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1318 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 18, NO. 6, DECEMBER 2009<br />

Room-Temperature Sealing <strong>of</strong> Microcavities<br />

by Cold Metal Welding<br />

Adit Decharat, Junchun Yu, Marc Boers, Göran Stemme, Fellow, IEEE, and Frank Niklaus, Member, IEEE<br />

Abstract—In this paper, we present a wafer-to-wafer attachment<br />

and sealing method for wafer-level manufacturing <strong>of</strong> microcavities<br />

using a room-temperature bonding process. The proposed<br />

attachment and sealing method is based on plastic deformation<br />

and cold welding <strong>of</strong> overlapping metal rings to create metal-tometal<br />

bonding and sealing. We present the results from experiments<br />

using various bonding process parameters and metal sealing<br />

ring designs including their impact on the resulting bond quality.<br />

The sealing properties against liquids and vapor <strong>of</strong> different sealing<br />

ring structures have been evaluated for glass wafers that are<br />

bonded to silicon wafers. In addition, wafer-level vacuum sealing<br />

<strong>of</strong> microcavities was demonstrated when bonding a silicon wafer to<br />

another silicon wafer with the proposed room-temperature sealing<br />

and bonding technique. [2008-0053]<br />

Index Terms—Bonding, fabrication, microelectromechanical<br />

devices, <strong>packaging</strong>.<br />

I. INTRODUCTION<br />

PACKAGING, assembly, and sealing are important parts in<br />

manufacturing <strong>of</strong> microelectromechanical systems [1]–[3]<br />

and micr<strong>of</strong>luidic systems [4] and can be responsible for between<br />

25% and 80% <strong>of</strong> the total cost [5]. One way <strong>of</strong> manufacturing<br />

microcavities is the use <strong>of</strong> low-temperature wafer-level<br />

attachment and bonding techniques. Commonly used waferlevel<br />

bonding techniques for manufacturing <strong>of</strong> microcavities are<br />

glass-frit bonding [6]–[8], anodic bonding [9], solder bonding<br />

[10], eutectic bonding [11], thermocompression bonding [12],<br />

and adhesive bonding [13], [14]. The aforementioned bonding<br />

techniques typically require elevated temperatures <strong>of</strong> 100 ◦Cto 450 ◦C. In solder and eutectic bonding, the oxides at the metal<br />

surfaces need to be removed using, e.g., flux or other methods<br />

and eutectic and thermocompression bonding require very flat<br />

surfaces to achieve consistent bonding results over large areas.<br />

Polymer adhesives are typically not suitable for manufacturing<br />

<strong>of</strong> hermetically sealed cavities, since polymers are permeable<br />

to gasses [13]. Bonding with localized heating has been used<br />

to reduce thermally induced stresses in the bonded packages<br />

Manuscript received March 3, 2008; revised June 8, 2009. First published<br />

October 16, 2009; current version published December 1, 2009. This work was<br />

supported in part by the Swedish Intelligent Vehicle Safety Systems program<br />

and in part by Autoliv Development AB. Subject Editor L. Spangler.<br />

A. Decharat, G. Stemme, and F. Niklaus are with the Microsystem<br />

Technology Laboratory, <strong>School</strong> <strong>of</strong> <strong>Electrical</strong> <strong>Engineering</strong>, Royal Institute<br />

<strong>of</strong> Technology, 10044 Stockholm, Sweden (e-mail: adit.decharat@ee.kth.se;<br />

frank.niklaus@ee.kth.se; stemme@ee.kth.se).<br />

J. Yu is with the Physics Department, Umea University, SE-901 87 Umea,<br />

Sweden (e-mail: yujunchun@hotmail.com).<br />

M. Boers is with Phonak Acoustic Implants SA, CH-1027 Lonay,<br />

Switzerland (e-mail: marc.boers@gmail.com).<br />

Color versions <strong>of</strong> one or more <strong>of</strong> the figures in this paper are available online<br />

at http://ieeexplore.ieee.org.<br />

Digital Object Identifier 10.1109/JMEMS.2009.2030956<br />

1057-7157/$26.00 © 2009 IEEE<br />

[3], [16]–[20]. For many applications, the use <strong>of</strong> elevated<br />

temperatures is not desirable in the assembly, <strong>packaging</strong>, and<br />

sealing process. Temperature sensitive materials or components<br />

that degrade or are destroyed at elevated temperature may be<br />

present in the cavities or at the wafer surfaces. Gas molecules<br />

that are absorbed in the surfaces <strong>of</strong> the substrates can outgas<br />

and contaminate the atmosphere inside the microcavities if<br />

the wafers are heated during the bonding process [21]. In<br />

addition, temperature-induced stresses can be created during<br />

the wafer bonding process if two wafers are bonded that consist<br />

<strong>of</strong> materials with different coefficients <strong>of</strong> thermal expansion.<br />

