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<strong>Evaluating</strong> <strong>the</strong> <strong>reliability</strong> <strong>of</strong> <strong>optical</strong> <strong>connectors</strong><br />

Report 1<br />

<strong>Evaluating</strong> <strong>the</strong> <strong>reliability</strong> <strong>of</strong> <strong>optical</strong> <strong>connectors</strong><br />

Yuichi Aoki Technical Development Headquarters, Reliability Research Section<br />

Kishichi Sasaki Reliability Center for Electronic Components <strong>of</strong> Japan, Environmental Testing Laboratory<br />

Kiyoyuki Mutaguchi Japan Aviation Electronics Industry, Limited, Connector Division<br />

W<br />

e performed <strong>the</strong> High Temperature Storage Test (Damp Heat) and <strong>the</strong><br />

Temperature Cycling Test on <strong>optical</strong> <strong>connectors</strong> in conformance to<br />

<strong>the</strong> Telcordia standards. During <strong>the</strong>se <strong>reliability</strong> tests, automatic<br />

measurements <strong>of</strong> <strong>the</strong> <strong>optical</strong> characteristics <strong>of</strong> <strong>the</strong> specimens were carried<br />

out and physical changes were compared. During <strong>the</strong> evaluation following<br />

<strong>the</strong> tests, we checked for physical changes in <strong>the</strong> tips <strong>of</strong> <strong>the</strong> <strong>optical</strong> <strong>connectors</strong>.<br />

We found pistoning changes occurring on <strong>the</strong> tips <strong>of</strong> <strong>the</strong> <strong>connectors</strong>, especially<br />

during <strong>the</strong> Temperature Cycling Test. However, <strong>the</strong>se pistoning changes caused<br />

almost no perceptible changes in <strong>optical</strong> characteristics. The ferrule tips were<br />

distorted after 2000 hours at 85°C and 85 percent relative humidity, exhibited<br />

flattening distortion.<br />

1<br />

Introduction<br />

Next-generation technology infrastructure using <strong>optical</strong> fiber has been on <strong>the</strong> march<br />

toward achieving widespread use during recent years. Acceptance <strong>of</strong> this technology has<br />

resulted in demand for lower cost and miniaturized <strong>optical</strong> components, but such<br />

improvements must be based on information from <strong>reliability</strong> testing assuring that quality<br />

can be maintained. Testing to evaluate <strong>reliability</strong> <strong>of</strong> <strong>optical</strong> components is generally<br />

performed in conformance to <strong>the</strong> Telcordia standards. *1 These standards include<br />

requirements for simultaneously measuring <strong>optical</strong> characteristics <strong>of</strong> multiple specimens<br />

during environmental testing. 1) Measurement methods are not affected by measurement<br />

margin <strong>of</strong> error when measuring with <strong>the</strong> <strong>connectors</strong> ei<strong>the</strong>r connected or disconnected.<br />

Additionally, automatic measuring is capable <strong>of</strong> efficiently ga<strong>the</strong>ring data at short<br />

measurement intervals. MTF (Mean Time to Failure) calculations are easy to perform using<br />

this system, for which published examples are available. 2,3) This report will focus on <strong>optical</strong><br />

<strong>connectors</strong>, which exhibit <strong>the</strong> basic characteristics <strong>of</strong> <strong>optical</strong> components. We shall also<br />

consider <strong>the</strong> results <strong>of</strong> <strong>reliability</strong> testing that incorporates automatic measuring in<br />

conformance to <strong>the</strong> Telcordia standards.<br />

Fig.1 Overview <strong>of</strong> <strong>optical</strong> components<br />

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2<br />

The Telcordia standards that require simultaneously measuring <strong>optical</strong> characteristics <strong>of</strong><br />

multiple specimens are mainly concerned with passive <strong>optical</strong> components. In this report<br />

<strong>the</strong> term "passive <strong>optical</strong> components" refers to such items as fiber, <strong>connectors</strong>,<br />

switches, couplers, attenuators, and all types <strong>of</strong> filters. Table 1 shows <strong>reliability</strong> tests for<br />

typical <strong>optical</strong> components.<br />

3<br />

Test standards for passive <strong>optical</strong> components<br />

Table 1 Telcordia test standards<br />

Standard Title<br />

GR-326-CORE<br />

Generic Requirements for Single-Mode Optical Connectors and<br />

Jumper Assemblies<br />

GR-1209-CORE Generic Requirements for Passive Optical Components<br />

GR-1221-CORE<br />

Generic Reliability Assurance Requirements for Passive Optical<br />

Components<br />

Structure <strong>of</strong> <strong>optical</strong> <strong>connectors</strong> and factors affecting <strong>the</strong>ir <strong>reliability</strong><br />

