 3 Electrical impedance <strong>of</strong> a 10MHz transducer<br />

To obtain more realistic simulations, and to get an<br />

estimate <strong>of</strong> the performance and limitations <strong>of</strong> the 1D<br />

analytical model, FEM models were created <strong>using</strong><br />

COMSOL Multiphysics s<strong>of</strong>tware version 3.4 (Comsol AB,<br />

Stockholm, Sweden). In FEM model, the anisotropic nature<br />

<strong>of</strong> Si is included, and the composite is made between Si and<br />

Epoxy posts. One half <strong>of</strong> a composite unit cell was modeled<br />

for 2-2 composite, whereas a quarter <strong>of</strong> cell was modeled for<br />

1-3 type. Symmetry boundary conditions were applied, as<br />

described in [9]. The sizes <strong>of</strong> the Si and polymer bars in the<br />

composite layer <strong>of</strong> the 10MHz transducer were designed to<br />

be 9µm and 23µm, respectively, to avoid interference from<br />

the lateral resonances into the thickness mode [10]. There is<br />

a good agreement between FEM simulation and analytical<br />

calculation (Fig.3). For 3 matching layer design, similar<br />

result is also achieved.<br />

IV. FABRICATION OF THE MATCHING LAYERS<br />

The novel and most important part in the transducer is the<br />

micromachined matching layer. This layer has been<br />

fabricated by <strong>using</strong> anisotropic wet etching method to form<br />

deep vertical trenches (2-2 type) into Silicon wafers,<br />

followed by vacuum impregnated these grooves by epoxy<br />

resin.<br />

The process starts with a 550 µm thick oriented Si<br />

wafer. A 1µm thin SiO2 was grown on the surfaces <strong>of</strong> the<br />

wafer. The main flat <strong>of</strong> the wafer is supposed to be<br />

parallel to the planes. However, the accuracy <strong>of</strong> this<br />

flat is approximately 1 0 , which is not efficient to have good<br />

alignment for our purposes. A two steps etching process<br />

therefore has been made. First, a mask with fan structures <strong>of</strong><br />

0.1 0 increasing step was transfer to the SiO2 layer by<br />

lithography. A 1.5 hours etch in KOH 25% at 80 0 C was then<br />

performed. All lines which are imprecisely aligned along<br />

planes were undercut and destroyed due to the nature<br />

<strong>of</strong> anisotropic wet etching. Remain lines were used to be the<br />

alignment marks for the next lithography. Fig. 4(a) shows<br />

the fan structure patterns on the plastic mask whereas the<br />

etched structures on Silicon after the first wet etching step<br />

are showed in Fig. 4(b). Due to anisotropic etching <strong>of</strong> the<br />

Silicon crystal, the circle on the mask turned to be hexagonal<br />

shape and only lines which are precisely aligned along<br />

planes have been survived completely.<br />

The grating pattern, i.e. 2-2 composite, was then<br />

transferred to the protected SiO2 layer, followed by<br />

anisotropic wet etching <strong>of</strong> the wafer for 1.5 hours to form<br />

deep trenches. A closed look <strong>of</strong> the etched structure before<br />

polymer filled is shown in Fig. 5. Obviously, straight walls<br />

have been achieved but there are steeps at the bottom <strong>of</strong> the<br />

trenches due to anisotropic behaviour <strong>of</strong> Silicon crystal.<br />

Then, the wafer was vacuum impregnated by polymer. It<br />

was done by placing the wafer into a vacuum chamber and<br />

pouring epoxy resin onto wafer’s surface. By applying a<br />

vacuum, small air bubbles in polymer were removed. The<br />

polymer was cured at room temperature for 24 hours. The<br />

sample after vacuum impregnated and cured is shown in Fig.<br />

6, where bright is Si and grey is polymer. It is clearly shown<br />

that air bubbles are removed in polymer.<br />

The sample was then lapped down to the desired<br />

thickness <strong>using</strong> a precise lapping machine (MultiPrep TM<br />

System, Allied <strong>High</strong> Tech Products Inc, USA). A PZT active<br />

layer was then glued on the sample for characterization.<br />

Characterization <strong>of</strong> these matching layers is ongoing.<br />

Fig. 4 (a) Fan structures on the glass mask (b) Patterns on Silicon wafer<br />

after the first step in Silicon wet etching process<br />

Fig. 5 Closed look <strong>of</strong> the etched structure before filled in with polymer


Fig. 6 Sample after polymer filled, bright is Silicon and grey is Polymer<br />

V. CONCLUSION<br />

The novel design <strong>of</strong> ultrasound transducers based on<br />

micromachining has been presented. A test prototype <strong>of</strong> the<br />

composite layers <strong>using</strong> wet etching has been made.<br />

Theoretical and FEM simulation show that transducers <strong>using</strong><br />

this structure to be matching layers provide 55% relative<br />

bandwidth. This is a little smaller than the optimal<br />

bandwidth that can be achieved with two matching layers<br />

but it is still reasonable. This is because we didn’t use epoxy<br />

with optimal acoustic impedance. Acoustic measurement <strong>of</strong><br />

this structure is ongoing.<br />

Active<br />

layer<br />

Passive<br />

layers<br />

Pz27<br />

[110]oriented<br />

Silicon<br />

Platinum<br />

Epoxy<br />

TABLE I<br />

MATERIAL PROPERTIES USED FOR SIMULATIONS<br />

REFERENCES<br />

[1] Q.Q. Zhang, F.T. Djuth, Q.F. Zou, C,H. Hu, J.H. Cha, K.K. Shung,<br />

“<strong>High</strong> frequency broadband PZT thick film ultrasonic transducers for<br />

medical imaging applications”.Ultrasonics, vol.44, p711-715, 2006.<br />

[2] M. Lukacs, M. Sayer, F.S. Foster, ”Single element high frequency<br />

(

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