Methods that have been reported for room-temperature mechanical<br />

attachment <strong>of</strong> substrates are the micro Velcro method<br />

[22], [23], the microbrush method [24], and cold welding <strong>of</strong><br />

metals [25]–[27]. The micro Velcro method provides substrateto-substrate<br />

attachment using mechanical interlocking and the<br />

microbrush method uses plastic deformation <strong>of</strong> metal-coated<br />

polymer studs to establish electrical contacts between the two<br />

substrates in addition to the substrate-to-substrate attachment<br />

feature. In cold welding, a metallic bond is formed at room<br />

temperature between two metal surfaces by the application <strong>of</strong><br />

pressure. Neither <strong>of</strong> the aforementioned methods has been used<br />

for manufacturing and sealing <strong>of</strong> microcavities. In this paper,<br />

we present a wafer-to-wafer attachment and sealing method<br />

for manufacturing <strong>of</strong> microcavities at room temperature. In the<br />

proposed method, corresponding metal sealing rings are located<br />

on the two wafer surfaces to be bonded. The two wafer surfaces<br />

with the corresponding and slightly overlapping sealing rings<br />

are aligned and pressed to each other. The resulting bonding<br />

pressure causes high shear and compressive strains and thus,<br />

plastic deformation and fusing at the overlapping areas <strong>of</strong><br />

the corresponding metal rings and ultimately sealing <strong>of</strong> the<br />

cavities. The proposed attachment and sealing process can be<br />

performed at room temperature and is, in principle, insensitive<br />

to rough surfaces at the bond rings because material fusion<br />

during bonding takes place at the side walls <strong>of</strong> the counterfitting<br />

style sealing rings. We present experimental results from roomtemperature<br />

bonding <strong>of</strong> glass wafers to silicon wafers and from<br />

room-temperature bonding <strong>of</strong> silicon wafers to silicon wafers<br />

containing corresponding gold metal sealing rings with varying<br />

overlapping areas, dimensions, and geometries.<br />

II. METAL-TO-METAL COLD WELDING FOR<br />

ROOM-TEMPERATURE SEALING OF MICROCAVITIES<br />

Fig. 1 shows a schematic cross-sectional view <strong>of</strong> a wafer<br />

pair containing corresponding metal sealing rings that define<br />

the cavities. Fig. 1(a) shows the wafer pair before and Fig. 1(b)<br />

Authorized licensed use limited to: KTH THE ROYAL INSTITUTE OF TECHNOLOGY. Downloaded on February 4, 2010 at 08:43 from IEEE Xplore. Restrictions apply.


DECHARAT et al.: ROOM-TEMPERATURE SEALING OF MICROCAVITIES BY COLD METAL WELDING 1319<br />

Fig. 1. Schematic cross-sectional view <strong>of</strong> the wafers with corresponding metal sealing rings (a) before and (b) after bonding.<br />

Fig. 2. (a) Top view <strong>of</strong> three types <strong>of</strong> microcavities with metal sealing rings on wafer 1 and corresponding metal sealing rings on the wafer 2. (b) Threedimensional<br />

view <strong>of</strong> the overlaying sealing rings <strong>of</strong> an aligned and bonded wafer pair.<br />

after the wafer pair is aligned and brought into contact. Fig. 2(a)<br />

shows a schematic top view <strong>of</strong> a first wafer with three different<br />

cavity structures containing 2, 3, and 5 metal sealing rings<br />

per cavity and the corresponding rings on the second wafer<br />

with 1, 2, and 4 metal sealing rings. When the wafers are<br />

properly aligned to each other, the corresponding metal sealing<br />

rings have small overlapping areas. The wafer pair is pressed<br />

together by applying a uniform force. As a result, the corresponding<br />

metal sealing rings wedge into each other, as shown<br />

in Figs. 1(b) and 2(b). This is due to the creation <strong>of</strong> large local<br />

shear and compressive strains at the overlapping edges <strong>of</strong> the<br />

metal sealing rings, resulting in localized plastic deformation<br />

and cold welding.<br />

The resulting bonded area that seals the cavities and holds<br />

the wafers together consists <strong>of</strong> the wedged overlapping areas <strong>of</strong><br />

the corresponding metal sealing rings. This area is very small<br />

in relation to the total wafer area and the forces to which the<br />

bond can be exposed by, e.g., wafer handling and dicing. To<br />

Fig. 3. Introduction <strong>of</strong> an underfill material in the gap in between the bonded<br />

wafer pair to reinforce the bond strength <strong>of</strong> the sealed bonds.<br />

reinforce the wafer bond, an underfill material (e.g., an underfill<br />

epoxy) can be introduced in the gap between the bonded wafer<br />

pair after the wafers are joined and the cavities are sealed, as<br />

shown in Fig. 3. The underfill material fills the gap between the<br />

wafers by capillary forces. Depending on the selected material,<br />

the hardening <strong>of</strong> the underfill material can be achieved at room<br />

temperature or at an increased curing temperature. The final<br />

Authorized licensed use limited to: KTH THE ROYAL INSTITUTE OF TECHNOLOGY. Downloaded on February 4, 2010 at 08:43 from IEEE Xplore. Restrictions apply.


