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13) O.$ A, Pozoteicny of Ri€c H6k Asb.,. Swedish rturitut for Buil

19) P.y., J.. rnd Mo@, J.,'Dcrehindion of /|mphN Siti6 ii Ric. HBI Arh by
! R pid An||yrh.f M.lhod", C.h6r .id C.rcrc& R64h, v 3 t,2@t, 221 _ 2Jt,
20) Skdfv.r! B.ngrJohd ; Yds, pa{it., .Th. Fouling BdNio. of tuc. Hurt Alh in
nuidizcdB.d ConbBdo. 2. Pih-Scd. ,rd Futlscllc M4u6aB.',
EndSy .d fu.ls. v 19, n a, July/Augu( 2005, p t5l2n 519
2l) Sh6e H.,Silic. WhiL Oh.in d Fm Rie Hqt in. Ftlidiz.d 8.d,, poydcr
tchnolo$, V I17, 2001, 0p 232-236
22) Fss M-, ExFriren|ll Sndy otr ru@ Hur Con$urion in CiEuhnng Ftuidizld
bcd . Fu.l Fc*ina t6hnolo$'_ V 85, 2O0t, ppl27t- t 282.
23) Ndr.r.ju E., lvdia orconbdion sd csiic{ion otRicc Hcl in nuidj2.d
B.d R€&!ou", BioN .trd bioo6S, v t4 t99& Dp 533-546
24) Nrn, Dep6 c,; l.grdish. K.S., "Rerirc poalls lirn Ri@ Hult A.h: An
Alrmdv. b C.Mt for Rnt Ho6ing,,.
Cffil md Corcel. R6ah, v t6, i 6, rw,2006, p tO62-!071
25) M&i. c., Jein4 T., "Highty R.etiv. Di.rtdm Sitjoc Synrhdi!.d by
HydDlll.ml Pre6ing . ,oumlotc.@t.nd Con@G Corpo.ir6, v 22,2000, F
315-3r9.
26) Flbi6r., M,. B'W, 8,, Nicol.x L., .E Liu Siliol. Hrtlr6 tnvdtg.lcd by
Solid-St{.HiehR@lurioirHrd \iNFl6M.g ric R@n.@-. C.mr lDd
concEl. R6eh, v t7i n 5, ,@, 2O{t, p 63t.638
121

I- PERSONAL INT1ORMATION
CURRICTJLUM \TTEAE
Nmq SI'ED IiASSAN Tt VED NAevI
P.Ir]r'@r Addr*: l1l A2, pujr! con. &,ptoy6 CdFEriE So.idy Ljnor.,
Prtisr.r 042-90294{t8, 042-90rt @
O.cnpliond Addslr: Aswiare pofdd, D.psnMt oI Ctdicd elgincdine.
Univmity of Engin@iii8 and Technology, Lrhor., -
Dal€ ofBinh: Apdl 04 19j6.
Ndio.dity: Patist d
EMil Add*sr uabirdiAiohil.oh
2- EDUCATION
M.Sc. Ct6ic.l En8i'Eins, Nd Jd!.y tsdm. of Tehmlogy USA. l9EE.
Tt6k ride SltFrginic M.tqiats in pdyffi Codcra.-
M.Sc Engire.nDg Md!8mdl, Nq J.6.y hrirutc ofT6llblogy USA l99l.
Th6is Titlq "R€tum On trvstne (ROt) fM snall pofildd Cd.nt pldr
B. S(. Clmisl EngiMn& Udvaity of En&n6irs.rd Tahnoto$,, kholq
Paltsta 1982.
128

:!n,llIOTllENT
l,A.si.t!tb&ro. 2{X[ io (b!
Urivdivof Bndn.d!t|tldT.4hob$r, khor!
2. Aldilllnl?Dfclor tgEf b 2OOo
Ud@iry of Bigin .!i!god T.lhlobry, h!@
rhi*dryof EDSin riDg od T.6otory, !.h$
+ MEIITEXAEIIE
1982to l9l5
rr.da,P.ritu8!si!*iqCoElR{hdlt!tuod&tb-.
rt ohq,P.lirlr' bri!!. ofcbi.l BryiFl
t4