Optical <strong>connectors</strong> are<br />

used to connect <strong>optical</strong><br />

fiber. Photo 1 shows<br />

some typical<br />

<strong>connectors</strong>. Fig.2<br />

shows <strong>the</strong> composition<br />

<strong>of</strong> <strong>the</strong> <strong>optical</strong><br />

<strong>connectors</strong> used in <strong>the</strong>se tests.<br />

The fiber is inserted into <strong>the</strong> housing, which is called a zirconia ferrule, and <strong>the</strong> fiber is<br />

held in place with a hardening epoxy adhesive. The adhesive used for <strong>the</strong> <strong>connectors</strong> is<br />

Epo-Tek353ND (Epoxy Technology, Inc.). The degradation <strong>of</strong> this adhesive is a crucial<br />

element leading to <strong>the</strong> loss <strong>of</strong> <strong>the</strong> <strong>reliability</strong> <strong>of</strong> <strong>the</strong> <strong>optical</strong> <strong>connectors</strong>. A major factor<br />

producing degradation is <strong>the</strong> absorption <strong>of</strong> humidity, which causes degradation to occur<br />

over time. 1~5) Photo 1 Optical <strong>connectors</strong><br />

The High Temperature Storage Test (Damp Heat) is used to evaluate<br />

humidity-induced degradation. As Fig.2 shows, adhesive degradation resulted in<br />

pistoning changes to <strong>the</strong> ferrule tip on <strong>the</strong> end <strong>of</strong> <strong>the</strong> <strong>optical</strong> <strong>connectors</strong>. A significant<br />

amount <strong>of</strong> pistoning causes such problems as an increase in air layers and an increase in<br />

leakage <strong>of</strong> insertion light. These problems result in an increase in <strong>optical</strong> loss.<br />

The Temperature Cycling Test was also run to evaluate <strong>the</strong> progression <strong>of</strong> cracking<br />

caused by micro-cracks in <strong>the</strong> fiber.<br />

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<strong>Evaluating</strong> <strong>the</strong> <strong>reliability</strong> <strong>of</strong> <strong>optical</strong> <strong>connectors</strong><br />

Fig.2 Structure <strong>of</strong> <strong>optical</strong> <strong>connectors</strong> and factors affecting <strong>the</strong>ir <strong>reliability</strong><br />

4<br />

Environmental test system for <strong>optical</strong> components<br />

An environmental test system for <strong>optical</strong> components was developed to be used in this<br />

research for testing <strong>the</strong> <strong>reliability</strong> <strong>of</strong> passive <strong>optical</strong> components. Photo 2 shows <strong>the</strong><br />

system, and Fig.3 shows a block diagram <strong>of</strong> <strong>the</strong> system.<br />

This measurement system selects <strong>the</strong> light source wavelength using an <strong>optical</strong> switch<br />

selector, and is capable <strong>of</strong> measuring a maximum <strong>of</strong> 170 channels simultaneously for<br />

multiple specimens during environmental testing. This capability puts <strong>the</strong> system in<br />

conformance to <strong>the</strong> requirements <strong>of</strong> <strong>the</strong> Telcordia standards. The system is capable <strong>of</strong><br />

measuring insertion loss, *4 return loss, *5 and PDL (Polarization Dependent Loss). *6<br />

Photo 2 Environmental Test System<br />

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5<br />

Test method<br />

Fig.3 System block diagram<br />

The High Temperature Storage Test (Damp Heat) and <strong>the</strong> Temperature Cycling Test<br />

were run using <strong>optical</strong> <strong>connectors</strong> as specimens. Table 2 shows <strong>the</strong> test conditions, and<br />

Table 3 shows <strong>the</strong> specimens. The test conditions complied with <strong>the</strong><br />

Telcordia-GR-1221-CORE standards. The specimens consisted <strong>of</strong> single mode *7 SC and FC<br />

<strong>connectors</strong>. As seen in Fig.4, <strong>the</strong> specimens were connected in groups <strong>of</strong> three <strong>optical</strong><br />