1320 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 18, NO. 6, DECEMBER 2009<br />

Fig. 4. (a) Cross-sectional pr<strong>of</strong>ile <strong>of</strong> the electroplated gold sealing rings with nominal dimensions (not to scale). (b) Cross-sectional SEM image <strong>of</strong> an<br />

electroplated gold sealing ring.<br />

bond strength is predominantly determined by the used underfill<br />

material.<br />

III. EXPERIMENTS<br />

A. Manufacturing <strong>of</strong> Sealing Rings<br />

In the experiments, electroplated gold was selected as metal<br />

for the sealing rings that define the microcavities because gold<br />

is a relative s<strong>of</strong>t and deformable material. The metal sealing<br />

rings are manufactured by sputtering a thin gold seed layer on<br />

the wafers. Next, a thick photoresist layer (> 30 μm) is coated<br />

and patterned, and thereby defines the areas for the sealing<br />

rings. Gold is electroplated at the areas where the photoresist is<br />

patterned (removed), and thus, the photoresist is functioning as<br />

a mold for the electroplated gold. Subsequently, the photoresist<br />

mold and the gold seed layer are removed with wet-etching<br />

processes, and the wafers are rinsed with deionized water and<br />

dried. Gold sealing rings with a height <strong>of</strong> 30 μm and a width<br />

<strong>of</strong> 50 μm have been used to define the microcavities. Fig. 4(a)<br />

shows a schematic cross section <strong>of</strong> an electroplated gold sealing<br />

ring pr<strong>of</strong>ile including the nominal dimensions, and Fig. 4(b)<br />

shows a scanning electron microscope (SEM) image <strong>of</strong> the<br />

cross section <strong>of</strong> an electroplated gold sealing ring. The convex<br />

side walls <strong>of</strong> the gold sealing ring origins from the patterning<br />

process <strong>of</strong> the positive photoresist mold. In principle, sealing<br />

rings with 90◦ angles or with concave side walls may also be<br />

suitable. The sealing rings for the microcavities are manufactured<br />

on 100-mm-diameter silicon and glass wafers. Each wafer<br />

pair contains 54 microcavities with different cavity shapes<br />

(rounded corners and squared corners), different cavity sizes<br />

(1000 μm × 3500 μm, 3500 μm × 3500 μm, and 8000 μm ×<br />

8000 μm), different numbers <strong>of</strong> sealing rings (2, 3, and 5 with<br />

matching 1, 2, and 4 sealing rings), and different overlapping<br />

lengths <strong>of</strong> the sealing rings (2, 3, 4, and 6 μm). The different<br />

cavity shapes and sizes are shown in Fig. 5. The overlapping<br />

lengths <strong>of</strong> the sealing rings, as shown in Fig. 1(b), are defined<br />

as the overlap (e.g., 2, 3, 4, or 6 μm) on each side <strong>of</strong> the upper<br />

outline <strong>of</strong> the sealing ring on one wafer with the upper outline<br />

<strong>of</strong> the corresponding sealing rings on the second wafer. The<br />

smallest overlapping length <strong>of</strong> 2 μm represents the best possible<br />

wafer-to-wafer alignment accuracy <strong>of</strong> the available alignment<br />

equipment. The total overlapping area <strong>of</strong> the gold sealing ring<br />

design used in the experiments are 12.78 · 10−6 m2 per wafer.<br />

Fig. 5. Evaluated cavity shapes and sizes with denotations. Measures are<br />

given in micrometers.<br />

The yield strength <strong>of</strong> gold has been reported to be on the order<br />

<strong>of</strong> 200 MPa [28]. The total required wafer bonding force to get<br />

plastic deformation in the overlapping gold sealing ring areas<br />

can be roughly estimated with F = σ · A, where σ is the stress<br />

and A is the total overlapping area <strong>of</strong> the corresponding sealing<br />

rings <strong>of</strong> the wafer pair.<br />

B. Wafer-Level Sealing <strong>of</strong> Cavities When Bonding Silicon<br />

Wafers to Glass Wafers<br />

A total <strong>of</strong> six silicon-glass wafer pairs have been bonded<br />

with the proposed room-temperature sealing and attachment<br />

method. The glass wafers are used in the experiments to be<br />

able to inspect and evaluate the sealing rings and the cavities<br />

after the wafer pairs are bonded. In four <strong>of</strong> the experiments, a<br />

500-μm-thick glass wafer was bonded to a 300-μm-thick<br />

double-sided polished silicon wafer. In two <strong>of</strong> the experiments,<br />

a 500-μm-thick glass wafer was bonded to a 500-μm-thick<br />

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DECHARAT et al.: ROOM-TEMPERATURE SEALING OF MICROCAVITIES BY COLD METAL WELDING 1321<br />

Fig. 6. View through the top glass wafer at the bond interface <strong>of</strong> a cavity.<br />