Annexure I
XRD and FTIR operating conditions
l]0

l.bftLd u!.Ln!h ty!.: 16,
K!?rOr hr6nCry nfo: o . 50
N.m.r FW3011/20 (Mtiiprcp_ ta1b etnde)
NrE: fry$x|/oo cu t"FF D(14735r6
acpri.ddsllv: xfr..r Dab co&

ToidrDGftd: Od7l!
InLorLd {:v€retd! typi tG,
xolKdr irre.ly drc o. 50
ibE m3ot12o 0rv!t |.!.rrrh0
'E mefttreo Or (FFq(l.ttF
ADolicdodw: )cfh o.r. cdad.
|ndrumdntrfd 61/v: xPERl.PRo
scnd'sbc): 10.ooo - ro.ooo
load riF 0rc} ta:ozl5
TEIB
tt2

lii.nd€d E€t€r€th tF: K.,
Kozil

FIIR OentlN Cobd iolj
Dot€ctr TOq
A0.da.do: cGrn.
Ap.due alb (r1 om)
s@nino Spo.d: Aulo (2 mntH)
Alro {3OOOo H2)
wavenomb tcrll
%1
End: ao@ 6 *1
D.rr 9ir.h 0.9€4233 *1
D.1. po nt.r 3236

Annexure 2
Method of determining amorphous silica and figures
lt5

Proc€dur. for .mrpiou. rilie d.G.ni..do! by .n.lydet mttod
l) Pr.p.nrior ol rtrd|qbr SolutioB
A 0.005M aqueous glr€ol $ln1ioo oi Ba{OH), is pEp@d frcm a sarurat.d aqu@s
$lulion of B4OHL (the slubiliiy of Aa(OH) in ward !t 30'C is 3.89 B/100 nn), uking
!n appropriare volune aft.r lillration (10.s ml of fil&lt€ w6 E*d lo pr€pd.250 ml of
6olution) dd mixing n wnh e aqu@u6 gllreDl solution in which the wltcr to slycerol
ario *6 l:1. Thc reulting $l on nusr b. porarcd fDm .[@sphdic CO:. An
llcoholic solution of phcnolphtnaLih (covering the pH rege 8-9.) wd used a .h
2) Atuu ofrin Eqole.Ltrr to 5 Dl ofcly..rol
A snl volume of glicerol b m6ur.d n a small beols or a porcelain capsule (using a
st{inge) ..d dowly dhted witn lhe !qu6u $lulior ol gltt@l B.(OH):. horn mixcd
widr a ma8ltetic sri@. Becaue $e high vi$osity of glrml th€ derddon ofthe cnd
poim of th. ibrion musr b. clEied out exrmlty of thc riEalion !@epr.cl.. Ite olor
chage oa $s slution n de|.mircd $ follows: fou dsp6 of the indjobr c ple.d on
! por.ehin plale .nd lou drops of rhc slldon b.ine litratcd addcd to it Deps ae nixed
wnh a gls md md this pmedue h Epsred !ftq each ad.Cnion oftitel. Tilrarion is
supposed to be complet€d when the color of th. solutioo ildicaror oh tn€ porceloin plale
cha.s6lo Dse. The mounl of tiftnt used N, n rlkcn inro lccoDt in subs.quenl
l16

J) AnNrt or Tlhrt !!.d fo.ltlnti!8 S[ie Dtslv.d In Clyc.rul
30J0 mC of ltandaid morphos silica GBiosly prc9ded and 6n.ly disp€s.d ii d
agate mrtar) h weighcd (m, and plac.d in 1he porceldin capsul. or b.ak.r, avcrcd with
s nl orglyccol ed lhe mixluE aound rog.rh6 (wirh lh. aid ofrhe @gneric stiF) ad
!ffer tlut mix.d wilh . mgn tic stiftr for 30 hin minimm Tn€ mntw is tnm ridied
a follo$: B(OH), solulion in e .moul equivrrenl to 5 ni ol glycctol is added lhe
sulr.rei@ mixed c!rcfuuy for 20 ninu6 lDd rit |lio! rhd cani€d out slovly a