<strong>connectors</strong> with fiber and with <strong>the</strong> measurement points n = 5 (groups). The<br />

measurement system was used to measure insertion loss and return loss. Table 4 shows<br />

<strong>the</strong> measurement conditions.<br />

The test specimens were measured after each 1000 hours <strong>of</strong> <strong>the</strong> High Temperature<br />

Storage Test (Damp Heat) and after <strong>the</strong> completion <strong>of</strong> <strong>the</strong> Temperature Cycling Test. A<br />

Ferrule Tip Condition Surveyor (Direct Optical Research Company) was used to measure<br />

ferrule tip curvature radius, *8 eccentricity, *9 and pistoning. Failure was determined using<br />

<strong>the</strong> Telcordia-GR-1221-CORE evaluation standards shown in Table 5.<br />

The Temperature Cycling Test was not effective for determining degradation, since<br />

changes occurred in both insertion loss and return loss in <strong>the</strong> <strong>optical</strong> fiber temperature<br />

characteristics in this test. The PVC sheath *10 coating in particular exhibited major<br />

changes at low temperatures, and so <strong>the</strong> test was run using Hytrel ® core *11 , which<br />

exhibited minimal loss at low temperatures as seen in Fig.5.<br />

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Table 2 Reliability test conditions<br />

Test items Test Conditions<br />

High<br />

Temperature<br />

Storage Test<br />

(Damp Heat)<br />

Temperature<br />

Cycling Test<br />

85°C, 85%rh,<br />

2000 h<br />

-40°C ←→ 85°C,<br />

1 hour each, 500<br />

cycles<br />

Fig.4 Test method<br />

Table 4 Measurement conditions<br />

Items Details<br />

Measurement items<br />

Insertion loss and<br />

return loss<br />

Light source<br />

wavelength<br />

1310 nm, 1550 nm<br />

Light source power 1 mW<br />

6<br />

Measurement<br />

intervals<br />

Test results<br />

Every 10 to 15 min.<br />

Specimens<br />

No. <strong>of</strong><br />

specimens<br />

Evaluation<br />

method<br />

- 5 -<br />

Table 3 Specimens<br />

FC <strong>connectors</strong>, SC <strong>connectors</strong><br />

(single mode)<br />

n = 5<br />

Insertion loss and return loss<br />

(<strong>optical</strong> component<br />

environmental test system)<br />

Tip condition measurement<br />

(pistoning, eccentricity, and<br />

curvature radius)<br />

Fig.5 Fiber temperature<br />

characteristics<br />

Table 5 Evaluation standards<br />

(from Telcordia GR-1221-CORE)<br />

Requirement Objective<br />

Insertion<br />

loss<br />

change<br />

0.3dB 0.2dB<br />

Return<br />

loss<br />

change<br />

6-1 Test results from <strong>the</strong> High Temperature Storage Test (Damp Heat)<br />

5dB 2dB<br />

Fig.6 shows <strong>the</strong> measurement results for <strong>the</strong> light source wavelength <strong>of</strong> 1310 nm for <strong>the</strong><br />

first 1000 hours <strong>of</strong> <strong>the</strong> 2000-hour High Temperature Storage Test (Damp Heat). After<br />

1000 hours and again after 2000 hours, we verified that fluctuation did not exceed any<br />

evaluation standards. In addition, identical trends were exhibited for both light source<br />

wavelengths, 1310 nm and 1550 nm. No major difference was seen between <strong>the</strong> FC<br />

<strong>connectors</strong> and <strong>the</strong> SC <strong>connectors</strong>.<br />

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<strong>Evaluating</strong> <strong>the</strong> <strong>reliability</strong> <strong>of</strong> <strong>optical</strong> <strong>connectors</strong><br />

Test time (h)<br />

(a) SC connector insertion loss<br />

Test time (h)<br />

(c) FC connector insertion loss<br />

- 6 -<br />

Test time (h)<br />

(b) SC connector return loss<br />

Test time (h)<br />

(d) FC connector return loss<br />

Fig.6 Results <strong>of</strong> <strong>the</strong> High Temperature Storage Test (Damp Heat)<br />

(light source wavelength: 1310 nm)<br />

6-2 Results <strong>of</strong> <strong>the</strong> Temperature Cycling Test<br />

Almost no differences were seen between <strong>the</strong> FC <strong>connectors</strong> and <strong>the</strong> SC <strong>connectors</strong> in<br />

