GC - Teknolab AS
GC - Teknolab AS
GC - Teknolab AS
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gas chromatography<br />
Heliflex ® USP 467<br />
Capillary Kits<br />
premium<br />
• Tested for organic volatile impurities<br />
• Kits for Method I and V for Method 467<br />
• Guard columns plus connector<br />
USP Method 467 deals with the determination of organic<br />
volatile impurities in pharmaceuticals, which results from<br />
solvents commonly used in the manufacturing process.<br />
Method I Kit Contains:<br />
AT-5, (USP G27) 30m x 0.53mm x 5.00μm; 5 x Universal<br />
FSOT Connectors; and 5 x 5m Deactivated Guard Columns<br />
(0.53mm i.d.).<br />
Method V Kit Contains:<br />
AT-624, (USP G43) 30m x 0.53mm x 3.00μm; 5 x Universal<br />
FSOT Connectors; and 5 x 5m Deactivated Guard Columns<br />
(0.53mm i.d.).<br />
Method I Kit Specifications<br />
Phase:<br />
(5% Phenyl)-95% Methylpolysiloxane<br />
Polarity: Non-Polar<br />
Temp. Limit: -60–350°C<br />
USP Code: G27<br />
Ideal For: Drug Analysis<br />
3<br />
5<br />
USP 467 - Trace Volatiles<br />
8<br />
1797<br />
1. Ethylene Oxide<br />
2. Impurity<br />
3. Methylene Chloride<br />
4. Chloroform<br />
5. Benzene<br />
6. Trichloroethylene<br />
7. 1,4-Dioxane<br />
8. Dimethyl Sulfoxide<br />
Method V Kit Specifications<br />
Phase:<br />
(6% Cyanopropylphenyl)-94% Methylpolysiloxane<br />
Polarity: Intermediate<br />
Temp. Limit: 20–260°C<br />
USP Code: G43<br />
Ideal For: Drug Analysis<br />
USP 467 - Method V<br />
1866<br />
4<br />
1. Ethylene Oxide<br />
2. Methylene Chloride<br />
2<br />
3. Chloroform<br />
4. Benzene<br />
5. Trichloroethylene<br />
6. 1,4-Dioxane<br />
5 6<br />
gc columns | capillary<br />
7<br />
1<br />
12<br />
4<br />
6<br />
3<br />
0 3 6 9 12 15 18 Min.<br />
Column: Heliflex ® AT-5, 30m x 0.53mm x 5.00μm<br />
(Part No. 16859)<br />
Temp: 35°C (5 min hold) to 175°C at 8°C/min<br />
Carrier Gas: Helium at 35cm/sec<br />
Detector: FID at 260°C<br />
0 4 8 12 16 20 Min.<br />
Column: Heliflex ® AT-624, 30m x 0.53mm x 3.00μm<br />
(Part No. 16889)<br />
Temp: 40°C<br />
Carrier Gas: Helium at 35cm/sec<br />
Detector: FID<br />
more info<br />
For more information on Pharmaceutical analysis,<br />
request brochure #470.<br />
USP 467 Capillary Kits<br />
Description<br />
Part No.<br />
Capillary Kits<br />
USP 467/Method I Capillary Kit 13963<br />
USP 467/Method V Capillary Kit 13971<br />
Replacement Components<br />
AT-5, 30m x 0.53mm x 5.0μm 16859<br />
AT-624, 30m x 0.53mm x 3.0μm 16889<br />
Universal FSOT Connectors, 5/pk 20400<br />
Deactivated Guard Columns, 5m x 0.53mm, 5/pk 13990<br />
www.discoverysciences.com<br />
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