Frg. Al, @ Ft'.i.d by udngo lN lottion ofXMnO. (.) wd Gd O) DtiGd G'{
Fi& A-2: C.l F!9.nd Aon u .€d.d d.. nG* (t Wa gd O) DiolciM 3ilic{' aotl
l18

(.)
l
o)
-f;+:*
.*!L

Fig, A-5r SEM
(b)
prcduccd fod uoteated ric€ hu6k.
Fig. A-6: SEM of FDicalciw silicarB. {a) tuce h6k Eqt d wi$ 0.0olN sludon oa
KMnOr lb) Ricc husk rcdred with 0.lN sdlulion ofKMnol.
(b)
I

Annexure 3
Published Research Papers

EXTNACNNG-9!rcA FBOI' fiICE HI'S(,FEAIED WIIT
P(ITASgUI PEhIAGAXATE
""-*i:,#:fi *xliT#*#9"#,YJ#tffi .*
&-&qE.s!6;E;ar
.t,i;.i;;-:,&H
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|infu66,ldffir;;b;;
; ;*Y:. I ff :i*'g'":" 1;_;#;ffi",:jff "ffi ,i##;
:- '.."1';S "#:"iil1 L::$ H::a*ie-ff Itrtr ::: nT ff f, :.fr fr ;H;** : :
;' *:li;.;J-";;i :; r,f";fr ;
ll,'lli:i:;;:::ii:,*
ffmt**l*1"8fffr,sffif.ffifrfi 11
ffi
ffi
ir lf"f t#JHt$j*;."-"jE;itr ifi ?.T L1 :"?.ffi t:,T ;;
:; ".:;";ffi #?H*rii{Hd!tr fl Ifi:ilt"r"il:"i"f::n':TiF1E,l: *sel."r* tr;l
s#lx;i.lj*x.;,il;f"l#Ffr ;:ffi x:j*"fr t1.t; -!
Ftri:tljf ffi HtrJ]#
r@"d .*,;_d 3.:"i5fi
-,_*, * ",".. *;;;;:,-dff &,ffi
5,f,ffn* *
ffi
t42

I.rl

ni.tr]lerhd16ieik.tuirDfu
Y. 'n 4s l}r r 4s, '4FDk 'r't.:d
hidd|gfullB@Ea1d.b
iHfifffitr"Ts*l5"rf
hb|blm'IdDhFid,edN,abrM!.1
d4,s'b !k q*! i h! ldr &a bj $;t
F@!bddrykht5t!ddL@d{!
145

!!sNe rs', lbh sd hd o! oebrd (Fiq 3r aid !E
snp&( rmocbeEbrcnbturdF
s'd o @h e|qcy,a 6Md .d. (re}a .tu
|bl|h'J'bdIcbDsdeh'n€'.@ht
r&r
tuh 16^ (ei!r. rrb' (LorFle,r*)
iBirr€ 6@ M! b ud 14 rr Bfte
F& d dFftr d hd Bd ^.[ (rB4 b, uiE
rd $ n.d lle n4di{ b,rlj/ldlffir
rlbb2'^hcDn.u.rn.'obn.idhhdd
4!dd'JA-l{laMMRidb
.m9.dbs'oA.sEM''!E€w|kidho
ld,h, tu mdrre e lftd. 16 50.fc
ri.'!n4dluFnFedb'Uid'd
F4ffieadrcfr&ly
Ms6-JEu46cq@.sd;dy2'
r!rn!n, E. rrr€ $.d d r.!li,le d
tlrnn'd d anstbs eb n,b i6rs
'ldFbdlshsf
t6