Three sealing rings with rounded corners on the silicon wafer and the corresponding<br />

two sealing rings on the glass wafer are shown. The inside <strong>of</strong> the<br />

cavity contains color traces from IPA vapor that has penetrated the cavity during<br />

a gross-leak test.<br />

double-sided polished silicon wafer. The room-temperature<br />

wafer-to-wafer attachment (bonding) and cavity sealing is done<br />

in a standard commercial wafer bonder. Two wafers with corresponding<br />

sealing rings are aligned using commercial wafer-towafer<br />

alignment equipment. The alignment keys on the wafers<br />

can be observed through the transparent glass wafer. After<br />

alignment, the wafer pair is fixed on a standard bond fixture <strong>of</strong><br />

the wafer bonder with the spacers <strong>of</strong> the bond fixture separating<br />

the two wafers. The aligned wafers on the bond fixture are<br />

transferred to the bond chamber and the chamber is evacuated<br />

to a pressure <strong>of</strong> 10 −4 mbar. The wafers remain in the vacuum<br />

atmosphere for 1 h to remove excess moisture and gasses<br />

from the wafer surfaces before the wafers are joined inside the<br />

vacuum atmosphere by removing the spacers in between them.<br />

Next, a bond force <strong>of</strong> 2.5 kN is applied for 10 min to the wafer<br />

stack with the bond tool. Thereafter, the bond force is removed,<br />

the bond chamber is vented, and the bonded wafer pair is taken<br />

out <strong>of</strong> the bond chamber. All bonding steps are performed at<br />

room temperature.<br />

After the wafer-to-wafer attachment process, the sealing<br />

rings are inspected with an optical microscope through the glass<br />

wafers. For all bonded wafer pairs and cavity types, the integrity<br />

<strong>of</strong> the gold sealing rings remained intact. Even if the wafers<br />

were slightly misaligned (on the order <strong>of</strong> 2 to 3 μm) prior to<br />

the wafer-to-wafer attachment, the gold sealing rings wedge<br />

into each other. Fig. 6 shows an image, taken through the top<br />

glass wafer <strong>of</strong> a bonded wafer pair, on which two gold sealing<br />

rings that are wedged into three corresponding sealing rings can<br />

be seen. Fig. 7 shows an image, taken through the top glass<br />

wafer <strong>of</strong> a bonded wafer pair, in which gold sealing rings that<br />

have squared corners can be seen. At the squared corners <strong>of</strong> the<br />

cavities, small fractures are visible in the surface <strong>of</strong> the glass<br />

wafer underneath the gold sealing rings.<br />

Fig. 8 shows a cross-sectional SEM image <strong>of</strong> a diced sample<br />

<strong>of</strong> a bonded wafer pair. The image depicts the end <strong>of</strong> sealing<br />

ring evaluation structures consisting <strong>of</strong> three gold sealing rings<br />

on the lower silicon wafer (wafer 2) and two gold sealing rings<br />

on the upper glass wafer (wafer 1). The sealing ring structures<br />

consist <strong>of</strong> straight lines and do not form an enclosed cavity. The<br />

cut for the cross section is done a few micrometers apart from<br />

the end <strong>of</strong> the sealing ring structures in order not to affect or<br />

damage the structures during dicing. As expected, the sealing<br />

ring structures are plastically deformed and wedged into each<br />

other.<br />

Fig. 7. View through the top glass wafer at the bond interface <strong>of</strong> a cavity. Two<br />

sealing rings with squared corners on the silicon wafer and the corresponding<br />

two sealing rings on the glass wafer are shown. Fractures in the glass wafer<br />

surface at the cavity corner are indicated.<br />

All microcavities <strong>of</strong> two <strong>of</strong> the bonded silicon-glass wafer<br />

pairs were evaluated with a gross-leak test to investigate the<br />

cavity sealing. In the gross leak tests, isopropanol alcohol<br />

(IPA) is injected in the 30- to 40-μm-wide gap that exists<br />

between the bonded wafers. The gap fills with the liquid IPA by<br />

capillary forces. Liquid and vapor IPA can enter the cavities that<br />

contain gross leaks. Liquid and vapor leakage into the cavities<br />

is visually detected through the glass wafer. When performing<br />

the gross leak tests, a number <strong>of</strong> cavities were immediately<br />

filled with liquid IPA, indicating gross leaks in these cavities.<br />

Most cavities on the silicon-glass wafer pairs were penetrated<br />

by IPA vapor, which then condenses inside the cavities, as<br />

shown in Fig. 6. For a total <strong>of</strong> six <strong>of</strong> the cavities, no penetration<br />

with IPA vapor was observed, indicating good sealing <strong>of</strong> these<br />

cavities. Table I shows the cavity designs that have been sealed<br />

without detectable gross leaks. Of the sealed cavities, one is<br />

8000 μm × 8000 μm (type A), four are 3500 μm × 3500 μm<br />

(type B, E, and F), and one is 1000 μm × 3500 μm (type D),<br />

and all cavities have rounded corners. As can be seen in Table I,<br />

five <strong>of</strong> the sealed cavities have three sealing rings on one wafer<br />

and two corresponding sealing rings on the second wafer, and<br />

one <strong>of</strong> the sealed cavities has five sealing rings on one wafer and<br />

four corresponding sealing rings on the second wafer. Four <strong>of</strong><br />

the sealed cavities have sealing rings with overlapping lengths<br />

<strong>of</strong> 2 μm and two with overlapping lengths <strong>of</strong> 4 μm.<br />

