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J-BNB - VPMThane.org

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N=normality of Na2S203<br />

Total Solids:-<br />

The total solids were determined by evaporation method.the total solids were the residur left after<br />

evaporation of unfiltered sample.the total dissolved solids were determined as the total residue left after<br />

evaporation of filtered sample while total suspended solids were the difference between the values of total<br />

solids and total dissolved solids.<br />

Formula,<br />

(1)Total suspended solids(mg/l)=W2-W3*1000*1000/vol. of sample.<br />

(2)Total dissolved solids(mg/l)=W2-W3*1000*1000/vol. of sample<br />

(3)Total solids(mg/l)=total suspended solids+total dissolved solids.<br />

Hardness :-<br />

Hardness was estimated by Argentiometric method.The titration of the sample was carried out<br />

against std. silver nitrate solution using Erichrome black-T as indicator where the end point was wine red<br />

to blue.<br />

Formula,<br />

Hardness(mg/l)=(A*B)*N*1000/vol. of sample<br />

Where,<br />

A=burette reading in ml<br />

B=1 as 1 ml, caco3 of titrant<br />

Chlorides:-<br />

The method used was Argentiometric method.The chloride ion was estimated by titration with<br />

std.AgNO3 using potassium chromate as the indicator. The end point was yellow to brick red.<br />

Formula,<br />

Chlorides(mg/l)=(A-B)*N*1000/vol. of sample<br />

Where,<br />

A=ml titration for sample<br />

B= ml titration for blank<br />

N= normality of AgNO3<br />

PH:-<br />

The ph of samples are calculated by ph meter,ph mpaper and by using universal indicator.<br />

59 J<strong>BNB</strong> (Vol. I ) Issue I January’2013

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