h,tut oI e"ah, a^d 1..hnohs Mqas,^t,l
Qualitr Improv€m€nr or Amorphou Sitio by Using KMoOr
. S. 8. Jaqt. S, N$r.d. t\. Fcmle, M. zsrur.
I r^(^n\.i Lutrre.nnr 4Iahnohqr Udrt( poklslor
NL ltcarr
\annu)lria lrrnan(tuI li(nuk & h.*tuh r:dr?t. Ne*at! . rFu
Ter. r'K.
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t.t ,. '..t:!,\ \ \ /\...,,ttt.s0, ,nttuht.,,., t.a ebn\nit. t.t.r
\Rt) rdknA ttt,t Alu"r,.1 uh!lt th.
..1. n..r..., n k .F..,1, \\..";,;;,;;;' ;:;;; ;;:,K\'J,:.:;:;,.;,:,,;:..,
:1.: llt.i, i,:, ..... Jh. r lueL qla1..,.c|n ,i..stul,1! !,r rn.\
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:.:'\'.. .,1 ,..rrrri,,r .\ s,irh rr,\u,.s r\(nrrtr!o.p.rrr) 3jcrrr)
'1..,.' ,-.,1 ,..r .c bbk.r n.c. ,J1JAr-.rl.,."r..h.-.,-.,r,
Onr uf rtr upr(h x. m!t. u* .r rhc r,- t!ht.
ned rhd 3r rr..", ru {5 ,,r, ."4, d,,,Jrp\uu.
ibn n {xnshn,no & subrumn*r. rr)L) Th.
t41

nrtnrt Q! a&tid and r khndo|t Mona@Ml
'l.rel(l|)mdn d :i *mnrrdt lqes rhd cs sh,cyc n&hrns
,rhd krs.r: J!
dN h.l
r
A rcv,s* ot rhe chcmrcrt
'nrcrcsr $hporr.n\ of rirr rt. n(.
$ \rb^ !{D!r.s hos brcn pubtrshcd h! Cov,.drtuo ro.r,ndrr) i)!|l
'
I
.
" |,1 rt,.RtJ.|.IJ\,Pf .h...
L{: !t rrdtr | tl !rl! mbr t
\ i !m :rr. |\ad qroir n, tr conlfnlrod rn rhe t&hbe,JN.r rnu n r on (r
ruu m( rnd ctrtdnrlr thc acc hLsk t(.hJnll,ls.khjr & t1rn,t0. t(x)51 ltj!
.,.t, .. .. i, , .!.. -r .,,m, ..
\, r,r, '.. r,.r ,. r{, rN rturnro cJ lindnrT\
..t..r.., u\t(.,..,. r;
_.,J,.r.,....d, r..a{,r, t, 1 ..1 ctn.. , i
I r. ,.rrJ d ..rhn littn lotr!., tErol oee r ,\ trunt,.! uNnE .\drmi
:]'1,-"^*:'0r''\'|.{PhUU.\|(ll'''1eUth.h''tlh!|nldt|'J''
.Jn |\ tr.cJ,,, trtc..,,J.u.kr..,., ridn t(..oi..
J qr. ol rynrhcsi.i,r! h,Sn pcnormarcc jtrcotr rDd r\
.."']:"'.i -'i ' '\ir+
ri'u' ,nG'u\'o/'g!.
' ir,,,pIrJr
LIi l,.:1 ,.r, ,. Jn hr F'udu.,r r rtr c30 c $,rr, J hnr$ns nmJ rc*
: i,,.lll,'t 1".,.',:,, In (ohmc(trr E,,,u,un !m.d,ns,h( ;mu,ph,i.,
\,r(.r,m$,. ,i{h.r!i4tli[F, r r],.t(,,tr L.k bL(rur.,1,1h., lrJ:n,,..
::':.11,:r, :'..,r,o'l r,:nF i.frhunht so,rc,.mc. 11( ru{ m.r,n!r\J\ i
,...,N.r er, In{J iih .,t,J,, Jnl nnm J 8tJ' phrr rhr pF\rnh rJ,,h(r
": ". ".i, ,,r'\r.\!r.,nl.pJIJ.'.!d\h.:.,{.' j.u J,/.u he,r
r.,..r(r
e,.\.j
a,.\,.i -nimrcr JL\
:,
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'.
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at'rncJ duc n, f. r\ ,.Jr(.t .rJpt on "l"i FrJnu.l .r\l
ri irdo h r.'riliu! rhc N,drmg pelss of rle nc. hlrt rn. u* or porr*,unr
i;. ,.:l'-lll.' " '*, '\6raded eo,_"," *,_"ng"_.r " "..r.ir , "
l.:,'].1:,.|],1 , ,"*", L.,A.,r,^ 'he !hem,crL hJ\,trr .onprs\ rJn!r..,r,1
rorr\tr'n' FnJngJtrrr€ \h.n hcnr.d gc\,lsonpoed rnd oryecn rs hbetund.
r ."