In addition to the aforementioned described experiments, one<br />

bonded wafer pair was separated using force. The force needed<br />

to separate the wafers is comparably small. This is because<br />

the regions that hold the bonded wafers together are limited to<br />

the comparably small sealing ring areas. When inspecting the<br />

fractured bond interface at the sealing rings, it was observed<br />

that on most parts <strong>of</strong> the wafer, the gold sealing rings are broken<br />

away from the glass wafer and still remain bonded to the gold<br />

rings on the silicon wafer. Fig. 9 shows a top view <strong>of</strong> a bonded<br />

gold ring after the top glass wafer has been removed by force.<br />

A piece <strong>of</strong> glass that was broken out <strong>of</strong> the glass wafer remains<br />

bonded to the gold sealing ring that was originally positioned<br />

on the glass wafer. This indicates very good bonding and cold<br />

welding <strong>of</strong> the corresponding overlapping gold sealing rings<br />

due to plastic deformation <strong>of</strong> these areas.<br />

C. Wafer-Level Sealing <strong>of</strong> Cavities When Bonding Silicon<br />

Wafers to SOI Wafers<br />

A total <strong>of</strong> two silicon-SOI wafer pairs have been bonded<br />

with the proposed room-temperature sealing and attachment<br />

Authorized licensed use limited to: KTH THE ROYAL INSTITUTE OF TECHNOLOGY. Downloaded on February 4, 2010 at 08:43 from IEEE Xplore. Restrictions apply.


1322 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 18, NO. 6, DECEMBER 2009<br />

Fig. 8. Cross-sectional SEM images with (a) counterfitting sealing ring structures that are wedged into each other and (b) close-up view <strong>of</strong> the interface <strong>of</strong> two<br />

counterfitting sealing ring structures.<br />

TABLE I<br />

SEALING RESULTS FROM THE GROSS LEAK EXPERIMENTS FOR CAVITIES WITH DIFFERENT SHAPES,<br />

SIZES, OVERLAP LENGTHS OF SEALING RINGS, AND NUMBER OF SEALING RINGS<br />

method. In both experiments, a 525-μm-thick SOI wafers was<br />

bonded to a 500-μm-thick double-sided polished silicon wafer.<br />

The silicon device layer <strong>of</strong> the SOI wafers is 20 μm thick,<br />

and the SiO2 layer is 1 μm thick. To be able to align the<br />

corresponding gold sealing rings on the nontransparent silicon<br />

and SOI wafers, a standard wafer-to-wafer alignment procedure<br />

is used that features wafer backside alignment keys together<br />

with digitized images. This is done using commercial waferto-wafer<br />

alignment equipment. After the wafer alignment, the<br />

wafer pair is fixed on the bond fixture <strong>of</strong> the wafer alignment<br />

equipment with the spacers from the bond fixture separating<br />

the two wafers. The aligned wafer pair on the bond fixture<br />

is transferred from the aligner to the bond chamber, and the<br />

chamber is evacuated to a pressure <strong>of</strong> 10 −4 mbar. The wafers<br />

remain in the vacuum atmosphere for 3 h to remove excess<br />

moisture and gasses from the wafer surfaces before the wafers<br />

are joined inside the vacuum atmosphere by removing the<br />

spacers. Next, the wafer stack is pressed together with the bond<br />

tool. Thereafter, the bond force is removed, the bond chamber is<br />

vented, and the bonded wafer pair is carefully taken out <strong>of</strong> the<br />

bond chamber. One wafer pair was pressed with a bond force<br />

<strong>of</strong> 2.5 kN for 10 min, and the second wafer pair was pressed<br />

with a bond force <strong>of</strong> 2.8 kN for 10 min. For both bonded wafer<br />

pairs, a low-viscosity two-component epoxy is introduced in<br />

between the gap <strong>of</strong> the wafers, as shown in Fig. 3. The twocomponent<br />

underfill epoxy cures at room temperature and reinforces<br />

the bond between the wafers at the corresponding sealing<br />

rings.<br />

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DECHARAT et al.: ROOM-TEMPERATURE SEALING OF MICROCAVITIES BY COLD METAL WELDING 1323<br />

Fig. 9. Top view <strong>of</strong> a sealing ring section on the silicon wafer after bonding<br />

and subsequent forceful separation <strong>of</strong> the wafer pair. The gold ring from the<br />

glass wafer is remaining in between the gold rings on the silicon wafer. A glass<br />

piece that has been broken out <strong>of</strong> the glass wafer remains on the gold sealing<br />

ring from the glass wafer.<br />

Fig. 10. (a) Bulk silicon <strong>of</strong> the SOI wafer is thinned down with DRIE.<br />

(b) Differential pressures between the inside and the outside atmospheres <strong>of</strong><br />

the microcavity cause the thin silicon lid membranes to deflect.<br />

To estimate the pressure level <strong>of</strong> the encapsulated atmosphere<br />

inside the microcavities and to detect possible gross leaks, the<br />

bulk silicon <strong>of</strong> the SOI wafer is removed by deep reactive ion<br />

etching (DRIE) and using the SiO2 layers <strong>of</strong> the SOI wafers<br />

as the etch stop, as shown in Fig. 10(a) and (b). Thus, only<br />

the 20-μm-thick silicon device layer together with the 1-μmthick<br />

SiO2 layer remains as lid on the sealed cavities. If a<br />

pressure difference exists between the atmospheres inside and<br />

outside a cavity, the thin silicon membrane deflects, as shown<br />

in Fig. 10(b).<br />

After thinning the bulk silicon <strong>of</strong> the SOI wafer with DRIE<br />

