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4.3.1 Development of a LabView Program for Semiconductor Hall ...

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38 Annual Report 2007 - Solid-State Electronics Department<br />

<strong>4.3.1</strong> <strong>Development</strong> <strong>of</strong> a <strong>LabView</strong> <strong>Program</strong> <strong>for</strong> <strong>Semiconductor</strong> <strong>Hall</strong><br />

Measurements<br />

Student<br />

Supervisor<br />

Technical Assistant:<br />

R. Shabanah<br />

I. Nannen<br />

U. Doerk<br />

Introduction<br />

<strong>Semiconductor</strong> transport measurements are routinely done by van-der-Pauw/<strong>Hall</strong> measurements. In<br />

this work a new s<strong>of</strong>tware plat<strong>for</strong>m based on <strong>LabView</strong> programme has been developed providing a<br />

user friendly interface and extended data storage utilities. It replaces the existing plat<strong>for</strong>m based on<br />

a HP Basic programme. Special emphasis was given in the optimization <strong>of</strong> the measurement data<br />

aquisition. This way the range <strong>of</strong> measurement conditions <strong>of</strong>fering precise transport data has been<br />

successfully extended.<br />

The <strong>Program</strong><br />

The transport <strong>of</strong> charged carriers in a rsemiconductor crystal is affected as by an magnetic field<br />

r r<br />

described by the <strong>of</strong> Lorenz <strong>for</strong>ce: FL<br />

= q⋅ ( v×<br />

B)<br />

. If the magnetic field is perpendicular to<br />

direction <strong>of</strong> current flow, the Lorenz <strong>for</strong>ce results into a accumulation <strong>of</strong> charge in a semiconductor<br />

sample which gives rise to the <strong>Hall</strong> voltage given here <strong>for</strong> electron transport:<br />

VH<br />

1<br />

= ⋅B⋅I<br />

q⋅n⋅ d . (1)<br />

The challenge <strong>of</strong> <strong>Hall</strong> measurement is a precise set up <strong>of</strong> the magnetic field B, the measurement<br />

current I, and the precise measurement <strong>of</strong> the <strong>Hall</strong> voltage V H in the presence <strong>of</strong> parasitic conditions<br />

like a remaining magnetic field, and a non-symmetric sample. For the control and read-out <strong>of</strong> the<br />

measurement data the <strong>LabView</strong> (Laboratory Virtual Instrumentation Engineering Workbench) has<br />

been adopted. <strong>LabView</strong> is a graphic programming language. The programming is carried out<br />

according to the data flow model. <strong>LabView</strong> programs are called virtual instruments or simply VIs.<br />

VIs consists <strong>of</strong> two components:<br />

- the front panel, that contains the Graphical User Interface<br />

- the block diagram <strong>of</strong> the graphic program code.<br />

Fig. 1 shows as an example the programming <strong>of</strong> the read out <strong>of</strong> the <strong>Hall</strong> voltage from a digital<br />

multimeter (Keithley 199). Every 0.5 ms measurement data are recorded. In a sub-VI the standard<br />

deviation and the mean value <strong>of</strong> four subsequent data are determined. The data are accepted if the<br />

standard deviation is less than 10% <strong>of</strong> the average value. An error message window will appear if<br />

the data are not valid. In the same manner the programming is done <strong>for</strong> the magnetic field<br />

adjustment and the various current source adjustments according to the van der Pauw technique.<br />

This program makes it possible to store results <strong>of</strong> measurement on the computer as HTML file<br />

which facilitates the exchange <strong>of</strong> the results over E-Mail and network. In order to pro<strong>of</strong> the ohmic


Annual Report 2007 - Solid-State Electronics Department 39<br />

conductivity <strong>of</strong> all contacts and the degree <strong>of</strong> symmetry <strong>of</strong> the sample, an integrated I-V test using<br />

the HP parameter analyser HP 4145B has been implemented.<br />

Fig. 1<br />

Block diagram <strong>of</strong> the read-out <strong>of</strong> measurement data using Lab View<br />

Results <strong>of</strong> measurement<br />

We report here on the precision <strong>of</strong> the <strong>Hall</strong> measurement in a wide range <strong>of</strong> measurement<br />

conditions. For this purpose, two InP-based samples with very different transport data have been<br />

selected: a highly p-type doped InGaAs layer as part <strong>of</strong> a pin diode and a high mobility twodimensional<br />

electron gas <strong>of</strong> a heterostructure field-effect transistor structure (InAlAs/InGaAs/InP).<br />