<strong>the</strong> Temperature Cycling Test. Fig.7 shows partial measurement results for <strong>the</strong> SC<br />

<strong>connectors</strong>. Some insertion loss change and return loss change was seen following<br />

temperature changes in <strong>the</strong> temperature chamber during <strong>the</strong> Temperature Cycling Test,<br />

but <strong>the</strong>se changes did not exceed <strong>the</strong> evaluation standard limits. The changes included<br />

insertion loss occurring at low temperatures, but no major fluctuation was seen at high<br />

temperatures. Return loss, however, tended to increase at high temperatures. Looking at<br />

<strong>the</strong> return loss changes over <strong>the</strong> long term confirms that as soon as return loss increases,<br />

<strong>the</strong> fluctuation stabilizes. This is thought to indicate that return loss quality stabilizes due<br />

to <strong>the</strong> adhesion <strong>of</strong> <strong>the</strong> <strong>connectors</strong> over time.<br />

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<strong>Evaluating</strong> <strong>the</strong> <strong>reliability</strong> <strong>of</strong> <strong>optical</strong> <strong>connectors</strong><br />

(a) Insertion loss<br />

(b) Return loss<br />

Fig.7 Results <strong>of</strong> <strong>the</strong> Temperature Cycling Test<br />

(SC <strong>connectors</strong>; light source wavelength, 1310 nm)<br />

6-3 Pistoning measurement results<br />

Measurement results for <strong>the</strong> ferrule tip surfaces did not indicate major changes in<br />

eccentricity and curvature radius, but <strong>the</strong> measurements confirmed that changes<br />

occurred in pistoning compared to <strong>the</strong> initial values.<br />

Fig.8 shows pistoning measurements after 1000 and 2000 hours <strong>of</strong> <strong>the</strong> High<br />

Temperature Storage Test (Damp Heat), and after 500 cycles <strong>of</strong> <strong>the</strong> Temperature Cycling<br />

Test. This report represents <strong>the</strong> direction <strong>of</strong> pistoning as a negative value. In <strong>the</strong> IEC, <strong>the</strong><br />

standard for tolerance is recommended as -50 to 100 nm, and this level is exceeded, but<br />

<strong>the</strong> insertion loss and return loss measurements did not exhibit conspicuous fluctuation.<br />

On <strong>the</strong> o<strong>the</strong>r hand, <strong>optical</strong> <strong>connectors</strong> with powerful insertion light may be subject to<br />

influence by pistoning. Because <strong>of</strong> this, we face <strong>the</strong> challenge <strong>of</strong> investigating <strong>the</strong><br />

relationship between pistoning and <strong>optical</strong> characteristics in such areas as manufacturing<br />

conditions.<br />

In this research, more pistoning occurred in <strong>the</strong> Temperature Cycling Test than in <strong>the</strong><br />

High Temperature Storage Test (Damp Heat), regardless <strong>of</strong> whe<strong>the</strong>r <strong>the</strong> type <strong>of</strong> fiber<br />

coating included Hytrel ® core or <strong>the</strong> PVC sheath. The cause for <strong>the</strong> increased pistoning is<br />

thought to include stress in <strong>the</strong> direction <strong>of</strong> <strong>the</strong> pistoning from contraction and peeling <strong>of</strong><br />

<strong>the</strong> adhesive. This, in turn, is thought to be possibly caused by <strong>the</strong> effects <strong>of</strong> humidity and<br />

<strong>the</strong> re-hardening <strong>of</strong> <strong>the</strong> adhesive at <strong>the</strong> test temperature (85°C) for <strong>reliability</strong> testing.<br />

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Test time (h)<br />

(85°C, 85%rh, PVC sheath coating)<br />

Test cycles<br />

(-40/85°C, 1 hour each, PVC sheath coating)<br />

Test cycles<br />

(-40/85°C, 1 hour each, Hytrel ® core)<br />

Fig.8 Changes in pistoning<br />

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6-4 Observation <strong>of</strong> <strong>the</strong> tip shape<br />

Fig.9 shows <strong>the</strong> results <strong>of</strong> observations made on <strong>the</strong> shape <strong>of</strong> <strong>the</strong> ferrule tip before and<br />

after <strong>the</strong> High Temperature Storage Test (Damp Heat). After 2000 hours at 85°C and 85<br />

percent relative humidity, <strong>the</strong> surface <strong>of</strong> <strong>the</strong> ferrule tip showed signs <strong>of</strong> pitting and was<br />

rougher than before testing. This roughness did not appear on <strong>the</strong> surface <strong>of</strong> <strong>the</strong> tip after<br />