from the wafer pair that was bonded with a bond force <strong>of</strong><br />

2.5 kN, about 50% <strong>of</strong> the membranes <strong>of</strong> the microcavities<br />

deflect strongly to the inside <strong>of</strong> the cavities. This indicates a<br />

significantly lower pressure inside these cavities as compared<br />

to the outside pressure. For all other cavities on this wafer, the<br />

20-μm-thin lid membranes were approximately leveled with a<br />

slight predeflection on the order <strong>of</strong> a few micrometers, most<br />

likely a result from the strain in the remaining SiO2 layer.<br />

Fig. 11 shows images <strong>of</strong> microcavities <strong>of</strong> types A, D, and E for<br />

which the membranes deflected to the inside <strong>of</strong> the cavities. It is<br />

shown in Fig. 11(a) that for the largest microcavity with a size<br />

<strong>of</strong> 8000 μm × 8000 μm (type A), the silicon membrane is deflected<br />

to an extent that it touches the bottom <strong>of</strong> the cavity. The<br />

Fig. 11. Images <strong>of</strong> sealed microcavities at atmospheric pressure with the lid<br />

membranes bending to the inside <strong>of</strong> the cavities. All successfully sealed cavities<br />

have rounded corners. The cavities are (a) type A (8000 μm × 8000 μm),<br />

(b) type D (1000 μm × 3500 μm), and (c) type E (3500 μm × 3500 μm).<br />

effective cavity height <strong>of</strong> this cavity has been measured with a<br />

pr<strong>of</strong>ilometer to be about 53 μm. This suggests that the wedging<br />

depth <strong>of</strong> the corresponding gold sealing rings for this cavity is<br />

on the order <strong>of</strong> 7 μm. None <strong>of</strong> the microcavity lid membranes <strong>of</strong><br />

the wafer pair bonded with a bond force <strong>of</strong> 2.8 kN are deflected<br />

after the bulk silicon <strong>of</strong> the SOI wafer was removed with DRIE.<br />

This indicates that none <strong>of</strong> the microcavities <strong>of</strong> this wafer are<br />

sealed.<br />

For an indicative estimate <strong>of</strong> the gas pressure inside the<br />

sealed cavities, they are placed in a vacuum chamber with a<br />

glass window. When decreasing the gas pressure in the vacuum<br />

chamber, the deflection <strong>of</strong> the cavity membranes decreases until<br />

the membranes level and then protrude to the outside <strong>of</strong> the<br />

cavities. Leveling <strong>of</strong> a cavity membrane happens when the<br />

pressure inside the cavity is on the same order as the pressure<br />

in the vacuum chamber. Leveling <strong>of</strong> the cavity membranes is<br />

detected by visual observation through the glass window <strong>of</strong><br />

the vacuum chamber. When lowering the gas pressure in the<br />

vacuum chamber, leveling <strong>of</strong> the cavity membranes happened<br />

for most sealed cavities at pressure levels on the order <strong>of</strong> 5 to<br />

10 mbar. For the microcavities with the lowest estimated gas<br />

pressures (type A), the membranes level at gas pressures below<br />

5 mbar. The pressure measurements have been repeated one<br />

month, three months, and six months after the sealing <strong>of</strong> the<br />

cavities. No detectable change in the vacuum pressures at which<br />

the cavity membranes level have been observed. However, it<br />

must be pointed out that the effective pressure differences<br />

between the inside and the outside <strong>of</strong> the microcavities are very<br />

small at the leveling point <strong>of</strong> the membranes. Thus, the visual<br />

detection <strong>of</strong> the cavity membrane deflection is not sufficiently<br />

accurate for reliable comparative measurements and provides<br />

only indicative estimates for the levels <strong>of</strong> the gas pressure<br />

inside the microcavities. A basic model for the deflection <strong>of</strong><br />

the cavity membrane has been used to verify the estimated<br />

pressure range inside the cavities. Cavity membranes are deflected<br />

by the difference in pressure ΔP between the outside<br />

<strong>of</strong> the cavities (atmospheric pressure Patm) and the inside <strong>of</strong><br />

the cavities (cavity pressure Pvac). Thus, the cavity pressure<br />

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1324 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 18, NO. 6, DECEMBER 2009<br />

relative to ambient atmospheric pressure can be estimated from<br />

Pvac = Patm − ΔP , where Patm = 1013 mbar. To estimate<br />

large load deflections <strong>of</strong> flat circular diaphragms (y0 < h/2),<br />

the analytical expression<br />

ΔPa4 =<br />

Eh4 16<br />

3(1 − μ2 yo 7 − μ<br />

+<br />

) h 3(1 − μ)<br />

can be used [29], where h is the membrane thickness, E is the<br />

Young’s modulus, μ is the Poisson’s ratio, a is the diaphragm<br />

radius, and y0 is the center deflection <strong>of</strong> the diaphragm. The<br />

resulting center deflection <strong>of</strong> the membranes from the circular<br />

cavities (type B, 3500-μm diameter) was measured with a<br />

pr<strong>of</strong>ilometer to be about 40 μm, excluding <strong>of</strong>fset deflection<br />

from the SiO2 strain. With a silicon membrane thickness <strong>of</strong><br />