ot,.at araMq 44a ha'4ot41 ,awsnd
1
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-'' - I "
tr.. .,.r rhJ n.c |.u.i ,. 1.c,
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r,,r.\ Jr!,.,J..r ,r
Jrl,!r,.,r., i.{,.\,irr rt,, \. 11.r. "{,.,..JtcJ r \1 r.,. !,i1t,.iii.,r i l
J.,..: I ' I 'r,", ,. .J rur.(, r ,rnrr..
"cn frcrl. (! ,4..,.cii.. |\ |
i; 11",^ ."''.", u 4,rcd \Jmprf -R trJ. d(, nrn{hr r., L";n",,.,..,
^ oi ,rnr ,rfi,< Dtrndtr, rx L
,l:-r:lrlr i.x I K. |, rc-.pa,r\cr\ r^1,.,r,r,.,",o.p". -..,g.u" -.., n
ll'''t "'iIn'. lrrnrr'cJ .ffrc,\1.|t) Nr,rLk-.,
,,!,r .q. : ! L\ r{ Fs.J rhrurgt, l, nclh .,c\c.. : t, rr-,,nJ nu.h,.. r..l
l. l llrnDArlvjnktri( .\.atrsj| I fCAI
$ ,rli lii . .'r,!r.' r{rnf,rd( qr n.6urcd L L{Jhh'h 'nc flrr.i LrT]l
j:;':' .', "", r'.1..{, rA.n{.Lfrf,. !.,,r1. ( .,,.,......., r
",r\,, i r
"r.r-" r,,,,.
i4J. j j1!(,t rh,iulh,, Bnu)h Or\g.n.urrJn\ Thc nurn,,.(.{
,rm,dr n,l'r. kr, unitri, rn,gsnen\tro,rnrnr h LJNDt4. r {,n h.p\,, r\,,.
-:,1
'liit",,,tl],
i,1nr- E.s.i n0m/tr.n,( .. .rrdj.,r".
I'o'n 4mnrcn' r.npe,JrrR ru ii s.n r 5Jmp,c..rr
In{, r,rh d,cArn \.( pr4€d
'1: r ptdlnu,n uu,bt. Jnd,he r.,roh, t.$
csurud independenrty .l.nc Ineono.gruns oj
!,rh h{r'LrrKt. -
Kl Kt lnd R $ rhosn ,n ais I
,1...""j11" l"l :y*., o*:.:,: .:.r k J,! ,rcd ,nr. ,nf ,,
.":::.'l'.:'F"i'.
,.^.ro'i n,)h.r"'h,hr,. r'r \i11'r'{,.F{
,,r{r I n r\^ r'd nh\ i.JI} rh$dd \Jk1. M.'tu, .res,rJrDn r:tc. ph Jr
rrr.1Fr?.,rc rhr.r..i\ Lnmisr,md rmnmr*i \r,t- h rh. .T..
...::; 'l)- hr!.{.rrtrrrr,.rdn.rrund {Bor rn,
nnvr r'e[1 thr \t,,nc\,,t.n,,( tr, tur. /.r,(.
.r,trLrYi,.r irr'mrt t!r,uJr,Jl nnrLS {h te t,!i,n !rr. (rr\crcd,,r.,rn,n
Tl.,(,,1..nJtJ...JJ,,r,idur\rmprc\I J!Kl
u!,1(, ntorc [c rnr,i rhcqrt dcp d.,f,r,.n ut mJrr,,at. li.: Jnd K.r nr r.,ic,
,",r. nDr a dr q 'hemJt dcerodJlon !i \rmtte Kt h c\c, 1{c, ,nnj .,tl
Lnc fn r,.,LT
K.(,. Vno. md "^1"." tr," ^r**.t ..rg", rnl