<strong>the</strong> Temperature Cycling Test, leading to <strong>the</strong> conclusion that <strong>the</strong> roughness was caused<br />

by humidity. Fig.10 shows a three-dimensional computer graphics rendition <strong>of</strong> <strong>the</strong> shape<br />

<strong>of</strong> <strong>the</strong> tip. After 2000 hours at 85°C and 85 percent relative humidity, <strong>the</strong> ferrule tip<br />

exhibited flattening distortion. However, pistoning measurements with <strong>the</strong> Ferrule Tip<br />

Condition Surveyor measured <strong>the</strong> position <strong>of</strong> <strong>the</strong> apex <strong>of</strong> <strong>the</strong> tip from <strong>the</strong> sphericity <strong>of</strong> <strong>the</strong><br />

ferrule tip, and, using that position as a standard, calculated <strong>the</strong> amount <strong>of</strong> pistoning.<br />

Accordingly, if <strong>the</strong> position <strong>of</strong> <strong>the</strong> tip section differs from <strong>the</strong>se measurements, <strong>the</strong><br />

amount <strong>of</strong> pistoning could be greater than that calculated.<br />

(a) Initial period<br />

(b) After testing<br />

Fig.9 Ferrule tip observation (85°C, 85%rh, 2000 h)<br />

(Initial period) (-40 /85°C, 500 cycles) (85°C, 85%rh, 2000 h)<br />

Fig.10 Three-dimensional shape <strong>of</strong> <strong>the</strong> ferrule tip<br />

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7<br />

The <strong>optical</strong> characteristics <strong>of</strong> <strong>the</strong> <strong>optical</strong> <strong>connectors</strong> reviewed for this study were<br />

automatically measured during <strong>the</strong> High Temperature Storage Test (Damp Heat) (at<br />

85°C and 85 percent relative humidity for 1000 hours) and <strong>the</strong> Temperature Cycling Test<br />

(at 85°C / -40°C for 500 cycles <strong>of</strong> one hour each). We obtained <strong>the</strong> following results.<br />

(1)No changes occurred in <strong>optical</strong> characteristics, but pistoning increased in <strong>the</strong><br />

<strong>connectors</strong>.<br />

(2)Increased pistoning <strong>of</strong> <strong>the</strong> ferrule tips was observed in both <strong>the</strong> Temperature Cycling<br />

Test and <strong>the</strong> High Temperature Storage Test (Damp Heat), but <strong>the</strong> major changes<br />

occurred in <strong>the</strong> Temperature Cycling Test.<br />

(3)The post-test condition <strong>of</strong> <strong>the</strong> ferrule tips after testing at 85°C and 85 percent relative<br />

humidity for 2000 hours exhibited flattening distortion. This result could indicate that<br />

<strong>the</strong> actual pistoning was greater than <strong>the</strong> calculated amount.<br />

8<br />

Conclusion<br />

Topics for future discussion<br />

Many aspects <strong>of</strong> <strong>the</strong> relationship between pistoning and <strong>optical</strong> characteristics have yet<br />

to be confirmed, and topics such as manufacturing conditions also require research.<br />

[Terminology]<br />

*1.Telcordia<br />

The breakup <strong>of</strong> <strong>the</strong> American communications giant AT&T (Bell Telephone) created<br />

seven regional telephone providers (<strong>the</strong> so-called "Baby Bells") and established a<br />

research and development company initially called Bellcore. Later, when this<br />

subsidiary was sold to a company unrelated to <strong>the</strong> original Bell, <strong>the</strong> company became<br />

known as Telcordia Technologies. In <strong>the</strong> field <strong>of</strong> communications in <strong>the</strong> U.S., <strong>the</strong><br />

Telcordia standards are widely referenced as <strong>the</strong> baseline standards for this field.<br />

*2.SC <strong>connectors</strong>, and *3. FC <strong>connectors</strong><br />

Both <strong>of</strong> <strong>the</strong>se <strong>optical</strong> <strong>connectors</strong> are zirconia ferrule (refer to Fig.2 above) <strong>connectors</strong><br />

developed in Japan that are widely used throughout <strong>the</strong> world. The stationary part <strong>of</strong><br />