20 μm (excluding the 1-μm-thick SiO2 layer), a Young’s<br />

modulus <strong>of</strong> 162 GPa, and a Poisson’s ratio <strong>of</strong> 0.22 [30], the<br />

estimated pressure difference ΔP can be calculated to be on<br />

the order <strong>of</strong> 970 mbar. Thus, the estimated gas pressure inside<br />

the cavity would be on the order <strong>of</strong> 40 mbar, which is in line<br />

with the estimates from the cavity membrane deflection inside<br />

a vacuum chamber.<br />

IV. DISCUSSION<br />

In the experiments, it was shown that the proposed roomtemperature<br />

wafer-to-wafer attachment and cavity sealing<br />

method works in principle. However, it was observed that<br />

localized fractures in glass wafers underneath the gold sealing<br />

rings can occur when bonding silicon wafers to glass wafers.<br />

Localized fractures underneath the gold sealing rings in the<br />

silicon wafers were not observed. It is believed that the large<br />

local stresses from the cold welding process near the overlapping<br />

areas <strong>of</strong> the gold sealing rings cause stress peaks in the<br />

glass that exceed its yield strength and, thus, cause the localized<br />

fractures <strong>of</strong> the glass. This is specifically the case for cavities<br />

with squared corners where the strain during bonding can<br />

aggregate at the squared corners, as shown in Fig. 6. The results<br />

from the experiments and the gross leak tests indicate that<br />

the main failure mechanism that causes the gross leaks in the<br />

experiments described in Table I are localized fractures <strong>of</strong> the<br />

glass wafers underneath the gold sealing rings due to excessive<br />

shear or compressive stresses. In the two bonding experiments<br />

in which silicon wafers were bonded to SOI wafers, the wafer<br />

pair that was bonded with the lower bonding force (lower strain<br />

in the sealing rings) achieved good sealing results (no gross<br />

leaks), while the wafer pair that was bonded with the higher<br />

bonding force did not achieve sealing <strong>of</strong> any <strong>of</strong> the cavities<br />

(contain gross leaks). The exact reason for this effect is not<br />

known. Possible explanations may be that the wafer pair was<br />

not sufficiently aligned before the wafer bonding step or the<br />

bonding force was too large and thus, causing local breakage<br />

<strong>of</strong> the silicon substrate material or delamination <strong>of</strong> the gold<br />

sealing rings from the silicon substrate surface due to excessive<br />

localized strain. It is interesting to point out that for the sealed<br />

microcavities, the wedging gold sealing rings penetrated each<br />

other only about 7 μm deep, which was sufficient to provide<br />

successful sealing without detectable gross leaks.<br />

y 3 o<br />

h 3<br />

(1)<br />

V. C ONCLUSION<br />

A room-temperature wafer attachment and sealing concept<br />

has been introduced and experimentally evaluated. Microcavities<br />

manufactured with this technique have been successfully<br />

sealed without detectable gross leaks. The shape <strong>of</strong> the cavities,<br />

the overlapping area <strong>of</strong> the sealing rings, and the wafer materials<br />

were found to influence the bonding and sealing results.<br />

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669, Sep. 2003.<br />

[10] D. Sparks, G. Queen, R. Weston, G. Woodward, M. Putty, L. Jordan,<br />

S. Zarabadi, and K. Jayakar, “Wafer-to-wafer bonding <strong>of</strong> nonplanarized<br />

MEMS surfaces using solder,” J. Micromech. Microeng., vol. 11, no. 6,<br />

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[11] R. F. Wolffenbuttel, “Low-temperature inter-mediate Au–Si wafer bonding;<br />

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“Low-temperature silicon wafer-scale thermocompression bonding using<br />

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[13] F. Niklaus, G. Stemme, J.-Q. Lu, and R. J. Gutmann, “Adhesive wafer<br />

bonding,” J. Appl. Phys., vol. 99, no. 3, pp. 031 101.1–031 101.28,<br />

Feb. 2006.<br />

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using thin-film parylene,” J. Microelectromech. Syst., vol. 14, no. 6,<br />

pp. 1347–1355, Dec. 2005.<br />

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Compon. Conf., San Francisco, CA, 1976, pp. 361–367.<br />

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[17] Y. T. Cheng, L. Lin, and K. Najafi, “Localized silicon fusion and eutectic<br />

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[20] H. A. Yang, M. Wu, and W. Fang, “Localized induction heating solder<br />

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pp. 75–82.<br />

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DECHARAT et al.: ROOM-TEMPERATURE SEALING OF MICROCAVITIES BY COLD METAL WELDING 1325<br />

[22] H. Han, L. E. Weiss, and M. L. Reed, “Mating and piercing mechanical<br />

structures for surface bonding applications,” in Proc. IEEE MEMS, Nara,<br />

Japan, 1991, pp. 253–258.<br />

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J. Microelectromech. Syst., vol. 1, no. 1, pp. 37–43, Mar. 1992.<br />

[24] S.-H. Lee, J. Chae, N. Yazdi, and K. Najafi, “Micro-brush press-on contact:<br />