Tab.1 shows the results <strong>of</strong> the initial 4-point measurement without a magnetic field <strong>of</strong> the van-der-<br />

Pauw technique <strong>for</strong> the determination <strong>of</strong> the sheet resistance. The measurement current I AB is<br />

applied to the contacts AB <strong>of</strong> the sample and the voltage drop V CD is measured at terminals CD.<br />

IAB [µA]<br />

HP-basic<br />

VCD [mV]<br />

<strong>LabView</strong> VCD[mV] ∆VCD [%]<br />

5 -0.26 -0.263 -1.2<br />

10 -0.516 -0.518 -0.4<br />

20 -1.02 -1.03 -1.0<br />

40 -2.05 -2.05 0.0<br />

100 -4.10 -4.10 0.0<br />

200 -5.12 -5.13 -0.2<br />

400 -20.5 -20.5 0.0<br />

1,000 -52.0 -52.2 -0.4<br />

2,000 -104 -105 -1.0<br />

4,000 -116 -117 -0.9<br />

Tab.1<br />

Comparision <strong>of</strong> digital multimeter read-out data <strong>of</strong> the <strong>LabView</strong> and the HP basic<br />

programme <strong>for</strong> the sheet resistance determination <strong>of</strong> p-doped sample without magnetic<br />

field.


40 Annual Report 2007 - Solid-State Electronics Department<br />

Tab. 1 shows that the agreement <strong>of</strong> voltage measurement <strong>of</strong> both plat<strong>for</strong>ms is very high (< 1%). In<br />

addition, the linearity <strong>of</strong> the measurement results over three orders <strong>of</strong> magnitude indicates that a<br />

very wide range <strong>of</strong> input currents give a precise measurement result.<br />

Next, the precision and range <strong>of</strong> measurement with applied magnetic field is investigated. For this<br />

purpose the high mobility sample has been chosen. Fig. 2 shows the transport data <strong>of</strong> twodimensional<br />

electron gas. As the thickness d is unknown, the sheet carrier concentration ns<br />

= n⋅<br />

d<br />

(cf. eq. 1) is determined. Both s<strong>of</strong>tware plat<strong>for</strong>ms were investigated in a wide range <strong>of</strong> applied<br />

magnetic fields B. The high precision <strong>of</strong> the measurement set-up enables a very reliable<br />

measurement at a magnetic field strength as low as B = 50 mTesla. There should be no physical<br />

dependence <strong>of</strong> measurement data up to approximately µ ⋅ B ≤ 1 which holds here because the<br />

mobility doe not exceed 10,000 cm²/Vs (cf. Fig. 2). There<strong>for</strong>e, the higher variation <strong>of</strong> the evaluated<br />

data in comparison to table 1 is attributed to the precision <strong>of</strong> the set-up <strong>of</strong> the magnetic field. The<br />

relative deviation <strong>of</strong> the mobility with the basic program is 5.88 % while with the new <strong>LabView</strong><br />

program a strongly reduced deviation <strong>of</strong> 1.38 % is achieved.<br />

mobility µ [cm²/Vs]<br />

9500<br />

9200<br />

8900<br />

8600<br />

HP-BASIC<br />

<strong>LabView</strong><br />

µ<br />

0 200 400 600 800<br />

magnetic field B /mT<br />

n s<br />

3.5<br />

3.0<br />

2.5<br />

sheet carrier concentration n s [cm²]<br />

Fig. 2<br />

Transport data <strong>of</strong> a two-dimensional electron gas determined at various magnetic field<br />

strength. (I = 20 µA, T=300K).<br />

Summary<br />

A new <strong>LabView</strong> program is developed, enabling user friendly van-the-Pauw/<strong>Hall</strong> measurements<br />

with extended data storage utilities. The program has been tested with exemplary samples like a<br />

high mobility two-dimensional electron gas and a low mobility p-type doped layer. The<br />

measurements shows a good agreement to the previous basic program. In addition, a wide<br />

measurement parameter regime <strong>for</strong> precise HALL measurements and an improved data acquisition<br />

could be demonstrated.

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