futadt tantn, atd li.hnllgt MMdNrlr
n(ioB\ir ptue\\ i o6 d€gn,brior of dE ncc hlsl tsunhcr h.lntrr
l.,ll:i. F+,)'trn ,..:,t'. rr, crcmnrJr A{r.!um rh. on.cir.,r pr.,..".;
hrtr'ne xfd .ctcrlros rhc rbnn un o,. cryjri j r.r o,
reqr) t.hc s jnce mc rins rr,rls rhc o\ rrlon
* or Kl thcmJt ,le&n,;J.on ,1 )Jmr { h , ,.
rirrrc r: TC:r orri, Kl.|(?.& ti3 undlr tror(n$vimnncd
Ir I r.'...,t rord. .,.t, \.!1, ch-r rr. r, r neJ kor rh.,nJ,(r\ o,,r c,l
rn r, r'ri r. E'.{'1 r.,\.. | trnr(!r i,.a i.ur,t.u.,r, idr r,er tu!
d),gnrr,r,,r rn, I a('Jor rhJr'n rhc€n3.or {{)0,cru &jir,r. K nor hJ\
::.,; ':.. . ,* "..
tt. K: rhc,crdurt\erthI Jnd .,\J cJA,.1.tr.
.r ..,nn. K. oc,4c, rrn .!rfr. R \c i4J r,,, ..
\'srF hrn Kj. pac rren,l ut ,tuln- Jr,{. rtrr ,\.,1
,,runrpnr(,nnnu[ or KMn(\ $8 f K2.
150

Jtua.t oIQ,ot , od frhrotas, t .nt!.r.d
1-,r'l! l: A*rug€d Rosidud weig[r & Hr.d C]rrbon In C{hcory r. Kt.
|Cr sr.,rt6
h,',xRl) d fTlR nrt),j\ rhe *,nunl spt.( R. Kt.
n x{r \: nd Xt
F\flr.
\c(
lnrrhre. tr.,...1
mJ pt*cd.n rhe .csbot,k,
'.:1i,^',:l .T::-1'T'"
{,r manrJnql d 590\
!tr,$n rrr\ rrd,. \ubJc(hngro tRDrilt 15.
r''I trr1" 'f
ll..{.:i. "."::::.,,"," pr..rrD.M.o. paN. ,}n..,r \.r n, f,r.,nrFr
.J,J.,1j,,.,,;,i,.'" --". e..1u'nJ'r''d,dueN( rhe rcp J/i""
Thr.I R,'r Jlflndnin prtrchs generjkd for $e mrenats rre shos n rn l,rguc l
r rr\ ri .h\."\, J' u ., d.r1.eJ p

6nd ota.dt, nr r.^,ors N.r.rad
l'l:::].f,*T .r h - !r bur suppon! rh. fornauon or r){Jr !.r. uhcn nc
JT^trd.r t\1J:\ r n Fmonelnarc.! tunh.r ,n(Eud ,o o.. N
flslEllr)r IRDotbmpt.l
filN 2(h[ x&Dottupt. Kt
r52

.Nt ota@, $rftenorry t .rFq.u
Flc!ru 4.r: xRD ot snrh Kl
ri.un 2(d): xRn.rlhpkR
re.n,. o.ch.mr !|lbnd.1si, r rdcnd vl
re.,)ru'rr1. i sc,r r; ,
'\
rhr,,Ldilrnotr riJ Jomfofn rr !na\ mrend.
h,n. $h J*,1 ,o db, n rh.
,fr!ri,.$rr
\F1i!
rrrnlfr'
tl|I,
rh, pc cr rf.hr,qr ApDRqrr! \ | n*!r 1.k -l
'lilll tou\.it\8,c.,.h tr mn.u. $-,
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