A new technique for room temperature electrical and mechanical<br />

attachment,” in Proc. IEEE MEMS, Istanbul, Turkey, 2006, pp. 342–345.<br />

[25] A. Singh, D. A. Horsley, M. B. Cohn, A. P. Pisano, and R. T. Howe,<br />

“Batch transfer <strong>of</strong> microstructures using flip-chip solder bonding,” J.<br />

Microelectromech. Syst., vol. 8, no. 1, pp. 27–33, Mar. 1999.<br />

[26] C. Kim, M. Shtein, and S. R. Forrest, “Nanolithography based on patterned<br />

metal transfer and its application to organic electronic devices,”<br />

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[27] W. Y. Zhang, G. S. Ferguson, and S. Tatic-Lucic, “Elastomer-supported<br />

cold welding for room temperature wafer-level bonding,” in Proc. MEMS,<br />

Maastricht, The Netherlands, 2004, pp. 741–744.<br />

[28] H. D. Espinosa and B. C. Prorok, “Effects <strong>of</strong> film thickness on the yielding<br />

behavior <strong>of</strong> polycrystalline gold films,” in Proc. MRS, 2002, vol. 695,<br />

pp. 349–354.<br />

[29] M. Giovanni, Flat and Corrugated Diaphragm Design Handbook. New<br />

York: Marcel Dekker, 1982.<br />

[30] B. Rashidian and M. G. Allen, “Electrothermal microactuators based on<br />

dielectric loss heating,” in Proc. IEEE Microelectromech. Syst. Workshop,<br />

Fort Lauderdale, FL, 1993, pp. 24–29.<br />

Adit Decharat received the M.Sc. degree in electrical<br />

engineering from King Mongkut’s Institute<br />

<strong>of</strong> Technology Ladkrabang, Bangkok, Thailand, in<br />

2002.<br />

In 2005, he joined the Department <strong>of</strong> <strong>Electrical</strong><br />

<strong>Engineering</strong>, Royal Institute <strong>of</strong> Technology,<br />

Stockholm, Sweden. His research interest is in<br />

MEMS integration and <strong>packaging</strong> for commercial<br />

IR cameras.<br />

Junchun Yu was born in Xiangtan, China, on<br />

July 17, 1983. He received the B.S. degree from<br />

Central South University, Changsha, China, and the<br />

M.S. degree in nanomaterials and nanotechnology<br />

from the Royal Institute <strong>of</strong> Technology, Stockholm,<br />

Sweden. He is currently working toward the Ph.D.<br />

degree in the Physics Department, Umea University,<br />

Umea, Sweden.<br />

Marc Boers received the M.S. degree in microengineering<br />

from Swiss Federal Institute <strong>of</strong> Technology,<br />

Lausanne, Switzerland, in 2006.<br />

During his M.S. studies, he served an internship at<br />

Microsystem Technology Group, Royal Institute <strong>of</strong><br />

Technology, Stockholm, Sweden, where he collaborated<br />

to develop a low-cost wafer-level-<strong>packaging</strong><br />

technology. He is currently a Development Engineer<br />

with the Phonak Acoustic Implants SA, Lonay,<br />

Switzerland, working in the medical industry on<br />

implantable hearing aid solutions.<br />

Göran Stemme (M’98–SM’04–F’06) received the<br />

M.Sc. degree in electrical engineering and the Ph.D.<br />

degree in solid-state electronics from Chalmers University<br />

<strong>of</strong> Technology, Gothenburg, Sweden, in 1981<br />

and 1987, respectively.<br />

In 1981, he joined the Department <strong>of</strong> Solid State<br />

Electronics, Chalmers University <strong>of</strong> Technology.<br />

There, in 1990, he became an Associate Pr<strong>of</strong>essor<br />

(docent) heading the silicon sensor research group.<br />

In 1991, he was appointed Pr<strong>of</strong>essor at the Royal<br />

Institute <strong>of</strong> Technology (KTH), Stockholm, Sweden,<br />

where he currently heads the Microsystem Technology Group, <strong>School</strong> <strong>of</strong><br />

<strong>Electrical</strong> <strong>Engineering</strong>. He has published more than 260 research journal and<br />

conference papers and has more than 22 patent proposals or granted patents.<br />

His research is devoted to microsystem technology based on micromachining<br />

<strong>of</strong> silicon.<br />

Dr. Stemme is a member <strong>of</strong> the Royal Swedish Academy <strong>of</strong> Sciences.<br />

Frank Niklaus (M’00) received the M.Sc. degree in<br />

mechanical engineering from the Technical University<br />

<strong>of</strong> Munich, Munich, Germany, in 1998, and the<br />

Ph.D. degree in MEMS from the Royal Institute <strong>of</strong><br />

Technology (KTH), Stockholm, Sweden, in 2002.<br />

He was working as a Consultant to industry and<br />

as a Visiting Scholar at Rensselaer Polytechnic Institute,<br />

Troy, NY, where he was working with 3-D IC<br />

technologies. He is currently an Associate Pr<strong>of</strong>essor<br />

in the Microsystem Technology Group, KTH, where<br />

he is the Team Leader for 3-D IC integrated MEMS<br />

and wafer-level <strong>packaging</strong> activities.<br />

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