<strong>the</strong> SC connector is made <strong>of</strong> plastic, and can be connected by merely being pressed<br />

on. The stationary part <strong>of</strong> <strong>the</strong> FC connector, though, is made <strong>of</strong> metal and must be<br />

attached with screws.<br />

*4.Insertion loss<br />

The transmission loss occurring when light passes through <strong>the</strong> part. This value<br />

compares <strong>the</strong> insertion light with <strong>the</strong> outgoing light, and is expressed in decibels.<br />

*5.Return loss<br />

This value compares <strong>the</strong> insertion light power and <strong>the</strong> reflected light power <strong>of</strong> <strong>the</strong><br />

reflected light returning inside <strong>the</strong> part. This value is expressed in decibels.<br />

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<strong>Evaluating</strong> <strong>the</strong> <strong>reliability</strong> <strong>of</strong> <strong>optical</strong> <strong>connectors</strong><br />

*6. PDL (Polarization Dependent Loss)<br />

The PDL value measures <strong>the</strong> change occurring in insertion loss caused by<br />

polarization. Polarization is a condition <strong>of</strong> deviation in <strong>the</strong> vibrational direction <strong>of</strong><br />

light.<br />

*7. Single mode<br />

Single mode is a condition which provides light with a single pathway <strong>of</strong> propagation.<br />

This mode contrasts with multi-mode, which consists <strong>of</strong> multiple pathways <strong>of</strong> light<br />

propagation. Due to <strong>the</strong> mode-dispersed loss occurring in multi-mode, single mode<br />

is used for long-distance transmission.<br />

*8. Curvature radius<br />

The length (in mm) <strong>of</strong> <strong>the</strong> radius <strong>of</strong> a circle from a circumference projected from a<br />

curved surface.<br />

*9. Eccentricity<br />

The length (in µm) <strong>of</strong> <strong>the</strong> deviation between <strong>the</strong> center <strong>of</strong> <strong>the</strong> ferrule and <strong>the</strong> center<br />

<strong>of</strong> <strong>the</strong> core <strong>of</strong> <strong>the</strong> <strong>optical</strong> fiber.<br />

*10.PVC sheath<br />

This polyvinyl chloride (PVC) sheath, referred to as <strong>optical</strong> fiber cable, has a<br />

protective fiber coating. This type <strong>of</strong> sheath is mainly used indoors.<br />

*11.Hytrel ® core<br />

Hytrel ® is a polyester elastomer made <strong>of</strong> <strong>the</strong>rmoplastic resin that was developed by<br />

<strong>the</strong> Dupont Corporation. This substance is an engineering plastic with superb<br />

features such as strength and heat characteristics. Hytrel ® core is a fiber optic<br />

stranded conductor coated with this elastomer.<br />

[Bibliography]<br />

1) "Generic Reliability Assurance Requirements for Passive Optical Components",<br />

Telcordia GR-1221-CORE Issue 2, 1999<br />

2) T. Tomasi, I. De Munari, V. Lista, L. Gherardi, A. Righetti, M. Villa: "Passive <strong>optical</strong><br />

components: from degradation data to <strong>reliability</strong> assessment-preliminary results",<br />

Microelectronics Reliability 42, p.1333-1338, 2002<br />

3) A. Piccirillo, G. Zaffiro, T. Tambosso, G. Gallo: "Reliability <strong>of</strong> Optical Branching<br />

Devices", IEEE (Institute <strong>of</strong> Electrical and Electronics Engineers), Journal <strong>of</strong> Selected<br />

Topics in Quantum Electronics, Vol.5 No.5, 1999<br />

4) F. Caloz, D. Ernst, P. Rossini, L. Gherardi, L. Grassi, J. Arnaud: "Reliability <strong>of</strong> <strong>optical</strong><br />

<strong>connectors</strong> - Humidity behavior <strong>of</strong> <strong>the</strong> adhesive", Microelectronics Reliability 42,<br />

p.1323-1328, 2002<br />

5) Tetso Kumazawa, Makoto Shimaoka, Kazuyuki Fukuda: "Moisture Absorbency <strong>of</strong><br />

Optical Components Resin Adhesive" Journal <strong>of</strong> Japan Institute <strong>of</strong> Electronics<br />

Packaging, Vol.4, No.7, p.621- 624, 2001<br />

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Espec Technology Report No20

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